CN206902281U - A kind of single crystal growing furnace - Google Patents

A kind of single crystal growing furnace Download PDF

Info

Publication number
CN206902281U
CN206902281U CN201620725534.5U CN201620725534U CN206902281U CN 206902281 U CN206902281 U CN 206902281U CN 201620725534 U CN201620725534 U CN 201620725534U CN 206902281 U CN206902281 U CN 206902281U
Authority
CN
China
Prior art keywords
heater
argon gas
single crystal
heat
growing furnace
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201620725534.5U
Other languages
Chinese (zh)
Inventor
陈五奎
刘强
付红霞
黄振华
冯加保
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Qinghai Tuori New Energy Technology Co Ltd
Original Assignee
Qinghai Tuori New Energy Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Qinghai Tuori New Energy Technology Co Ltd filed Critical Qinghai Tuori New Energy Technology Co Ltd
Priority to CN201620725534.5U priority Critical patent/CN206902281U/en
Application granted granted Critical
Publication of CN206902281U publication Critical patent/CN206902281U/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Crystals, And After-Treatments Of Crystals (AREA)

Abstract

The utility model discloses a kind of single crystal growing furnace.The single crystal growing furnace in air inlet pipe by setting gas preheating unit, gas preheating unit can heat to entering the argon gas in body of heater, avoid the relatively low argon gas of temperature from entering in body of heater and large effect is caused to the temperature in body of heater, during single crystal growing furnace works, it can ensure that the temperature in body of heater is maintained in a stable scope, the growth to crystal bar is avoided to cause large effect, the silicon rod quality for ensureing finally to grow up to reaches higher quality level, in addition, the useless argon gas of high temperature for being discharged aspirating hole using aspiration pump is passed through air entraining pipe and imported in cavity, new argon gas is preheated using the high temperature argon gas that gives up, the heat contained in the useless argon gas of high temperature can not only be made full use of, realize energy-saving and emission-reduction, simultaneously, the argon gas being preheated is passed through in body of heater, argon gas can be reduced and take away heat in body of heater, further realize energy-saving and emission-reduction.It is adapted in monocrystalline production equipment field popularization and application.

