DE102013009390A1 - Verfahren zur Oberflächenbehandlung von anorganischen Pigmentpartikeln - Google Patents
Verfahren zur Oberflächenbehandlung von anorganischen Pigmentpartikeln Download PDFInfo
- Publication number
- DE102013009390A1 DE102013009390A1 DE102013009390.2A DE102013009390A DE102013009390A1 DE 102013009390 A1 DE102013009390 A1 DE 102013009390A1 DE 102013009390 A DE102013009390 A DE 102013009390A DE 102013009390 A1 DE102013009390 A1 DE 102013009390A1
- Authority
- DE
- Germany
- Prior art keywords
- particles
- pigment particles
- inorganic
- titanium dioxide
- inorganic pigment
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000002245 particle Substances 0.000 title claims abstract description 78
- 238000000034 method Methods 0.000 title claims abstract description 34
- 239000001023 inorganic pigment Substances 0.000 title claims abstract description 23
- 238000004381 surface treatment Methods 0.000 title claims abstract description 17
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 83
- 239000000049 pigment Substances 0.000 claims abstract description 73
- 239000004408 titanium dioxide Substances 0.000 claims abstract description 41
- 239000002244 precipitate Substances 0.000 claims abstract description 18
- 239000011164 primary particle Substances 0.000 claims abstract description 14
- 229910010272 inorganic material Inorganic materials 0.000 claims abstract description 11
- 239000007900 aqueous suspension Substances 0.000 claims abstract description 10
- 150000002484 inorganic compounds Chemical class 0.000 claims abstract description 10
- 239000013078 crystal Substances 0.000 claims abstract description 9
- 239000007864 aqueous solution Substances 0.000 claims abstract description 6
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims abstract description 3
- 239000000725 suspension Substances 0.000 claims description 29
- 229910052782 aluminium Inorganic materials 0.000 claims description 20
- 238000001556 precipitation Methods 0.000 claims description 19
- 239000000243 solution Substances 0.000 claims description 15
- -1 aluminum compound Chemical class 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 13
- 238000000576 coating method Methods 0.000 claims description 12
- 230000002378 acidificating effect Effects 0.000 claims description 11
- 239000000047 product Substances 0.000 claims description 9
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 8
- 239000002253 acid Substances 0.000 claims description 7
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 7
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 claims description 5
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 4
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 2
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims description 2
- 239000004033 plastic Substances 0.000 claims description 2
- 229920003023 plastic Polymers 0.000 claims description 2
- 229910052710 silicon Inorganic materials 0.000 claims description 2
- 239000010703 silicon Substances 0.000 claims description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims 1
- 239000010936 titanium Substances 0.000 claims 1
- 229910052719 titanium Inorganic materials 0.000 claims 1
- 229910052726 zirconium Inorganic materials 0.000 claims 1
- 239000000839 emulsion Substances 0.000 abstract description 4
- 239000003973 paint Substances 0.000 abstract description 4
- 239000000123 paper Substances 0.000 description 38
- 229910010413 TiO 2 Inorganic materials 0.000 description 36
