DE102009006777A1 - Verfahren zur Herstellung von Fettsäureestern und Glycerin durch Umesterung von pflanzlichen und tierischen Fetten und Ölen - Google Patents

Verfahren zur Herstellung von Fettsäureestern und Glycerin durch Umesterung von pflanzlichen und tierischen Fetten und Ölen Download PDF

Info

Publication number
DE102009006777A1
DE102009006777A1 DE200910006777 DE102009006777A DE102009006777A1 DE 102009006777 A1 DE102009006777 A1 DE 102009006777A1 DE 200910006777 DE200910006777 DE 200910006777 DE 102009006777 A DE102009006777 A DE 102009006777A DE 102009006777 A1 DE102009006777 A1 DE 102009006777A1
Authority
DE
Germany
Prior art keywords
catalyst
oxides
fatty acid
glycerol
rare earth
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE200910006777
Other languages
German (de)
English (en)
Inventor
Wolfgang F. Prof. Dr. Hölderich
Bernhard Markus Ernst Rußbüldt
Marius Maximilian Maronna
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to DE200910006777 priority Critical patent/DE102009006777A1/de
Priority to PCT/DE2010/000109 priority patent/WO2010085947A1/fr
Priority to DE201011000206 priority patent/DE112010000206A5/de
Publication of DE102009006777A1 publication Critical patent/DE102009006777A1/de
Withdrawn legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/10—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of rare earths
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/082—Decomposition and pyrolysis
    • B01J37/086—Decomposition of an organometallic compound, a metal complex or a metal salt of a carboxylic acid
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/021—After-treatment of oxides or hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/003—Titanates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
    • C10L1/026—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only for compression ignition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/02—Boron or aluminium; Oxides or hydroxides thereof
    • B01J21/04—Alumina
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/30—Three-dimensional structures
    • C01P2002/36—Three-dimensional structures pyrochlore-type (A2B2O7)
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Wood Science & Technology (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Catalysts (AREA)
  • Fats And Perfumes (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE200910006777 2009-01-30 2009-01-30 Verfahren zur Herstellung von Fettsäureestern und Glycerin durch Umesterung von pflanzlichen und tierischen Fetten und Ölen Withdrawn DE102009006777A1 (de)

Priority Applications (3)

Application Number Priority Date Filing Date Title
DE200910006777 DE102009006777A1 (de) 2009-01-30 2009-01-30 Verfahren zur Herstellung von Fettsäureestern und Glycerin durch Umesterung von pflanzlichen und tierischen Fetten und Ölen
PCT/DE2010/000109 WO2010085947A1 (fr) 2009-01-30 2010-01-29 Procédé de production d'esters d'acides gras et de glycérol par transestérification de graisses et d'huiles végétales et animales
DE201011000206 DE112010000206A5 (de) 2009-01-30 2010-01-29 Verfahren zur Herstellung von Fettsäureestern und Glycerin durch Umesterung von pflanzlichen und tierischen Fetten und Ölen

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE200910006777 DE102009006777A1 (de) 2009-01-30 2009-01-30 Verfahren zur Herstellung von Fettsäureestern und Glycerin durch Umesterung von pflanzlichen und tierischen Fetten und Ölen

Publications (1)

Publication Number Publication Date
DE102009006777A1 true DE102009006777A1 (de) 2010-08-05

Family

ID=42197685

Family Applications (2)

Application Number Title Priority Date Filing Date
DE200910006777 Withdrawn DE102009006777A1 (de) 2009-01-30 2009-01-30 Verfahren zur Herstellung von Fettsäureestern und Glycerin durch Umesterung von pflanzlichen und tierischen Fetten und Ölen
DE201011000206 Withdrawn DE112010000206A5 (de) 2009-01-30 2010-01-29 Verfahren zur Herstellung von Fettsäureestern und Glycerin durch Umesterung von pflanzlichen und tierischen Fetten und Ölen

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE201011000206 Withdrawn DE112010000206A5 (de) 2009-01-30 2010-01-29 Verfahren zur Herstellung von Fettsäureestern und Glycerin durch Umesterung von pflanzlichen und tierischen Fetten und Ölen

Country Status (2)

