CN204251759U - Single crystal growing furnace - Google Patents
Single crystal growing furnace Download PDFInfo
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- CN204251759U CN204251759U CN201420734946.6U CN201420734946U CN204251759U CN 204251759 U CN204251759 U CN 204251759U CN 201420734946 U CN201420734946 U CN 201420734946U CN 204251759 U CN204251759 U CN 204251759U
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Abstract
The utility model discloses a kind of can very easily by single crystal growing furnace that the center of quartz crucible is aimed at the axis of seed crystal rod.This single crystal growing furnace, comprise upper furnace, lower hearth, described upper furnace top is provided with seed crystal and rotates and upgrades mechanism, heat-preservation cylinder is provided with in lower hearth, plumbago crucible is provided with in heat-preservation cylinder, quartz crucible is provided with in described plumbago crucible, plumbago crucible arranged outside having heaters, crucible rotation lifting body is provided with bottom described plumbago crucible, described plumbago crucible and crucible rotation lifting body are provided with circular graphite supporting plate, by arranging and groove suitable bottom plumbago crucible at the upper surface of graphite supporting plate, the outside of described graphite supporting plate is arranged with spacing back-up ring, spacing back-up ring and groove limit the placement location of plumbago crucible jointly, thus, the center of the plumbago crucible placed is naturally just with the central axial alignment of seed crystal rod, without the need to repeatedly adjusting, place also very convenient.Be adapted at monocrystalline production unit field to apply.
Description
Technical field
The utility model relates to monocrystalline production unit field, especially a kind of single crystal growing furnace.
Background technology
21 century, world energy sources crisis facilitates the development of photovoltaic market, and crystal silicon solar energy battery is the leading product of photovoltaic industry.Along with countries in the world are to the further attention of solar photovoltaic industry, particularly developed country has formulated a series of support policy, encourage to develop sun power, in addition, along with the continuous expansion of silicon solar cell application surface, the demand of solar cell is increasing, and the demand of silicon single crystal material is also just increasing.
Silicon single crystal is a kind of semiconductor material, and be generally used for and manufacture unicircuit and other electronic components, monocrystalline silicon growing technology has two kinds: one is zone melting method, and another kind is vertical pulling method, and wherein vertical pulling method makes the current method generally adopted.
The method of monocrystalline growth with czochralski silicon is as follows: the quartz crucible highly purified polycrystalline silicon raw material being put into single crystal growing furnace, then heat fused under the protection of slumpability gas is had in rough vacuum, the silicon single crystal in particular growth direction (being also called seed crystal) is had to load in seed crystal clamping device one, and seed crystal is contacted with silicon solution, the temperature of adjustment molten silicon solution, make it close to melting temperature, then seed crystal is driven to stretch in the silicon solution of melting and to rotate from top to bottom, then slowly upper lifting seed is brilliant, now, silicon single crystal enters the growth of conical part, when the diameter of cone is close to aimed dia, improve the pulling speed of seed crystal, monocrystalline silicon body diameter is made no longer to increase and enter the middle part growth phase of crystal, at the end of monocrystalline silicon body growth is close, improve the pulling speed of seed crystal again, monocrystalline silicon body departs from molten silicon gradually, form lower cone and terminate growth.The silicon single crystal grown out in this way, its shape is two sections of tapered right cylinders, is cut into slices by this right cylinder, namely obtains single-crystal semiconductor raw material, and this circular single crystal silicon chip just can as the material of unicircuit or sun power.
