DE112007001382B4 - Alkalimetalltitanate und Verfahren zu deren Synthese - Google Patents

Alkalimetalltitanate und Verfahren zu deren Synthese

Info

Publication number
DE112007001382B4
DE112007001382B4 DE112007001382.6T DE112007001382T DE112007001382B4 DE 112007001382 B4 DE112007001382 B4 DE 112007001382B4 DE 112007001382 T DE112007001382 T DE 112007001382T DE 112007001382 B4 DE112007001382 B4 DE 112007001382B4
Authority
DE
Germany
Prior art keywords
zirconium
alkali metal
titanium
mixture
doped
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
DE112007001382.6T
Other languages
German (de)
English (en)
Other versions
DE112007001382T5 (de
Inventor
Pu Zhang
Suresh Mani
Michael R. Wixom
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
A123 Systems LLC
Original Assignee
A123 Systems N D Ges D Staates Delaware LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by A123 Systems N D Ges D Staates Delaware LLC filed Critical A123 Systems N D Ges D Staates Delaware LLC
Publication of DE112007001382T5 publication Critical patent/DE112007001382T5/de
Application granted granted Critical
Publication of DE112007001382B4 publication Critical patent/DE112007001382B4/de
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/003—Titanates
    • C01G23/005—Alkali titanates
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/04—Processes of manufacture in general
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/131—Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/485—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/50—Solid solutions
    • C01P2002/52—Solid solutions containing elements as dopants
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
DE112007001382.6T 2006-06-05 2007-06-05 Alkalimetalltitanate und Verfahren zu deren Synthese Active DE112007001382B4 (de)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
US81094206P 2006-06-05 2006-06-05
US60/810,942 2006-06-05
US82267506P 2006-08-17 2006-08-17
US60/822,675 2006-08-17
US11/757,658 US7879493B2 (en) 2006-06-05 2007-06-04 Alkali metal titanates and methods for their synthesis
US11/757,658 2007-06-04
PCT/US2007/070387 WO2007143640A2 (en) 2006-06-05 2007-06-05 Alkali metal titanates and methods for their synthesis

Publications (2)

Publication Number Publication Date
DE112007001382T5 DE112007001382T5 (de) 2009-05-07
DE112007001382B4 true DE112007001382B4 (de) 2026-01-08

Family

ID=38790638

Family Applications (1)

Application Number Title Priority Date Filing Date
DE112007001382.6T Active DE112007001382B4 (de) 2006-06-05 2007-06-05 Alkalimetalltitanate und Verfahren zu deren Synthese

Country Status (6)

Country Link
US (1) US7879493B2 (https=)
JP (1) JP5362555B2 (https=)
KR (1) KR101410844B1 (https=)
CA (1) CA2654605A1 (https=)
DE (1) DE112007001382B4 (https=)
WO (1) WO2007143640A2 (https=)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102008064651A1 (de) * 2008-06-03 2010-06-02 Süd-Chemie AG Lithium-Ionen-Batterie mit einer Anode enthaltend Lithiumtitan-Spinell
DE102009049470A1 (de) * 2009-10-15 2011-04-28 Süd-Chemie AG Verfahren zur Herstellung von feinteiligen Lithiumtitan-Spinellen und deren Verwendung
DE102009049693A1 (de) * 2009-10-16 2011-04-21 Süd-Chemie AG Phasenreines Lithiumaluminiumtitanphosphat und Verfahren zur Herstellung und dessen Verwendung
WO2011145443A1 (ja) * 2010-05-18 2011-11-24 株式会社 村田製作所 電極活物質およびその製造方法、ならびにそれを備えた非水電解質二次電池
JP5672859B2 (ja) 2010-08-26 2015-02-18 宇部興産株式会社 微細な炭素繊維と複合化されたリチウムチタン複合酸化物電極材料
WO2012111293A1 (ja) * 2011-02-15 2012-08-23 パナソニック株式会社 リチウムイオン二次電池用負極活物質材料およびその製造方法
US20120214067A1 (en) * 2011-02-15 2012-08-23 Goto Natsumi Negative electrode active material for lithium ion secondary battery and method for producing the same
KR101262054B1 (ko) 2011-02-17 2013-05-09 이화여자대학교 산학협력단 2차원 나노구조 리튬 티타늄 산화물, 그 제조방법 및 상기 2차원 나노구조 리튬 티타늄 산화물을 포함한 전극 물질
US8920976B2 (en) 2011-04-20 2014-12-30 Panasonic Corporation Nonaqueous electrolyte secondary battery
CN102842706B (zh) * 2011-06-22 2015-05-13 比亚迪股份有限公司 一种钛酸锂材料的制备方法及钛酸锂材料、锂离子电池
JP5897444B2 (ja) * 2011-10-28 2016-03-30 富士フイルム株式会社 非水二次電池用電解液及び二次電池
WO2013081231A1 (ko) * 2011-11-30 2013-06-06 주식회사 휘닉스소재 이종 금속이 도핑된 리튬 티탄 복합 산화물의 제조 방법, 및 이에 의하여 제조된 이종 금속이 도핑된 리튬 티탄 복합 산화물
DE102012208608A1 (de) * 2012-05-23 2013-11-28 Robert Bosch Gmbh Verfahren zum Herstellen einer Elektrode für einen elektrochemischen Energiespeicher und Elektrode
CN102780005B (zh) * 2012-08-20 2015-11-11 山东大学 一种钇改性的钛酸锂负极材料及其制备方法
CN103771500B (zh) * 2012-10-18 2015-06-24 上海纳米技术及应用国家工程研究中心有限公司 锂离子二次电池a、b位同时掺杂纳米钛酸锂的制备方法
GB201306814D0 (en) * 2013-04-15 2013-05-29 Johnson Matthey Plc Improvements in lithium-containing materials
KR101796233B1 (ko) * 2013-05-23 2017-12-01 주식회사 포스코 이종 금속이 도핑된 리튬 티탄 복합 산화물의 제조 방법, 및 이에 의하여 제조된 이종 금속이 도핑된 리튬 티탄 복합 산화물
RU2558140C1 (ru) * 2014-02-18 2015-07-27 Общество с ограниченной ответственностью "Научный центр "Автономные источники тока" (ООО "Научный центр "АИТ") АНОДНЫЙ МАТЕРИАЛ ЛИТИЙ-ИОННОГО АККУМУЛЯТОРА НА ОСНОВЕ LiCrTiO4 СО СТРУКТУРОЙ ШПИНЕЛИ И СПОСОБ ЕГО ПОЛУЧЕНИЯ
WO2015138019A1 (en) * 2014-03-12 2015-09-17 Imra America,Inc. Negative electrode active material for energy storage devices and method for making the same
KR101940249B1 (ko) * 2015-12-24 2019-01-18 주식회사 엘지화학 출력 특성이 향상된 음극 활물질 상기 음극 활물질을 포함하는 전기화학소자용 전극
CN108417823B (zh) * 2018-02-28 2021-03-30 华南理工大学 一种利用重复球磨法制备的Li2FeTi1-yMoyO4材料及其制备方法与应用
JP7771597B2 (ja) * 2020-09-28 2025-11-18 Ｕｂｅ株式会社 チタン酸リチウム粉末、それを用いた電極、及び蓄電デバイス

