CZ2002570A3 - Způsob membránové filtrace cukrové řepy - Google Patents
Způsob membránové filtrace cukrové řepy Download PDFInfo
- Publication number
- CZ2002570A3 CZ2002570A3 CZ2002570A CZ2002570A CZ2002570A3 CZ 2002570 A3 CZ2002570 A3 CZ 2002570A3 CZ 2002570 A CZ2002570 A CZ 2002570A CZ 2002570 A CZ2002570 A CZ 2002570A CZ 2002570 A3 CZ2002570 A3 CZ 2002570A3
- Authority
- CZ
- Czechia
- Prior art keywords
- ultrafiltration
- juice
- filtrate
- residue
- nanofiltration
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 167
- 230000008569 process Effects 0.000 title claims abstract description 52
- 241000219310 Beta vulgaris subsp. vulgaris Species 0.000 title claims abstract description 25
- 235000021536 Sugar beet Nutrition 0.000 title claims abstract description 25
- 238000005374 membrane filtration Methods 0.000 title claims description 35
- 238000000108 ultra-filtration Methods 0.000 claims abstract description 219
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 215
- 229930006000 Sucrose Natural products 0.000 claims abstract description 141
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims abstract description 141
- 239000012528 membrane Substances 0.000 claims abstract description 127
- 235000016068 Berberis vulgaris Nutrition 0.000 claims abstract description 120
- 241000335053 Beta vulgaris Species 0.000 claims abstract description 120
- 239000005720 sucrose Substances 0.000 claims abstract description 107
- 238000001728 nano-filtration Methods 0.000 claims abstract description 89
- 235000000346 sugar Nutrition 0.000 claims abstract description 75
- 238000001914 filtration Methods 0.000 claims abstract description 47
- 150000008163 sugars Chemical class 0.000 claims abstract description 17
- 238000009792 diffusion process Methods 0.000 claims abstract description 16
- 239000011148 porous material Substances 0.000 claims abstract description 8
- 239000000706 filtrate Substances 0.000 claims description 147
- 238000011026 diafiltration Methods 0.000 claims description 62
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 60
- 239000002002 slurry Substances 0.000 claims description 54
- 238000002425 crystallisation Methods 0.000 claims description 43
- 230000008025 crystallization Effects 0.000 claims description 43
- 235000020357 syrup Nutrition 0.000 claims description 38
- 239000006188 syrup Substances 0.000 claims description 38
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 36
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims description 31
- 235000011941 Tilia x europaea Nutrition 0.000 claims description 31
- 239000004571 lime Substances 0.000 claims description 31
- 239000007788 liquid Substances 0.000 claims description 31
- 238000000909 electrodialysis Methods 0.000 claims description 29
- 239000000463 material Substances 0.000 claims description 28
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 claims description 26
- 238000000605 extraction Methods 0.000 claims description 24
- 238000002803 maceration Methods 0.000 claims description 24
- 238000005520 cutting process Methods 0.000 claims description 23
- MUPFEKGTMRGPLJ-RMMQSMQOSA-N Raffinose Natural products O(C[C@H]1[C@@H](O)[C@H](O)[C@@H](O)[C@@H](O[C@@]2(CO)[C@H](O)[C@@H](O)[C@@H](CO)O2)O1)[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 MUPFEKGTMRGPLJ-RMMQSMQOSA-N 0.000 claims description 22
- MUPFEKGTMRGPLJ-UHFFFAOYSA-N UNPD196149 Natural products OC1C(O)C(CO)OC1(CO)OC1C(O)C(O)C(O)C(COC2C(C(O)C(O)C(CO)O2)O)O1 MUPFEKGTMRGPLJ-UHFFFAOYSA-N 0.000 claims description 22
- 239000012452 mother liquor Substances 0.000 claims description 22
- MUPFEKGTMRGPLJ-ZQSKZDJDSA-N raffinose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO[C@@H]2[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO)O2)O)O1 MUPFEKGTMRGPLJ-ZQSKZDJDSA-N 0.000 claims description 22
- 238000005342 ion exchange Methods 0.000 claims description 21
- 239000000835 fiber Substances 0.000 claims description 20
- 238000000926 separation method Methods 0.000 claims description 19
- 238000001704 evaporation Methods 0.000 claims description 16
- 239000000203 mixture Substances 0.000 claims description 16
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 14
- 235000013379 molasses Nutrition 0.000 claims description 14
- 238000004519 manufacturing process Methods 0.000 claims description 12
- 238000001223 reverse osmosis Methods 0.000 claims description 12
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 11
- 230000008020 evaporation Effects 0.000 claims description 10
- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 claims description 10
- 238000005119 centrifugation Methods 0.000 claims description 9
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical class OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 claims description 8
- 239000002245 particle Substances 0.000 claims description 8
- 238000000746 purification Methods 0.000 claims description 8
- 239000001569 carbon dioxide Substances 0.000 claims description 7
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 7
- 230000002879 macerating effect Effects 0.000 claims description 7
- 229910052700 potassium Inorganic materials 0.000 claims description 7
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims description 6
- 229910052749 magnesium Inorganic materials 0.000 claims description 6
- 238000007873 sieving Methods 0.000 claims description 6
- 239000010802 sludge Substances 0.000 claims description 6
- 239000011734 sodium Substances 0.000 claims description 6
- 229910052708 sodium Inorganic materials 0.000 claims description 6
- 238000003828 vacuum filtration Methods 0.000 claims description 6
- 229960003237 betaine Drugs 0.000 claims description 5
- 230000015572 biosynthetic process Effects 0.000 claims description 5
- 229910052791 calcium Inorganic materials 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 5
- 238000012545 processing Methods 0.000 claims description 5
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical class OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 claims description 4
- 102000005840 alpha-Galactosidase Human genes 0.000 claims description 4
- 108010030291 alpha-Galactosidase Proteins 0.000 claims description 4
- 238000004140 cleaning Methods 0.000 claims description 4
- 239000012141 concentrate Substances 0.000 claims description 4
- GRWZHXKQBITJKP-UHFFFAOYSA-L dithionite(2-) Chemical class [O-]S(=O)S([O-])=O GRWZHXKQBITJKP-UHFFFAOYSA-L 0.000 claims description 4
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 claims description 3
- 235000008504 concentrate Nutrition 0.000 claims description 3
- WBZKQQHYRPRKNJ-UHFFFAOYSA-L disulfite Chemical class [O-]S(=O)S([O-])(=O)=O WBZKQQHYRPRKNJ-UHFFFAOYSA-L 0.000 claims description 3
- 150000001449 anionic compounds Chemical class 0.000 claims description 2
- 150000002891 organic anions Chemical class 0.000 claims description 2
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims 2
- 230000008016 vaporization Effects 0.000 claims 2
- 230000000379 polymerizing effect Effects 0.000 claims 1
- 230000002000 scavenging effect Effects 0.000 claims 1
- 238000012216 screening Methods 0.000 claims 1
- 238000009966 trimming Methods 0.000 claims 1
- 239000007787 solid Substances 0.000 abstract description 34
- 239000012466 permeate Substances 0.000 abstract description 10
- 239000012465 retentate Substances 0.000 abstract description 7
- 239000000047 product Substances 0.000 description 35
- 238000002474 experimental method Methods 0.000 description 17
- 239000000243 solution Substances 0.000 description 17
- 238000004040 coloring Methods 0.000 description 15
- 239000013078 crystal Substances 0.000 description 13
- 239000012535 impurity Substances 0.000 description 12
- 239000000126 substance Substances 0.000 description 12
- 235000015191 beet juice Nutrition 0.000 description 11
- 239000011347 resin Substances 0.000 description 10
- 229920005989 resin Polymers 0.000 description 10
- 239000002699 waste material Substances 0.000 description 10
- 238000011282 treatment Methods 0.000 description 8
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 7
- 235000009508 confectionery Nutrition 0.000 description 7
- 150000002605 large molecules Chemical class 0.000 description 7
- 238000005987 sulfurization reaction Methods 0.000 description 7
- 238000005406 washing Methods 0.000 description 7
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 6
- 230000008901 benefit Effects 0.000 description 6
- 150000001768 cations Chemical class 0.000 description 6
- 238000013375 chromatographic separation Methods 0.000 description 6
- 238000005352 clarification Methods 0.000 description 6
- 239000012065 filter cake Substances 0.000 description 6
- 238000002347 injection Methods 0.000 description 6
- 239000007924 injection Substances 0.000 description 6
- 238000003860 storage Methods 0.000 description 6
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 5
- 125000002091 cationic group Chemical group 0.000 description 5
- 238000010586 diagram Methods 0.000 description 5
- 239000013505 freshwater Substances 0.000 description 5
- 238000004128 high performance liquid chromatography Methods 0.000 description 5
- 239000011777 magnesium Substances 0.000 description 5
- 230000014759 maintenance of location Effects 0.000 description 5
- AOSFMYBATFLTAQ-UHFFFAOYSA-N 1-amino-3-(benzimidazol-1-yl)propan-2-ol Chemical compound C1=CC=C2N(CC(O)CN)C=NC2=C1 AOSFMYBATFLTAQ-UHFFFAOYSA-N 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 239000006227 byproduct Substances 0.000 description 4
- 239000011575 calcium Substances 0.000 description 4
- 210000004027 cell Anatomy 0.000 description 4
- 238000002386 leaching Methods 0.000 description 4
- 229920002521 macromolecule Polymers 0.000 description 4
- 150000007524 organic acids Chemical class 0.000 description 4
- 239000005416 organic matter Substances 0.000 description 4
- 230000003647 oxidation Effects 0.000 description 4
- 238000007254 oxidation reaction Methods 0.000 description 4
- 238000003672 processing method Methods 0.000 description 4
- 238000005507 spraying Methods 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical group C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 3
- 235000019738 Limestone Nutrition 0.000 description 3
- 241001465754 Metazoa Species 0.000 description 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 3
- 125000000129 anionic group Chemical group 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 210000002421 cell wall Anatomy 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 238000007796 conventional method Methods 0.000 description 3
- 239000000284 extract Substances 0.000 description 3
- 239000006028 limestone Substances 0.000 description 3
- 235000005985 organic acids Nutrition 0.000 description 3
- 239000011368 organic material Substances 0.000 description 3
- 238000010979 pH adjustment Methods 0.000 description 3
- 238000006116 polymerization reaction Methods 0.000 description 3
- 239000011591 potassium Substances 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- 230000009467 reduction Effects 0.000 description 3
- 239000012529 ultrafiltration/diafiltration (UF/DF) membrane Substances 0.000 description 3
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
