DD270124A5 - Verfahren zur heliumgewinnung - Google Patents

Verfahren zur heliumgewinnung Download PDF

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Publication number
DD270124A5
DD270124A5 DD88315902A DD31590288A DD270124A5 DD 270124 A5 DD270124 A5 DD 270124A5 DD 88315902 A DD88315902 A DD 88315902A DD 31590288 A DD31590288 A DD 31590288A DD 270124 A5 DD270124 A5 DD 270124A5
Authority
DD
German Democratic Republic
Prior art keywords
pressure
helium
adsorption
adsorber
gas
Prior art date
Application number
DD88315902A
Other languages
German (de)
English (en)
Inventor
Karl Knoblauch
Erwin Pilarczyk
Klaus Giessler
Hans Bukowski
Amico Joseph S D
Herbert Reinhold
Original Assignee
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Application filed by �����@������������������k�� filed Critical �����@������������������k��
Publication of DD270124A5 publication Critical patent/DD270124A5/de

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047Pressure swing adsorption
    • B01D53/0476Vacuum pressure swing adsorption
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B23/00Noble gases; Compounds thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10Inorganic adsorbents
    • B01D2253/102Carbon
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10Inorganic adsorbents
    • B01D2253/116Molecular sieves other than zeolites
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/25Coated, impregnated or composite adsorbents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/30Physical properties of adsorbents
    • B01D2253/302Dimensions
    • B01D2253/308Pore size
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2256/00Main component in the product gas stream after treatment
    • B01D2256/18Noble gases
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/10Single element gases other than halogens
    • B01D2257/102Nitrogen
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/70Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
    • B01D2257/702Hydrocarbons
    • B01D2257/7022Aliphatic hydrocarbons
    • B01D2257/7025Methane
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2259/00Type of treatment
    • B01D2259/40Further details for adsorption processes and devices
    • B01D2259/40001Methods relating to additional, e.g. intermediate, treatment of process gas
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2259/00Type of treatment
    • B01D2259/40Further details for adsorption processes and devices
    • B01D2259/40011Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40028Depressurization
    • B01D2259/4003Depressurization with two sub-steps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2259/00Type of treatment
    • B01D2259/40Further details for adsorption processes and devices
    • B01D2259/40011Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40035Equalization
    • B01D2259/40037Equalization with two sub-steps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2259/00Type of treatment
    • B01D2259/40Further details for adsorption processes and devices
    • B01D2259/40011Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40035Equalization
    • B01D2259/40041Equalization with more than three sub-steps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2259/00Type of treatment
    • B01D2259/40Further details for adsorption processes and devices
    • B01D2259/40011Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40058Number of sequence steps, including sub-steps, per cycle
    • B01D2259/40066Six
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2259/00Type of treatment
    • B01D2259/40Further details for adsorption processes and devices
    • B01D2259/40011Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40058Number of sequence steps, including sub-steps, per cycle
    • B01D2259/40071Nine
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2259/00Type of treatment
    • B01D2259/40Further details for adsorption processes and devices
    • B01D2259/404Further details for adsorption processes and devices using four beds
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02CCAPTURE, STORAGE, SEQUESTRATION OR DISPOSAL OF GREENHOUSE GASES [GHG]
    • Y02C20/00Capture or disposal of greenhouse gases
    • Y02C20/20Capture or disposal of greenhouse gases of methane
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/151Reduction of greenhouse gas [GHG] emissions, e.g. CO2
    • Y02P20/156Methane [CH4]

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Separation Of Gases By Adsorption (AREA)
DD88315902A 1987-05-20 1988-05-19 Verfahren zur heliumgewinnung DD270124A5 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE3716899A DE3716899C1 (de) 1987-05-20 1987-05-20 Verfahren und Vorrichtung zur Heliumgewinnung

Publications (1)

Publication Number Publication Date
DD270124A5 true DD270124A5 (de) 1989-07-19

Family

ID=6327951

Family Applications (1)

Application Number Title Priority Date Filing Date
DD88315902A DD270124A5 (de) 1987-05-20 1988-05-19 Verfahren zur heliumgewinnung

Country Status (10)