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH10251020A (ja) 1997-03-11 1998-09-22 Ishihara Sangyo Kaisha Ltd 金属置換チタン酸リチウムおよびその製造方法ならびにそれを用いてなるリチウム電池
US6372384B1 (en) 1999-03-25 2002-04-16 Sanyo Electric Co., Ltd. Rechargeable lithium battery comprising substituted lithium titanate electrodes
US20030073001A1 (en) 2001-10-02 2003-04-17 Jeremy Barker Synthesis of lithiated transition metal titanates for lithium cells

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3502118B2 (ja) 1993-03-17 2004-03-02 松下電器産業株式会社 リチウム二次電池およびその負極の製造法
KR100444804B1 (ko) 1996-06-14 2004-10-14 히다치 마쿠세루가부시키가이샤 리튬 2차전지
US6221531B1 (en) 1998-07-09 2001-04-24 The University Of Chicago Lithium-titanium-oxide anodes for lithium batteries
US6645673B2 (en) 1999-02-16 2003-11-11 Toho Titanium Co., Ltd. Process for producing lithium titanate and lithium ion battery and negative electrode therein
JP4540167B2 (ja) 1999-02-16 2010-09-08 東邦チタニウム株式会社 チタン酸リチウムの製造方法
JP2001354421A (ja) * 2000-06-08 2001-12-25 Toyota Central Res & Dev Lab Inc リチウム二次電池電極活物質用リチウムチタン複合酸化物およびその製造方法
US7211350B2 (en) * 2001-01-29 2007-05-01 Rutgers University Foundation Nanostructure lithium titanate electrode for high cycle rate rechargeable electrochemical cell
US6827921B1 (en) 2001-02-01 2004-12-07 Nanopowder Enterprises Inc. Nanostructured Li4Ti5O12 powders and method of making the same
AU2002319587B2 (en) 2001-07-20 2007-05-10 Altair Nanomaterials Inc. Process for making lithium titanate
US6881393B2 (en) 2002-03-08 2005-04-19 Altair Nanomaterials Inc. Process for making nano-sized and sub-micron-sized lithium-transition metal oxides
DE10319464A1 (de) 2003-04-29 2004-11-18 Basf Ag Verfahren zur Herstellung von nanokristallinen Lithiumtitanat-Spinellen

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH10251020A (ja) 1997-03-11 1998-09-22 Ishihara Sangyo Kaisha Ltd 金属置換チタン酸リチウムおよびその製造方法ならびにそれを用いてなるリチウム電池
US6372384B1 (en) 1999-03-25 2002-04-16 Sanyo Electric Co., Ltd. Rechargeable lithium battery comprising substituted lithium titanate electrodes
US20030073001A1 (en) 2001-10-02 2003-04-17 Jeremy Barker Synthesis of lithiated transition metal titanates for lithium cells

