DE1618273A1 - Verfahren zur Herstellung von 1,2-Dichloraethan durch direkte Chlorierung von AEthylen - Google Patents
Verfahren zur Herstellung von 1,2-Dichloraethan durch direkte Chlorierung von AEthylenInfo
- Publication number
- DE1618273A1 DE1618273A1 DE19671618273 DE1618273A DE1618273A1 DE 1618273 A1 DE1618273 A1 DE 1618273A1 DE 19671618273 DE19671618273 DE 19671618273 DE 1618273 A DE1618273 A DE 1618273A DE 1618273 A1 DE1618273 A1 DE 1618273A1
- Authority
- DE
- Germany
- Prior art keywords
- ethylene
- dichloroethane
- pump
- production
- chlorine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 title claims description 20
- 239000005977 Ethylene Substances 0.000 title claims description 20
- 238000000034 method Methods 0.000 title claims description 13
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 title description 6
- 238000005660 chlorination reaction Methods 0.000 title description 3
- 238000006243 chemical reaction Methods 0.000 claims description 9
- 239000007795 chemical reaction product Substances 0.000 claims description 9
- 238000009835 boiling Methods 0.000 claims description 8
- 238000004821 distillation Methods 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 2
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 claims description 2
- 229910052736 halogen Inorganic materials 0.000 claims 2
- 150000002367 halogens Chemical class 0.000 claims 2
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 239000000460 chlorine Substances 0.000 description 16
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 15
- 229910052801 chlorine Inorganic materials 0.000 description 15
- 239000007788 liquid Substances 0.000 description 10
- 239000000047 product Substances 0.000 description 8
- 239000011541 reaction mixture Substances 0.000 description 8
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical compound CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 3
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000000376 reactant Substances 0.000 description 3
- UBOXGVDOUJQMTN-UHFFFAOYSA-N 1,1,2-trichloroethane Chemical compound ClCC(Cl)Cl UBOXGVDOUJQMTN-UHFFFAOYSA-N 0.000 description 2
- IBYHHJPAARCAIE-UHFFFAOYSA-N 1-bromo-2-chloroethane Chemical compound ClCCBr IBYHHJPAARCAIE-UHFFFAOYSA-N 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- 229910021578 Iron(III) chloride Inorganic materials 0.000 description 2
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- 238000010626 work up procedure Methods 0.000 description 2
- UKDOTCFNLHHKOF-FGRDZWBJSA-N (z)-1-chloroprop-1-ene;(z)-1,2-dichloroethene Chemical group C\C=C/Cl.Cl\C=C/Cl UKDOTCFNLHHKOF-FGRDZWBJSA-N 0.000 description 1
- UOCLXMDMGBRAIB-UHFFFAOYSA-N 1,1,1-trichloroethane Chemical compound CC(Cl)(Cl)Cl UOCLXMDMGBRAIB-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 1
- HRYZWHHZPQKTII-UHFFFAOYSA-N chloroethane Chemical compound CCCl HRYZWHHZPQKTII-UHFFFAOYSA-N 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 230000000994 depressogenic effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 229960003750 ethyl chloride Drugs 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/013—Preparation of halogenated hydrocarbons by addition of halogens
- C07C17/02—Preparation of halogenated hydrocarbons by addition of halogens to unsaturated hydrocarbons
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DED0052409 | 1967-03-01 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1618273A1 true DE1618273A1 (de) | 1970-10-29 |
Family
ID=7054149
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19671618273 Pending DE1618273A1 (de) | 1967-03-01 | 1967-03-01 | Verfahren zur Herstellung von 1,2-Dichloraethan durch direkte Chlorierung von AEthylen |
Country Status (9)
| Country | Link |
|---|---|
| AT (1) | AT274758B (enrdf_load_stackoverflow) |
| BE (1) | BE711415A (enrdf_load_stackoverflow) |
| BG (1) | BG17511A3 (enrdf_load_stackoverflow) |
| CH (1) | CH498063A (enrdf_load_stackoverflow) |
| DE (1) | DE1618273A1 (enrdf_load_stackoverflow) |
| ES (1) | ES351053A1 (enrdf_load_stackoverflow) |
| FR (1) | FR1555234A (enrdf_load_stackoverflow) |
| GB (1) | GB1184778A (enrdf_load_stackoverflow) |
| NL (1) | NL6802864A (enrdf_load_stackoverflow) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2427045A1 (de) * | 1973-06-11 | 1975-01-02 | Stauffer Chemical Co | Verfahren zur herstellung von aethylendichlorid |
| DE2803285A1 (de) | 1978-01-26 | 1979-08-02 | Wacker Chemie Gmbh | Verfahren zur kontinuierlichen chlorierung von olefinen in fluessiger phase sowie messanordnung zur chlorkonzentrationsbestimmung und -regelung als bestandteil einer vorrichtung zur durchfuehrung des verfahrens |
-
1967
- 1967-03-01 DE DE19671618273 patent/DE1618273A1/de active Pending
-
1968
- 1968-02-15 BG BG009413A patent/BG17511A3/xx unknown
- 1968-02-26 CH CH270868A patent/CH498063A/de not_active IP Right Cessation
- 1968-02-28 BE BE711415D patent/BE711415A/xx unknown
- 1968-02-28 AT AT190968A patent/AT274758B/de active
- 1968-02-28 FR FR1555234D patent/FR1555234A/fr not_active Expired
- 1968-02-29 NL NL6802864A patent/NL6802864A/xx unknown
- 1968-02-29 ES ES351053A patent/ES351053A1/es not_active Expired
- 1968-03-01 GB GB1021568A patent/GB1184778A/en not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2427045A1 (de) * | 1973-06-11 | 1975-01-02 | Stauffer Chemical Co | Verfahren zur herstellung von aethylendichlorid |
| DE2803285A1 (de) | 1978-01-26 | 1979-08-02 | Wacker Chemie Gmbh | Verfahren zur kontinuierlichen chlorierung von olefinen in fluessiger phase sowie messanordnung zur chlorkonzentrationsbestimmung und -regelung als bestandteil einer vorrichtung zur durchfuehrung des verfahrens |
Also Published As
| Publication number | Publication date |
|---|---|
| CH498063A (de) | 1970-10-31 |
| FR1555234A (enrdf_load_stackoverflow) | 1969-01-24 |
| GB1184778A (en) | 1970-03-18 |
| AT274758B (de) | 1969-09-25 |
| NL6802864A (enrdf_load_stackoverflow) | 1968-09-02 |
| ES351053A1 (es) | 1969-05-16 |
| BG17511A3 (bg) | 1973-11-10 |
| BE711415A (enrdf_load_stackoverflow) | 1968-07-01 |
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