CN1982874A - 快速检测滴丸剂有效成分含量的近红外漫反射光谱法 - Google Patents
快速检测滴丸剂有效成分含量的近红外漫反射光谱法 Download PDFInfo
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Abstract
Description
样品数量平均含量(%)STDRSD(%)最大值(%)最小值(%)含量范围 | 校正集 | 预测集 | ||||
丹参素 | 原儿茶醛 | 丹酚酸B | 丹参素 | 原儿茶醛 | 丹酚酸B | |
0.58550.196733.5961.00001.000 | 440.20690.099748.18150.430600.4306 | 0.30240.171256.61920.908600.9086 | 0.55720.062711.25850.66470.48230.1824 | 160.20610.026812.98840.25610.15280.1033 | 0.28950.041214.23180.39590.25170.1442 |
丹参素 | 原儿茶醛 | 丹酚酸B | |
波段(cm-1) | 8700.00~7305.006600.00~6350.004950.00~4150.00 | 9770.00~7155.006950.00~5150.004700.00~4500.00 | 9852.00~7057.006728.00~5143.004935.00~4449.00 |
有效成分 | R2 | RMSEC | RMSEP | RSEC(%) | RSEP(%) |
丹参素原儿茶醛丹酚酸B | 0.99420.99650.9714 | 0.02100.00820.0402 | 0.03260.01930.0363 | 3.40373.574311.7347 | 5.81619.291712.4232 |
R2 | RMSEC | RMSECV | RMSEP | RSEC(%) | RSEP(%) | |
柴胡皂苷A | 0.9925 | 0.0093 | 0.0179 | 0.0156 | 3.9368 | 7.2550 |
黄芪甲苷 | 丹参素 | |
波段(cm-1) | 9140~78906980~62404870~4450 | 8570~74606490~62404740~4310 |
R2 | RMSEC | RMSECV | RMSEP | RSEC(%) | RSEP(%) | |
黄芪甲苷丹参素 | 0.98970.9904 | 0.02100.0161 | 0.02960.0198 | 0.03150.0227 | 3.84153.8711 | 5.34296.6879 |
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Cited By (10)
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CN102297846A (zh) * | 2011-07-28 | 2011-12-28 | 山东福瑞达生物医药有限公司 | 一种快速测定发酵液中透明质酸含量的方法 |
CN102914596A (zh) * | 2011-08-01 | 2013-02-06 | 漳州片仔癀药业股份有限公司 | 一种利用近红外光谱快速测定片仔癀质量的方法 |
CN103674884A (zh) * | 2012-09-17 | 2014-03-26 | 福建中烟工业有限责任公司 | 基于近红外光谱信息的烟叶风格特征的随机森林分类方法 |
CN103698281A (zh) * | 2013-12-31 | 2014-04-02 | 四川新绿色药业科技发展股份有限公司 | 补骨脂及其衍生产品的近红外漫反射测定方法 |
CN106164646A (zh) * | 2014-03-28 | 2016-11-23 | 江原大学校产学协力团 | 利用近红外分光法同时分析不同原料及形态的多种食品中营养成分含量的方法 |
CN107907612A (zh) * | 2017-11-16 | 2018-04-13 | 广州白云山和记黄埔中药有限公司 | 复方丹参片中丹酚酸b和冰片含量的测定方法和应用 |
CN108051396A (zh) * | 2017-12-14 | 2018-05-18 | 山东沃华医药科技股份有限公司 | 一种心可舒片有效成分含量的快速检测方法 |
CN109030408A (zh) * | 2018-06-29 | 2018-12-18 | 无锡济民可信山禾药业股份有限公司 | 一种快速的儿茶药材检测方法 |
CN110320286A (zh) * | 2018-03-29 | 2019-10-11 | 广州白云山光华制药股份有限公司 | 小柴胡颗粒有效成分的含量测定方法 |
CN111380832A (zh) * | 2018-12-27 | 2020-07-07 | 广州白云山光华制药股份有限公司 | 复方甘草片有效成分含量测定校正模型构建、检测方法 |
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CN1425909A (zh) * | 2002-12-31 | 2003-06-25 | 天津大学 | 中药滴丸制剂中有效成分的红外光谱检测方法 |
US7274457B2 (en) * | 2004-05-12 | 2007-09-25 | Pioneer Hi-Bred International, Inc. | Non-destructive derivation of weight of single seed or several seeds |
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CN102297846A (zh) * | 2011-07-28 | 2011-12-28 | 山东福瑞达生物医药有限公司 | 一种快速测定发酵液中透明质酸含量的方法 |
CN102914596A (zh) * | 2011-08-01 | 2013-02-06 | 漳州片仔癀药业股份有限公司 | 一种利用近红外光谱快速测定片仔癀质量的方法 |
CN102914596B (zh) * | 2011-08-01 | 2014-03-05 | 漳州片仔癀药业股份有限公司 | 一种利用近红外光谱快速测定片仔癀质量的方法 |
CN103674884A (zh) * | 2012-09-17 | 2014-03-26 | 福建中烟工业有限责任公司 | 基于近红外光谱信息的烟叶风格特征的随机森林分类方法 |
CN103698281A (zh) * | 2013-12-31 | 2014-04-02 | 四川新绿色药业科技发展股份有限公司 | 补骨脂及其衍生产品的近红外漫反射测定方法 |
CN106164646A (zh) * | 2014-03-28 | 2016-11-23 | 江原大学校产学协力团 | 利用近红外分光法同时分析不同原料及形态的多种食品中营养成分含量的方法 |
CN106164646B (zh) * | 2014-03-28 | 2019-01-04 | 江原大学校产学协力团 | 利用近红外分光法同时分析不同原料及形态的多种食品中营养成分含量的方法 |
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CN110320286A (zh) * | 2018-03-29 | 2019-10-11 | 广州白云山光华制药股份有限公司 | 小柴胡颗粒有效成分的含量测定方法 |
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