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 21
- ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 description 12
- 229910001388 sodium aluminate Inorganic materials 0.000 description 12
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 description 11
- 239000011248 coating agent Substances 0.000 description 9
- 239000010410 layer Substances 0.000 description 9
- 238000003917 TEM image Methods 0.000 description 8
- 229910004298 SiO 2 Inorganic materials 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 7
- 239000011259 mixed solution Substances 0.000 description 7
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 6
- 150000001875 compounds Chemical class 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 230000003287 optical effect Effects 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- ILRRQNADMUWWFW-UHFFFAOYSA-K aluminium phosphate Chemical compound O1[Al]2OP1(=O)O2 ILRRQNADMUWWFW-UHFFFAOYSA-K 0.000 description 4
- 238000011065 in-situ storage Methods 0.000 description 4
- 229920005989 resin Polymers 0.000 description 4
- 239000011347 resin Substances 0.000 description 4
- 125000006850 spacer group Chemical group 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 3
- 229910019142 PO4 Inorganic materials 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000000945 filler Substances 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 3
- 239000010452 phosphate Substances 0.000 description 3
- 235000019353 potassium silicate Nutrition 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 229910002651 NO3 Inorganic materials 0.000 description 2
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- 150000008043 acidic salts Chemical class 0.000 description 2
- 229910052910 alkali metal silicate Inorganic materials 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000005282 brightening Methods 0.000 description 2
- 239000003518 caustics Substances 0.000 description 2
- BUACSMWVFUNQET-UHFFFAOYSA-H dialuminum;trisulfate;hydrate Chemical compound O.[Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O BUACSMWVFUNQET-UHFFFAOYSA-H 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000012065 filter cake Substances 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 159000000011 group IA salts Chemical class 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 229910044991 metal oxide Inorganic materials 0.000 description 2
- 150000004706 metal oxides Chemical class 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- 239000011574 phosphorus Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- BUHVIAUBTBOHAG-FOYDDCNASA-N (2r,3r,4s,5r)-2-[6-[[2-(3,5-dimethoxyphenyl)-2-(2-methylphenyl)ethyl]amino]purin-9-yl]-5-(hydroxymethyl)oxolane-3,4-diol Chemical compound COC1=CC(OC)=CC(C(CNC=2C=3N=CN(C=3N=CN=2)[C@H]2[C@@H]([C@H](O)[C@@H](CO)O2)O)C=2C(=CC=CC=2)C)=C1 BUHVIAUBTBOHAG-FOYDDCNASA-N 0.000 description 1
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 description 1
- 239000005995 Aluminium silicate Substances 0.000 description 1
- 239000004606 Fillers/Extenders Substances 0.000 description 1
- 239000004640 Melamine resin Substances 0.000 description 1
- 229920000877 Melamine resin Polymers 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- 229910006404 SnO 2 Inorganic materials 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 description 1
- GEIAQOFPUVMAGM-UHFFFAOYSA-N ZrO Inorganic materials [Zr]=O GEIAQOFPUVMAGM-UHFFFAOYSA-N 0.000 description 1
