CN1824851A - Preparation of original bamboo fiber by bioenzyme method - Google Patents
Preparation of original bamboo fiber by bioenzyme method Download PDFInfo
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- CN1824851A CN1824851A CN 200510022616 CN200510022616A CN1824851A CN 1824851 A CN1824851 A CN 1824851A CN 200510022616 CN200510022616 CN 200510022616 CN 200510022616 A CN200510022616 A CN 200510022616A CN 1824851 A CN1824851 A CN 1824851A
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Abstract
The invention discloses a method to make bamboo origin fiber that the process includes following steps: cutting the bamboo and dissecting into sheet, adding to boiling water, taking out and crushing, hammering to filament, adding into pressure cooker to boil, dipping the processed bamboo filament into solution that contains biology enzyme to gain fibrin fiber, cleaning, whitening, oil pumping, softening, shredding the fibrin fiber, the bamboo origin fiber would be gained.
Description
Technical field
The present invention relates to a kind of the weaving, be meant especially and utilize bamboo to produce the technology of weaving, belong to field of textiles with bamboo fiber with the manufacture craft of natural bamboo fibres.
Background technology
Bamboo is that a kind of growth period is short, output height, the perennial plant of Yi Zaipei.Very abundant at China's bamboo resource, there be the grow thickly scattered bamboo kind of single-shaft variant of bamboo kind, subtropical zone growth and the strong multiple axle type of cold resistance of high latitude area growth of the sympodium type that is suitable for torrid zone growth to mix living bamboo kind.According to statistics, national bamboo plant has 48 genus, kind more than 500.These bamboo kinds are distributed on the vast territory on the south 40 ° of the north latitude.The existing bamboo grove area of China reaches 4,210,000 hectares, and savings are measured 1.27 hundred million tons.First of bamboo kind, savings, the output Jun Ju world, have the title of " bamboo kingdom ".Bamboo is the fastest plant that grows in the world, and whenever can grow tall round the clock when fast reaches 150-200 centimetre.Be 3-5 the growth period of bamboo, and the old root in bamboo felling back bears the Hsinchu naturally, if bamboo is not felled for a long time, can cause the death of full wafer bamboo grove on the contrary.Therefore, rationally fell bamboo, help environmental protection.
Utilizing bamboo to make textile fiber is the new direction that bamboo is used.Bamboo fiber is the cellulose fibre that directly extracts in the bamboo, is 100% degradable, its goods environmentally safe.Bamboo fiber also has natural antibacterial ability, the inside of fiber has been covered with big and small space, can and evaporate moisture content in transient absorption, therefore excellent hygroscopicity is arranged, and gas permeability is described as the fiber of " can breathe ", it also has good ABRASION RESISTANCE, drapability, dyeability is excellent clothes fiber.
The manufacturing of bamboo fiber is the focus that people are researching and developing always, at present existingly much openly reports about the document of the Chinese invention patent application of bamboo fiber.As number of patent application: 02151265.5,02133494.3,200310108826.1 and 200410060809.X, all explained a kind of weaving bamboo fiber manufacture method, adopt acid or alkali or other chemicals to come bamboo is handled, but can produce a large amount of reluctant sewage, cause environmental pollution; Number of patent application: 01123617.5 only is protection treatment process program and roll unit; Number of patent application: 02111380.7 protection content is the treatment process program, wherein mentions with softening agent is softening and handling, and does not all relate to as for the composition and the softening process condition of softening agent; Number of patent application: 200410046802.2 and 200410046835.7 is to take the straw mould that bamboo is carried out a biological disposal upon, the microorganism mould is handled to be actually to bamboo and utilizes the enzyme of mould generation that the non-cellulose thing in the bamboo is decomposed, and the mould synzyme is subjected to the dual control of gene and substrate, different concentration of substrate, the nitrogenous source kind, incubation time, the variation of pH value, trace element, surfactants etc. all are the factors that enzyme is produced in influence, therefore mould is handled bamboo to processing environment, incubation is strict, so it is that the cycle is long that this processing method is produced the shortcoming of bamboo fiber maximum, quality is unstable again.
