DE102013002724B3 - Verfahren und Vorrichtung zur Bestimmung der Permeationsrate von Barrierematerialien - Google Patents

Verfahren und Vorrichtung zur Bestimmung der Permeationsrate von Barrierematerialien Download PDF

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DE102013002724B3
DE102013002724B3 DE102013002724.1A DE102013002724A DE102013002724B3 DE 102013002724 B3 DE102013002724 B3 DE 102013002724B3 DE 102013002724 A DE102013002724 A DE 102013002724A DE 102013002724 B3 DE102013002724 B3 DE 102013002724B3
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concentration
measuring
time
permeate
measurement
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Wulf Grählert
Harald Beese
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Fraunhofer Gesellschaft zur Foerderung der Angewandten Forschung eV
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Fraunhofer Gesellschaft zur Foerderung der Angewandten Forschung eV
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Priority to DE102013002724.1A priority Critical patent/DE102013002724B3/de
Priority to EP14152470.2A priority patent/EP2781905B1/de
Priority to JP2014023683A priority patent/JP6041218B2/ja
Priority to US14/178,634 priority patent/US9470615B2/en
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    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/082—Investigating permeability by forcing a fluid through a sample
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/082—Investigating permeability by forcing a fluid through a sample
    • G01N15/0826—Investigating permeability by forcing a fluid through a sample and measuring fluid flow rate, i.e. permeation rate or pressure change
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/0806—Details, e.g. sample holders, mounting samples for testing
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
    • G01N2015/086—Investigating permeability, pore-volume, or surface area of porous materials of films, membranes or pellicules
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/39—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using tunable lasers
    • G01N2021/396—Type of laser source
    • G01N2021/399—Diode laser
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/01—Arrangements or apparatus for facilitating the optical investigation
    • G01N21/03—Cuvette constructions
    • G01N21/031—Multipass arrangements
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/33—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using ultraviolet light
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/3504—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing gases, e.g. multi-gas analysis
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/3581—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light using far infrared light; using Terahertz radiation
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/359—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light using near infrared light

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  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Biochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Fluid Mechanics (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)
  • Sampling And Sample Adjustment (AREA)
DE102013002724.1A 2013-02-12 2013-02-12 Verfahren und Vorrichtung zur Bestimmung der Permeationsrate von Barrierematerialien Active DE102013002724B3 (de)

Priority Applications (4)

Application Number Priority Date Filing Date Title
DE102013002724.1A DE102013002724B3 (de) 2013-02-12 2013-02-12 Verfahren und Vorrichtung zur Bestimmung der Permeationsrate von Barrierematerialien
EP14152470.2A EP2781905B1 (de) 2013-02-12 2014-01-24 Verfahren und vorrichtung zur bestimmung der permeationsrate von barrierematerialien
JP2014023683A JP6041218B2 (ja) 2013-02-12 2014-02-10 バリア材の透過度を測定する方法及び装置
US14/178,634 US9470615B2 (en) 2013-02-12 2014-02-12 Method and apparatus for determining the permeation rate of barrier materials

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102013002724.1A DE102013002724B3 (de) 2013-02-12 2013-02-12 Verfahren und Vorrichtung zur Bestimmung der Permeationsrate von Barrierematerialien

Publications (1)

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DE102013002724B3 true DE102013002724B3 (de) 2014-07-03

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US (1) US9470615B2 (enExample)
EP (1) EP2781905B1 (enExample)
JP (1) JP6041218B2 (enExample)
DE (1) DE102013002724B3 (enExample)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2528096A (en) * 2014-07-09 2016-01-13 Paraytec Ltd Method
DE102015113026A1 (de) 2015-08-07 2017-02-09 Eisenhuth Gmbh & Co. Kg Verfahren und Vorrichtung zum Erfassen einer Permeationsrate durch ein flächiges Prüfobjekt
CN116148155A (zh) * 2023-02-27 2023-05-23 贝士德仪器科技(北京)有限公司 气体分离膜渗透率及分离系数测试仪及其测试方法
DE102022204158A1 (de) 2022-04-28 2023-11-02 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung eingetragener Verein Verfahren und Vorrichtung zum Ermitteln einer Durchlässigkeit einer Probe
DE102022211645B3 (de) 2022-11-04 2024-01-18 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung eingetragener Verein Verfahren zur Bestimmung der Permeationsrate mindestens eines Permeaten durch ein Barrierematerial