- URRHWTYOQNLUKY-UHFFFAOYSA-N [AlH3].[P] Chemical class [AlH3].[P] URRHWTYOQNLUKY-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910000323 aluminium silicate Inorganic materials 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 235000010216 calcium carbonate Nutrition 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000011093 chipboard Substances 0.000 description 1
- 239000011247 coating layer Substances 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000009408 flooring Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 239000010954 inorganic particle Substances 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 238000010979 pH adjustment Methods 0.000 description 1
- 239000005011 phenolic resin Substances 0.000 description 1
- 229920001568 phenolic resin Polymers 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 235000012222 talc Nutrition 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 229920001187 thermosetting polymer Polymers 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- QXJQHYBHAIHNGG-UHFFFAOYSA-N trimethylolethane Chemical compound OCC(C)(CO)CO QXJQHYBHAIHNGG-UHFFFAOYSA-N 0.000 description 1
- 239000012463 white pigment Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 229910052724 xenon Inorganic materials 0.000 description 1
- FHNFHKCVQCLJFQ-UHFFFAOYSA-N xenon atom Chemical compound [Xe] FHNFHKCVQCLJFQ-UHFFFAOYSA-N 0.000 description 1
- 229910001928 zirconium oxide Inorganic materials 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/36—Compounds of titanium
- C09C1/3607—Titanium dioxide
- C09C1/3653—Treatment with inorganic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/02—Ingredients treated with inorganic substances
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/36—Compounds of titanium
- C09C1/3607—Titanium dioxide
- C09C1/3653—Treatment with inorganic compounds
- C09C1/3661—Coating
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/06—Treatment with inorganic compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/06—Treatment with inorganic compounds
- C09C3/063—Coating
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
- D21H17/69—Water-insoluble compounds, e.g. fillers, pigments modified, e.g. by association with other compositions prior to incorporation in the pulp or paper
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/28—Colorants ; Pigments or opacifying agents
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/28—Colorants ; Pigments or opacifying agents
- D21H21/285—Colorants ; Pigments or opacifying agents insoluble
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
- D21H27/18—Paper- or board-based structures for surface covering
- D21H27/22—Structures being applied on the surface by special manufacturing processes, e.g. in presses
- D21H27/26—Structures being applied on the surface by special manufacturing processes, e.g. in presses characterised by the overlay sheet or the top layers of the structures
- D21H27/28—Structures being applied on the surface by special manufacturing processes, e.g. in presses characterised by the overlay sheet or the top layers of the structures treated to obtain specific resistance properties, e.g. against wear or weather
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
- C01P2006/62—L* (lightness axis)
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Nanotechnology (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Composite Materials (AREA)
- Physics & Mathematics (AREA)
- Medicinal Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Polymers & Plastics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Paper (AREA)
- Paints Or Removers (AREA)
