DE102016209981A1

DE102016209981A1 - "Mehrkomponenten-Verpackungseinheit und Verfahren für die reduktive Entfärbung von gefärbten keratinischen Fasern"

"Mehrkomponenten-Verpackungseinheit und Verfahren für die reduktive Entfärbung von gefärbten keratinischen Fasern" Download PDF

Info

Publication number: DE102016209981A1
Authority: DE; Germany
Prior art keywords: agent; acid; container; amino; tin
Prior art date: 2016-06-07
Legal status : Withdrawn

Application number

DE102016209981.7A

Other languages

German (de)

English (en)

Inventor

Jürgen Schöpgens

Burkhard Müller

Constanze Neuba

Current Assignee

Henkel AG and Co KGaA

Original Assignee

Henkel AG and Co KGaA

Priority date

2016-06-07

Filing date

2016-06-07

Publication date

2017-12-07

2016-06-07 Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA

2016-06-07 Priority to DE102016209981.7A priority Critical patent/DE102016209981A1/de

2017-05-31 Priority to US15/609,024 priority patent/US20170347771A1/en

2017-05-31 Priority to FR1754784A priority patent/FR3052054B1/fr

2017-06-06 Priority to GB1708979.8A priority patent/GB2556134B/en

2017-12-07 Publication of DE102016209981A1 publication Critical patent/DE102016209981A1/de