How neither needing any chemical treatment, can make constant product quality again, is that people study a difficult problem of wanting to solve and never solving.
Summary of the invention
The technological deficiency of holding at above-mentioned existence the objective of the invention is to: having proposed does not a kind ofly need that any chemical treatment, simple to operate, processing time are short, the preparation of bamboo protofibre for weave by biological enzyme of constant product quality.
Technical scheme of the present invention is achieved in that a kind of preparation of bamboo protofibre for weave by biological enzyme, and its production technology is:
1. at first bamboo is blocked and cuts open into bamboo chip.Bamboo chip is put into boiling water boiling-off deliquescing, takes out crushing, filament hammer out.Put into the pressure cooker boiling again, remove part pectin, hemicellulose, lignin;
2. above-mentioned pretreated bamboo silk, immerse in the solution that contains biology enzyme and handle, allow biology enzyme decompose lignin, hemicellulose, pectin in the bamboo silk, to obtain the cellulose fibre in the bamboo;
3. when decomposing lignin, hemicellulose, pectin, also can in treatment fluid, add a certain amount of can cellulolytic enzyme, to obtain softness, very thin bamboo fibre;
4. the bamboo cellulose fibre after enzyme being decomposed cleans, bleaches, oils, soft, shredding can be for the bamboo fiber of the usefulness of weaving.
The enzyme preparation that the present invention adopts is industrial pure preparation, the purity height is arranged, activity stabilized, proportioning is accurate, this preparation of bamboo protofibre for weave by biological enzyme method of using, having during use on the historical facts or anecdotes border does not need any chemical treatment, simple to operate, the processing time short, the advantage of constant product quality.
The specific embodiment
Embodiment one:
A kind of preparation of bamboo protofibre for weave by biological enzyme, its production technology is:
1. mao bamboon is blocked and cuts open into bamboo chip, put into boiling water and boiled 1 hour, take out crushing, filament hammer out.Put into 120 ℃ of pressure cookers again and boiled 4 hours, remove part pectin, hemicellulose, lignin;
2. above-mentioned pretreated bamboo silk, the pectase that immerses 40 ℃ is that 1.0mg/ml, hemicellulase are that 1.0mg/ml, lignoenzyme are to handle 7 days in the solution of 2.0mg/ml;
3. the bamboo cellulose fibre after enzyme being decomposed takes out and cleans, bleaches, oils, soft, shredding, and obtaining average fineness is the 1050 public bamboo fibers that prop up.
Embodiment two:
A kind of preparation of bamboo protofibre for weave by biological enzyme, its production technology is:
1. the green bamboo rascal is blocked and cut open into bamboo chip, put into boiling water and boiled 2 hours, take out crushing, filament hammer out.Put into 100 ℃ of pressure cookers again and boiled 6 hours, remove part pectin, hemicellulose, lignin;
2. above-mentioned pretreated bamboo silk, the pectase that immerses 30 ℃ is that 20mg/ml, hemicellulase are that 15mg/m l, lignoenzyme are that 20mg/ml, cellulase are to handle 3 days in the solution of 5mg/ml;
3. the bamboo cellulose fibre after enzyme being decomposed takes out and cleans, bleaches, oils, soft, shredding, and obtaining average fineness is the 2700 public bamboo fibers that prop up.
Embodiment three:
A kind of preparation of bamboo protofibre for weave by biological enzyme, its production technology is:
1. mao bamboon is blocked and cuts open into small pieces, put into boiling water and boiled 1.5 hours, take out crushing, filament hammer out.Put into 110 ℃ of pressure cookers again and boiled 3 hours, remove part pectin, hemicellulose, lignin;
2. above-mentioned pretreated bamboo silk, the pectase that immerses 60 ℃ is that 50mg/ml, hemicellulase are that 40mg/ml, lignoenzyme are to handle 4 days in the solution of 50mg/ml;
3. the bamboo cellulose fibre after enzyme being decomposed takes out and cleans, bleaches, oils, soft, shredding, and obtaining average fineness is the 2650 public bamboo fibers that prop up.
Embodiment four:
A kind of preparation of bamboo protofibre for weave by biological enzyme, its production technology is:
1. the green bamboo rascal is blocked and cuts open in flakes, put into boiling water and boiled 1 hour, take out crushing, filament hammer out.Put into 105 ℃ of pressure cookers again and boiled 0.5 hour, remove part pectin, hemicellulose, lignin;
2. above-mentioned pretreated bamboo silk, the pectase that immerses 10 ℃ is that 25mg/ml, hemicellulase are that 20mg/ml, lignoenzyme are that 25mg/ml, cellulase are to handle 3 days in the solution of 10mg/ml;
3. the bamboo cellulose fibre after enzyme being decomposed takes out and cleans, bleaches, oils, soft, shredding, and obtaining average fineness is the 1560 public bamboo fibers that prop up.
Embodiment five:
A kind of preparation of bamboo protofibre for weave by biological enzyme, its production technology is:
1. go sinocalamus latiflorus rascal to block and cut open into small pieces, put into water and boiled 2 hours, take out crushing, filament hammer out.Put into 120 ℃ of pressure cookers again and boiled 3 hours, remove part pectin, hemicellulose, lignin;
2. above-mentioned pretreated bamboo silk, the pectase that immerses 35 ℃ is that 20mg/ml, hemicellulase are that 15mg/ml, lignoenzyme are that 20mg/ml, cellulase are to handle 3 days in the solution of 10mg/ml;
3. the bamboo cellulose fibre after enzyme being decomposed takes out and cleans, bleaches, oils, soft, shredding, and obtaining average fineness is the 2950 public bamboo fibers that prop up.
Embodiment six:
A kind of preparation of bamboo protofibre for weave by biological enzyme, its production technology is:
1. small pieces are blocked and cutd open into to blue or green bamboo, put into boiling water and boiled 2 hours, take out crushing, filament hammer out.Put into 115 ℃ of pressure cookers again and boiled 3.5 hours, remove part pectin, hemicellulose, lignin;
2. above-mentioned pretreated bamboo silk, the pectase that immerses 45 ℃ is that 2.0mg/ml, hemicellulase are that 5.0mg/ml, lignoenzyme are to handle 1 day in the solution of 3.0mg/ml;
3. the bamboo cellulose fibre after enzyme being decomposed takes out and cleans, bleaches, oils, soft, shredding, and obtaining average fineness is the 1320 public bamboo fibers that prop up.
Enzyme preparation in the foregoing description is commercial commodity, and the embodiment content helps to understand the present invention, but does not limit content of the present invention.
Claims (9)
1. preparation of bamboo protofibre for weave by biological enzyme, it is characterized in that: this technical process is as follows:
A, at first bamboo is blocked and cuts open into bamboo chip.Bamboo chip is put into boiling water boiling-off deliquescing, takes out crushing, filament hammer out.Put into the pressure cooker boiling again, remove part pectin, hemicellulose, lignin;
B, above-mentioned pretreated bamboo silk, immerse in the solution contain biology enzyme and handle, allow biology enzyme decompose lignin, hemicellulose, pectin in the bamboo silk, to obtain the cellulose fibre in the bamboo;
C, when decomposing lignin, hemicellulose, pectin, also can in treatment fluid, add a certain amount of can cellulolytic enzyme, to obtain softness, very thin bamboo fibre;
D, the bamboo cellulose fibre after enzyme decomposed clean, bleach, oil, soft, shredding can be for the bamboo fiber of the usefulness of weaving.
2. preparation of bamboo protofibre for weave by biological enzyme according to claim 1 is characterized in that: it is 1-2 hour that described bamboo chip is put into the boiling water boiling time.
3. preparation of bamboo protofibre for weave by biological enzyme according to claim 1 is characterized in that: the described pressure cooker boiling temperature of putting into is 80 ℃-120 ℃; Described digestion time is 0.5-6 hour.
4. preparation of bamboo protofibre for weave by biological enzyme according to claim 1 is characterized in that: described biology enzyme comprises pectase, hemicellulase, lignoenzyme, and the temperature that described enzyme is handled is 10-60 ℃; Described enzyme processing time is 1-7 days.