Priority Applications (17)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102013009390.2A DE102013009390A1 (de) | 2012-06-29 | 2013-06-05 | Verfahren zur Oberflächenbehandlung von anorganischen Pigmentpartikeln |
| JP2015518887A JP6265980B2 (ja) | 2012-06-29 | 2013-06-20 | 無機粒子の表面処理方法 |
| PCT/EP2013/001827 WO2014000873A1 (de) | 2012-06-29 | 2013-06-20 | Verfahren zur oberflächenbehandlung von anorganischen partikeln |
| MYPI2014703972A MY172701A (en) | 2012-06-29 | 2013-06-20 | Method for the surface treatment of inorganic pigment particles |
| UAA201411747A UA116443C2 (uk) | 2012-06-29 | 2013-06-20 | Спосіб поверхневої обробки частинок неорганічного пігменту |
| BR112014029985-4A BR112014029985B1 (pt) | 2012-06-29 | 2013-06-20 | Partículas de pigmento de dióxido de titânio, processo para o tratamento superficial das mesmas e seu uso |
| EP13753808.8A EP2875077B1 (de) | 2012-06-29 | 2013-06-20 | Verfahren zur oberflächenbehandlung von anorganischen partikeln |
| IN130MUN2015 IN2015MN00130A (https=) | 2012-06-29 | 2013-06-20 | |
| ES13753808T ES2794001T3 (es) | 2012-06-29 | 2013-06-20 | Procedimiento para el tratamiento de superficie de partículas inorgánicas |
| RU2015102919A RU2607402C2 (ru) | 2012-06-29 | 2013-06-20 | Способ обработки поверхности частиц неорганического пигмента и способ производства пластмасс, покрытий и ламинатов с помощью вышеуказанного полученного неорганического пигмента |
| KR1020157002040A KR102016900B1 (ko) | 2012-06-29 | 2013-06-20 | 무기 입자의 표면 처리 방법 |
| CN201380034839.0A CN104395412A (zh) | 2012-06-29 | 2013-06-20 | 将无机色素粒子作表面处理的方法 |
| MX2014015250A MX338027B (es) | 2012-06-29 | 2013-06-20 | Metodo para el tratamiento de superficie de las particulas de pigmento inorganico. |
| AU2013283882A AU2013283882B2 (en) | 2012-06-29 | 2013-06-20 | Method for the surface treatment of inorganic particles |
| US13/930,100 US8845803B2 (en) | 2012-06-29 | 2013-06-28 | Method for the surface treatment of inorganic pigment particles |
| US14/449,249 US9096762B2 (en) | 2012-06-29 | 2014-08-01 | Method for surface treatment of inorganic pigment particles |
| ZA2014/08259A ZA201408259B (en) | 2012-06-29 | 2014-11-11 | Method for the surface treatment of inorganic particles |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102012012931.9 | 2012-06-29 | ||
| DE102012012931 | 2012-06-29 | ||
| DE102013009390.2A DE102013009390A1 (de) | 2012-06-29 | 2013-06-05 | Verfahren zur Oberflächenbehandlung von anorganischen Pigmentpartikeln |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE102013009390A1 true DE102013009390A1 (de) | 2014-01-02 |
Family
ID=49754216
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE102013009390.2A Withdrawn DE102013009390A1 (de) | 2012-06-29 | 2013-06-05 | Verfahren zur Oberflächenbehandlung von anorganischen Pigmentpartikeln |
Country Status (18)
| Country | Link |
|---|---|
| US (2) | US8845803B2 (https=) |
| EP (1) | EP2875077B1 (https=) |
| JP (1) | JP6265980B2 (https=) |
| KR (1) | KR102016900B1 (https=) |
| CN (1) | CN104395412A (https=) |
| AU (1) | AU2013283882B2 (https=) |
| BR (1) | BR112014029985B1 (https=) |
| DE (1) | DE102013009390A1 (https=) |
| ES (1) | ES2794001T3 (https=) |
| IN (1) | IN2015MN00130A (https=) |
| MX (1) | MX338027B (https=) |
| MY (1) | MY172701A (https=) |
| RU (1) | RU2607402C2 (https=) |
| SA (2) | SA113340682B1 (https=) |
| TW (1) | TWI613261B (https=) |
| UA (1) | UA116443C2 (https=) |
| WO (1) | WO2014000873A1 (https=) |