Pulling single crystal silicon generally carries out in single crystal growing furnace, at present, the single crystal growing furnace used comprises upper furnace, lower hearth, upper furnace is arranged on above lower hearth and upper furnace is fixed on lower hearth top by segregaion valve, described upper furnace top is provided with seed crystal and rotates and upgrades mechanism, heat-preservation cylinder is provided with in described lower hearth, plumbago crucible is provided with in described heat-preservation cylinder, quartz crucible is provided with in described plumbago crucible, plumbago crucible arranged outside having heaters, well heater is positioned at heat-preservation cylinder, described well heater is fixed on bottom lower hearth by heating electrode, the top of lower hearth is connected with tunger tube, described tunger tube extend in lower hearth through lower hearth, the bottom of described lower hearth is provided with vacuum pumping port, described vacuum pumping port is connected with delivery pipe, delivery pipe end is connected with vacuum pump, the import of vacuum pump is connected with the outlet of delivery pipe, seed crystal clamping device is provided with above described quartz crucible, described seed crystal clamping device rotates and upgrades mechanism by transmission rod and seed crystal and is connected, crucible rotation lifting body is provided with bottom described plumbago crucible, described plumbago crucible and crucible rotation lifting body are provided with circular graphite supporting plate, there is following problem in this single crystal growing furnace: first in actual use, due in single crystal growing furnace produce single crystal process, must ensure that the center of quartz crucible overlaps with the axis of seed crystal rod, the boule diameter uniformity that such guarantee is finally formed, and crucible can not impact crystal bar in the process rotated, thus need the axis of the center of crucible with seed crystal rod to aim at placement crucible, existing single crystal growing furnace is all by manual-alignment when placing crucible at single crystal growing furnace and does not have corresponding alignment fiducials, need repeatedly to adjust, adjust bothersome effort, and be difficult to the axis of the center of crucible with seed crystal rod to aim at, very large inconvenience is brought to operator, secondly, the mainly effect one of argon gas is that protection silicon rod is not oxidized, two is take away the waste gas such as the interior carbon monoxide produced of lower hearth, carbon monoxide has very strong corrodibility, if discharge can cause corrosion to the various equipment in lower hearth and burner hearth not in time, reduce its work-ing life, existing single crystal growing furnace is all directly argon gas is passed into lower hearth internal upper part, owing to not arranging distribution device in lower hearth, therefore, argon gas can not be dispersed in the top of lower hearth uniformly, argon gas is in the process moved downward, the waste gas in places all in lower hearth is difficult to take out of, the carbon monoxide waste gas of prolonged stay can cause corrosion to the parts of stove, affect its work-ing life, moreover, because general lower hearth is only provided with a vacuum pumping port, be positioned at argon gas near vacuum pumping port and waste gas can be easy to be drawn out of, but the waste gas being positioned at vacuum pumping port place far away is just difficult to be extracted out in time, the carbon monoxide waste gas of prolonged stay can cause corrosion to the parts of stove, affects its work-ing life, in addition, existing single crystal growing furnace needed first to utilize in lower hearth to be evacuated to certain vacuum tightness before carrying out crystal pulling technique, and then carry out crystal pulling technique, in crystal pulling technique process, vacuum pump its object one that always works keeps certain vacuum tightness in lower hearth to ensure, the waste gas simultaneously also crystal pulling produced argon gas wrap up in band under discharge, owing to only having the delivery pipe that an internal diameter is thicker between the vacuum pump of existing single crystal growing furnace and vacuum pumping port, this delivery pipe internal diameter is thicker, by better for effect when vacuumizing in lower hearth before crystal pulling technique, but, in crystal pulling technique process, because delivery pipe internal diameter is thicker, gas in single crystal growing furnace can be taken away fast, in order to avoid silicon rod oxidation, need in lower hearth to keep certain density argon gas, so just, need to pass in a large amount of argon gas guarantee lower hearths and keep certain density argon gas, the demand of argon gas is larger, and argon gas is expensive, cause production cost higher, moreover, in the process of single crystal growing furnace work, temperature in lower hearth need remain in a stable scope, because existing single crystal growing furnace is all directly pass in lower hearth by the argon gas of room temperature, because the temperature in lower hearth is higher, the height of usual Dou Shiji Baidu, the argon gas of normal temperature enters in lower hearth and will certainly cause larger impact to the temperature in lower hearth, if in lower hearth temperature fluctuation change greatly can cause larger impact to the growth of crystal bar, the crystal bar quality finally grown up to also can level uneven, in crystal pulling process, crucible need rotate and keep certain speed to rise, the crucible rotation jacking apparatus of existing single crystal growing furnace is all realize by a crucible shaft, crucible shaft can make crucible rise and rotate in the process of rotating simultaneously, but there is a problem in this crucible rotation jacking apparatus, namely the speed of rotation of crucible is limited to the lift velocity of crucible, if the speed of rotation of crucible is accelerated to cause the lift velocity of crucible to be accelerated, the two can not separate and controls separately, sometimes, the speed of rotation accelerating crucible is needed still not increase the lift velocity of crucible, existing single crystal growing furnace just cannot realize above-mentioned functions, this state modulator for crystal pulling technique is very inconvenient.
Utility model content
Technical problem to be solved in the utility model be to provide a kind of can very easily by single crystal growing furnace that the center of quartz crucible is aimed at the axis of seed crystal rod.
