DE102013110453A1 - Verfahren zur Herstellung eines porösen Kohlenstofferzeugnisses - Google Patents
Verfahren zur Herstellung eines porösen Kohlenstofferzeugnisses Download PDFInfo
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- DE102013110453A1 DE102013110453A1 DE201310110453 DE102013110453A DE102013110453A1 DE 102013110453 A1 DE102013110453 A1 DE 102013110453A1 DE 201310110453 DE201310110453 DE 201310110453 DE 102013110453 A DE102013110453 A DE 102013110453A DE 102013110453 A1 DE102013110453 A1 DE 102013110453A1
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- C04B2111/00853—Uses not provided for elsewhere in C04B2111/00 in electrochemical cells or batteries, e.g. fuel cells
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
- H01M4/583—Carbonaceous material, e.g. graphite-intercalation compounds or CFx
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/86—Inert electrodes with catalytic activity, e.g. for fuel cells
- H01M4/96—Carbon-based electrodes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/50—Fuel cells
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Ceramic Engineering (AREA)
- Structural Engineering (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Thermal Sciences (AREA)
- Physics & Mathematics (AREA)
- Nanotechnology (AREA)
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- Carbon And Carbon Compounds (AREA)
- Battery Electrode And Active Subsutance (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE201310110453 DE102013110453A1 (de) | 2013-09-20 | 2013-09-20 | Verfahren zur Herstellung eines porösen Kohlenstofferzeugnisses |
| JP2016515387A JP6440693B2 (ja) | 2013-09-20 | 2014-09-19 | 多孔質の炭素製品を製造する方法 |
| US15/022,340 US9718690B2 (en) | 2013-09-20 | 2014-09-19 | Method for producing a porous carbon product |
| KR1020167010262A KR102090778B1 (ko) | 2013-09-20 | 2014-09-19 | 다공성 탄소 제품의 제조 방법 |
| EP14772108.8A EP3046891B1 (de) | 2013-09-20 | 2014-09-19 | Verfahren zur herstellung eines porösen kohlenstofferzeugnisses |
| PCT/EP2014/070044 WO2015040186A1 (de) | 2013-09-20 | 2014-09-19 | Verfahren zur herstellung eines porösen kohlenstofferzeugnisses |
| CN201480051216.9A CN105531241B (zh) | 2013-09-20 | 2014-09-19 | 制造多孔碳产品的方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE201310110453 DE102013110453A1 (de) | 2013-09-20 | 2013-09-20 | Verfahren zur Herstellung eines porösen Kohlenstofferzeugnisses |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE102013110453A1 true DE102013110453A1 (de) | 2015-03-26 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE201310110453 Withdrawn DE102013110453A1 (de) | 2013-09-20 | 2013-09-20 | Verfahren zur Herstellung eines porösen Kohlenstofferzeugnisses |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US9718690B2 (https=) |
| EP (1) | EP3046891B1 (https=) |
| JP (1) | JP6440693B2 (https=) |
| KR (1) | KR102090778B1 (https=) |
| CN (1) | CN105531241B (https=) |
| DE (1) | DE102013110453A1 (https=) |
| WO (1) | WO2015040186A1 (https=) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2022167450A1 (de) * | 2021-02-02 | 2022-08-11 | Salihovic Miralem | Verfahren zur herstellung eines kohlenstoffhaltigen formkörpers |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106098396B (zh) * | 2016-07-18 | 2018-05-29 | 南京邮电大学 | 一种用于超级电容器的垂直孔碳复合薄膜及其制备方法 |
| EP3476815B1 (en) * | 2017-10-27 | 2023-11-29 | Heraeus Quarzglas GmbH & Co. KG | Production of a porous product including post-adapting a pore structure |
| EP3476475B1 (en) * | 2017-10-27 | 2022-04-06 | Heraeus Battery Technology GmbH | Production of a porous carbon product |
| EP3476817A1 (en) | 2017-10-27 | 2019-05-01 | Heraeus Battery Technology GmbH | A process for the preparation of a porous carbon material using an improved amphiphilic species |
| EP3476818A1 (en) | 2017-10-27 | 2019-05-01 | Heraeus Battery Technology GmbH | A process for the preparation of a porous carbon material using an improved carbon source |
| JP7112192B2 (ja) * | 2017-11-07 | 2022-08-03 | 株式会社日本触媒 | 炭素材料の製造方法 |
| CN109081704A (zh) * | 2018-08-17 | 2018-12-25 | 苏州宏久航空防热材料科技有限公司 | 一种孔径梯度变化的碳泡沫的制备方法 |