| ZA (1) | ZA201408259B (https=) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI613261B (zh) * | 2012-06-29 | 2018-02-01 | 克洛諾斯國際有限公司 | 將無機色素粒子作表面處理的方法 |
| US10094069B2 (en) | 2013-01-09 | 2018-10-09 | The Chemours Company Fc, Llc | Process for making a décor paper having improved optical performance |
| CA2895946C (en) * | 2013-01-09 | 2020-10-20 | E. I. Du Pont De Nemours And Company | Decor paper having improved optical performance comprising treated inorganic particles |
| EP3190159A1 (de) * | 2016-01-08 | 2017-07-12 | Kronos International, Inc. | Verfahren zur oberflächenbeschichtung eines substrats |
| EP3199595A1 (de) * | 2016-01-27 | 2017-08-02 | Kronos International, Inc. | Herstellung von titandioxidpigment nach dem sulfatverfahren mit enger partikelgrössenverteilung |
| CN107163623A (zh) * | 2017-06-27 | 2017-09-15 | 安徽金星钛白(集团)有限公司 | 一种兼具高热稳定性和遮盖力的钛白粉制备方法 |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3591398A (en) | 1968-04-05 | 1971-07-06 | Du Pont | Process for producing titanium dioxide pigments |
| US4075031A (en) | 1976-09-30 | 1978-02-21 | E. I. Du Pont De Nemours And Company | TiO2 Pigment coated with dense silica and porous alumina/silica |
| WO2002077107A2 (de) | 2001-03-28 | 2002-10-03 | Kronos Titan Gmbh & Co. Ohg | Titandioxid-pigmentzusammensetzung |
| DE10332650A1 (de) | 2003-07-18 | 2005-02-10 | Kronos International, Inc. | Verfahren zur Oberflächenbehandlung eines Titandioxid-Pigments |
| DE102011015856A1 (de) | 2011-04-01 | 2012-10-04 | Kronos International, Inc. | Verfahren zur Oberflächenbehandlung eines Titandioxid-Pigments |
Family Cites Families (32)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1008652A (en) * | 1961-07-19 | 1965-11-03 | British Titan Products | Titanium dioxide pigment |
| GB1226554A (https=) * | 1967-07-11 | 1971-03-31 | ||
| GB1365411A (en) * | 1972-03-23 | 1974-09-04 | British Titan Ltd | Pigment production |
| DE2255826C3 (de) * | 1972-11-15 | 1980-10-02 | Bayer Ag, 5090 Leverkusen | Herstellung von nicht nachcalcinierten Titandioxidpigmenten mit hoher Vergrauungsstabilität für Harzkompositionen |
| FI52351C (fi) * | 1973-02-20 | 1977-08-10 | Kemira Oy | Menetelmä tekokuitujen himmentämiseen soveltuvan valonkestävän titaani dioksidipigmentin valmistamiseksi |
| FR2311823A1 (fr) * | 1975-05-23 | 1976-12-17 | Du Pont | Pigment tio2 revetu de silice dense et d'alumine/silice poreuse |
| GB1479989A (en) | 1975-07-17 | 1977-07-13 | Tioxide Group Ltd | Treatment of pigment |
| JPS5930749B2 (ja) * | 1976-03-12 | 1984-07-28 | 石原産業株式会社 | 二酸化チタン顔料組成物及びその製法 |
| DE3528256A1 (de) * | 1985-08-07 | 1987-02-19 | Merck Patent Gmbh | Eisenoxidbeschichtete perlglanzpigmente |
| DE4105345A1 (de) * | 1991-02-21 | 1992-08-27 | Kronos Int Inc | Verfahren zur herstellung von feinteiligem titandioxid und feinteiliges titandioxid |
| DE4222905A1 (de) * | 1992-07-11 | 1994-01-13 | Kronos Titan Gmbh | Subpigmentäres Titandioxid mit verbesserter Photostabilität |
| FR2727125B1 (fr) * | 1994-11-23 | 1999-01-29 | Rhone Poulenc Chimie | Procede de traitement de pigments de dioxyde de titane, nouveau pigment de dioxyde de titane et son utilisation dans la fabrication du papier |
| US6740312B2 (en) * | 1996-02-15 | 2004-05-25 | Rhodia Chimie | Titanium dioxide particles |
| AU706130B2 (en) * | 1996-03-04 | 1999-06-10 | Fp-Pigments Oy | Pigment particles coated with precipitated calcium carbonate and a process for the preparation thereof |
| US6045914A (en) * | 1996-06-03 | 2000-04-04 | Engelhard Corporation | Pearlescent glass pigment |