The utility model solves the technical scheme that its technical problem adopts: this single crystal growing furnace, comprise upper furnace, lower hearth, upper furnace is arranged on above lower hearth and upper furnace is fixed on lower hearth top by segregaion valve, described upper furnace top is provided with seed crystal and rotates and upgrades mechanism, heat-preservation cylinder is provided with in described lower hearth, plumbago crucible is provided with in described heat-preservation cylinder, quartz crucible is provided with in described plumbago crucible, plumbago crucible arranged outside having heaters, well heater is positioned at heat-preservation cylinder, described well heater is fixed on bottom lower hearth by heating electrode, the top of lower hearth is connected with tunger tube, described tunger tube extend in lower hearth through lower hearth, the bottom of described lower hearth is provided with vacuum pumping port, described vacuum pumping port is connected with delivery pipe, delivery pipe end is connected with vacuum pump, the import of vacuum pump is connected with the outlet of delivery pipe, seed crystal clamping device is provided with above described quartz crucible, described seed crystal clamping device rotates and upgrades mechanism by transmission rod and seed crystal and is connected, crucible rotation lifting body is provided with bottom described plumbago crucible, described plumbago crucible and crucible rotation lifting body are provided with circular graphite supporting plate, the upper surface of described graphite supporting plate be provided with plumbago crucible bottom suitable groove, the outside of described graphite supporting plate is arranged with spacing back-up ring, the inner surface of described spacing back-up ring is provided with webge slot, the side of described graphite supporting plate is provided with the wedge matched with webge slot, external diameter bottom the internal diameter of described spacing back-up ring and plumbago crucible matches.
Be further, annular air distribution plate is provided with in described lower hearth, described annular air distribution plate is horizontally set on the top of plumbago crucible, described annular air distribution plate is sandwich structure, comprise the first top plate and the first lower plywood, seal formation first mezzanine space between described first top plate and the first lower plywood, described tunger tube is communicated with the first mezzanine space, described first lower plywood is provided with multiple first breather hole, the uniform setting on the first lower plywood of described multiple first breather hole.
Be further, suction plate is provided with bottom described lower hearth, described suction plate is horizontally disposed with, described suction plate is sandwich structure, comprise the second top plate and the second lower plywood, seal formation second mezzanine space between described second top plate and the second lower plywood, described vacuum pumping port is communicated with the second mezzanine space, described second top plate is provided with multiple second breather hole, the uniform setting on the second top plate of described multiple second breather hole.
Be further, bypass tube is provided with between the import of described vacuum pump and vacuum pumping port, described bypass tube is provided with the by-pass valve for making bypass tube conducting or closedown, described delivery pipe is provided with the technique valve for making delivery pipe conducting or closedown, the internal diameter of described bypass tube is the 1/3-1/2 of delivery pipe internal diameter.
Be further, described technique valve, by-pass valve are magnetic valve, described technique valve is connected with the first touch switch, described by-pass valve is connected with the second touch switch, vacuumometer is provided with in described lower hearth, also comprise controller, described first touch switch, the second touch switch, vacuumometer are electrically connected with controller respectively.
Be further, described tunger tube is provided with gas-heating apparatus, described gas-heating apparatus comprises columnar shape basal, columniform gas heating cavity is provided with in described columnar shape basal, described columnar shape basal is provided with and the inlet mouth of gas heating cavity connects and air outlet, described inlet mouth is communicated with argon gas source by tracheae, and described air outlet is communicated with tunger tube, the surface wrap of described columnar shape basal has heater strip, and described heater strip is connected on power supply.
Further, be provided with temp controlled meter between described heater strip and power supply, be provided with temp probe in described gas heating cavity, described temp probe is connected with temp controlled meter.
Be further, described crucible rotation lifting body comprises the turning axle be fixed on bottom graphite supporting plate, described turning axle is fixed with swing pinion, base is provided with bottom described turning axle, described turning axle is fixed on base by bearing, and described base is provided with drive-motor, and the output shaft of described drive-motor is provided with driving gear, described driving gear and swing pinion intermesh, and are provided with the lifting device for making base move up and down below described base.
Further, described lifting device is hydraulic cylinder.
Further, between described heat-preservation cylinder and the inwall of lower hearth, be provided with insulation quilt, the inwall of described heat-preservation cylinder scribble thermal radiation reflecting layer.
The beneficial effects of the utility model are: by arranging and groove suitable bottom plumbago crucible at the upper surface of graphite supporting plate, the outside of described graphite supporting plate is arranged with spacing back-up ring, the inner surface of described spacing back-up ring is provided with webge slot, the side of described graphite supporting plate is provided with the wedge matched with webge slot, external diameter bottom the internal diameter of described spacing back-up ring and plumbago crucible matches, because graphite supporting plate is fixed, only the center of groove need be aimed at the central axis of seed crystal rod in the position of to adjust graphite supporting plate first, below when placement crucible, spacing back-up ring is pulled upwardly to certain position, spacing back-up ring and groove limit the placement location of plumbago crucible jointly, thus, the center of the plumbago crucible placed is naturally just with the central axial alignment of seed crystal rod, quartz crucible overlaps with the center of plumbago crucible, thus, center also nature and the seed crystal rod central axial alignment of quartz crucible, without the need to repeatedly adjusting, because spacing back-up ring and groove limit the placement location of plumbago crucible jointly, place also very convenient, very large facility is brought to operator.