Also Published As

Publication number Publication date
JP5362555B2 (ja) 2013-12-11
CA2654605A1 (en) 2007-12-13
KR20090015131A (ko) 2009-02-11
WO2007143640A3 (en) 2008-10-09
KR101410844B1 (ko) 2014-06-23
US7879493B2 (en) 2011-02-01
WO2007143640A2 (en) 2007-12-13
US20070281211A1 (en) 2007-12-06
DE112007001382T5 (de) 2009-05-07
JP2009542562A (ja) 2009-12-03

Similar Documents

Publication Publication Date Title
DE112007001382B4 (de) Alkalimetalltitanate und Verfahren zu deren Synthese
EP2303780B1 (de) Verfahren zur herstellung von lithiumtitan-spinell
DE69605952T2 (de) Spinel-Lithium-Manganoxid-Material, Verfahren zu seiner Herstellung und seine Verwendung
EP3335262B1 (de) Siliciumpartikel enthaltende anodenmaterialien für lithium-ionen-batterien
EP2569249B1 (de) Verfahren zur einkapselung von metalloxiden mit graphen und die verwendung dieser materialien
EP2528862B1 (de) Substituiertes lithium-mangan-metallphosphat
DE69415011T2 (de) VERFAHREN ZUR HERSTELLUNG VON VERBINDUNGEN DES TYPS LixMn2O4 FÜR ELEKTRODEN IN SEKUNDÄRBATTERIEN HOHER KAPAZITÄT
EP3011621B1 (de) Elektrodenmaterial und dessen verwendung in lithium-ionen-batterien
EP2304828B1 (de) Mischoxid enthaltend einen lithium-mangan-spinell und verfahren zu dessen herstellung
DE69501435T2 (de) Interkalationsverbindungen auf der Basis von Manganoxid zur Verwendung als aktives Material einer positiven Elektrode einer Lithium-Sekondärbatterie
DE69518719T2 (de) Positives aktives Elektrodenmaterial für nichtwässrige Zelle und Herstellungsverfahren
EP3523848B1 (de) Lithium-ionen-batterien
DE69805853T2 (de) Modifizierte lithium-vanadium-oxidelektrodenmaterialien, produkte und verfahren
JPH0672708A (ja) リチウム遷移金属酸化物
DE4115951A1 (de) Manganoxidverbindung, verfahren zu ihrer herstellung, elektrochemische zelle, die sie als kathode enthaelt, sowie ihre verwendung zur herstellung einer lithiummanganoxidverbindung und elektrochemische zelle, die diese lithiummanganoxidverbindung als kathode enthaelt
DE102014223147A1 (de) Chromdotiertes Lithium-Titanat als Kathodenmaterial
EP3329532B1 (de) Lithium-ionen-batterien
EP3337764A1 (de) Lithium-nickel-mangan-basierte übergangsmetalloxidpartikel, deren herstellung sowie deren verwendung als elektrodenmaterial
EP0735004A1 (de) Verfahren zur Herstellung von Litium-Interkalationsverbindungen
DE69600855T2 (de) Lithium-Mangan-Oxid vom Spinelltyp als aktives Kathodenmaterial in einer nichtwässrigen Lithiumbatterie
DE112018000205T5 (de) Ein verfahren zur herstellung eines leistungsstarken lithiumtitanat-anodenmaterials für anwendungen von lithium-ionen-akkumulatoren
DE112021007772T5 (de) Ionenleitender feststoff und feststoffbatterie
WO2022262981A1 (de) Verfahren zur prälithiierung einer siliciumhaltigen anode in einer lithium-ionen-batterie
EP3807214B1 (de) Thermische behandlung von siliziumpartikeln
WO1998029342A1 (de) Verfahren zur herstellung von lithium-mangan-oxiden

Legal Events

Date Code Title Description
8127 New person/name/address of the applicant

Owner name: A123 SYSTEMS INC. ( N.D. GES. D. STAATES DELAW, US

R081 Change of applicant/patentee

Owner name: A123 SYSTEMS INC. ( N.D. GES. D. STAATES DELAW, US

Free format text: FORMER OWNER: T/J TECHNOLOGIES, INC., ANN ARBOR, MICH., US

Effective date: 20110204

Owner name: A123 SYSTEMS, LLC (N. D. GES. D. STAATES DELAW, US

Free format text: FORMER OWNER: T/J TECHNOLOGIES, INC., ANN ARBOR, MICH., US

Effective date: 20110204

R012 Request for examination validly filed

Effective date: 20140603

R082 Change of representative

Representative=s name: DTS PATENT- UND RECHTSANWAELTE SCHNEKENBUEHL U, DE

R081 Change of applicant/patentee

Owner name: A123 SYSTEMS, LLC (N. D. GES. D. STAATES DELAW, US

Free format text: FORMER OWNER: A123 SYSTEMS INC. ( N.D. GES. D. STAATES DELAWARE ), WATERTOWN, MASS., US

R082 Change of representative

Representative=s name: DTS PATENT- UND RECHTSANWAELTE SCHNEKENBUEHL U, DE

R016 Response to examination communication
R016 Response to examination communication
R018 Grant decision by examination section/examining division