- 238000003915 air pollution Methods 0.000 description 2
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 description 2
- 239000002518 antifoaming agent Substances 0.000 description 2
- 239000003963 antioxidant agent Substances 0.000 description 2
- 239000003729 cation exchange resin Substances 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000006835 compression Effects 0.000 description 2
- 238000007906 compression Methods 0.000 description 2
- 238000010411 cooking Methods 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- GRWZHXKQBITJKP-UHFFFAOYSA-N dithionous acid Chemical class OS(=O)S(O)=O GRWZHXKQBITJKP-UHFFFAOYSA-N 0.000 description 2
- 230000008030 elimination Effects 0.000 description 2
- 238000003379 elimination reaction Methods 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 150000004676 glycans Chemical class 0.000 description 2
- 239000012510 hollow fiber Substances 0.000 description 2
- 229960004903 invert sugar Drugs 0.000 description 2
- 239000003456 ion exchange resin Substances 0.000 description 2
- 229920003303 ion-exchange polymer Polymers 0.000 description 2
- 239000001630 malic acid Substances 0.000 description 2
- 235000011090 malic acid Nutrition 0.000 description 2
- 238000001471 micro-filtration Methods 0.000 description 2
- 230000000813 microbial effect Effects 0.000 description 2
- 235000006408 oxalic acid Nutrition 0.000 description 2
- 230000035699 permeability Effects 0.000 description 2
- 229920001282 polysaccharide Polymers 0.000 description 2
- 239000005017 polysaccharide Substances 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 238000011045 prefiltration Methods 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 238000007670 refining Methods 0.000 description 2
- 230000000717 retained effect Effects 0.000 description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 238000010186 staining Methods 0.000 description 2
- 239000011593 sulfur Substances 0.000 description 2
- 229910052717 sulfur Inorganic materials 0.000 description 2
- 238000010977 unit operation Methods 0.000 description 2
- PJVXUVWGSCCGHT-ZPYZYFCMSA-N (2r,3s,4r,5r)-2,3,4,5,6-pentahydroxyhexanal;(3s,4r,5r)-1,3,4,5,6-pentahydroxyhexan-2-one Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O.OC[C@@H](O)[C@@H](O)[C@H](O)C(=O)CO PJVXUVWGSCCGHT-ZPYZYFCMSA-N 0.000 description 1
- 241000283690 Bos taurus Species 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- NPYPAHLBTDXSSS-UHFFFAOYSA-N Potassium ion Chemical group [K+] NPYPAHLBTDXSSS-UHFFFAOYSA-N 0.000 description 1
- 101000749830 Rattus norvegicus Connector enhancer of kinase suppressor of ras 2 Proteins 0.000 description 1
- 235000011449 Rosa Nutrition 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- DWAQJAXMDSEUJJ-UHFFFAOYSA-M Sodium bisulfite Chemical compound [Na+].OS([O-])=O DWAQJAXMDSEUJJ-UHFFFAOYSA-M 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000005273 aeration Methods 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- WQZGKKKJIJFFOK-PHYPRBDBSA-N alpha-D-galactose Chemical compound OC[C@H]1O[C@H](O)[C@H](O)[C@@H](O)[C@H]1O WQZGKKKJIJFFOK-PHYPRBDBSA-N 0.000 description 1
- 230000003254 anti-foaming effect Effects 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- ZETCGWYACBNPIH-UHFFFAOYSA-N azane;sulfurous acid Chemical compound N.OS(O)=O ZETCGWYACBNPIH-UHFFFAOYSA-N 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 1
- 159000000007 calcium salts Chemical class 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 150000001793 charged compounds Chemical class 0.000 description 1
- 229920001429 chelating resin Polymers 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- ZCDOYSPFYFSLEW-UHFFFAOYSA-N chromate(2-) Chemical compound [O-][Cr]([O-])(=O)=O ZCDOYSPFYFSLEW-UHFFFAOYSA-N 0.000 description 1
- 235000015165 citric acid Nutrition 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 102000038379 digestive enzymes Human genes 0.000 description 1
- 108091007734 digestive enzymes Proteins 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000006862 enzymatic digestion Effects 0.000 description 1
- 238000009778 extrusion testing Methods 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 229930182830 galactose Natural products 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 235000021384 green leafy vegetables Nutrition 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 235000019534 high fructose corn syrup Nutrition 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
- 239000001095 magnesium carbonate Substances 0.000 description 1
- 229910000021 magnesium carbonate Inorganic materials 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 230000002906 microbiologic effect Effects 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 150000007522 mineralic acids Chemical class 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 229920001542 oligosaccharide Polymers 0.000 description 1
- 150000002482 oligosaccharides Chemical class 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- 150000003891 oxalate salts Chemical class 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 235000021395 porridge Nutrition 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 229910001414 potassium ion Inorganic materials 0.000 description 1
- 238000004094 preconcentration Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 150000003384 small molecules Chemical class 0.000 description 1
- 235000010267 sodium hydrogen sulphite Nutrition 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000012607 strong cation exchange resin Substances 0.000 description 1
- 125000000185 sucrose group Chemical group 0.000 description 1
- IIACRCGMVDHOTQ-UHFFFAOYSA-N sulfamic acid Chemical compound NS(O)(=O)=O IIACRCGMVDHOTQ-UHFFFAOYSA-N 0.000 description 1
- 238000013060 ultrafiltration and diafiltration Methods 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B10/00—Production of sugar juices
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/16—Purification of sugar juices by physical means, e.g. osmosis or filtration
- C13B20/165—Purification of sugar juices by physical means, e.g. osmosis or filtration using membranes, e.g. osmosis, ultrafiltration
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Water Supply & Treatment (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Medicines Containing Plant Substances (AREA)
- Jellies, Jams, And Syrups (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/376,026 US6387186B1 (en) | 1999-08-19 | 1999-08-19 | Process for production of purified beet juice for sugar manufacture |
| US09/618,831 US6440222B1 (en) | 2000-07-18 | 2000-07-18 | Sugar beet membrane filtration process |
| US09/618,416 US6406547B1 (en) | 2000-07-18 | 2000-07-18 | Sugar beet membrane filtration process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CZ2002570A3 true CZ2002570A3 (cs) | 2002-11-13 |
Family
ID=27409274
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CZ2002570A CZ2002570A3 (cs) | 1999-08-19 | 2000-08-15 | Způsob membránové filtrace cukrové řepy |
Country Status (9)
| Country | Link |
|---|---|
| EP (3) | EP1788100A2 (hu) |
| AT (1) | ATE358187T1 (hu) |
| AU (1) | AU6906300A (hu) |
| CZ (1) | CZ2002570A3 (hu) |
| DE (1) | DE60034127T2 (hu) |
| HU (1) | HUP0204353A3 (hu) |
| PL (1) | PL353772A1 (hu) |
| SK (1) | SK3772002A3 (hu) |
| WO (1) | WO2001014594A2 (hu) |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2297041T3 (es) * | 2001-08-24 | 2008-05-01 | Danisco Sugar A/S | Un procedimiento para la preparacion de azucar blanco y moreno a partir de remolacha azucarera. |