Accompanying drawing explanation
Fig. 1 is the structural representation of the utility model single crystal growing furnace;
Be labeled as in figure: upper furnace 1, lower hearth 2, segregaion valve 3, seed crystal rotates and upgrades mechanism 4, heat-preservation cylinder 5, plumbago crucible 6, quartz crucible 7, well heater 8, heating electrode 9, tunger tube 10, vacuum pumping port 11, delivery pipe 12, vacuum pump 13, seed crystal clamping device 14, transmission rod 15, crucible rotation lifting body 16, turning axle 161, swing pinion 162, base 163, drive-motor 164, driving gear 165, lifting device 166, graphite supporting plate 17, groove 18, spacing back-up ring 19, annular air distribution plate 20, first top plate 201, first lower plywood 202, first mezzanine space 203, first breather hole 204, suction plate 21, second top plate 211, second lower plywood 212, second mezzanine space 213, second breather hole 214, bypass tube 22, by-pass valve 23, technique valve 24, first touch switch 25, second touch switch 26, vacuumometer 27, controller 28, gas-heating apparatus 29, columnar shape basal 291, gas heating cavity 292, argon gas source 293, heater strip 294, power supply 295, temp controlled meter 296, temp probe 297, insulation quilt 30, thermal radiation reflecting layer 31.
Embodiment
Below in conjunction with accompanying drawing, the utility model is further illustrated.
As shown in Figure 1, this single crystal growing furnace, comprise upper furnace 1, lower hearth 2, upper furnace 1 is arranged on above lower hearth 2 and upper furnace 1 is fixed on lower hearth 2 top by segregaion valve 3, described upper furnace 1 top is provided with seed crystal and rotates and upgrades mechanism 4, heat-preservation cylinder 5 is provided with in described lower hearth 2, plumbago crucible 6 is provided with in described heat-preservation cylinder 5, quartz crucible 7 is provided with in described plumbago crucible 6, plumbago crucible 6 arranged outside having heaters 8, well heater 8 is positioned at heat-preservation cylinder 5, described well heater 8 is fixed on bottom lower hearth 2 by heating electrode 9, the top of lower hearth 2 is connected with tunger tube 10, described tunger tube 10 extend in lower hearth 2 through lower hearth 2, the bottom of described lower hearth 2 is provided with vacuum pumping port 11, described vacuum pumping port 11 is connected with delivery pipe 12, delivery pipe 12 end is connected with vacuum pump 13, the import of vacuum pump 13 is connected with the outlet of delivery pipe 12, seed crystal clamping device 14 is provided with above described quartz crucible 7, described seed crystal clamping device 14 rotates and upgrades mechanism 4 by transmission rod 15 and seed crystal and is connected, crucible rotation lifting body 16 is provided with bottom described plumbago crucible 6, described plumbago crucible 6 is provided with circular graphite supporting plate 17 with crucible rotation lifting body 16, the upper surface of described graphite supporting plate 17 be provided with plumbago crucible 6 bottom suitable groove 18, the outside of described graphite supporting plate 17 is arranged with spacing back-up ring 19, the inner surface of described spacing back-up ring 19 is provided with webge slot, the side of described graphite supporting plate 17 is provided with the wedge matched with webge slot, external diameter bottom the internal diameter of described spacing back-up ring 19 and plumbago crucible 6 matches.By arranging and groove 18 suitable bottom plumbago crucible 6 at the upper surface of graphite supporting plate 17, the outside of described graphite supporting plate 17 is arranged with spacing back-up ring 19, the inner surface of described spacing back-up ring 19 is provided with webge slot, the side of described graphite supporting plate 17 is provided with the wedge matched with webge slot, external diameter bottom the internal diameter of described spacing back-up ring 19 and plumbago crucible 6 matches, because graphite supporting plate 17 is fixed, only the center of groove 18 need be aimed at the central axis of seed crystal rod in the position of to adjust graphite supporting plate 17 first, below when placement crucible, spacing back-up ring 19 is pulled upwardly to certain position, spacing back-up ring 19 and groove 18 limit the placement location of plumbago crucible 6 jointly, thus, the center of the plumbago crucible 6 placed is naturally just with the central axial alignment of seed crystal rod, quartz crucible 7 overlaps with the center of plumbago crucible 6, thus, center also nature and the seed crystal rod central axial alignment of quartz crucible 7, without the need to repeatedly adjusting, because spacing back-up ring 19 and groove 18 limit the placement location of plumbago crucible 6 jointly, place also very convenient, very large facility is brought to operator.