Country Link
DE (2) DE102009006777A1 (fr)
WO (1) WO2010085947A1 (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013190038A2 (fr) * 2012-06-22 2013-12-27 Symrise Ag Catalyseurs supportés permettant de produire des produits de condensation aldolique

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8070836B2 (en) 2007-10-16 2011-12-06 Wayne State University Combined homogeneous and heterogeneous catalytic transesterification process for biodiesel production
CN105026316B (zh) 2013-07-11 2018-06-22 沙特基础工业全球技术公司 制备烧绿石的方法

Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3932514A1 (de) 1989-09-29 1991-04-18 Henkel Kgaa Kontinuierliches verfahren zum herstellen niederer alkylester
DE4123928A1 (de) 1991-07-19 1993-01-21 Metallgesellschaft Ag Verfahren zum erzeugen von fettsaeure-methylester oder fettsaeure-aethylester und glycerin durch umesterung von oelen oder fetten
DE4209779C1 (fr) 1992-03-26 1993-07-15 Oelmuehle Leer Connemann Gmbh & Co., 2950 Leer, De
US5908946A (en) 1996-08-08 1999-06-01 Institut Francais Du Petrole Process for the production of esters from vegetable oils or animal oils alcohols
US6147196A (en) 1997-12-18 2000-11-14 Institut Francais Du Petrole Process for producing esters of fatty substances and the high purity esters produced
US6359157B2 (en) 1999-10-20 2002-03-19 Siegfried Peter Process for the transesterification of fat and/or oil of biological origin by means of alcoholysis
US6878837B2 (en) 2002-04-11 2005-04-12 Institut Francais Du Petrole Process for producing alkyl esters from a vegetable or animal oil and an aliphatic monoalcohol
JP2006104316A (ja) 2004-10-05 2006-04-20 Tohoku Techno Arch Co Ltd 脂肪酸エステルの製造方法
FR2882052A1 (fr) 2005-02-15 2006-08-18 Arkema Sa Procede de deshydratation du glycerol en acroleine
FR2882053A1 (fr) 2005-02-15 2006-08-18 Arkema Sa Procede de deshydratation du glycerol en acrolene
WO2008012275A1 (fr) 2006-07-26 2008-01-31 Vlaamse Instelling Voor Technologisch Onderzoek (Vito) Nouveau procédé de production de biodiesel utilisant un catalyseur immobilisé

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4102939A (en) * 1976-11-08 1978-07-25 Phillips Petroleum Company Olefin disproportionation over silica-rare earth metal oxide catalysts
FR2811984B1 (fr) * 2000-07-19 2004-02-06 Pharmascience Lab Procede de preparation d'un ester de corps gras et son utilisation dans les domaines pharmaceutique, cosmetique ou alimentaire
TW200536821A (en) * 2004-02-05 2005-11-16 Showa Denko Kk Production process of 3-alkoxy-1-propanols, and 3-alkoxy-1-propanols obtained by the production process
JP2008274030A (ja) * 2007-04-26 2008-11-13 Oita Univ バイオディーゼル燃料の製造方法
PH12010501172A1 (en) * 2007-12-19 2009-06-25 Bayer Technology Services Gmbh Method for producing fatty acid alkyl esters

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3932514A1 (de) 1989-09-29 1991-04-18 Henkel Kgaa Kontinuierliches verfahren zum herstellen niederer alkylester
DE4123928A1 (de) 1991-07-19 1993-01-21 Metallgesellschaft Ag Verfahren zum erzeugen von fettsaeure-methylester oder fettsaeure-aethylester und glycerin durch umesterung von oelen oder fetten
DE4209779C1 (fr) 1992-03-26 1993-07-15 Oelmuehle Leer Connemann Gmbh & Co., 2950 Leer, De
US5908946A (en) 1996-08-08 1999-06-01 Institut Francais Du Petrole Process for the production of esters from vegetable oils or animal oils alcohols
US6147196A (en) 1997-12-18 2000-11-14 Institut Francais Du Petrole Process for producing esters of fatty substances and the high purity esters produced
US6359157B2 (en) 1999-10-20 2002-03-19 Siegfried Peter Process for the transesterification of fat and/or oil of biological origin by means of alcoholysis
US6878837B2 (en) 2002-04-11 2005-04-12 Institut Francais Du Petrole Process for producing alkyl esters from a vegetable or animal oil and an aliphatic monoalcohol
JP2006104316A (ja) 2004-10-05 2006-04-20 Tohoku Techno Arch Co Ltd 脂肪酸エステルの製造方法
FR2882052A1 (fr) 2005-02-15 2006-08-18 Arkema Sa Procede de deshydratation du glycerol en acroleine
FR2882053A1 (fr) 2005-02-15 2006-08-18 Arkema Sa Procede de deshydratation du glycerol en acrolene
WO2008012275A1 (fr) 2006-07-26 2008-01-31 Vlaamse Instelling Voor Technologisch Onderzoek (Vito) Nouveau procédé de production de biodiesel utilisant un catalyseur immobilisé