| WO2003089673A1 (en) * | 2002-04-15 | 2003-10-30 | Co2 Solutions, Llc | A system to produce sugar from plant materials |
| FR2838751B1 (fr) * | 2002-04-17 | 2007-03-09 | Applexion Ste Nouvelle De Rech | Procede et installation de fabrication de sucre raffine a partir de jus sucre |
| FI20021251A0 (fi) | 2002-06-26 | 2002-06-26 | Finnfeeds Finland Oy | Menetelmä betaiinin talteenottamiseksi |
| GB2408262B (en) * | 2003-11-24 | 2007-09-12 | British Sugar Plc | A method of preparation of L-arabinose |
| GB2433518A (en) | 2005-12-21 | 2007-06-27 | Danisco | Process for the recovery of sucrose and non-sucrose materials |
| FI20065363A0 (fi) * | 2006-05-30 | 2006-05-30 | Danisco Sweeteners Oy | Erotusmenetelmä |
| FR2928817B1 (fr) | 2008-03-19 | 2010-12-17 | Ecopsi | Procede et unite de production de dreches de betteraves et de jus sucre a partir de betteraves |
| WO2012019266A1 (en) * | 2010-08-13 | 2012-02-16 | Filho Jose Raimundo | Method and composition for reducing the color of sugar |
| UA112671C2 (uk) | 2011-12-23 | 2016-10-10 | Нестек С.А. | Спосіб одержання смако-ароматичної композиції зі смаком і ароматом умамі |
| US9487840B2 (en) * | 2013-09-16 | 2016-11-08 | Api Intellectual Property Holdings, Llc | Processes and apparatus for refining sugarcane to produce sugars, biofuels, and/or biochemicals |
| CN105154591B (zh) * | 2015-08-13 | 2018-11-20 | 开远滇蔗园科技有限公司 | 一种甘蔗原汁红糖粉的生产方法 |
| RU2619309C2 (ru) * | 2015-10-19 | 2017-05-15 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Московский государственный университет технологий и управления имени К.Г. Разумовского (Первый казачий университет" (ФГБОУ ВО "МГУТУ им. К.Г. Разумовского (ПКУ)") | Способ производства кристаллического сахара |
| CN111269181B (zh) * | 2019-12-31 | 2023-09-19 | 江苏久吾高科技股份有限公司 | 一种盐酸青藤碱的提纯方法及装置 |
| CA3190261A1 (en) * | 2020-07-31 | 2022-04-21 | Hydrite Chemical Co. | Method for controlling microbial growth in sugar processing |
| CN116600656A (zh) * | 2020-11-30 | 2023-08-15 | 新东日本制糖株式会社 | 原料糖及精制糖的制造工艺 |
| CN115260335B (zh) * | 2022-09-28 | 2023-01-03 | 中国农业大学 | 同时提取刺梨渣中刺梨多糖、刺梨多酚、刺梨SOD和Vc的方法和系统 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB477312A (en) * | 1935-05-07 | 1937-12-23 | Jose Antich | Improvements in or relating to the treatment of carob beans (ceratonia siliqua l) and similar plants |
| GB1361674A (en) * | 1971-04-23 | 1974-07-30 | Danske Sukkerfab | Process for the purification and clarification of sugar juices |
| GB1428790A (en) * | 1973-09-28 | 1976-03-17 | Tate & Lyle Ltd | Production of cane sugar |
| US4057437A (en) * | 1976-06-09 | 1977-11-08 | Sparkler Mfg. Co. | Continuous belt filter and filtration method |
| SE441932B (sv) * | 1981-01-14 | 1985-11-18 | Danske Sukkerfab | Forfarande for rening av sockersaft framstelld genom extraktion av sockerbetssnitsel |
| NL8301786A (nl) * | 1983-05-19 | 1984-12-17 | Suiker Unie | Werkwijze voor het winnen van disacchariden uit disacchariden bevattende knolgewassen, onder toepassing van een extractie met onverwarmd water. |
| AU635352B2 (en) * | 1990-11-09 | 1993-03-18 | Applied Membrane Systems Pty Ltd | A method and apparatus for fractionation of sugar containing solution |
| US5281279A (en) * | 1991-11-04 | 1994-01-25 | Gil Enrique G | Process for producing refined sugar from raw juices |
| US5554227A (en) * | 1993-11-12 | 1996-09-10 | Societe Nouvelle De Recherches Et D'applications Industrielles D'echangeurs D'ions Applexion | Process of manufacturing crystal sugar from an aqueous sugar juice such as cane juice or sugar beet juice |
| US5468300A (en) * | 1994-04-07 | 1995-11-21 | International Food Processing Incorporated | Process for producing refined sugar directly from sugarcane |