Description

A kind of single crystal growing furnace
Technical field
Monocrystalline production equipment field is the utility model is related to, especially a kind of single crystal growing furnace.
Background technology
21 century, world energy sources crisis promote the development of photovoltaic market, and crystal silicon solar energy battery is photovoltaic industry Leading products.With further attention of the countries in the world to solar photovoltaic industry, particularly developed country has formulated a series of Support policy, encourage utilization solar energy, in addition, with the continuous expansion of silicon solar cell application surface, solar-electricity The demand in pond is increasing, and the demand of silicon single crystal material is also just increasing.
Monocrystalline silicon is a kind of semi-conducting material, is generally used for manufacturing integrated circuit and other electronic components, monocrystalline silicon growing Technology has two kinds:One kind is zone-melting process, and another kind is vertical pulling method, and wherein vertical pulling method is the method generally used at present.
The method of monocrystalline growth with czochralski silicon is as follows:The polycrystalline silicon raw material of high-purity is put into the silica crucible of single crystal growing furnace It is interior, fusing is then heated under the protection of low vacuum and inert gas, the monocrystalline silicon for having a particular growth direction ( It is called seed crystal) it is fitted into seed crystal clamping device, and seed crystal is contacted with silicon solution, the temperature of molten silicon solution is adjusted, connects it Nearly melting temperature, seed crystal is stretched into from top to bottom in the silicon solution of melting and rotate, then slowly upper lifting seed is brilliant, now, Monocrystalline silicon enters the growth of conical section, when the diameter of cone is close to aimed dia, improves the lifting speed of seed crystal, makes monocrystalline Silicon body diameter no longer increases into the middle part growth phase of crystal, in monocrystalline silicon body growth at the end of, then improves seed crystal Lifting speed, monocrystalline silicon body progressively disengages molten silicon, forms lower cone and terminate to grow.The list to grow out in this way Crystal silicon, it is shaped as two sections of tapered cylinders, the cylinder is cut into slices, that is, obtains single-crystal semiconductor raw material, this circle Shape monocrystalline silicon piece can serve as the material of integrated circuit or solar cell.
Pulling single crystal silicon is carried out typically in single crystal growing furnace, and at present, used single crystal growing furnace includes body of heater, the furnace interior Provided with graphite crucible, the graphite crucible bottom is mutually fixed by crucible axis with bottom of furnace body, and stone is provided with the graphite crucible English crucible, graphite crucible outside are provided with side heater, and the bottom of furnace body sets aspirating hole, in addition to tunger tube, described Tunger tube is extend into silica crucible through body of heater, and it is in order to avoid crystal bar is in crystal pulling growth course that argon gas is passed through in single crystal growing furnace In be oxidized.Problems with actual use be present in this single crystal growing furnace:First, during single crystal growing furnace works, stove Internal temperature need to be maintained in a stable scope, because existing single crystal growing furnace is all that the argon gas of room temperature directly is passed through into stove In vivo, generally all it is the height of several Baidu, the argon gas of normal temperature enters will certainly be to stove in body of heater because the temperature in body of heater is higher Internal temperature causes large effect, if in body of heater temperature fluctuation change greatly can growth to crystal bar cause larger shadow Ring, the crystal bar finally grown up to is of low quality.
Utility model content
Technical problem to be solved in the utility model is to provide a kind of single crystal growing furnace that can improve production efficiency.
Technical scheme is used by the utility model solves its technical problem:The single crystal growing furnace, including body of heater, the body of heater Inside is provided with graphite crucible, and the graphite crucible bottom is mutually fixed with bottom of furnace body by crucible axis, set in the graphite crucible There is silica crucible, be provided with side heater on the outside of graphite crucible, aspirating hole, in addition to argon gas are provided with the sidewall of the furnace body Pipe and argon gas source, the argon gas source are connected with tunger tube by air inlet pipe, and the end of the tunger tube extend into stone through body of heater In English crucible, gas preheating unit is provided with the air inlet pipe, the gas preheating unit includes closed cavity, the sky Intracavitary is provided with heat exchanger tube, and the both ends of the heat exchanger tube extend respectively to connect outside cavity and with air inlet pipe, in the argon gas source Argon gas flowed into successively along air inlet pipe, heat exchanger tube, tunger tube along crucible, the sealing of the junction of the heat exchanger tube and cavity is described Air entraining pipe and blast pipe are connected with cavity, one end of the air entraining pipe connects with the aspirating hole set on body of heater, air entraining pipe The other end is connected with cavity inside, and aspiration pump is provided with the air entraining pipe, and the blast pipe connects with cavity inside.