Status Withdrawn legal-status Critical Current

Links

238000004806 packaging method and process Methods 0.000 title claims abstract description 110
239000000835 fiber Substances 0.000 title claims abstract description 109
238000004042 decolorization Methods 0.000 title claims abstract description 61
230000002829 reductive effect Effects 0.000 title claims abstract description 58
238000000034 method Methods 0.000 title claims abstract description 30
239000003795 chemical substances by application Substances 0.000 claims abstract description 360
239000003638 chemical reducing agent Substances 0.000 claims abstract description 47
150000003839 salts Chemical class 0.000 claims abstract description 45
239000002537 cosmetic Substances 0.000 claims abstract description 29
210000004209 hair Anatomy 0.000 claims abstract description 27
229910052751 metal Inorganic materials 0.000 claims abstract description 27
239000002184 metal Substances 0.000 claims abstract description 27
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims abstract description 26
229910052717 sulfur Inorganic materials 0.000 claims abstract description 26
239000011593 sulfur Substances 0.000 claims abstract description 26
IUTCEZPPWBHGIX-UHFFFAOYSA-N tin(2+) Chemical class [Sn+2] IUTCEZPPWBHGIX-UHFFFAOYSA-N 0.000 claims abstract description 17
CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical class [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 claims abstract description 8
WAEMQWOKJMHJLA-UHFFFAOYSA-N Manganese(2+) Chemical class [Mn+2] WAEMQWOKJMHJLA-UHFFFAOYSA-N 0.000 claims abstract description 7
CMWCOKOTCLFJOP-UHFFFAOYSA-N titanium(3+) Chemical class [Ti+3] CMWCOKOTCLFJOP-UHFFFAOYSA-N 0.000 claims abstract description 7
MJOXZELXZLIYPI-UHFFFAOYSA-N titanium(2+) Chemical class [Ti+2] MJOXZELXZLIYPI-UHFFFAOYSA-N 0.000 claims abstract description 5
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 35
239000002253 acid Substances 0.000 claims description 26
RXILGWFNTZZRRF-UHFFFAOYSA-N [bis(sulfinomethyl)amino]methanesulfinic acid Chemical compound OS(=O)CN(CS(O)=O)CS(O)=O RXILGWFNTZZRRF-UHFFFAOYSA-N 0.000 claims description 25
239000011734 sodium Substances 0.000 claims description 25
CWERGRDVMFNCDR-UHFFFAOYSA-N thioglycolic acid Chemical compound OC(=O)CS CWERGRDVMFNCDR-UHFFFAOYSA-N 0.000 claims description 21
ZSUXOVNWDZTCFN-UHFFFAOYSA-L tin(ii) bromide Chemical compound Br[Sn]Br ZSUXOVNWDZTCFN-UHFFFAOYSA-L 0.000 claims description 20
PENRVBJTRIYHOA-UHFFFAOYSA-L zinc dithionite Chemical compound [Zn+2].[O-]S(=O)S([O-])=O PENRVBJTRIYHOA-UHFFFAOYSA-L 0.000 claims description 20
PMNLUUOXGOOLSP-UHFFFAOYSA-N 2-mercaptopropanoic acid Chemical compound CC(S)C(O)=O PMNLUUOXGOOLSP-UHFFFAOYSA-N 0.000 claims description 18
150000007513 acids Chemical class 0.000 claims description 18
NYYSPVRERVXMLJ-UHFFFAOYSA-N 4,4-difluorocyclohexan-1-one Chemical compound FC1(F)CCC(=O)CC1 NYYSPVRERVXMLJ-UHFFFAOYSA-N 0.000 claims description 17
229910021626 Tin(II) chloride Inorganic materials 0.000 claims description 15
238000002156 mixing Methods 0.000 claims description 14
238000002360 preparation method Methods 0.000 claims description 14
JVBXVOWTABLYPX-UHFFFAOYSA-L sodium dithionite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])=O JVBXVOWTABLYPX-UHFFFAOYSA-L 0.000 claims description 14
230000003113 alkalizing effect Effects 0.000 claims description 12