| FR2773167A1 (fr) | 1997-12-30 | 1999-07-02 | Rhodia Chimie Sa | Procede de preparation de flocs mineraux mixtes a base de tio2, composition a base de tio2 et de sio2 et son utilisation a titre d'agent opacifiant notamment en industrie papetiere |
| US6695906B2 (en) * | 2000-04-12 | 2004-02-24 | Millennium Inorganic Chemicals, Inc. | Continuous processes for producing titanium dioxide pigments |
| US7285162B2 (en) * | 2001-07-30 | 2007-10-23 | Millennium Inorganic Chemicals, Inc. | Titanium dioxide pigment having improved light stability |
| JP3745688B2 (ja) * | 2002-01-22 | 2006-02-15 | メルク株式会社 | 化粧用体質顔料およびその製造方法 |
| AU2003207551A1 (en) * | 2002-05-03 | 2003-11-17 | David O. Cummings | Paper coating pigments |
| JP4105971B2 (ja) * | 2003-03-27 | 2008-06-25 | 株式会社資生堂 | 多孔質酸化チタン粉体及びその製造方法 |
| US20050129634A1 (en) * | 2003-12-16 | 2005-06-16 | Frerichs Scott R. | Passivated nano-titanium dioxide particles and methods of making the same |
| US7288146B1 (en) * | 2006-03-16 | 2007-10-30 | Kronos International, Inc. | Titanium dioxide pigment coated with hollow bodies and method for its manufacture |
| DE102006012564B4 (de) * | 2006-03-16 | 2008-11-06 | Kronos International, Inc. | Mit Mikrohohlkugeln beschichtetes Titandioxid-Pigment und Verfahren zur Herstellung |
| US9005638B2 (en) * | 2006-10-12 | 2015-04-14 | Jgc Catalysts And Chemicals Ltd. | Cosmetics containing a multi-functional composite powder |
| US7264672B1 (en) * | 2006-10-31 | 2007-09-04 | National Titanium Dioxide Co. Ltd. (Cristal) | Titanium dioxide pigment composite and method of making same |
| DE102006059849A1 (de) * | 2006-12-15 | 2008-06-19 | Kronos International, Inc. | Verfahren zur Oberflächenbehandlung von Festkörperpartikeln, insbesondere Titandioxid-Pigmentpartikel |
| DE102008026300A1 (de) * | 2008-06-02 | 2009-12-03 | Kronos International, Inc. | Verfahren zur Oberflächenbeschichtung von anorganischen Festkörperpartikeln, insbesondere Titandioxid-Pigmentpartikel |
| DE102008058351A1 (de) * | 2008-11-20 | 2010-06-02 | Kronos International, Inc. | Oberflächenbehandelte Titandioxid-Pigmente für Kunststoffe und Verfahren zur Herstellung |
| US8840719B2 (en) * | 2011-03-09 | 2014-09-23 | Tronox Llc | Titanium dioxide pigments and manufacturing method |
| US9481797B2 (en) * | 2011-08-09 | 2016-11-01 | Cristal Usa Inc. | Pigment for paper and paper laminate |
| TWI613261B (zh) * | 2012-06-29 | 2018-02-01 | 克洛諾斯國際有限公司 | 將無機色素粒子作表面處理的方法 |
-
2013
- 2013-06-05 TW TW102119889A patent/TWI613261B/zh not_active IP Right Cessation
- 2013-06-05 DE DE102013009390.2A patent/DE102013009390A1/de not_active Withdrawn
- 2013-06-20 MY MYPI2014703972A patent/MY172701A/en unknown
- 2013-06-20 KR KR1020157002040A patent/KR102016900B1/ko active Active
- 2013-06-20 BR BR112014029985-4A patent/BR112014029985B1/pt active IP Right Grant
- 2013-06-20 ES ES13753808T patent/ES2794001T3/es active Active
- 2013-06-20 EP EP13753808.8A patent/EP2875077B1/de active Active
- 2013-06-20 UA UAA201411747A patent/UA116443C2/uk unknown
- 2013-06-20 RU RU2015102919A patent/RU2607402C2/ru active
- 2013-06-20 AU AU2013283882A patent/AU2013283882B2/en not_active Ceased
- 2013-06-20 WO PCT/EP2013/001827 patent/WO2014000873A1/de not_active Ceased
- 2013-06-20 CN CN201380034839.0A patent/CN104395412A/zh active Pending
- 2013-06-20 MX MX2014015250A patent/MX338027B/es active IP Right Grant
- 2013-06-20 JP JP2015518887A patent/JP6265980B2/ja not_active Expired - Fee Related
- 2013-06-20 IN IN130MUN2015 patent/IN2015MN00130A/en unknown
- 2013-06-26 SA SA113340682A patent/SA113340682B1/ar unknown
- 2013-06-26 SA SA115360608A patent/SA115360608B1/ar unknown