It is further that the heat exchanger tube is metal coil pipe.
It is further that the heat exchanger tube is made using copper pipe.
It is further that heat-preservation cylinder is provided with the body of heater, graphite crucible, silica crucible, side heater, is respectively positioned on In heat-preservation cylinder.
It is further to be provided with insulation quilt between the body of heater and heat-preservation cylinder.
It is further that heat radiation reflecting layer is scribbled on the inwall of the heat-preservation cylinder.
The beneficial effects of the utility model are:By setting gas preheating unit in air inlet pipe, gas preheating unit can With to enter body of heater in argon gas heat, avoid the relatively low argon gas of temperature enter body of heater in the temperature in body of heater is caused compared with Big influence, during single crystal growing furnace works, it is ensured that the temperature in body of heater is maintained in a stable scope, is ensured The silicon rod quality finally grown up to reaches higher quality level, the argon gas in addition, high temperature for being discharged aspirating hole using aspiration pump is given up Imported by air entraining pipe in cavity, new argon gas is preheated using the high temperature argon gas that gives up, can not only make full use of high temperature to give up The heat contained in argon gas, energy-saving and emission-reduction are realized, meanwhile, the argon gas being preheated is passed through in body of heater, it is possible to reduce argon gas takes away stove Internal heat, further realizes energy-saving and emission-reduction, reduces the production cost of crystal bar.
Brief description of the drawings
Fig. 1 is the structural representation of the utility model single crystal growing furnace;
In figure mark for:Body of heater 1, graphite crucible 2, crucible axis 3, silica crucible 4, side heater 5, aspirating hole 6, argon gas Pipe 7, heat-preservation cylinder 12, insulation quilt 13, air inlet pipe 14, argon gas source 15, gas preheating unit 16, cavity 161, heat exchanger tube 162, bleed Pipe 163, blast pipe 164, aspiration pump 165, heat radiation reflecting layer 17.
Embodiment
The utility model is further illustrated below in conjunction with the accompanying drawings.
As shown in figure 1, the single crystal growing furnace, including body of heater 1, the inside of body of heater 1 are provided with graphite crucible 2, the graphite crucible 2 Bottom is mutually fixed by crucible axis 3 and the bottom of body of heater 1, and silica crucible 4 is provided with the graphite crucible 2, and the outside of graphite crucible 2 is set Side heater 5 is equipped with, aspirating hole 6, in addition to tunger tube 7 and argon gas source 15, the argon gas are provided with the side wall of body of heater 1 Source 15 is connected with tunger tube 7 by air inlet pipe 14, and the end of the tunger tube 7 is extend into silica crucible 4 through body of heater 1, institute State and gas preheating unit 16 is provided with air inlet pipe 14, the gas preheating unit 16 includes closed cavity 161, the cavity Heat exchanger tube 162 is provided with 161, the both ends of the heat exchanger tube 162 extend respectively to connect outside cavity 161 and with air inlet pipe 14, Argon gas in the argon gas source 15 is flowed into crucible 6 along air inlet pipe 14, heat exchanger tube 162, air inlet pipe 14 successively, the heat exchanger tube 162 are sealed with the junction of cavity 161, and air entraining pipe 163 and blast pipe 164, the air entraining pipe are connected with the cavity 161 163 one end connects with the aspirating hole 2 set on body of heater 1, and the other end of air entraining pipe 163 connects with the inside of cavity 161, described to draw Aspiration pump 165 is provided with tracheae 163, the blast pipe 164 connects with the inside of cavity 161.By being set in air inlet pipe 14 Gas preheating unit 16, gas preheating unit 16 can heat to entering the argon gas in body of heater 1, avoid the argon that temperature is relatively low Gas enters in body of heater 1 causes large effect to the temperature in body of heater 1, during single crystal growing furnace works, it is ensured that body of heater 1 Interior temperature is maintained in a stable scope, and the crystal bar quality for ensureing finally to grow up to reaches higher quality level, in addition, The high temperature of being discharged aspirating hole 2 using aspiration pump 165 argon gas that gives up is imported in cavity 161 by air entraining pipe 163, is given up argon using high temperature Gas preheats to new argon gas, can not only make full use of the heat contained in the useless argon gas of high temperature, realize energy-saving and emission-reduction, together When, the argon gas being preheated is passed through in body of heater 1, it is possible to reduce and argon gas takes away the heat in body of heater 1, further realizes energy-saving and emission-reduction, Reduce the production cost of crystal bar.
In order to improve heat exchange efficiency, extend heat-exchange time, the heat exchanger tube 162 is metal coil pipe.In order to further improve Heat exchange efficiency, the heat exchanger tube 162 are made using copper pipe.
In order to reduce thermal loss, the energy is saved, energy consumption is reduced, heat-preservation cylinder 12, graphite crucible is provided with the body of heater 1 2nd, silica crucible 4, side heater 5, be respectively positioned in heat-preservation cylinder 12.In order to further reduce thermal loss, the body of heater 1 with Insulation quilt 13 is additionally provided between heat-preservation cylinder 12, while heat radiation reflecting layer 17 is scribbled on the inwall of heat-preservation cylinder 12.

