DE1244128B - Verfahren zum Trocknen, Reinigen und Kuehlen von rohem, gasfoermigem Chlor - Google Patents
Verfahren zum Trocknen, Reinigen und Kuehlen von rohem, gasfoermigem ChlorInfo
- Publication number
- DE1244128B DE1244128B DEH47848A DEH0047848A DE1244128B DE 1244128 B DE1244128 B DE 1244128B DE H47848 A DEH47848 A DE H47848A DE H0047848 A DEH0047848 A DE H0047848A DE 1244128 B DE1244128 B DE 1244128B
- Authority
- DE
- Germany
- Prior art keywords
- sulfuric acid
- chlorine
- chlorine gas
- drying
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000460 chlorine Substances 0.000 title claims description 19
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 title claims description 18
- 229910052801 chlorine Inorganic materials 0.000 title claims description 18
- 238000000034 method Methods 0.000 title claims description 17
- 238000001035 drying Methods 0.000 title claims description 14
- 238000001816 cooling Methods 0.000 title claims description 12
- 238000004140 cleaning Methods 0.000 title claims description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 115
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 claims description 49
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- 239000007788 liquid Substances 0.000 claims description 4
- 238000010586 diagram Methods 0.000 claims description 3
- 239000002253 acid Substances 0.000 description 9
- 239000007787 solid Substances 0.000 description 6
- 239000012535 impurity Substances 0.000 description 5
- 239000012071 phase Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 3
- FWFGVMYFCODZRD-UHFFFAOYSA-N oxidanium;hydrogen sulfate Chemical compound O.OS(O)(=O)=O FWFGVMYFCODZRD-UHFFFAOYSA-N 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- -1 is obtained Chemical compound 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 238000010587 phase diagram Methods 0.000 description 2
- 239000012266 salt solution Substances 0.000 description 2
- 229920006395 saturated elastomer Polymers 0.000 description 2
- 239000007790 solid phase Substances 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- RVSIFWBAGVMQKT-UHFFFAOYSA-N 1,1,1,3,3-pentachloropropan-2-one Chemical compound ClC(Cl)C(=O)C(Cl)(Cl)Cl RVSIFWBAGVMQKT-UHFFFAOYSA-N 0.000 description 1
- JHBKHLUZVFWLAG-UHFFFAOYSA-N 1,2,4,5-tetrachlorobenzene Chemical compound ClC1=CC(Cl)=C(Cl)C=C1Cl JHBKHLUZVFWLAG-UHFFFAOYSA-N 0.000 description 1
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- DOJXGHGHTWFZHK-UHFFFAOYSA-N Hexachloroacetone Chemical compound ClC(Cl)(Cl)C(=O)C(Cl)(Cl)Cl DOJXGHGHTWFZHK-UHFFFAOYSA-N 0.000 description 1
- MFSIEROJJKUHBQ-UHFFFAOYSA-N O.[Cl] Chemical class O.[Cl] MFSIEROJJKUHBQ-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- XFKVHUONJVDEIW-UHFFFAOYSA-N [Cl].S(O)(O)(=O)=O Chemical compound [Cl].S(O)(O)(=O)=O XFKVHUONJVDEIW-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 229910052794 bromium Inorganic materials 0.000 description 1
- 229910052729 chemical element Inorganic materials 0.000 description 1
- BULLHNJGPPOUOX-UHFFFAOYSA-N chloroacetone Chemical compound CC(=O)CCl BULLHNJGPPOUOX-UHFFFAOYSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 150000004683 dihydrates Chemical class 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- CKAPSXZOOQJIBF-UHFFFAOYSA-N hexachlorobenzene Chemical compound ClC1=C(Cl)C(Cl)=C(Cl)C(Cl)=C1Cl CKAPSXZOOQJIBF-UHFFFAOYSA-N 0.000 description 1
- VHHHONWQHHHLTI-UHFFFAOYSA-N hexachloroethane Chemical compound ClC(Cl)(Cl)C(Cl)(Cl)Cl VHHHONWQHHHLTI-UHFFFAOYSA-N 0.000 description 1
- 150000004677 hydrates Chemical class 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 238000010409 ironing Methods 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 150000004682 monohydrates Chemical class 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- UGNWTBMOAKPKBL-UHFFFAOYSA-N tetrachloro-1,4-benzoquinone Chemical compound ClC1=C(Cl)C(=O)C(Cl)=C(Cl)C1=O UGNWTBMOAKPKBL-UHFFFAOYSA-N 0.000 description 1
- 150000004685 tetrahydrates Chemical class 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B11/00—Oxides or oxyacids of halogens; Salts thereof
- C01B11/02—Oxides of chlorine
- C01B11/022—Chlorine dioxide (ClO2)
- C01B11/023—Preparation from chlorites or chlorates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/16—Fractionating columns in which vapour bubbles through liquid
- B01D3/18—Fractionating columns in which vapour bubbles through liquid with horizontal bubble plates
- B01D3/20—Bubble caps; Risers for vapour; Discharge pipes for liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/16—Fractionating columns in which vapour bubbles through liquid
- B01D3/22—Fractionating columns in which vapour bubbles through liquid with horizontal sieve plates or grids; Construction of sieve plates or grids
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/01—Chlorine; Hydrogen chloride
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Drying Of Gases (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Cleaning Or Drying Semiconductors (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US164319A US3215504A (en) | 1961-06-26 | 1962-01-04 | Plate tower |
| US482969A US3308606A (en) | 1962-01-04 | 1965-07-15 | Method of drying moisture bearing chlorine gas |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1244128B true DE1244128B (de) | 1967-07-13 |
Family
ID=26860445
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEH47848A Pending DE1244128B (de) | 1962-01-04 | 1962-12-31 | Verfahren zum Trocknen, Reinigen und Kuehlen von rohem, gasfoermigem Chlor |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3308606A (en, 2012) |
| BE (1) | BE626796A (en, 2012) |
| CH (1) | CH430670A (en, 2012) |
| DE (1) | DE1244128B (en, 2012) |
| GB (2) | GB1036822A (en, 2012) |
| NL (2) | NL280131A (en, 2012) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3957950A (en) * | 1972-04-01 | 1976-05-18 | Friedhelm Geiger | Process for preparing pure chlorine |
| FR2334379A1 (fr) * | 1975-12-13 | 1977-07-08 | Albach & Co | Dispositif de melange pour un extincteur a mousse |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4227890A (en) * | 1978-05-11 | 1980-10-14 | Olin Corporation | Process for cooling and drying chlorine gas |
| US4247532A (en) * | 1979-08-13 | 1981-01-27 | Shell Oil Company | Purification of electrolytically-produced chlorine |
| US5296017A (en) * | 1991-05-28 | 1994-03-22 | Mitsui Toatsu Chemicals, Inc. | Method and apparatus for concentrating chlorine gas |
| CN106237824B (zh) * | 2016-08-23 | 2019-02-19 | 陈淼 | 一种使用超低排放脱硫除尘旋流托盘喷射塔的脱硫除尘方法 |
| WO2025126011A1 (en) * | 2023-12-15 | 2025-06-19 | Polaris S.R.L. | Distillation column comprising intermediate liquid holder for quick restart after interruption and method to use thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE744367C (de) * | 1941-01-19 | 1944-01-14 | Ig Farbenindustrie Ag | Verfahren zur Reinigung von Chlorgas |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2108976A (en) * | 1934-08-15 | 1938-02-22 | Mathieson Alkali Works Inc | Production of chlorine dioxide |
| US2553557A (en) * | 1949-08-06 | 1951-05-22 | Diamond Alkali Co | Process of obtaining dry chlorine gas from a gaseous mixture comprising elemental chlrine as the principal component thereof |
| US3152866A (en) * | 1961-02-02 | 1964-10-13 | Du Pont | Cyclic process for converting hydrogen chloride to elemental chlorine and sulfur dioxide to sulfuric acid |
-
0
- BE BE626796D patent/BE626796A/xx unknown
- NL NL133808D patent/NL133808C/xx active
- NL NL280131D patent/NL280131A/xx unknown
-
1962
- 1962-12-31 DE DEH47848A patent/DE1244128B/de active Pending
-
1963
- 1963-01-03 CH CH5463A patent/CH430670A/de unknown
- 1963-01-04 GB GB546/63A patent/GB1036822A/en not_active Expired
- 1963-01-04 GB GB545/63A patent/GB1035241A/en not_active Expired
-
1965
- 1965-07-15 US US482969A patent/US3308606A/en not_active Expired - Lifetime
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE744367C (de) * | 1941-01-19 | 1944-01-14 | Ig Farbenindustrie Ag | Verfahren zur Reinigung von Chlorgas |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3957950A (en) * | 1972-04-01 | 1976-05-18 | Friedhelm Geiger | Process for preparing pure chlorine |
| FR2334379A1 (fr) * | 1975-12-13 | 1977-07-08 | Albach & Co | Dispositif de melange pour un extincteur a mousse |
Also Published As
| Publication number | Publication date |
|---|---|
| NL280131A (en, 2012) | |
| CH430670A (de) | 1967-02-28 |
| GB1035241A (en) | 1966-07-06 |
| NL133808C (en, 2012) | |
| US3308606A (en) | 1967-03-14 |
| GB1036822A (en) | 1966-07-20 |
| BE626796A (en, 2012) |
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