5. preparation of bamboo protofibre for weave by biological enzyme according to claim 1 is characterized in that: described can cellulolytic enzyme be cellulase.
6. preparation of bamboo protofibre for weave by biological enzyme according to claim 1 is characterized in that: the amount of described pectase is 1.0-50mg/ml.
7. preparation of bamboo protofibre for weave by biological enzyme according to claim 1 is characterized in that: the amount of described hemicellulase is 1.0-40mg/ml.
8. preparation of bamboo protofibre for weave by biological enzyme according to claim 1 is characterized in that: the amount of described lignoenzyme is 2.0-50mg/ml.
9. preparation of bamboo protofibre for weave by biological enzyme according to claim 1 is characterized in that: the amount of described cellulase is 0-10mg/ml.
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| Application Number | Priority Date | Filing Date | Title |
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| CNB200510022616XA CN100381620C (en) | 2005-12-26 | 2005-12-26 | Preparation of original bamboo fiber by bioenzyme method |
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| CNB200510022616XA CN100381620C (en) | 2005-12-26 | 2005-12-26 | Preparation of original bamboo fiber by bioenzyme method |
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| CN1824851A true CN1824851A (en) | 2006-08-30 |
| CN100381620C CN100381620C (en) | 2008-04-16 |
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| CNB200510022616XA Expired - Fee Related CN100381620C (en) | 2005-12-26 | 2005-12-26 | Preparation of original bamboo fiber by bioenzyme method |
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| CN101864602A (en) * | 2009-08-06 | 2010-10-20 | 廖大中 | Method for preparing bamboo fibers by separating bamboo |
| CN101538743B (en) * | 2009-04-28 | 2011-07-27 | 福建海博斯化学技术有限公司 | Solvent method for biologically preparing bamboo fiber |
| CN101781800B (en) * | 2010-01-22 | 2012-09-12 | 安吉德迈竹木机械有限公司 | Production method of bamboo fiber |
| CN102735567A (en) * | 2011-04-13 | 2012-10-17 | 中国农业大学 | Method for determining neutral detergent fiber content in pasture |
| CN102735566A (en) * | 2011-04-13 | 2012-10-17 | 中国农业大学 | Method for determining acid detergent fiber content in pasture |
| CN102959142A (en) * | 2011-03-21 | 2013-03-06 | 美国华益科技有限公司 | Production technology for natural bamboo fibers |
| CN103506084A (en) * | 2012-06-29 | 2014-01-15 | 中原工学院 | Preparation method of bamboo fiber/expanded graphite composite fiber adsorbing material |
| CN104178877A (en) * | 2014-07-29 | 2014-12-03 | 宁波华乐特汽车装饰布有限公司 | Processing method for automotive bamboo fiber interior fabric |
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| CN106012044A (en) * | 2016-07-12 | 2016-10-12 | 宜宾长顺竹木产业有限公司 | Degumming technology of natural bamboo fiber |
| CN108166070A (en) * | 2017-12-25 | 2018-06-15 | 福建农林大学 | A kind of preparation method of short bamboo fiber |
| CN109265940A (en) * | 2018-07-26 | 2019-01-25 | 嘉善天惠服饰有限公司 | One kind is for degradable PLA Biocomposite material of garment accessories and preparation method thereof |
| CN109321985A (en) * | 2018-11-20 | 2019-02-12 | 武汉纺织大学 | A method of it is extracted from reed straw and is used for textile fabric cellulose fiber |
| CN109733016A (en) * | 2018-12-11 | 2019-05-10 | 佛山市名洲纺织有限公司 | A kind of bamboo fiber-based porous fluffy nanofiber fabric and preparation method thereof of high-strength wind resistance heat preservation |
