DE160834C - - Google Patents
Info
- Publication number
- DE160834C DE160834C DENDAT160834D DE160834DA DE160834C DE 160834 C DE160834 C DE 160834C DE NDAT160834 D DENDAT160834 D DE NDAT160834D DE 160834D A DE160834D A DE 160834DA DE 160834 C DE160834 C DE 160834C
- Authority
- DE
- Germany
- Prior art keywords
- alcohol
- magnesium
- esters
- water
- percent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- FYYHWMGAXLPEAU-UHFFFAOYSA-N magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 9
- 239000011777 magnesium Substances 0.000 claims description 9
- 229910052749 magnesium Inorganic materials 0.000 claims description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- 150000003509 tertiary alcohols Chemical class 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 6
- 150000002148 esters Chemical class 0.000 claims description 6
- SFEOKXHPFMOVRM-BQYQJAHWSA-N Ionone Chemical compound CC(=O)\C=C\C1C(=C)CCCC1(C)C SFEOKXHPFMOVRM-BQYQJAHWSA-N 0.000 claims description 4
- 229930002839 ionones Natural products 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 3
- 150000007513 acids Chemical class 0.000 claims 1
- 150000001923 cyclic compounds Chemical class 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 8
- KPJPHPFMCOKUMW-UHFFFAOYSA-N iodomethane Chemical compound I[CH2] KPJPHPFMCOKUMW-UHFFFAOYSA-N 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 125000002015 acyclic group Chemical group 0.000 description 2
- -1 cyclic citral derivatives Chemical class 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N n-butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
- 230000035943 smell Effects 0.000 description 2
- 229910014033 C-OH Inorganic materials 0.000 description 1
- 229910014570 C—OH Inorganic materials 0.000 description 1
- 235000012544 Viola sororia Nutrition 0.000 description 1
- 241001106476 Violaceae Species 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 238000007429 general method Methods 0.000 description 1
- 239000011630 iodine Substances 0.000 description 1
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 description 1
- 229910052740 iodine Inorganic materials 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 150000002901 organomagnesium compounds Chemical class 0.000 description 1
- DNIAPMSPPWPWGF-UHFFFAOYSA-N propylene glycol Chemical group CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 1
- 150000003385 sodium Chemical class 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- DKGAVHZHDRPRBM-UHFFFAOYSA-N t-BuOH Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C403/00—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone
- C07C403/06—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone having side-chains substituted by singly-bound oxygen atoms
- C07C403/08—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone having side-chains substituted by singly-bound oxygen atoms by hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/16—Systems containing only non-condensed rings with a six-membered ring the ring being unsaturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fats And Perfumes (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE160834C true DE160834C (da) |
Family
ID=426763
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT160834D Active DE160834C (da) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE160834C (da) |
-
0
- DE DENDAT160834D patent/DE160834C/de active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE2427609C3 (de) | 4-Isopropenylcyclohexyl-methylester bzw. -methyläther und 4-Isopropylcyclohexyl-methylester bzw.-methyläther sowie die Verwendung dieser Verbindungen als Riechstoff bzw. Riechstoffkomponente und als Geschmacksstoffe oder Geschmacksstoffzusätze | |
| DE2748633B2 (de) | Tetramethyl-substituierte Acetophenone, Verfahren zu deren Herstellung und deren Verwendung als Riechstoffe | |
| DE160834C (da) | ||
| DE1223974B (de) | Riechstoffkompositionen | |
| DE2844949A1 (de) | Verfahren zur herstellung von 4-acyloxy-2-methylcrotonaldehyden | |
| DE1902074A1 (de) | Sauerstoffhaltige Derivate acyclischer Olefine | |
| DE2733857A1 (de) | Verfahren zur herstellung von riechstoffen und riechstoffkompositionen | |
| DE1817918C3 (de) | Ester des 1.7.7-Trimethyl-bicyclo- [4.4.0] -decanols-(3) | |
| EP1572844A1 (de) | Verfahren zur herstellung von konjugierter linolsäure | |
| DE2225612C2 (de) | Cyclische Methyl-fumardialdehyd-monoacetale und Verfahren zu ihrer Herstellung | |
| DE2530227C3 (de) | 2-Methylsubstituierte Pentensäureester, 2-Methyl-cis-3-pentensäure, sowie deren Säure- und Estergemische, deren Herstellungsverfahren und Verwendung | |
| EP0120274A1 (de) | Neue 2-Methylpentansäureester, deren Herstellung und Verwendung als Riechstoffe sowie diese enthaltende Riechstoff-Kompositionen | |
| DE3300341A1 (de) | Aliphatische ether des cyclododecen-2-ols, verfahren zu ihrer herstellung sowie ihre verwendung zur herstellung von riechstoffkompositionen | |
| DE964594C (de) | Verfahren zur Herstellung von y-Dihydrojonon | |
| EP0291849B1 (de) | 4-Methyl-4-phenyl-1-pentanale, deren Herstellung und Verwendung als Riechstoffe | |
| EP0341538B1 (de) | 1-Tert.-Butoxy-omega-alkene und deren Verwendung als Riechstoffe | |
| DE118351C (da) | ||
| DE3108867A1 (de) | Duftstoffzusammensetzung und verfahren zu ihrer herstellung | |
| DE3415067A1 (de) | Verwendung von 1-phenylpenten-4-on-1 und dessen methylhomologen zur vergroesserung oder steigerung des aromas von parfumzusammensetzungen, koelnisch waessern und parfuemierten artikeln | |
| DE892440C (de) | Verfahren zur Herstellung von substituierten Glutardialdehyden | |
| EP0735032B1 (de) | Verfahren zur Herstellung von 5-Hydroxy-4-methyl-2(5H)-furanon | |
| DE138141C (da) | ||
| DE657069C (de) | Verfahren zur Herstellung von ª‡-Oxyisobuttersaeuremethylester | |
| DE2521651A1 (de) | Verfahren zur herstellung von alpha-substituierten cyclischen ketonen | |
| DE101549C (da) |