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Catalysis Communications 8 (2007) 1969-1972

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013190038A2 (fr) * 2012-06-22 2013-12-27 Symrise Ag Catalyseurs supportés permettant de produire des produits de condensation aldolique
WO2013190038A3 (fr) * 2012-06-22 2014-03-06 Symrise Ag Catalyseurs supportés permettant de produire des produits de condensation aldolique

Also Published As

Publication number Publication date
WO2010085947A1 (fr) 2010-08-05
DE112010000206A5 (de) 2012-05-16

Similar Documents

Publication Publication Date Title
EP0339426B1 (fr) Utilisation d'hydrotalcites calcinées comme catalyseurs d'éthoxylation ou de propoxylation
JP5576271B2 (ja) 油脂からの脂肪酸アルキルエステル及び／又はグリセリンの製造方法
Zheng et al. Transesterification of glycerol with dimethyl carbonate over calcined Ca-Al hydrocalumite
EP3684751B1 (fr) Catalyseur pour l'esterification oxydative d'aldehydes en esters d'acide carbonique
WO2007029851A1 (fr) Procédé de production d’esters d’alkyle d'acides gras et/ou de glycérine
CN103801282B (zh) 一种固体碱催化剂及其制备和应用
WO2010052181A2 (fr) Procédé de fabrication de 3-aminopropan-1-ols n,n-substitués
EP2358851B1 (fr) Utilisation de l'acide méthanesulfonique pour la fabrication d'esters d'acide gras
WO2010020053A1 (fr) Catalyseurs hétérogènes solides et procédés d'utilisation
DE102009006777A1 (de) Verfahren zur Herstellung von Fettsäureestern und Glycerin durch Umesterung von pflanzlichen und tierischen Fetten und Ölen
KR100644246B1 (ko) 동·식물유로부터 지방산 알킬 에스테르를 제조하는 방법
DE2810391A1 (de) Katalysator und verfahren zur hydrierung von estern
US9089833B2 (en) Calcium and lanthanum solid base catalysts for transesterification
WO2014064418A2 (fr) Procédé
EP2595945A1 (fr) Procédé de production de pseudo-ionone
CN104525241B (zh) 一种固体碱催化剂及其制备方法和在甘油醇解反应中的应用
CN105296167B (zh) 一种催化制备生物柴油的方法
TWI590868B (zh) 固體金屬氧化觸媒在轉酯化與交換酯化反應之應用
KR101072674B1 (ko) 지방산 알킬에스테르의 제조방법
JP2013072071A (ja) 油脂からの脂肪酸アルキルエステル及び／又はグリセリンの製造方法
JP5186083B2 (ja) 油脂からの脂肪酸アルキルエステル及び／又はグリセリンの製造方法
KR101330183B1 (ko) 바이오디젤 제조용 고체상 촉매 및 이를 이용한바이오디젤의 제조방법
CN102698797A (zh) 一种制备介孔固体酸催化剂的方法
DE1768262C3 (de) Verfahren zur Herstellung aromatischer Alkohole
JPWO2008133189A1 (ja) 油脂からの脂肪酸アルキルエステル及び／又はグリセリンの製造方法

Legal Events

Date Code Title Description
R119 Application deemed withdrawn, or ip right lapsed, due to non-payment of renewal fee

Effective date: 20110802