The mainly effect one of argon gas is that protection silicon rod is not oxidized, two is take away the waste gas such as the interior carbon monoxide produced of lower hearth 2, carbon monoxide has very strong corrodibility, in order to the waste gas such as carbon monoxide in lower hearth 2 can be discharged in time, annular air distribution plate 20 is provided with in described lower hearth 2, described annular air distribution plate 20 is horizontally set on the top of plumbago crucible 6, described annular air distribution plate 20 is sandwich structure, comprise the first top plate 201 and the first lower plywood 202, formation first mezzanine space 203 is sealed between described first top plate 201 and the first lower plywood 202, described tunger tube 10 is communicated with the first mezzanine space 203, described first lower plywood 202 is provided with multiple first breather hole 204, the uniform setting on the first lower plywood 202 of described multiple first breather holes 204.By being provided with annular air distribution plate 20 in lower hearth 2, argon gas first incorporates in the mezzanine space of annular air distribution plate 20, and then spray from multiple first breather holes 204 that the first lower plywood 202 is arranged, because annular air distribution plate 20 is horizontally set on the top of plumbago crucible 6, argon gas through annular air distribution plate 20 uniform after, whole lower hearth 2 top have the argon gas of ejection downwards, the waste gas produced in lower hearth 2 will be wrapped up in time and take away by such argon gas in the process flowed downward, carbon monoxide waste gas prolonged stay is avoided to cause corrosion to equipment, can work-ing life of extension device.
Be further, suction plate 21 is provided with bottom described lower hearth 2, described suction plate 21 is horizontally disposed with, described suction plate 21 is sandwich structure, comprise the second top plate 211 and the second lower plywood 212, formation second mezzanine space 213 is sealed between described second top plate 211 and the second lower plywood 212, described vacuum pumping port 11 is communicated with the second mezzanine space 213, described second top plate 211 is provided with multiple second breather hole 214, the uniform setting on the second top plate 211 of described multiple second breather holes 214.By arranging suction plate 21 bottom lower hearth 2, because vacuum pumping port 11 is communicated with the second mezzanine space 213 of suction plate 21, therefore, suction can be formed in the second mezzanine space 213, the argon gas and waste gas that are positioned at lower hearth 2 are sucked the second mezzanine space 213 from the second breather hole 214 of the second top plate 211, and then again it is extracted out in vacuum pumping port 11, all argon gas and waste gas bottom whole lower hearth 2 can all absorb by suction plate 21 easily, carbon monoxide waste gas prolonged stay is avoided to cause corrosion to equipment, can work-ing life of extension device.
In addition, bypass tube 22 is provided with between the import of described vacuum pump 13 and vacuum pumping port 11, described bypass tube 22 is provided with the by-pass valve 23 for making bypass tube 22 conducting or closedown, described delivery pipe 12 is provided with the technique valve 24 for making delivery pipe 12 conducting or closedown, the internal diameter of described bypass tube 22 is the 1/3-1/2 of delivery pipe 12 internal diameter.By arranging bypass tube 22, make to form two passes between the import of vacuum pump 13 and vacuum pumping port 11, needed first to utilize in lower hearth 2 when being evacuated to certain vacuum tightness before carrying out crystal pulling technique, by-pass valve 23 cuts out, technique valve 24 is opened, certain vacuum tightness can be evacuated to fast like this by lower hearth 2, when entering the crystal pulling technique stage after vacuumizing, technique valve 24 cuts out and by-pass valve 23 is opened, in crystal pulling technique process, vacuum pump 13 works always and its objective is to ensure the vacuum tightness that the interior maintenance of lower hearth 2 is certain, internal diameter due to bypass tube 22 is less only has about 1/1 to two/3rd of delivery pipe 12 internal diameter, such vacuum pump 13 operationally, the gas volume extracted just reduces greatly, so only need pass into a small amount of argon gas can make to keep certain density argon gas in lower hearth 2, the demand decreasing argon gas is larger, reduce production cost.
Moreover, in order to make technique valve 24, by-pass valve 23 can control automatically, realize unattended, described technique valve 24, by-pass valve 23 are magnetic valve, described technique valve 24 is connected with the first touch switch 25, described by-pass valve 23 is connected with the second touch switch 26, in described lower hearth 2, be provided with vacuumometer 27, also comprise controller 28, described first touch switch 25, second touch switch 26, vacuumometer 27 are electrically connected with controller 28 respectively.When vacuum pump 13 is started working, controller 28 controls the first touch switch 25 to be made by-pass valve 23 close bypass tube 22 to close, controlling the second touch switch 26 makes technique valve 24 open delivery pipe 12 conducting, vacuum pump 13 continuous firing, vacuumometer 27 is used for the vacuum tightness measured in body of heater the vacuum values recorded is passed to controller 28, when controller 28 detects that the numerical value of vacuumometer 27 reaches specified requirement, controller 28 controls the first touch switch 25 makes by-pass valve 23 open bypass tube 22 conducting, control the second touch switch 26 to make technique valve 24 close delivery pipe 12 to close, now enter the crystal pulling technique stage, whole process is without the need to manually controlling technique valve 24 and by-pass valve 23, achieve unattended.
