DE1493310B2 - Verfahren zur kontinuierlichen herstellung von trockenen metallseifen - Google Patents
Verfahren zur kontinuierlichen herstellung von trockenen metallseifenInfo
- Publication number
- DE1493310B2 DE1493310B2 DE1964U0010542 DEU0010542A DE1493310B2 DE 1493310 B2 DE1493310 B2 DE 1493310B2 DE 1964U0010542 DE1964U0010542 DE 1964U0010542 DE U0010542 A DEU0010542 A DE U0010542A DE 1493310 B2 DE1493310 B2 DE 1493310B2
- Authority
- DE
- Germany
- Prior art keywords
- dry
- saponification
- metal
- fatty acids
- soap
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000344 soap Substances 0.000 title claims description 18
- 238000004519 manufacturing process Methods 0.000 title claims description 5
- 238000000034 method Methods 0.000 title claims 12
- 239000000203 mixture Substances 0.000 claims description 20
- 238000007127 saponification reaction Methods 0.000 claims description 14
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 13
- 239000000194 fatty acid Substances 0.000 claims description 13
- 229930195729 fatty acid Natural products 0.000 claims description 13
- 150000004665 fatty acids Chemical class 0.000 claims description 13
- 239000000843 powder Substances 0.000 claims description 11
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 239000007795 chemical reaction product Substances 0.000 claims description 6
- 238000002844 melting Methods 0.000 claims description 5
- 230000008018 melting Effects 0.000 claims description 5
- 239000000047 product Substances 0.000 claims description 5
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 3
- 235000013339 cereals Nutrition 0.000 claims description 3
- 239000008187 granular material Substances 0.000 claims description 3
- 235000015927 pasta Nutrition 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 2
- 238000011065 in-situ storage Methods 0.000 claims description 2
- 239000000463 material Substances 0.000 claims description 2
- 238000003801 milling Methods 0.000 claims description 2
- 239000000376 reactant Substances 0.000 claims description 2
- 229910052751 metal Inorganic materials 0.000 claims 11
- 239000002184 metal Substances 0.000 claims 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims 3
- 238000010309 melting process Methods 0.000 claims 3
- 238000002156 mixing Methods 0.000 claims 3
- 238000001556 precipitation Methods 0.000 claims 3
- GNRZYLVLEDQAKH-UHFFFAOYSA-N 5,7-dihydroxy-2-methyl-6,8-bis(3-methylbut-2-enyl)chromen-4-one Chemical compound O1C(C)=CC(=O)C2=C(O)C(CC=C(C)C)=C(O)C(CC=C(C)C)=C21 GNRZYLVLEDQAKH-UHFFFAOYSA-N 0.000 claims 2
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims 2
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims 2
- 150000004649 carbonic acid derivatives Chemical class 0.000 claims 2
- 239000003795 chemical substances by application Substances 0.000 claims 2
- 238000010924 continuous production Methods 0.000 claims 2
- 238000001035 drying Methods 0.000 claims 2
- 150000003839 salts Chemical class 0.000 claims 2
- 239000007787 solid Substances 0.000 claims 2
- 239000002904 solvent Substances 0.000 claims 2
- 239000001993 wax Substances 0.000 claims 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims 1
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 claims 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims 1
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 150000007513 acids Chemical class 0.000 claims 1
- 239000003513 alkali Substances 0.000 claims 1
- 150000001447 alkali salts Chemical class 0.000 claims 1
- 150000001342 alkaline earth metals Chemical class 0.000 claims 1
- 229910052782 aluminium Inorganic materials 0.000 claims 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims 1
- 230000015572 biosynthetic process Effects 0.000 claims 1
- 229910052793 cadmium Inorganic materials 0.000 claims 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 claims 1
- 238000001816 cooling Methods 0.000 claims 1
- 229910052802 copper Inorganic materials 0.000 claims 1
- 239000010949 copper Substances 0.000 claims 1
- 239000003085 diluting agent Substances 0.000 claims 1
- 239000004744 fabric Substances 0.000 claims 1
- 239000003925 fat Substances 0.000 claims 1
- 239000012065 filter cake Substances 0.000 claims 1
- 238000001914 filtration Methods 0.000 claims 1
- 235000021588 free fatty acids Nutrition 0.000 claims 1
- 150000004679 hydroxides Chemical class 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 229910052749 magnesium Inorganic materials 0.000 claims 1
- 239000011777 magnesium Substances 0.000 claims 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 claims 1
- 229910052753 mercury Inorganic materials 0.000 claims 1
- 125000005608 naphthenic acid group Chemical group 0.000 claims 1
- 239000003921 oil Substances 0.000 claims 1
- 239000002244 precipitate Substances 0.000 claims 1
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- 229910052725 zinc Inorganic materials 0.000 claims 1
- 239000011701 zinc Substances 0.000 claims 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 3
- 239000000920 calcium hydroxide Substances 0.000 description 3
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 3
- 230000002301 combined effect Effects 0.000 description 3