- 2013-06-28 US US13/930,100 patent/US8845803B2/en not_active Expired - Fee Related
-
2014
- 2014-08-01 US US14/449,249 patent/US9096762B2/en active Active
- 2014-11-11 ZA ZA2014/08259A patent/ZA201408259B/en unknown
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3591398A (en) | 1968-04-05 | 1971-07-06 | Du Pont | Process for producing titanium dioxide pigments |
| US4075031A (en) | 1976-09-30 | 1978-02-21 | E. I. Du Pont De Nemours And Company | TiO2 Pigment coated with dense silica and porous alumina/silica |
| WO2002077107A2 (de) | 2001-03-28 | 2002-10-03 | Kronos Titan Gmbh & Co. Ohg | Titandioxid-pigmentzusammensetzung |
| DE10332650A1 (de) | 2003-07-18 | 2005-02-10 | Kronos International, Inc. | Verfahren zur Oberflächenbehandlung eines Titandioxid-Pigments |
| DE102011015856A1 (de) | 2011-04-01 | 2012-10-04 | Kronos International, Inc. | Verfahren zur Oberflächenbehandlung eines Titandioxid-Pigments |
Non-Patent Citations (1)
| Title |
|---|
| DIN 6174 |
Also Published As
| Publication number | Publication date |
|---|---|
| RU2015102919A (ru) | 2016-08-20 |
| EP2875077B1 (de) | 2020-03-25 |
| KR102016900B1 (ko) | 2019-09-02 |
| SA115360608B1 (ar) | 2016-01-27 |
| MX2014015250A (es) | 2015-03-05 |
| MX338027B (es) | 2016-03-31 |
| WO2014000873A1 (de) | 2014-01-03 |
| US20140000483A1 (en) | 2014-01-02 |
| BR112014029985B1 (pt) | 2022-01-18 |
| WO2014000873A8 (de) | 2014-12-31 |
| MY172701A (en) | 2019-12-10 |
| CN104395412A (zh) | 2015-03-04 |
| ES2794001T3 (es) | 2020-11-17 |
| UA116443C2 (uk) | 2018-03-26 |
| EP2875077A1 (de) | 2015-05-27 |
| JP6265980B2 (ja) | 2018-01-24 |
| US8845803B2 (en) | 2014-09-30 |
| TWI613261B (zh) | 2018-02-01 |
| AU2013283882B2 (en) | 2015-12-24 |
| US9096762B2 (en) | 2015-08-04 |
| KR20150034738A (ko) | 2015-04-03 |
| TW201402714A (zh) | 2014-01-16 |
| BR112014029985A2 (pt) | 2017-06-27 |
| SA113340682B1 (ar) | 2015-07-30 |
| US20140338566A1 (en) | 2014-11-20 |
| RU2607402C2 (ru) | 2017-01-10 |
| JP2015527429A (ja) | 2015-09-17 |
| ZA201408259B (en) | 2017-08-30 |
| IN2015MN00130A (https=) | 2015-10-16 |
| AU2013283882A1 (en) | 2015-01-22 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP1989264B1 (de) | Titandioxid-pigment mit hoher opazität und verfahren zur herstellung | |
| EP2694599B1 (de) | Verfahren zur oberflächenbehandlung eines titandioxid-pigments | |
| EP1603978B1 (de) | Verfahren zur oberflächenbehandlung eines titandioxid-pigments | |
| EP1646692B1 (de) | Verfahren zur oberflächenbehandlung eines titandioxid-pigments | |
| EP1994098A2 (de) | Mit hohlkörpern beschichtetes titandioxid-pigment und verfahren zur herstellung | |
| DE69005926T3 (de) | Verfahren zum Beschichten von Titandioxidpigmenten. | |
| EP2877539B1 (de) | Titandioxid-haltige und carbonat-haltige kompositpigmente und verfahren zu ihrer herstellung | |
| WO2006012950A1 (de) | Witterungsstabiles titandioxid-pigment und verfahren zu seiner herstellung | |
| EP2875077B1 (de) | Verfahren zur oberflächenbehandlung von anorganischen partikeln | |
| DE102012017854A1 (de) | Infrarot-reflektierendes Pigment auf Basis Titandioxid sowie Verfahren zu seiner Herstellung | |
| DE102004037272B4 (de) | Verfahren zur Nachbehandlung von Titandioxid-Pigmenten | |
| EP1373412B1 (de) | Titandioxid-pigmentzusammensetzung | |
| WO2016142042A1 (de) | Aluminiumhydroxid-haltige kompositpigmente und verfahren zu ihrer herstellung |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| R005 | Application deemed withdrawn due to failure to request examination |