Described tunger tube 10 is provided with gas-heating apparatus 29, described gas-heating apparatus 29 comprises columnar shape basal 291, columniform gas heating cavity 292 is provided with in described columnar shape basal 291, described columnar shape basal 291 is provided with the inlet mouth be communicated with gas heating cavity 292 and air outlet, described inlet mouth is communicated with argon gas source 293 by tracheae, described air outlet is communicated with tunger tube 10, the surface wrap of described columnar shape basal 291 has heater strip 294, and described heater strip 294 is connected on power supply 295.By arranging gas-heating apparatus 29 on tunger tube 10, gas-heating apparatus 29 can heat the argon gas entered in lower hearth 2, the argon gas avoiding temperature lower enters in lower hearth 2 and causes larger impact to the temperature in lower hearth 2, in the process of single crystal growing furnace work, the temperature that can ensure in lower hearth 2 remains in a stable scope, avoid causing larger impact to the growth of crystal bar, ensure that the crystal bar quality finally grown up to reaches higher quality level, in addition, utilize heater strip 294 can rapid heating, and gas heating cavity 292 is cylindrical, thus, can ensure that argon gas has enough heat-up times, all argon gas can be made to be heated to same temperature, heats is better.Be further, temp controlled meter 296 is provided with between described heater strip 294 and power supply 295, temp probe 297 is provided with in described gas heating cavity 292, described temp probe 297 is connected with temp controlled meter 296, the temperature in gas heating cavity 292 can be adjusted by temp controlled meter 296, the temperature of rare gas element freely can be adjusted according to different situations, very easy to use.
In order to the speed of rotation and lift velocity that can realize crucible control separately, described crucible rotation lifting body 16 comprises the turning axle 161 be fixed on bottom graphite supporting plate 17, described turning axle 161 is fixed with swing pinion 162, base 163 is provided with bottom described turning axle 161, described turning axle 161 is fixed on base 163 by bearing, described base 163 is provided with drive-motor 164, the output shaft of described drive-motor 164 is provided with driving gear 165, described driving gear 165 intermeshes with swing pinion 162, the lifting device 166 for making base 163 move up and down is provided with below described base 163.The working process of this crucible rotation lifting body 16 is as follows: the rotation of plumbago crucible 6 controls by drive-motor 164, concrete, drive-motor 164 makes the driving gear 165 be arranged on output shaft rotate, driving gear 165 can rotate by driven rotary gear 162, because swing pinion 162 is fixed on turning axle 161, thus can rotate by driven rotary axle 161, turning axle 161 is fixed on bottom graphite supporting plate 17, thus graphite supporting plate 17 can be driven to rotate, plumbago crucible 6 is placed on graphite supporting plate 17, graphite supporting plate 17 rotation can drive plumbago crucible 6 to rotate, because turning axle 161 is fixed on base 163 by bearing, thus when turning axle 161 rotates, base 163 is motionless, moving up and down of base 163 is realized by lifting device 166, can move up by driven rotary axle 161 when base 163 moves up, and then graphite supporting plate 17 can be driven to rise, thus realize the rising of plumbago crucible 6, therefore, the rising of plumbago crucible 6 and rotary independent control, its lift velocity and speed of rotation control respectively by drive-motor 164 and lifting device 166, the two controls separately to bring great convenience to the state modulator of crystal pulling technique.
Further, described lifting device 166 is can for electric pushrod, cylinder etc., as preferably: described lifting device 166 be hydraulic cylinder, and hydraulic cylinder has larger top lift and controls to facilitate.
In order to reduce calorific loss, save energy, reduces energy consumption, is provided with insulation quilt 30, the inwall of described heat-preservation cylinder 5 scribbles thermal radiation reflecting layer 31 between described heat-preservation cylinder 5 and the inwall of lower hearth 2.