HCNOVMLURFQZNZ-UHFFFAOYSA-L CS(=O)ON(CS(=O)[O-])CS(=O)[O-].[K+].[K+].[K+] Chemical compound CS(=O)ON(CS(=O)[O-])CS(=O)[O-].[K+].[K+].[K+] HCNOVMLURFQZNZ-UHFFFAOYSA-L 0.000 claims description 11
235000011150 stannous chloride Nutrition 0.000 claims description 11
DAOANAATJZWTSJ-UHFFFAOYSA-N N-Decanoylmorpholine Chemical compound CCCCCCCCCC(=O)N1CCOCC1 DAOANAATJZWTSJ-UHFFFAOYSA-N 0.000 claims description 10
239000000470 constituent Substances 0.000 claims description 10
PNOXNTGLSKTMQO-UHFFFAOYSA-L diacetyloxytin Chemical compound CC(=O)O[Sn]OC(C)=O PNOXNTGLSKTMQO-UHFFFAOYSA-L 0.000 claims description 10
SBGKURINHGJRFN-UHFFFAOYSA-N hydroxymethanesulfinic acid Chemical compound OCS(O)=O SBGKURINHGJRFN-UHFFFAOYSA-N 0.000 claims description 10
OHFNPZKURJNQGA-UHFFFAOYSA-K trisodium;[bis(sulfinatomethyl)amino]methanesulfinate Chemical compound [Na+].[Na+].[Na+].[O-]S(=O)CN(CS([O-])=O)CS([O-])=O OHFNPZKURJNQGA-UHFFFAOYSA-K 0.000 claims description 10
OQBLGYCUQGDOOR-UHFFFAOYSA-L 1,3,2$l^{2}-dioxastannolane-4,5-dione Chemical compound O=C1O[Sn]OC1=O OQBLGYCUQGDOOR-UHFFFAOYSA-L 0.000 claims description 9
GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 claims description 9
UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 8
XUJNEKJLAYXESH-REOHCLBHSA-N L-Cysteine Chemical compound SC[C@H](N)C(O)=O XUJNEKJLAYXESH-REOHCLBHSA-N 0.000 claims description 8
ISLGHAYMGURDSU-UHFFFAOYSA-N aminomethanesulfinic acid Chemical compound NCS(O)=O ISLGHAYMGURDSU-UHFFFAOYSA-N 0.000 claims description 8
AXZWODMDQAVCJE-UHFFFAOYSA-L tin(II) chloride (anhydrous) Chemical compound [Cl-].[Cl-].[Sn+2] AXZWODMDQAVCJE-UHFFFAOYSA-L 0.000 claims description 8
WRIREHMDTACSLC-UHFFFAOYSA-L 2-hydroxypropanoate;tin(2+) Chemical compound [Sn+2].CC(O)C([O-])=O.CC(O)C([O-])=O WRIREHMDTACSLC-UHFFFAOYSA-L 0.000 claims description 7
YXTDAZMTQFUZHK-UHFFFAOYSA-L 5,6-dihydroxy-1,3,2$l^{2}-dioxastannepane-4,7-dione Chemical compound [Sn+2].[O-]C(=O)C(O)C(O)C([O-])=O YXTDAZMTQFUZHK-UHFFFAOYSA-L 0.000 claims description 7
RGHNJXZEOKUKBD-SQOUGZDYSA-M D-gluconate Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O RGHNJXZEOKUKBD-SQOUGZDYSA-M 0.000 claims description 7
229940050410 gluconate Drugs 0.000 claims description 7
HEZHYQDYRPUXNJ-UHFFFAOYSA-L potassium dithionite Chemical compound [K+].[K+].[O-]S(=O)S([O-])=O HEZHYQDYRPUXNJ-UHFFFAOYSA-L 0.000 claims description 7
QHGNHLZPVBIIPX-UHFFFAOYSA-N tin(ii) oxide Chemical compound [Sn]=O QHGNHLZPVBIIPX-UHFFFAOYSA-N 0.000 claims description 7
HNBOJFKSERQBAH-UHFFFAOYSA-N (sulfinomethylamino)methanesulfinic acid Chemical compound OS(=O)CNCS(O)=O HNBOJFKSERQBAH-UHFFFAOYSA-N 0.000 claims description 6
LJWYXUQRXGRAGM-UHFFFAOYSA-N 1-(1-sulfinoethylamino)ethanesulfinic acid Chemical compound OS(=O)C(C)NC(C)S(O)=O LJWYXUQRXGRAGM-UHFFFAOYSA-N 0.000 claims description 6
QDTLBJBCSDJSCT-UHFFFAOYSA-N 1-aminoethanesulfinic acid Chemical compound CC(N)S(O)=O QDTLBJBCSDJSCT-UHFFFAOYSA-N 0.000 claims description 6
DWAQJAXMDSEUJJ-UHFFFAOYSA-M Sodium bisulfite Chemical compound [Na+].OS([O-])=O DWAQJAXMDSEUJJ-UHFFFAOYSA-M 0.000 claims description 6
PQUCIEFHOVEZAU-UHFFFAOYSA-N Diammonium sulfite Chemical compound [NH4+].[NH4+].[O-]S([O-])=O PQUCIEFHOVEZAU-UHFFFAOYSA-N 0.000 claims description 5
XYXNTHIYBIDHGM-UHFFFAOYSA-N ammonium thiosulfate Chemical compound [NH4+].[NH4+].[O-]S([O-])(=O)=S XYXNTHIYBIDHGM-UHFFFAOYSA-N 0.000 claims description 5