| CN108892803B (zh) * | 2018-08-22 | 2021-03-12 | 苏州纳微科技股份有限公司 | 一种耐盐阴离子交换层析介质及其制备方法 |
| EP3733598A1 (en) * | 2019-04-30 | 2020-11-04 | Heraeus Battery Technology GmbH | A formulation comprising a graphitizable and a non-graphitizable carbon source |
| GB202010406D0 (en) * | 2020-07-07 | 2020-08-19 | Johnson Matthey Fuel Cells Ltd | Catalyst preparation |
| CN113078292B (zh) * | 2021-03-29 | 2022-08-19 | 宁德新能源科技有限公司 | 一种负极和包含该负极的电化学装置和电子装置 |
| CN113264771B (zh) * | 2021-06-17 | 2022-07-08 | 兰州理工大学 | 一种快速制备高强度碳泡沫的方法 |
| CN113796588B (zh) * | 2021-10-12 | 2025-04-25 | 松湖神健科技(东莞)有限公司 | 多孔碳发热体及其制备方法、电加热雾化芯及电子烟 |
| CN118419902A (zh) * | 2024-04-30 | 2024-08-02 | 西北工业大学 | 一种模板法结合发泡法合成多孔碳的方法及多孔碳 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2946688A1 (de) | 1978-11-21 | 1980-06-12 | Shandon Southern Prod | Verfahren zur herstellung von poroesem kohlenstoff sowie poroeser kohlenstoff |
| US20050169829A1 (en) | 2004-02-03 | 2005-08-04 | Sheng Dai | Robust carbon monolith having hierarchical porosity |
| DE69934256T2 (de) | 1998-06-08 | 2007-06-14 | UT-Battelle, LLC., Oak Ridge | Kühlkörper aus kohlenstoffschaum auf pechbasis mit material, welches phasenübergänge eingeht |
| WO2012011966A1 (en) | 2010-07-23 | 2012-01-26 | Kristian Eide | Solar panel racking system |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH10316411A (ja) * | 1997-05-12 | 1998-12-02 | Furukawa Co Ltd | 糖類の熱分解方法 |
| JP3885905B2 (ja) * | 1997-06-05 | 2007-02-28 | 古河機械金属株式会社 | 電気二重層コンデンサー |
| US6033506A (en) | 1997-09-02 | 2000-03-07 | Lockheed Martin Engery Research Corporation | Process for making carbon foam |
| DE102010005954B4 (de) * | 2010-01-27 | 2020-11-19 | Heraeus Quarzglas Gmbh & Co. Kg | Poröses Kohlenstofferzeugnis |
| DE102011013075B4 (de) * | 2011-03-04 | 2019-03-28 | Heraeus Quarzglas Gmbh & Co. Kg | Verfahren zur Herstellung eines porösen Kohlenstofferzeugnisses |
| JP5751582B2 (ja) * | 2011-06-03 | 2015-07-22 | 国立研究開発法人物質・材料研究機構 | 多孔性炭素膜の製造方法 |
| US9233366B2 (en) | 2012-10-16 | 2016-01-12 | Board Of Trustees Of The University Of Alabama | Catalysis by metal nanoparticles dispersed within a hierarchically porous carbon material |
-
2013
- 2013-09-20 DE DE201310110453 patent/DE102013110453A1/de not_active Withdrawn
-
2014
- 2014-09-19 WO PCT/EP2014/070044 patent/WO2015040186A1/de not_active Ceased
- 2014-09-19 CN CN201480051216.9A patent/CN105531241B/zh active Active
- 2014-09-19 EP EP14772108.8A patent/EP3046891B1/de active Active
- 2014-09-19 KR KR1020167010262A patent/KR102090778B1/ko active Active
- 2014-09-19 JP JP2016515387A patent/JP6440693B2/ja active Active
- 2014-09-19 US US15/022,340 patent/US9718690B2/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2946688A1 (de) | 1978-11-21 | 1980-06-12 | Shandon Southern Prod | Verfahren zur herstellung von poroesem kohlenstoff sowie poroeser kohlenstoff |
| DE69934256T2 (de) | 1998-06-08 | 2007-06-14 | UT-Battelle, LLC., Oak Ridge | Kühlkörper aus kohlenstoffschaum auf pechbasis mit material, welches phasenübergänge eingeht |
| US20050169829A1 (en) | 2004-02-03 | 2005-08-04 | Sheng Dai | Robust carbon monolith having hierarchical porosity |
| WO2012011966A1 (en) | 2010-07-23 | 2012-01-26 | Kristian Eide | Solar panel racking system |
Non-Patent Citations (1)
| Title |
|---|
| Lu, An-Hui; Schüth, Ferdi: Nanocasting: A Versatile Strategy for Creating Nanostructured Porous Materials. In: Adv. Mater., 18, 2006, 1793-1805. * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2022167450A1 (de) * | 2021-02-02 | 2022-08-11 | Salihovic Miralem | Verfahren zur herstellung eines kohlenstoffhaltigen formkörpers |
Also Published As
| Publication number | Publication date |
|---|---|
| JP6440693B2 (ja) | 2018-12-19 |
| EP3046891A1 (de) | 2016-07-27 |
| WO2015040186A1 (de) | 2015-03-26 |
| JP2016531818A (ja) | 2016-10-13 |
| KR20160060108A (ko) | 2016-05-27 |
| EP3046891B1 (de) | 2017-08-16 |
| KR102090778B1 (ko) | 2020-03-19 |
| CN105531241A (zh) | 2016-04-27 |
| US9718690B2 (en) | 2017-08-01 |
| US20160289077A1 (en) | 2016-10-06 |
| CN105531241B (zh) | 2017-11-14 |
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