Claims (10)
1. single crystal growing furnace, comprise upper furnace (1), lower hearth (2), upper furnace (1) is arranged on lower hearth (2) top and upper furnace (1) is fixed on lower hearth (2) top by segregaion valve (3), described upper furnace (1) top is provided with seed crystal and rotates and upgrades mechanism (4), heat-preservation cylinder (5) is provided with in described lower hearth (2), plumbago crucible (6) is provided with in described heat-preservation cylinder (5), quartz crucible (7) is provided with in described plumbago crucible (6), plumbago crucible (6) arranged outside having heaters (8), well heater (8) is positioned at heat-preservation cylinder (5), described well heater (8) is fixed on lower hearth (2) bottom by heating electrode (9), the top of lower hearth (2) is connected with tunger tube (10), described tunger tube (10) extend in lower hearth (2) through lower hearth (2), the bottom of described lower hearth (2) is provided with vacuum pumping port (11), described vacuum pumping port (11) is connected with delivery pipe (12), delivery pipe (12) end is connected with vacuum pump (13), the import of vacuum pump (13) is connected with the outlet of delivery pipe (12), described quartz crucible (7) top is provided with seed crystal clamping device (14), described seed crystal clamping device (14) rotates and upgrades mechanism (4) by transmission rod (15) and seed crystal and is connected, described plumbago crucible (6) bottom is provided with crucible rotation lifting body (16), described plumbago crucible (6) and crucible rotation lifting body (16) are provided with circular graphite supporting plate (17), it is characterized in that: the upper surface of described graphite supporting plate (17) is provided with the groove (18) suitable with plumbago crucible (6) bottom, the outside of described graphite supporting plate (17) is arranged with spacing back-up ring (19), the inner surface of described spacing back-up ring (19) is provided with webge slot, the side of described graphite supporting plate (17) is provided with the wedge matched with webge slot, the external diameter of the internal diameter of described spacing back-up ring (19) and plumbago crucible (6) bottom matches.
2. single crystal growing furnace as claimed in claim 1, it is characterized in that: in described lower hearth (2), be provided with annular air distribution plate (20), described annular air distribution plate (20) is horizontally set on the top of plumbago crucible (6), described annular air distribution plate (20) is sandwich structure, comprise the first top plate (201) and the first lower plywood (202), formation first mezzanine space (203) is sealed between described first top plate (201) and the first lower plywood (202), described tunger tube (10) is communicated with the first mezzanine space (203), described first lower plywood (202) is provided with multiple first breather hole (204), described multiple first breather hole (204) is in the upper uniform setting of the first lower plywood (202).
3. single crystal growing furnace as claimed in claim 2, it is characterized in that: described lower hearth (2) bottom is provided with suction plate (21), described suction plate (21) is horizontally disposed with, described suction plate (21) is sandwich structure, comprise the second top plate (211) and the second lower plywood (212), formation second mezzanine space (213) is sealed between described second top plate (211) and the second lower plywood (212), described vacuum pumping port (11) is communicated with the second mezzanine space (213), described second top plate (211) is provided with multiple second breather hole (214), described multiple second breather hole (214) is in the upper uniform setting of the second top plate (211).
4. single crystal growing furnace as claimed in claim 3, it is characterized in that: between the import of described vacuum pump (13) and vacuum pumping port (11), be provided with bypass tube (22), described bypass tube (22) is provided with the by-pass valve (23) for making bypass tube (22) conducting or closedown, described delivery pipe (12) is provided with the technique valve (24) for making delivery pipe (12) conducting or closedown, the internal diameter of described bypass tube (22) is the 1/3-1/2 of delivery pipe (12) internal diameter.
5. single crystal growing furnace as claimed in claim 4, it is characterized in that: described technique valve (24), by-pass valve (23) are magnetic valve, described technique valve (24) is connected with the first touch switch (25), described by-pass valve (23) is connected with the second touch switch (26), vacuumometer (27) is provided with in described lower hearth (2), also comprise controller (28), described first touch switch (25), the second touch switch (26), vacuumometer (27) are electrically connected with controller (28) respectively.
6. single crystal growing furnace as claimed in claim 5, it is characterized in that: described tunger tube (10) is provided with gas-heating apparatus (29), described gas-heating apparatus (29) comprises columnar shape basal (291), columniform gas heating cavity (292) is provided with in described columnar shape basal (291), described columnar shape basal (291) is provided with the inlet mouth and air outlet that are communicated with gas heating cavity (292), described inlet mouth is communicated with argon gas source (293) by tracheae, described air outlet is communicated with tunger tube (10), the surface wrap of described columnar shape basal (291) has heater strip (294), described heater strip (294) is connected on power supply (295).
7. single crystal growing furnace as claimed in claim 6, it is characterized in that: between described heater strip (294) and power supply (295), be provided with temp controlled meter (296), be provided with temp probe (297) in described gas heating cavity (292), described temp probe (297) is connected with temp controlled meter (296).
8. single crystal growing furnace as claimed in claim 7, it is characterized in that: described crucible rotation lifting body (16) comprises the turning axle (161) being fixed on graphite supporting plate (17) bottom, described turning axle (161) is fixed with swing pinion (162), described turning axle (161) bottom is provided with base (163), described turning axle (161) is fixed on base (163) by bearing, described base (163) is provided with drive-motor (164), the output shaft of described drive-motor (164) is provided with driving gear (165), described driving gear (165) and swing pinion (162) intermesh, described base (163) below is provided with the lifting device (166) for making base (163) move up and down.
9. single crystal growing furnace as claimed in claim 8, is characterized in that: described lifting device (166) is hydraulic cylinder.
10. single crystal growing furnace as claimed in claim 9, it is characterized in that: between the inwall of described heat-preservation cylinder (5) and lower hearth (2), be provided with insulation quilt (30), the inwall of described heat-preservation cylinder (5) scribbles thermal radiation reflecting layer (31).
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| Application Number | Priority Date | Filing Date | Title |
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| CN201420734946.6U CN204251759U (en) | 2014-11-27 | 2014-11-27 | Single crystal growing furnace |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420734946.6U CN204251759U (en) | 2014-11-27 | 2014-11-27 | Single crystal growing furnace |
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| CN204251759U true CN204251759U (en) | 2015-04-08 |
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| CN201420734946.6U Expired - Fee Related CN204251759U (en) | 2014-11-27 | 2014-11-27 | Single crystal growing furnace |
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| CN (1) | CN204251759U (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105135880A (en) * | 2015-08-26 | 2015-12-09 | 潘玲玉 | Graphite crucible furnace |
| CN107601515A (en) * | 2017-10-27 | 2018-01-19 | 北方民族大学 | A kind of device for preparing SiO powder |
| CN108106426A (en) * | 2018-01-19 | 2018-06-01 | 苏州楚翰真空科技有限公司 | A kind of pyrographite stove crucible |
| CN108193263A (en) * | 2018-01-26 | 2018-06-22 | 山东大海新能源发展有限公司 | A kind of monocrystalline produces stove |
| CN110359082A (en) * | 2019-08-15 | 2019-10-22 | 胡正阳 | A kind of single crystal growing furnace that thermal field is stable |
| CN110528064A (en) * | 2019-09-17 | 2019-12-03 | 大同新成新材料股份有限公司 | A kind of monocrystalline silicon growing device and monocrystalline silicon growing method |
| CN113136617A (en) * | 2021-04-16 | 2021-07-20 | 曲靖阳光能源硅材料有限公司 | Czochralski method single crystal furnace and melt temperature gradient control method thereof |
| CN113337883A (en) * | 2021-06-09 | 2021-09-03 | 广东民鑫机械设备科技有限公司 | Ceramic production process |
| CN115161769A (en) * | 2022-06-07 | 2022-10-11 | 连城凯克斯科技有限公司 | Furnace chassis and automatic crucible lifting control equipment |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105135880A (en) * | 2015-08-26 | 2015-12-09 | 潘玲玉 | Graphite crucible furnace |
| CN105135880B (en) * | 2015-08-26 | 2017-10-20 | 石哲文 | A kind of graphite crucible stove |
| CN107601515A (en) * | 2017-10-27 | 2018-01-19 | 北方民族大学 | A kind of device for preparing SiO powder |
| CN108106426A (en) * | 2018-01-19 | 2018-06-01 | 苏州楚翰真空科技有限公司 | A kind of pyrographite stove crucible |
| CN108106426B (en) * | 2018-01-19 | 2024-05-17 | 苏州楚翰真空科技有限公司 | Crucible of high-temperature graphite furnace |
| CN108193263A (en) * | 2018-01-26 | 2018-06-22 | 山东大海新能源发展有限公司 | A kind of monocrystalline produces stove |
| CN110359082A (en) * | 2019-08-15 | 2019-10-22 | 胡正阳 | A kind of single crystal growing furnace that thermal field is stable |
| CN110528064A (en) * | 2019-09-17 | 2019-12-03 | 大同新成新材料股份有限公司 | A kind of monocrystalline silicon growing device and monocrystalline silicon growing method |
| CN113136617A (en) * | 2021-04-16 | 2021-07-20 | 曲靖阳光能源硅材料有限公司 | Czochralski method single crystal furnace and melt temperature gradient control method thereof |
| CN113337883A (en) * | 2021-06-09 | 2021-09-03 | 广东民鑫机械设备科技有限公司 | Ceramic production process |
| CN115161769A (en) * | 2022-06-07 | 2022-10-11 | 连城凯克斯科技有限公司 | Furnace chassis and automatic crucible lifting control equipment |
| CN115161769B (en) * | 2022-06-07 | 2024-04-16 | 连城凯克斯科技有限公司 | Automatic lifting control equipment for furnace bottom plate and crucible |
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