XUJNEKJLAYXESH-UHFFFAOYSA-N cysteine Natural products SCC(N)C(O)=O XUJNEKJLAYXESH-UHFFFAOYSA-N 0.000 claims description 5
FGRVOLIFQGXPCT-UHFFFAOYSA-L dipotassium;dioxido-oxo-sulfanylidene-$l^{6}-sulfane Chemical compound [K+].[K+].[O-]S([O-])(=O)=S FGRVOLIFQGXPCT-UHFFFAOYSA-L 0.000 claims description 5
DJEHXEMURTVAOE-UHFFFAOYSA-M potassium bisulfite Chemical compound [K+].OS([O-])=O DJEHXEMURTVAOE-UHFFFAOYSA-M 0.000 claims description 5
BHZRJJOHZFYXTO-UHFFFAOYSA-L potassium sulfite Chemical compound [K+].[K+].[O-]S([O-])=O BHZRJJOHZFYXTO-UHFFFAOYSA-L 0.000 claims description 5
229940079827 sodium hydrogen sulfite Drugs 0.000 claims description 5
235000010267 sodium hydrogen sulphite Nutrition 0.000 claims description 5
AKHNMLFCWUSKQB-UHFFFAOYSA-L sodium thiosulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=S AKHNMLFCWUSKQB-UHFFFAOYSA-L 0.000 claims description 5
HXLUMDQZOJRCRR-UHFFFAOYSA-L C(C)S(=O)ONC(C)S(=O)[O-].[K+].[K+].S(=O)([O-])C(C)NOS(=O)CC Chemical compound C(C)S(=O)ONC(C)S(=O)[O-].[K+].[K+].S(=O)([O-])C(C)NOS(=O)CC HXLUMDQZOJRCRR-UHFFFAOYSA-L 0.000 claims description 4
HZMRJLMURDUYSC-UHFFFAOYSA-L C(C)S(=O)ONC(C)S(=O)[O-].[Na+].[Na+].S(=O)([O-])C(C)NOS(=O)CC Chemical compound C(C)S(=O)ONC(C)S(=O)[O-].[Na+].[Na+].S(=O)([O-])C(C)NOS(=O)CC HZMRJLMURDUYSC-UHFFFAOYSA-L 0.000 claims description 4
YEWXTDRHOITQBV-UHFFFAOYSA-L CS(=O)ONCS(=O)[O-].[Na+].[Na+].S(=O)([O-])CNOS(=O)C Chemical compound CS(=O)ONCS(=O)[O-].[Na+].[Na+].S(=O)([O-])CNOS(=O)C YEWXTDRHOITQBV-UHFFFAOYSA-L 0.000 claims description 4
229910021577 Iron(II) chloride Inorganic materials 0.000 claims description 4
JVTAAEKCZFNVCJ-UHFFFAOYSA-M Lactate Chemical compound CC(O)C([O-])=O JVTAAEKCZFNVCJ-UHFFFAOYSA-M 0.000 claims description 4
ATPYDEXARGRGDG-UHFFFAOYSA-L [K+].[K+].CS(=O)ONCS(=O)[O-].S(=O)([O-])CNOS(=O)C Chemical compound [K+].[K+].CS(=O)ONCS(=O)[O-].S(=O)([O-])CNOS(=O)C ATPYDEXARGRGDG-UHFFFAOYSA-L 0.000 claims description 4
XTGCBCGHRJUXKQ-UHFFFAOYSA-L [K+].[K+].[K+].S(=O)([O-])C(C)N(CC)C(C)S(=O)[O-] Chemical compound [K+].[K+].[K+].S(=O)([O-])C(C)N(CC)C(C)S(=O)[O-] XTGCBCGHRJUXKQ-UHFFFAOYSA-L 0.000 claims description 4
235000018417 cysteine Nutrition 0.000 claims description 4
HIHFHNYIBMQZDK-UHFFFAOYSA-M potassium 1-aminoethanesulfinate Chemical compound NC(C)S(=O)[O-].[K+] HIHFHNYIBMQZDK-UHFFFAOYSA-M 0.000 claims description 4
235000010259 potassium hydrogen sulphite Nutrition 0.000 claims description 4
235000019252 potassium sulphite Nutrition 0.000 claims description 4
235000010265 sodium sulphite Nutrition 0.000 claims description 4
235000019345 sodium thiosulphate Nutrition 0.000 claims description 4
SPLFRNZYENMTIS-UHFFFAOYSA-M sodium;1-aminoethanesulfinate Chemical compound [Na+].CC(N)S([O-])=O SPLFRNZYENMTIS-UHFFFAOYSA-M 0.000 claims description 4
OHZCFWMJMWFNFP-ZVGUSBNCSA-L (2r,3r)-2,3-dihydroxybutanedioate;iron(2+) Chemical compound [Fe+2].[O-]C(=O)[C@H](O)[C@@H](O)C([O-])=O OHZCFWMJMWFNFP-ZVGUSBNCSA-L 0.000 claims description 3
YXTDAZMTQFUZHK-ZVGUSBNCSA-L (2r,3r)-2,3-dihydroxybutanedioate;tin(2+) Chemical compound [Sn+2].[O-]C(=O)[C@H](O)[C@@H](O)C([O-])=O YXTDAZMTQFUZHK-ZVGUSBNCSA-L 0.000 claims description 3
CKUJRAYMVVJDMG-IYEMJOQQSA-L (2r,3s,4r,5r)-2,3,4,5,6-pentahydroxyhexanoate;tin(2+) Chemical compound [Sn+2].OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O CKUJRAYMVVJDMG-IYEMJOQQSA-L 0.000 claims description 3