- 241000283690 Bos taurus Species 0.000 description 2
- 235000021355 Stearic acid Nutrition 0.000 description 2
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 2
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 2
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 239000008117 stearic acid Substances 0.000 description 2
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 1
- TWJNQYPJQDRXPH-UHFFFAOYSA-N 2-cyanobenzohydrazide Chemical compound NNC(=O)C1=CC=CC=C1C#N TWJNQYPJQDRXPH-UHFFFAOYSA-N 0.000 description 1
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 1
- DCXXMTOCNZCJGO-UHFFFAOYSA-N Glycerol trioctadecanoate Natural products CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 1
- 239000005639 Lauric acid Substances 0.000 description 1
- 235000021360 Myristic acid Nutrition 0.000 description 1
- TUNFSRHWOTWDNC-UHFFFAOYSA-N Myristic acid Natural products CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 239000013065 commercial product Substances 0.000 description 1
- 230000003503 early effect Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- VLHZUYUOEGBBJB-UHFFFAOYSA-N hydroxy stearic acid Natural products OCCCCCCCCCCCCCCCCCC(O)=O VLHZUYUOEGBBJB-UHFFFAOYSA-N 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 229910052740 iodine Inorganic materials 0.000 description 1
- 239000011630 iodine Substances 0.000 description 1
- 239000000395 magnesium oxide Substances 0.000 description 1
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 1
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 239000003760 tallow Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/02—Boiling soap; Refining
- C11D13/04—Continuous methods therefor
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/41—Preparation of salts of carboxylic acids
- C07C51/412—Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Detergent Compositions (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB841063A GB1074093A (en) | 1963-03-01 | 1963-03-01 | Improvements in or relating to the manufacture of dry metallic soaps |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE1493310A1 DE1493310A1 (de) | 1969-04-10 |
| DE1493310B2 true DE1493310B2 (de) | 1973-01-25 |
Family
ID=9852006
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE1964U0010542 Pending DE1493310B2 (de) | 1963-03-01 | 1964-02-29 | Verfahren zur kontinuierlichen herstellung von trockenen metallseifen |
Country Status (8)
| Country | Link |
|---|---|
| AT (1) | AT241655B (enrdf_load_stackoverflow) |
| BE (1) | BE644431A (enrdf_load_stackoverflow) |
| CH (1) | CH449826A (enrdf_load_stackoverflow) |
| DE (1) | DE1493310B2 (enrdf_load_stackoverflow) |
| ES (1) | ES297060A1 (enrdf_load_stackoverflow) |
| GB (1) | GB1074093A (enrdf_load_stackoverflow) |
| LU (1) | LU45510A1 (enrdf_load_stackoverflow) |
| NL (1) | NL6401873A (enrdf_load_stackoverflow) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2913592C2 (de) * | 1979-04-04 | 1988-11-10 | Chemische Werke München Otto Bärlocher GmbH, 8000 München | Verfahen zur Herstellung von Metallseifen |
| US4307027A (en) | 1979-04-09 | 1981-12-22 | Dart Industries Inc. | Continuous process for preparing dry metallic salts of higher fatty acids |
| DE3728811A1 (de) * | 1987-08-28 | 1989-03-09 | Henkel Kgaa | Verfahren zur kontinuierlichen herstellung von fettsaeureseifen |
| US5191098A (en) * | 1989-07-26 | 1993-03-02 | Henkel Corporation | Continuous process for preparation of aqueous dispersions of metal soaps |
| BR9007561A (pt) * | 1989-07-26 | 1992-06-23 | Henkel Corp | Processo continuo para a preparacao de uma dispersao aquosa de um sabao metalico |
| AU3032497A (en) * | 1996-06-20 | 1998-01-07 | Basf Aktiengesellschaft | Process for the production of alkaline metal salts and earth alkali metal salts of aryloxy-c1-c4-alkaline carboxylic |
| DE19624607A1 (de) * | 1996-06-20 | 1998-01-02 | Basf Ag | Verfahren zur Herstellung von Salzen von Säuregruppen tragenden pharmazeutischen Wirkstoffen |
| US7255873B2 (en) | 2000-02-24 | 2007-08-14 | Nichiyu Solution Incorporation | Process for producing fatty acid salt and livestock feed containing the fatty acid salt |
| AT519431B1 (de) * | 2016-12-12 | 2020-04-15 | Chemson Polymer Additive Ag | Verfahren zur Herstellung einer Stabilisatorzusammensetzung und damit hergestellte Stabilisatorzusammensetzung |
-
1963
- 1963-03-01 GB GB841063A patent/GB1074093A/en not_active Expired
-
1964
- 1964-02-24 LU LU45510A patent/LU45510A1/xx unknown
- 1964-02-26 CH CH234764A patent/CH449826A/de unknown
- 1964-02-27 NL NL6401873A patent/NL6401873A/xx unknown
- 1964-02-27 BE BE644431A patent/BE644431A/xx unknown
- 1964-02-28 AT AT173164A patent/AT241655B/de active
- 1964-02-29 DE DE1964U0010542 patent/DE1493310B2/de active Pending
- 1964-02-29 ES ES0297060A patent/ES297060A1/es not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| CH449826A (de) | 1968-01-15 |
| NL6401873A (enrdf_load_stackoverflow) | 1964-09-02 |
| GB1074093A (en) | 1967-06-28 |
| DE1493310A1 (de) | 1969-04-10 |
| AT241655B (de) | 1965-08-10 |
| BE644431A (enrdf_load_stackoverflow) | 1964-06-15 |
| ES297060A1 (es) | 1964-05-16 |
| LU45510A1 (enrdf_load_stackoverflow) | 1964-04-24 |
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