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EP2872872A4 (en) * 2012-07-12 2016-03-30 Univ Florida METHOD AND DEVICE FOR INCREASING THE SPEED AND / OR RESOLUTION OF GAS PERMEATION MEASUREMENTS
FR2997763B1 (fr) * 2012-11-06 2015-01-16 Commissariat Energie Atomique Dispositif et procede d'estimation d'un flux de gaz dans une enceinte maintenue en depression vis-a-vis du gaz
EP3111229B1 (en) * 2014-02-24 2021-12-01 Mocon, Inc. Protocol adaptive computer controlled target-analyte permeation testing instrument
FR3028950B1 (fr) * 2014-11-24 2018-03-23 Commissariat A L'energie Atomique Et Aux Energies Alternatives Procede et dispositif de mesure de permeation par spectrometrie de masse
JP6818483B2 (ja) * 2016-09-23 2021-01-20 日東電工株式会社 動的透湿性評価装置、動的透湿性評価方法及び動的透湿性評価プログラム
EP3781929B1 (en) * 2018-04-20 2022-06-08 Flo2R Aps Gas analysis system and method
CN109470616B (zh) * 2018-10-31 2021-11-23 重庆大学 岩石多功能渗流测试系统
US11181460B1 (en) * 2019-06-20 2021-11-23 The United States Of America As Represented By The Secretary Of The Army Apparatus and method for measuring permeation of contaminants through a complex protective material swatch
CN110376115B (zh) * 2019-08-30 2024-04-30 贵州大学 一种两环一体的双环渗水试验装置及其操作方法
DE102019220561B4 (de) * 2019-12-23 2021-09-30 Greenerity Gmbh Verfahren und Vorrichtung zur Analyse einer funktionalen Schicht einer elektrochemischen Zelle oder einer elektrochemischen Sensorenanwendung
CN111189943B (zh) * 2020-03-05 2022-12-09 中国烟草总公司郑州烟草研究院 一种烟片中甘油渗透速率的检测方法
KR102479085B1 (ko) * 2021-03-11 2022-12-16 경상국립대학교산학협력단 비등방성 유동 투과율 측정 방법 및 이를 이용한 비등방성 유동 투과율 측정 장치
US11959696B2 (en) * 2022-04-11 2024-04-16 Whirlpool Corporation Vacuum insulated appliance with pressure monitoring

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DE1673032A1 (de) * 1966-07-21 1971-04-29 Sentralinst For Ind Forskning Verfahren und Vorrichtung zum Messen der Gas- oder Dampfdurchlaessigkeit von Filmen
DE2514848A1 (de) * 1974-04-10 1975-10-23 Modern Controls Inc Verfahren und vorrichtung zum messen der gasdurchlaessigkeit von verpackungsmaterialien
US4852389A (en) * 1988-03-28 1989-08-01 Modern Controls, Inc. System for controlled humidity tests
US4944180A (en) * 1988-08-26 1990-07-31 The Dow Chemical Company Permeation measurement device
US5591898A (en) * 1995-10-12 1997-01-07 Modern Controls, Inc. Method for measuring material permeability characteristics
US5817924A (en) * 1998-01-21 1998-10-06 Modern Controls, Inc. Method and apparatus for measuring oxygen transmission through contact lenses
US20040123646A1 (en) * 2002-12-25 2004-07-01 Matsushita Electric Industrial Co., Ltd Gas permeability measurement method and gas permeability measurement device
US6964191B1 (en) * 2002-10-15 2005-11-15 Murthy Tata Apparatus and technique for measuring permeability and permeant sorption
DE102007014182A1 (de) * 2006-03-30 2007-12-06 Technolox Ltd. Verfahren und Vorrichtung zur Bestimmung der Rate der Permeation von Gasen und Dämpfen durch Materialien
DE102007026073A1 (de) * 2007-05-25 2008-11-27 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Vorrichtung und Verfahren zur Bestimmung der Permeationsrate mindestens eines Permeaten, durch ein eine Diffusionssperre bildendes Element
US20100294025A1 (en) * 2007-09-28 2010-11-25 Daisuke Omori Apparatus and method for measurement of water vapor permeability

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US6598463B2 (en) * 2001-05-02 2003-07-29 Du Pont Method for determining gas accumulation rates
JP2002357533A (ja) * 2001-05-31 2002-12-13 Sony Corp 透過性評価方法及びその装置
JP2006071340A (ja) * 2004-08-31 2006-03-16 Kurita Water Ind Ltd 液体中の溶存気体濃度の測定方法、測定装置及び窒素ガス溶解水の製造装置
JP2010190751A (ja) * 2009-02-18 2010-09-02 Mitsubishi Chemicals Corp フィルム材料のガス透過度測定装置及びガス透過度測定方法
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JP5275473B2 (ja) * 2009-11-10 2013-08-28 株式会社アルバック 水蒸気透過量測定装置及び水蒸気透過量測定方法
JPWO2011132391A1 (ja) * 2010-04-23 2013-07-18 株式会社アルバック 透湿度測定装置及び透湿度測定方法
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Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1673032A1 (de) * 1966-07-21 1971-04-29 Sentralinst For Ind Forskning Verfahren und Vorrichtung zum Messen der Gas- oder Dampfdurchlaessigkeit von Filmen
DE2514848A1 (de) * 1974-04-10 1975-10-23 Modern Controls Inc Verfahren und vorrichtung zum messen der gasdurchlaessigkeit von verpackungsmaterialien
US4852389A (en) * 1988-03-28 1989-08-01 Modern Controls, Inc. System for controlled humidity tests
US4944180A (en) * 1988-08-26 1990-07-31 The Dow Chemical Company Permeation measurement device
US5591898A (en) * 1995-10-12 1997-01-07 Modern Controls, Inc. Method for measuring material permeability characteristics
US5817924A (en) * 1998-01-21 1998-10-06 Modern Controls, Inc. Method and apparatus for measuring oxygen transmission through contact lenses
US6964191B1 (en) * 2002-10-15 2005-11-15 Murthy Tata Apparatus and technique for measuring permeability and permeant sorption
US20040123646A1 (en) * 2002-12-25 2004-07-01 Matsushita Electric Industrial Co., Ltd Gas permeability measurement method and gas permeability measurement device
DE102007014182A1 (de) * 2006-03-30 2007-12-06 Technolox Ltd. Verfahren und Vorrichtung zur Bestimmung der Rate der Permeation von Gasen und Dämpfen durch Materialien
DE102007026073A1 (de) * 2007-05-25 2008-11-27 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Vorrichtung und Verfahren zur Bestimmung der Permeationsrate mindestens eines Permeaten, durch ein eine Diffusionssperre bildendes Element
US20100294025A1 (en) * 2007-09-28 2010-11-25 Daisuke Omori Apparatus and method for measurement of water vapor permeability

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2528096A (en) * 2014-07-09 2016-01-13 Paraytec Ltd Method
US9891156B2 (en) 2014-07-09 2018-02-13 Paraytec Limited Method for determining the permeation of a permeant through a membrane
DE102015113026A1 (de) 2015-08-07 2017-02-09 Eisenhuth Gmbh & Co. Kg Verfahren und Vorrichtung zum Erfassen einer Permeationsrate durch ein flächiges Prüfobjekt
DE102015113026B4 (de) * 2015-08-07 2021-03-04 Eisenhuth Gmbh & Co. Kg Verfahren und Vorrichtung zum Erfassen einer Permeationsrate durch ein flächiges Prüfobjekt
DE102022204158A1 (de) 2022-04-28 2023-11-02 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung eingetragener Verein Verfahren und Vorrichtung zum Ermitteln einer Durchlässigkeit einer Probe
WO2023209163A1 (de) 2022-04-28 2023-11-02 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Verfahren und vorrichtung zum ermitteln einer durchlässigkeit einer probe
DE102022211645B3 (de) 2022-11-04 2024-01-18 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung eingetragener Verein Verfahren zur Bestimmung der Permeationsrate mindestens eines Permeaten durch ein Barrierematerial
CN116148155A (zh) * 2023-02-27 2023-05-23 贝士德仪器科技(北京)有限公司 气体分离膜渗透率及分离系数测试仪及其测试方法
CN116148155B (zh) * 2023-02-27 2023-09-29 贝士德仪器科技(北京)有限公司 气体分离膜渗透率及分离系数测试仪及其测试方法

Also Published As

Publication number Publication date
JP2014160069A (ja) 2014-09-04
EP2781905B1 (de) 2019-05-22
US20140223999A1 (en) 2014-08-14
US9470615B2 (en) 2016-10-18
JP6041218B2 (ja) 2016-12-07
EP2781905A1 (de) 2014-09-24

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