239000004277 Ferrous carbonate Substances 0.000 claims description 3
DKKCQDROTDCQOR-UHFFFAOYSA-L Ferrous lactate Chemical compound [Fe+2].CC(O)C([O-])=O.CC(O)C([O-])=O DKKCQDROTDCQOR-UHFFFAOYSA-L 0.000 claims description 3
229910021575 Iron(II) bromide Inorganic materials 0.000 claims description 3
RAQDACVRFCEPDA-UHFFFAOYSA-L ferrous carbonate Chemical compound [Fe+2].[O-]C([O-])=O RAQDACVRFCEPDA-UHFFFAOYSA-L 0.000 claims description 3
235000019268 ferrous carbonate Nutrition 0.000 claims description 3
239000004222 ferrous gluconate Substances 0.000 claims description 3
235000013924 ferrous gluconate Nutrition 0.000 claims description 3
235000013925 ferrous lactate Nutrition 0.000 claims description 3
239000004225 ferrous lactate Substances 0.000 claims description 3
NMCUIPGRVMDVDB-UHFFFAOYSA-L iron dichloride Chemical compound Cl[Fe]Cl NMCUIPGRVMDVDB-UHFFFAOYSA-L 0.000 claims description 3
BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims description 3
OWZIYWAUNZMLRT-UHFFFAOYSA-L iron(2+);oxalate Chemical compound [Fe+2].[O-]C(=O)C([O-])=O OWZIYWAUNZMLRT-UHFFFAOYSA-L 0.000 claims description 3
229910000015 iron(II) carbonate Inorganic materials 0.000 claims description 3
229910021506 iron(II) hydroxide Inorganic materials 0.000 claims description 3
229910000155 iron(II) phosphate Inorganic materials 0.000 claims description 3
229910000359 iron(II) sulfate Inorganic materials 0.000 claims description 3
GYCHYNMREWYSKH-UHFFFAOYSA-L iron(ii) bromide Chemical compound [Fe+2].[Br-].[Br-] GYCHYNMREWYSKH-UHFFFAOYSA-L 0.000 claims description 3
FZGIHSNZYGFUGM-UHFFFAOYSA-L iron(ii) fluoride Chemical compound [F-].[F-].[Fe+2] FZGIHSNZYGFUGM-UHFFFAOYSA-L 0.000 claims description 3
VRIVJOXICYMTAG-IYEMJOQQSA-L iron(ii) gluconate Chemical compound [Fe+2].OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O VRIVJOXICYMTAG-IYEMJOQQSA-L 0.000 claims description 3
NCNCGGDMXMBVIA-UHFFFAOYSA-L iron(ii) hydroxide Chemical compound [OH-].[OH-].[Fe+2] NCNCGGDMXMBVIA-UHFFFAOYSA-L 0.000 claims description 3
SDEKDNPYZOERBP-UHFFFAOYSA-H iron(ii) phosphate Chemical compound [Fe+2].[Fe+2].[Fe+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O SDEKDNPYZOERBP-UHFFFAOYSA-H 0.000 claims description 3
229940007163 stannous tartrate Drugs 0.000 claims description 3
229910001407 tin (II) carbonate Inorganic materials 0.000 claims description 3
UNYGOTXWMGACLR-UHFFFAOYSA-L tin(2+);carbonate Chemical compound [Sn+2].[O-]C([O-])=O UNYGOTXWMGACLR-UHFFFAOYSA-L 0.000 claims description 3
FBGKGORFGWHADY-UHFFFAOYSA-L tin(2+);dihydroxide Chemical compound O[Sn]O FBGKGORFGWHADY-UHFFFAOYSA-L 0.000 claims description 3
FSBZGYYPMXSIEE-UHFFFAOYSA-H tin(2+);diphosphate Chemical compound [Sn+2].[Sn+2].[Sn+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O FSBZGYYPMXSIEE-UHFFFAOYSA-H 0.000 claims description 3
OBBXFSIWZVFYJR-UHFFFAOYSA-L tin(2+);sulfate Chemical compound [Sn+2].[O-]S([O-])(=O)=O OBBXFSIWZVFYJR-UHFFFAOYSA-L 0.000 claims description 3
229910021509 tin(II) hydroxide Inorganic materials 0.000 claims description 3
229910000375 tin(II) sulfate Inorganic materials 0.000 claims description 3
ZQQLPDMCGIBPIM-UHFFFAOYSA-L trisodium 1-[ethylsulfinyloxy(1-sulfinatoethyl)amino]ethanesulfinate Chemical compound C(C)S(=O)ON(C(C)S(=O)[O-])C(C)S(=O)[O-].[Na+].[Na+].[Na+] ZQQLPDMCGIBPIM-UHFFFAOYSA-L 0.000 claims description 3
MCDLETWIOVSGJT-UHFFFAOYSA-N acetic acid;iron Chemical compound [Fe].CC(O)=O.CC(O)=O MCDLETWIOVSGJT-UHFFFAOYSA-N 0.000 claims description 2
229960001645 ferrous gluconate Drugs 0.000 claims description 2
229940037907 ferrous lactate Drugs 0.000 claims description 2
229940062993 ferrous oxalate Drugs 0.000 claims description 2
229940116007 ferrous phosphate Drugs 0.000 claims description 2
229940057006 ferrous tartrate Drugs 0.000 claims description 2
KWIIZYLMTBRKMO-UHFFFAOYSA-N CCN(C(C)S(=O)O)C(C)S(=O)O Chemical compound CCN(C(C)S(=O)O)C(C)S(=O)O KWIIZYLMTBRKMO-UHFFFAOYSA-N 0.000 claims 1
239000000194 fatty acid Substances 0.000 description 48
235000014113 dietary fatty acids Nutrition 0.000 description 46
229930195729 fatty acid Natural products 0.000 description 46
PEDCQBHIVMGVHV-UHFFFAOYSA-N glycerol group Chemical group OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 42
-1 sulfinatoethyl Chemical group 0.000 description 39
239000000975 dye Substances 0.000 description 33
150000004665 fatty acids Chemical class 0.000 description 28
239000000203 mixture Substances 0.000 description 26
MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 23
150000001875 compounds Chemical class 0.000 description 21
102000011782 Keratins Human genes 0.000 description 20
108010076876 Keratins Proteins 0.000 description 20
IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 18
239000003925 fat Substances 0.000 description 17
235000019197 fats Nutrition 0.000 description 17
150000002191 fatty alcohols Chemical class 0.000 description 17
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 16
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 16
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 16
125000004432 carbon atom Chemical group C* 0.000 description 16
JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 16
KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 15
VKOBVWXKNCXXDE-UHFFFAOYSA-N icosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCC(O)=O VKOBVWXKNCXXDE-UHFFFAOYSA-N 0.000 description 15
238000007254 oxidation reaction Methods 0.000 description 15
229920000642 polymer Polymers 0.000 description 15
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 14
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 14
229920001577 copolymer Polymers 0.000 description 14
238000004043 dyeing Methods 0.000 description 14
235000011187 glycerol Nutrition 0.000 description 14
230000003647 oxidation Effects 0.000 description 14
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 11
OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 11
239000007800 oxidant agent Substances 0.000 description 11
AFVFQIVMOAPDHO-UHFFFAOYSA-N Methanesulfonic acid Chemical compound CS(O)(=O)=O AFVFQIVMOAPDHO-UHFFFAOYSA-N 0.000 description 10
WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 10
239000000047 product Substances 0.000 description 10
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
239000007864 aqueous solution Substances 0.000 description 9
239000000982 direct dye Substances 0.000 description 9
HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 description 8
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 8
FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 8
DBVJJBKOTRCVKF-UHFFFAOYSA-N Etidronic acid Chemical compound OP(=O)(O)C(O)(C)P(O)(O)=O DBVJJBKOTRCVKF-UHFFFAOYSA-N 0.000 description 8
OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 8
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239000000419 plant extract Substances 0.000 description 1
229920001521 polyalkylene glycol ether Polymers 0.000 description 1
150000008442 polyphenolic compounds Chemical class 0.000 description 1
235000013824 polyphenols Nutrition 0.000 description 1
229920001451 polypropylene glycol Polymers 0.000 description 1
229950008882 polysorbate Drugs 0.000 description 1
229940068965 polysorbates Drugs 0.000 description 1
229920002451 polyvinyl alcohol Polymers 0.000 description 1
XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 1
239000011736 potassium bicarbonate Substances 0.000 description 1
235000015497 potassium bicarbonate Nutrition 0.000 description 1
229910000028 potassium bicarbonate Inorganic materials 0.000 description 1
229910000027 potassium carbonate Inorganic materials 0.000 description 1
235000011181 potassium carbonates Nutrition 0.000 description 1
TYJJADVDDVDEDZ-UHFFFAOYSA-M potassium hydrogencarbonate Chemical compound [K+].OC([O-])=O TYJJADVDDVDEDZ-UHFFFAOYSA-M 0.000 description 1
235000011118 potassium hydroxide Nutrition 0.000 description 1
HYTYHTSMCRDHIM-UHFFFAOYSA-M potassium;2-sulfanylacetate Chemical compound [K+].[O-]C(=O)CS HYTYHTSMCRDHIM-UHFFFAOYSA-M 0.000 description 1
239000000843 powder Substances 0.000 description 1
150000003141 primary amines Chemical class 0.000 description 1
239000003380 propellant Substances 0.000 description 1
239000003531 protein hydrolysate Substances 0.000 description 1
239000001944 prunus armeniaca kernel oil Substances 0.000 description 1
JEXVQSWXXUJEMA-UHFFFAOYSA-N pyrazol-3-one Chemical class O=C1C=CN=N1 JEXVQSWXXUJEMA-UHFFFAOYSA-N 0.000 description 1
PZRKPUQWIFJRKZ-UHFFFAOYSA-N pyrimidine-2,4,5,6-tetramine Chemical compound NC1=NC(N)=C(N)C(N)=N1 PZRKPUQWIFJRKZ-UHFFFAOYSA-N 0.000 description 1
150000003254 radicals Chemical class 0.000 description 1
239000000376 reactant Substances 0.000 description 1
238000006479 redox reaction Methods 0.000 description 1
235000002020 sage Nutrition 0.000 description 1
238000010517 secondary reaction Methods 0.000 description 1
229920005573 silicon-containing polymer Polymers 0.000 description 1
229940047670 sodium acrylate Drugs 0.000 description 1
229910000029 sodium carbonate Inorganic materials 0.000 description 1
235000017550 sodium carbonate Nutrition 0.000 description 1
229940057950 sodium laureth sulfate Drugs 0.000 description 1
MDSQKJDNWUMBQQ-UHFFFAOYSA-M sodium myreth sulfate Chemical compound [Na+].CCCCCCCCCCCCCCOCCOCCOCCOS([O-])(=O)=O MDSQKJDNWUMBQQ-UHFFFAOYSA-M 0.000 description 1
NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
229910052911 sodium silicate Inorganic materials 0.000 description 1
GNBVPFITFYNRCN-UHFFFAOYSA-M sodium thioglycolate Chemical compound [Na+].[O-]C(=O)CS GNBVPFITFYNRCN-UHFFFAOYSA-M 0.000 description 1
229940046307 sodium thioglycolate Drugs 0.000 description 1
GTKIEPUIFBBXJQ-UHFFFAOYSA-M sodium;2-[(4-hydroxy-9,10-dioxoanthracen-1-yl)amino]-5-methylbenzenesulfonate Chemical compound [Na+].[O-]S(=O)(=O)C1=CC(C)=CC=C1NC1=CC=C(O)C2=C1C(=O)C1=CC=CC=C1C2=O GTKIEPUIFBBXJQ-UHFFFAOYSA-M 0.000 description 1
FTUYQIPAPWPHNC-UHFFFAOYSA-M sodium;4-[[4-[benzyl(ethyl)amino]phenyl]-[4-[benzyl(ethyl)azaniumylidene]cyclohexa-2,5-dien-1-ylidene]methyl]benzene-1,3-disulfonate Chemical compound [Na+].C=1C=C(C(=C2C=CC(C=C2)=[N+](CC)CC=2C=CC=CC=2)C=2C(=CC(=CC=2)S([O-])(=O)=O)S([O-])(=O)=O)C=CC=1N(CC)CC1=CC=CC=C1 FTUYQIPAPWPHNC-UHFFFAOYSA-M 0.000 description 1