| CN109853051A (en) * | 2019-01-21 | 2019-06-07 | 泸州锦兰科技有限公司 | A kind of bamboo staple fiber extractive technique |
| CN110791815A (en) * | 2019-11-11 | 2020-02-14 | 徐州诺克非医药科技有限公司 | Preparation method of bamboo fiber powder based on chemical industry |
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| TW490376B (en) * | 2001-07-27 | 2002-06-11 | Bing-Hung Chen | Method for processing bamboo fiber |
| CN1208505C (en) * | 2002-04-10 | 2005-06-29 | 赵子群 | Bamboo fiber and its making process |
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| CN101538743B (en) * | 2009-04-28 | 2011-07-27 | 福建海博斯化学技术有限公司 | Solvent method for biologically preparing bamboo fiber |
| CN101864602A (en) * | 2009-08-06 | 2010-10-20 | 廖大中 | Method for preparing bamboo fibers by separating bamboo |
| CN101781800B (en) * | 2010-01-22 | 2012-09-12 | 安吉德迈竹木机械有限公司 | Production method of bamboo fiber |
| CN102959142A (en) * | 2011-03-21 | 2013-03-06 | 美国华益科技有限公司 | Production technology for natural bamboo fibers |
| CN102959142B (en) * | 2011-03-21 | 2016-01-06 | 张毅 | The production technology of natural bamboo fibres |
| CN102735567A (en) * | 2011-04-13 | 2012-10-17 | 中国农业大学 | Method for determining neutral detergent fiber content in pasture |
| CN102735566A (en) * | 2011-04-13 | 2012-10-17 | 中国农业大学 | Method for determining acid detergent fiber content in pasture |
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| CN103506084A (en) * | 2012-06-29 | 2014-01-15 | 中原工学院 | Preparation method of bamboo fiber/expanded graphite composite fiber adsorbing material |
| CN103506084B (en) * | 2012-06-29 | 2015-09-02 | 中原工学院 | The preparation method of a kind of bamboo fibre/expanded graphite composite fibre sorbing material |
| CN104178877A (en) * | 2014-07-29 | 2014-12-03 | 宁波华乐特汽车装饰布有限公司 | Processing method for automotive bamboo fiber interior fabric |
| CN104532364A (en) * | 2014-12-11 | 2015-04-22 | 青岛佰众化工技术有限公司 | Method for degumming hemp fiber |
| CN106012044A (en) * | 2016-07-12 | 2016-10-12 | 宜宾长顺竹木产业有限公司 | Degumming technology of natural bamboo fiber |
| CN106012044B (en) * | 2016-07-12 | 2018-06-01 | 宜宾长顺竹木产业有限公司 | A kind of degumming tech of bamboo fiber |
| CN108166070A (en) * | 2017-12-25 | 2018-06-15 | 福建农林大学 | A kind of preparation method of short bamboo fiber |
| CN108166070B (en) * | 2017-12-25 | 2019-08-30 | 福建农林大学 | A kind of preparation method of short bamboo fiber |
| CN109265940A (en) * | 2018-07-26 | 2019-01-25 | 嘉善天惠服饰有限公司 | One kind is for degradable PLA Biocomposite material of garment accessories and preparation method thereof |
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| CN109321985B (en) * | 2018-11-20 | 2021-08-31 | 武汉纺织大学 | Method for extracting cellulose fiber for textile from reed straw |
| CN109733016A (en) * | 2018-12-11 | 2019-05-10 | 佛山市名洲纺织有限公司 | A kind of bamboo fiber-based porous fluffy nanofiber fabric and preparation method thereof of high-strength wind resistance heat preservation |
| CN109853051A (en) * | 2019-01-21 | 2019-06-07 | 泸州锦兰科技有限公司 | A kind of bamboo staple fiber extractive technique |
| CN110791815A (en) * | 2019-11-11 | 2020-02-14 | 徐州诺克非医药科技有限公司 | Preparation method of bamboo fiber powder based on chemical industry |
| CN111979762A (en) * | 2020-08-26 | 2020-11-24 | 常熟市亿盛日用品有限公司 | Preparation method of bamboo fiber antibacterial cleaning cloth |
| CN113308902A (en) * | 2021-06-18 | 2021-08-27 | 东莞市骏腾贸易有限公司 | Production process of bio-based leather |
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