| WO1996004406A1 (en) * | 1994-08-03 | 1996-02-15 | International Food Processing, Incorporated | Process for producing refined sugar |
| US5759283A (en) * | 1996-05-14 | 1998-06-02 | The Western Sugar Company | Method for processing sugar beets to produce a purified beet juice product |
-
2000
- 2000-08-15 WO PCT/US2000/022301 patent/WO2001014594A2/en active IP Right Grant
- 2000-08-15 AU AU69063/00A patent/AU6906300A/en not_active Abandoned
- 2000-08-15 DE DE60034127T patent/DE60034127T2/de not_active Expired - Fee Related
- 2000-08-15 AT AT00957444T patent/ATE358187T1/de not_active IP Right Cessation
- 2000-08-15 PL PL00353772A patent/PL353772A1/xx not_active Application Discontinuation
- 2000-08-15 CZ CZ2002570A patent/CZ2002570A3/cs unknown
- 2000-08-15 SK SK377-2002A patent/SK3772002A3/sk not_active Application Discontinuation
- 2000-08-15 HU HU0204353A patent/HUP0204353A3/hu unknown
- 2000-08-15 EP EP07003542A patent/EP1788100A2/en not_active Withdrawn
- 2000-08-15 EP EP00957444A patent/EP1204767B1/en not_active Expired - Lifetime
- 2000-08-15 EP EP07003541A patent/EP1788099A2/en not_active Withdrawn
Also Published As
| Publication number | Publication date |
|---|---|
| EP1204767A2 (en) | 2002-05-15 |
| HUP0204353A3 (en) | 2004-12-28 |
| EP1204767B1 (en) | 2007-03-28 |
| HUP0204353A2 (en) | 2003-05-28 |
| EP1788099A2 (en) | 2007-05-23 |
| WO2001014594A2 (en) | 2001-03-01 |
| SK3772002A3 (en) | 2002-11-06 |
| DE60034127D1 (de) | 2007-05-10 |
| AU6906300A (en) | 2001-03-19 |
| PL353772A1 (en) | 2003-12-01 |
| EP1788100A2 (en) | 2007-05-23 |
| WO2001014594A3 (en) | 2001-12-06 |
| DE60034127T2 (de) | 2007-12-06 |
| ATE358187T1 (de) | 2007-04-15 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US6440222B1 (en) | Sugar beet membrane filtration process | |
| US6406548B1 (en) | Sugar cane membrane filtration process | |
| RU2260056C2 (ru) | Способ производства сахара | |
| CZ2002570A3 (cs) | Způsob membránové filtrace cukrové řepy | |
| WO2001014595A2 (en) | Sugar cane membrane filtration process | |
| US3799806A (en) | Process for the purification and clarification of sugar juices,involving ultrafiltration | |
| US8893612B2 (en) | Process for reducing the lime consumption in sugar beet juice purification | |
| US4115147A (en) | Process for producing nutritive sugar from cane juice | |
| US6406547B1 (en) | Sugar beet membrane filtration process | |
| US6174378B1 (en) | Process for production of extra low color cane sugar | |
| WO1992008810A1 (en) | A method and apparatus for fractionation of sugar containing solution | |
| US6375751B2 (en) | Process for production of purified cane juice for sugar manufacture | |
| US20040231663A1 (en) | Process for the preparation of white and brown sugar from sugar beets | |
| RU2002106827A (ru) | Способ мембранной фильтрации сахарной свеклы | |
| US9133528B2 (en) | Raw juice alkalinization | |
| JP7374080B2 (ja) | 予備石灰処理汁から凝固物を分離する際の糖損失の減少方法、並びに凝固物の濃厚化方法、デカンタ型遠心分離機の使用、タンパク質含有画分及び予備石灰処理ビート汁 | |
| EP1649068A2 (en) | Method for purification of high purity sucrose material | |
| EP0126512B1 (en) | Process for the recovery of disaccharides from disaccharides containing tuberous plants by means of an extraction with unwarmed water | |
| US11679371B2 (en) | Method for producing functionally improved carbolime | |
| US5928429A (en) | Process for the enhancement of recovery of sugar | |
| Lipnizki | Membrane processes for sugar and starch processing | |
| CA1208632A (en) | Method of recovering sucrose | |
| US6508886B1 (en) | Method for preparing a purified sugary juice from raw juices obtained from sacchariferous material of vegetable origin | |
| RU2118664C1 (ru) | Способ производства сиропа из сахаросодержащего сырья | |
| NL8400836A (nl) | Werkwijze voor het winnen van suiker uit suikerbieten. |