NJOYSONZACYNBD-UHFFFAOYSA-M sodium;aminomethanesulfinate Chemical compound [Na+].NCS([O-])=O NJOYSONZACYNBD-UHFFFAOYSA-M 0.000 description 1
239000000243 solution Substances 0.000 description 1
239000003549 soybean oil Substances 0.000 description 1
235000012424 soybean oil Nutrition 0.000 description 1
ANOBYBYXJXCGBS-UHFFFAOYSA-L stannous fluoride Chemical compound F[Sn]F ANOBYBYXJXCGBS-UHFFFAOYSA-L 0.000 description 1
229960002799 stannous fluoride Drugs 0.000 description 1
150000003452 sulfinic acid derivatives Chemical class 0.000 description 1
150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
239000002600 sunflower oil Substances 0.000 description 1
230000000475 sunscreen effect Effects 0.000 description 1
239000000516 sunscreening agent Substances 0.000 description 1
230000008961 swelling Effects 0.000 description 1
229920001864 tannin Polymers 0.000 description 1
235000018553 tannin Nutrition 0.000 description 1
239000001648 tannin Substances 0.000 description 1
229940095064 tartrate Drugs 0.000 description 1
235000012756 tartrazine Nutrition 0.000 description 1
UJMBCXLDXJUMFB-GLCFPVLVSA-K tartrazine Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)C1=NN(C=2C=CC(=CC=2)S([O-])(=O)=O)C(=O)C1\N=N\C1=CC=C(S([O-])(=O)=O)C=C1 UJMBCXLDXJUMFB-GLCFPVLVSA-K 0.000 description 1
239000004149 tartrazine Substances 0.000 description 1
SYRHIZPPCHMRIT-UHFFFAOYSA-N tin(4+) Chemical class [Sn+4] SYRHIZPPCHMRIT-UHFFFAOYSA-N 0.000 description 1
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
150000003626 triacylglycerols Chemical class 0.000 description 1
150000005691 triesters Chemical class 0.000 description 1
AAAQKTZKLRYKHR-UHFFFAOYSA-N triphenylmethane Chemical compound C1=CC=CC=C1C(C=1C=CC=CC=1)C1=CC=CC=C1 AAAQKTZKLRYKHR-UHFFFAOYSA-N 0.000 description 1
UJMBCXLDXJUMFB-UHFFFAOYSA-K trisodium;5-oxo-1-(4-sulfonatophenyl)-4-[(4-sulfonatophenyl)diazenyl]-4h-pyrazole-3-carboxylate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)C1=NN(C=2C=CC(=CC=2)S([O-])(=O)=O)C(=O)C1N=NC1=CC=C(S([O-])(=O)=O)C=C1 UJMBCXLDXJUMFB-UHFFFAOYSA-K 0.000 description 1
125000004417 unsaturated alkyl group Chemical group 0.000 description 1
150000003672 ureas Chemical class 0.000 description 1
229940099259 vaseline Drugs 0.000 description 1
235000015112 vegetable and seed oil Nutrition 0.000 description 1
239000008158 vegetable oil Substances 0.000 description 1
235000013311 vegetables Nutrition 0.000 description 1
239000003981 vehicle Substances 0.000 description 1
150000003722 vitamin derivatives Chemical class 0.000 description 1
239000001993 wax Substances 0.000 description 1
210000002268 wool Anatomy 0.000 description 1
239000011701 zinc Substances 0.000 description 1
229910052725 zinc Inorganic materials 0.000 description 1
PICXIOQBANWBIZ-UHFFFAOYSA-N zinc;1-oxidopyridine-2-thione Chemical compound [Zn+2].[O-]N1C=CC=CC1=S.[O-]N1C=CC=CC1=S PICXIOQBANWBIZ-UHFFFAOYSA-N 0.000 description 1
HPNCVECJEUYJQK-UHFFFAOYSA-L zinc;aminomethanesulfinate Chemical compound [Zn+2].NCS([O-])=O.NCS([O-])=O HPNCVECJEUYJQK-UHFFFAOYSA-L 0.000 description 1
CAAIULQYGCAMCD-UHFFFAOYSA-L zinc;hydroxymethanesulfinate Chemical compound [Zn+2].OCS([O-])=O.OCS([O-])=O CAAIULQYGCAMCD-UHFFFAOYSA-L 0.000 description 1