Country Link
US (1) US5080694A (fr)
EP (2) EP0291976B1 (fr)
JP (1) JPH02503552A (fr)
AU (1) AU604127B2 (fr)
DD (1) DD270124A5 (fr)
DE (2) DE3716899C1 (fr)
ES (1) ES2023977B3 (fr)
PL (1) PL160298B1 (fr)
RU (1) RU1816228C (fr)
WO (1) WO1988009305A1 (fr)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3716898A1 (de) * 1987-05-20 1988-12-15 Bergwerksverband Gmbh Verfahren und vorrichtung zur heliumanreicherung
ZA915939B (en) * 1990-08-23 1992-06-24 Boc Group Inc Process for helium purification
US5368067A (en) * 1993-03-23 1994-11-29 The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration Gas storage and recovery system
US5632803A (en) * 1994-10-21 1997-05-27 Nitrotec Corporation Enhanced helium recovery
US5792239A (en) * 1994-10-21 1998-08-11 Nitrotec Corporation Separation of gases by pressure swing adsorption
US5542966A (en) * 1994-10-21 1996-08-06 Nitrotec Corporation Helium recovery
US5707425A (en) * 1994-10-21 1998-01-13 Nitrotec Corporation Helium recovery from higher helium content streams
DE19528784C1 (de) * 1995-08-04 1996-08-29 Inst Neuwertwirtschaft Gmbh Verfahren zur Reinigung von Inertgasen mittels Sorbenzien
US5906673A (en) * 1997-05-15 1999-05-25 Nitrotec Corporation Pressure swing system with auxiliary adsorbent bed
DE10007440A1 (de) * 2000-02-18 2001-08-23 Linde Ag Verfahren zum Abtrennen einer Helium-reichen Fraktion aus einem wenigstens Methan, Stickstoff und Helium enthaltenden Strom
FR2818920B1 (fr) * 2000-12-29 2003-09-26 Air Liquide Procede de traitement d'un gaz par absorption et installation correspondante
MXPA04000965A (es) * 2001-07-31 2005-02-22 Praxair Technology Inc Recuperacion de helio.
US20040194513A1 (en) * 2003-04-04 2004-10-07 Giacobbe Frederick W Fiber coolant system including improved gas seals
US6824098B1 (en) 2003-05-28 2004-11-30 Gregorio M. Belloso VTOL parafoil aircraft
US7780764B2 (en) 2008-06-27 2010-08-24 Praxair Technology, Inc. Methods and systems for helium recovery
US8152898B2 (en) * 2008-10-24 2012-04-10 Praxair Technology, Inc. Helium recovery process
WO2013171856A1 (fr) 2012-05-16 2013-11-21 石油資源開発株式会社 Procédé de traitement et dispositif de traitement pour gaz naturel
US9623370B2 (en) 2015-02-10 2017-04-18 Praxair Technology, Inc. Integrated process and apparatus for recovery of helium rich streams
US9676628B2 (en) 2015-02-10 2017-06-13 Praxair Technology, Inc. Integrated process and apparatus for recovery of helium rich streams
US10478770B2 (en) 2017-12-21 2019-11-19 Air Products And Chemicals, Inc. Separation process and apparatus for light noble gas
US10843121B2 (en) 2017-12-21 2020-11-24 Air Products And Chemicals, Inc. Separation process and apparatus for light noble gas
CN116281896B (zh) * 2022-12-01 2024-04-16 煤炭科学技术研究院有限公司 一种含氦煤层气浓缩低温提氦的方法

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3430418A (en) * 1967-08-09 1969-03-04 Union Carbide Corp Selective adsorption process
US3564816A (en) * 1968-12-30 1971-02-23 Union Carbide Corp Selective adsorption process
US3636679A (en) * 1971-01-04 1972-01-25 Union Carbide Corp Selective adsorption gas separation process
US3738087A (en) * 1971-07-01 1973-06-12 Union Carbide Corp Selective adsorption gas separation process
GB1449864A (en) * 1973-10-24 1976-09-15 Boc International Ltd Adsorption system
DE2504653A1 (de) * 1974-04-26 1975-11-13 Le T I Cholodil Verfahren zur reinigung eines neonhelium-gemisches
US4077779A (en) * 1976-10-15 1978-03-07 Air Products And Chemicals, Inc. Hydrogen purification by selective adsorption
DE3122701A1 (de) * 1981-06-06 1982-12-23 Bergwerksverband Gmbh, 4300 Essen Verfahren zur trennung von gasgemischen mittels druckwechseltechnik
FR2510539A1 (fr) * 1981-07-28 1983-02-04 Expertises Sa Cie Maritime Procede et installation d'epuration de l'helium contenu dans un melange de gaz
DE3132758A1 (de) * 1981-08-19 1983-03-03 Linde Ag, 6200 Wiesbaden Absorptionsverfahren
DE3214771A1 (de) * 1982-04-21 1983-10-27 Bergwerksverband Gmbh, 4300 Essen Verfahren zur gewinnung von edelgasen mit kleinen atomdurchmessern, insbesondere helium, aus sauerstoff und/oder stickstoff enthaltenden gasgemischen
US4477265A (en) * 1982-08-05 1984-10-16 Air Products And Chemicals, Inc. Argon purification
JPS5992907A (ja) 1982-11-19 1984-05-29 Seitetsu Kagaku Co Ltd 高濃度アルゴンの製造方法
DE3716898A1 (de) * 1987-05-20 1988-12-15 Bergwerksverband Gmbh Verfahren und vorrichtung zur heliumanreicherung
US4892565A (en) * 1987-12-29 1990-01-09 Air Products And Chemicals, Inc. Adsorptive separation utilizing multiple adsorption beds
US4790858A (en) * 1988-01-29 1988-12-13 Air Products And Chemicals, Inc. Fractionation of multicomponent gas mixtures by pressure swing adsorption
US4913709A (en) * 1989-02-17 1990-04-03 Ravi Kumar Adsorption process for recovering two high purity gas products from multicomponent gas mixtures
US4914218A (en) * 1989-02-17 1990-04-03 Ravi Kumar Adsorptive process for separating multicomponent gas mixtures

Also Published As

Publication number Publication date
US5080694A (en) 1992-01-14
AU604127B2 (en) 1990-12-06
PL160298B1 (pl) 1993-02-26
EP0291976A1 (fr) 1988-11-23
ES2023977B3 (es) 1992-02-16
RU1816228C (ru) 1993-05-15
PL272593A1 (en) 1989-02-06
JPH0577604B2 (fr) 1993-10-27
WO1988009305A1 (fr) 1988-12-01
DE3716899C1 (de) 1988-08-04
EP0358700A1 (fr) 1990-03-21
JPH02503552A (ja) 1990-10-25
AU1781588A (en) 1988-12-21
EP0291976B1 (fr) 1991-07-10
DE3863585D1 (de) 1991-08-14

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