Claims (6)

1. a kind of single crystal growing furnace, including body of heater (1), the body of heater (1) is internal to be provided with graphite crucible (2), graphite crucible (2) bottom Portion is mutually fixed by crucible axis (3) and body of heater (1) bottom, and silica crucible (4), graphite crucible are provided with the graphite crucible (2) (2) outside is provided with side heater (5), is provided with aspirating hole (6) in body of heater (1) side wall, in addition to tunger tube (7) with Argon gas source (15), the argon gas source (15) are connected with tunger tube (7) by air inlet pipe (14), and the end of the tunger tube (7) is worn Body of heater (1) is crossed to extend into silica crucible (4), it is characterised in that:Gas preheating unit is provided with the air inlet pipe (14) (16), the gas preheating unit (16) includes closed cavity (161), and heat exchanger tube is provided with the cavity (161) (162), the both ends of the heat exchanger tube (162) extend respectively to cavity (161) outside and connected with air inlet pipe (14), the argon gas source (15) argon gas in is flowed into silica crucible (4) along air inlet pipe (14), heat exchanger tube (162), tunger tube (7) successively, the heat exchange Manage (162) and the junction of cavity (161) seal, air entraining pipe (163) and blast pipe (164) are connected with the cavity (161), One end of the air entraining pipe (163) connects with the aspirating hole (6) set on body of heater (1), the other end and cavity of air entraining pipe (163) (161) it is internal to connect, aspiration pump (165) is provided with the air entraining pipe (163), the blast pipe (164) is interior with cavity (161) Portion connects.
2. single crystal growing furnace as claimed in claim 1, it is characterised in that:The heat exchanger tube (162) is metal coil pipe.
3. single crystal growing furnace as claimed in claim 2, it is characterised in that:The heat exchanger tube (162) is made using copper pipe.
4. single crystal growing furnace as claimed in claim 3, it is characterised in that:Heat-preservation cylinder (12), graphite earthenware are provided with the body of heater (1) Crucible (2), silica crucible (4), side heater (5), it is respectively positioned in heat-preservation cylinder (12).
5. single crystal growing furnace as claimed in claim 4, it is characterised in that:Guarantor is provided between the body of heater (1) and heat-preservation cylinder (12) Warm felt (13).
6. single crystal growing furnace as claimed in claim 5, it is characterised in that:Heat radiation reflection is scribbled on the inwall of the heat-preservation cylinder (12) Layer (17).
CN201620725534.5U 2016-07-11 2016-07-11 A kind of single crystal growing furnace Active CN206902281U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620725534.5U CN206902281U (en) 2016-07-11 2016-07-11 A kind of single crystal growing furnace

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620725534.5U CN206902281U (en) 2016-07-11 2016-07-11 A kind of single crystal growing furnace

Publications (1)

Publication Number Publication Date
CN206902281U true CN206902281U (en) 2018-01-19

Family

ID=61293958

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201620725534.5U Active CN206902281U (en) 2016-07-11 2016-07-11 A kind of single crystal growing furnace

Country Status (1)

Country Link
CN (1) CN206902281U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108179469A (en) * 2018-02-13 2018-06-19 南京晶能半导体科技有限公司 A kind of exhaust apparatus and single crystal growing furnace of semiconductor grade monocrystal stove
CN108193263A (en) * 2018-01-26 2018-06-22 山东大海新能源发展有限公司 A kind of monocrystalline produces stove

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108193263A (en) * 2018-01-26 2018-06-22 山东大海新能源发展有限公司 A kind of monocrystalline produces stove
CN108179469A (en) * 2018-02-13 2018-06-19 南京晶能半导体科技有限公司 A kind of exhaust apparatus and single crystal growing furnace of semiconductor grade monocrystal stove

Similar Documents

Publication Publication Date Title
CN202558970U (en) Single crystal like silicon ingot furnace
CN102352530B (en) Heat shield device for CZ-Si single crystal furnace
CN102367588A (en) Straight-pull eight-inch silicon single crystal thermal field and production method of eight-inch silicon single crystal
CN206736402U (en) Single crystal growing furnace for vertical pulling method production silicon single crystal rod
CN202989351U (en) Ingot furnace thermal field structure based on multiple heaters
CN206157273U (en) Novel single crystal growing furnace
CN206799790U (en) Single crystal growing furnace
CN201485535U (en) Double-heating system monocrystalline silicon growing device
CN202380126U (en) Heat shield device for straight pull silicon single crystal furnace
CN206902281U (en) A kind of single crystal growing furnace
CN202786496U (en) Composite heat shielding device applied to single crystal furnace
CN103628127A (en) DSS (directional solidification system) quasi-monocrystal silicon growth furnace and growth method of quasi-monocrystal silicon
CN204251761U (en) Thermal field structure of single crystal furnace
CN104264213A (en) EFG (edge-defined film-fed growth) device of large-size doped sapphire crystals and growth process thereof
CN202730297U (en) Czochralski method single crystal furnace thermal field structure
CN206188916U (en) Vertical pulling single crystal cooling device
CN106894082B (en) Monocrystalline silicon growing furnace
CN106149047A (en) Single crystal growing furnace
CN102433585A (en) Thermal field structure of quasi-monocrystal ingot furnace
CN208517582U (en) A kind of monocrystalline silica crucible
CN201942779U (en) Heat shield device applied to single crystal furnace
CN208517581U (en) A kind of monocrystalline silica crucible
CN201990762U (en) Heating device of czochralski single crystal furnace
CN203065635U (en) Bottom enhanced cooling device
CN202187081U (en) Thermal field of single crystal furnace

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant