CN1820834A - 包括聚醚/聚酯的分散树脂 - Google Patents
包括聚醚/聚酯的分散树脂 Download PDFInfo
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- CN1820834A CN1820834A CNA2006100062978A CN200610006297A CN1820834A CN 1820834 A CN1820834 A CN 1820834A CN A2006100062978 A CNA2006100062978 A CN A2006100062978A CN 200610006297 A CN200610006297 A CN 200610006297A CN 1820834 A CN1820834 A CN 1820834A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G81/00—Macromolecular compounds obtained by interreacting polymers in the absence of monomers, e.g. block polymers
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L71/00—Compositions of polyethers obtained by reactions forming an ether link in the main chain; Compositions of derivatives of such polymers
- C08L71/02—Polyalkylene oxides
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0084—Dispersions of dyes
- C09B67/0085—Non common dispersing agents
- C09B67/009—Non common dispersing agents polymeric dispersing agent
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- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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- C09D11/32—Inkjet printing inks characterised by colouring agents
- C09D11/324—Inkjet printing inks characterised by colouring agents containing carbon black
- C09D11/326—Inkjet printing inks characterised by colouring agents containing carbon black characterised by the pigment dispersant
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D179/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen, with or without oxygen, or carbon only, not provided for in groups C09D161/00 - C09D177/00
- C09D179/02—Polyamines
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- C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
- C09K23/14—Derivatives of phosphoric acid
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- C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
- C09K23/16—Amines or polyamines
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
- C09K23/52—Natural or synthetic resins or their salts
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- C—CHEMISTRY; METALLURGY
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- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L67/00—Compositions of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Compositions of derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L71/00—Compositions of polyethers obtained by reactions forming an ether link in the main chain; Compositions of derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L79/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen with or without oxygen or carbon only, not provided for in groups C08L61/00 - C08L77/00
- C08L79/02—Polyamines
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Abstract
Description
聚酯 | 结构 |
1 | 月桂酸∶ε-己内酯(1∶12) |
2 | 硬脂酸∶ε-己内酯(1∶5) |
3 | 癸酸∶ε-己内酯∶δ-戊内酯(1∶12∶4) |
4 | 癸酸∶ε-己内酯∶δ-戊内酯(1∶8∶4) |
5 | 油酸∶ε-己内酯(1∶4) |
6 | 油酸∶ε-己内酯∶羟基十二内酯(1∶10∶2) |
7 | 月桂醇∶ε-己内酯∶δ-戊内酯(1∶5∶2) |
聚醚 | R | e | f | g | h | i |
I | 异壬基 | 4 | 4 | 4 | 0 | 1.0 |
II | 异壬基 | 1 | 5 | 0 | 0 | 1.0 |
III | 异壬基 | 1 | 9 | 0 | 0 | 1.0 |
IV | 丁基 | 3 | 0 | 0 | 2 | 2.5 |
V | 丁基 | 2 | 0 | 4 | 0 | 1.0 |
VI | 丁基 | 0 | 9 | 0 | 0 | 0.4 |
实施例 | 分散树脂 | 聚酯(PES) | 量[g] | 聚醚(PE) | 量[g] | PEI(Mn) | 量[g] | 重量比PES∶PE∶PEI |
1 | 1 | 1 | 90.0 | I | 7.2 | 25000 | 7.9 | 11.4∶0.9∶1 |
2 | 2 | 1 | 416.3 | IV | 14.5 | 5000 | 29.1 | 14.3∶0.5∶1 |
3 | 3 | 2 | 406.9 | I | 62.6 | 25000 | 75.0 | 5.4∶0.8∶1 |
4 | 4 | 3 | 352.2 | VI | 29.4 | 10000 | 58.7 | 10.0∶0.8∶1 |
5 | 5 | 4 | 243.1 | VI | 42.9 | 10000 | 14.3 | 9.0∶1.6∶1 |
6 | 6 | 4 | 156.5 | II | 36.4 | 10000 | 36.4 | 4.3∶1∶1 |
7 | 7 | 4 | 97.0 | II | 15.4 | 10000 | 7.7 | 12.6∶2∶1 |
8 | 8 | 4 | 463.6 | II | 33.7 | 5000 | 25.9 | 17.9∶1.3∶1 |
9 | 9 | 4 | 61.6 | II | 9.2 | 5000 | 6.1 | 10.1∶1.5∶1 |
10 | 10 | 4 | 266.0 | II | 14.0 | 1200 | 20.0 | 13.3∶0.7∶1 |
11 | 11 | 4 | 327.6 | II | 79.9 | 1200 | 42.0 | 7.8∶1.9∶1 |
12 | 12 | 4 | 661.0 | III | 33.0 | 10000 | 66.1 | 10.0∶0.5∶1 |
13 | 13 | 8 | 409.9 | II | 19.9 | 10000 | 39.8 | 10.3∶0.5∶1 |
14 | 14 | 4 | 409.9 | II | 19.9 | 5000 | 39.8 | 10.3∶0.5∶1 |
15 | 15 | 4 | 409.9 | II | 19.9 | 1200 | 39.8 | 10.3∶0.5∶1 |
16 | 16 | 5 | 51.7 | V | 18.8 | 10000 | 12.5 | 4.1∶1.5∶1 |
17 | 17 | 5 | 288.8 | II | 10.1 | PEI 1 | 52.6 | 5.5∶0.2∶1 |
18 | 18 | 6 | 288.8 | II | 10.1 | PEI 2 | 20.2 | 14.3∶0.5∶1 |
有机彩色颜料 | 碳黑颜料 | |
原料 | 重量% | 重量% |
Ebecryl812(UCB) | 25.75 | 25.08 |
Ebecryl220(UCB) | 6.57 | 6.40 |
LaromerTPGDA(BASF) | 29.02 | 28.27 |
LaromerTMPTA(BASF) | 16.27 | 15.85 |
分散树脂或对比例 | 1.77 | 2.39 |
颜料 | 11.79 | 13.40 |
Airex920(Tego) | 0.98 | 0.96 |
Irgacure1300(Ciba) | 5.89 | 5.74 |
Darocure1173(Ciba) | 1.96 | 1.91 |
合计 | 100.00 | 100.00 |
原料 | 重量% |
Ebecryl812(UCB) | 30.0 |
Ebecryl220(UCB) | 8.6 |
LaromerTPGDA(BASF) | 19.4 |
LaromerTMPTA(BASF) | 12.9 |
Kronos1075(KRONOS Int.) | 25.7 |
Irgacure819(Ciba) | 1.4 |
Darocure1173(Ciba) | 1.4 |
Airex920(Tego) | 0.6 |
实施例 | 分散树脂 | L* |
19 | 1 | 50.25 |
20 | 2 | 50.03 |
21 | 3 | 50.71 |
22 | 4 | 50.84 |
23 | 5 | 50.24 |
24 | 6 | 50.83 |
25 | 7 | 50.56 |
26 | 8 | 50.93 |
27 | 9 | 50.72 |
28 | 10 | 50.76 |
29 | 11 | 50.14 |
30 | 12 | 50.35 |
31 | 13 | 50.48 |
32 | 14 | 50.90 |
33 | 15 | 50.50 |
34 | 16 | 50.59 |
35 | 17 | 50.65 |
36 | 18 | 51.09 |
37 | 14+18;(50重量%∶50重量%) | 51.23 |
对比例 | C1 | 52.31 |
对比例 | C2 | 51.69 |
Raven450 | L* | 以mPas计的粘度(10l/s;25℃) |
空白样品 | 82.24 | 2491 |
对比例C1 | 73.02 | 1603 |
对比例C4 | 66.45 | 1367 |
对比例C5 | 70.07 | 1587 |
对比例C6 | 65.89 | 1355 |
分散树脂1 | 63.96 | 959 |
Spezialschwarz250 | L* | 以mPas计的粘度(10l/s;25℃) |
空白样品 | 59.18 | 962 |
对比例C1 | 52.31 | 901 |
对比例C4 | 50.50 | 348 |
对比例C5 | 50.57 | 316 |
对比例C6 | 50.49 | 304 |
分散树脂1 | 50.25 | 261 |
HostapermViolet P-RL | C* | 以mPas计的粘度(10l/s;25℃) |
空白样品 | 34.82 | 1061 |
对比例C1 | 35.04 | 989 |
对比例C4 | 37.25 | 583 |
对比例C5 | 37.47 | 666 |
对比例C6 | 37.32 | 592 |
分散树脂1 | 37.77 | 523 |
IrgaliteYellow BAW | b* | 以mPas计的粘度(10l/s;25℃) |
空白样品 | 26.05 | 3084 |
对比例C1 | 37.94 | 2021 |
对比例C4 | 49.04 | 1447 |
对比例C5 | 46.97 | 1843 |
对比例C6 | 48.98 | 1458 |
分散树脂1 | 49.70 | 1457 |
原料 | 初始质量,g |
DesmophenAVPLS 2350粘合剂(Bayer AG) | 462.0 |
KRONOS2310二氧化钛(KRONOS Int.) | 369.6 |
二甲苯 | 25.0 |
乙酸甲氧基丙酯(MPA) | 25.0 |
乙酸丁酯(BuAc) | 25.0 |
将上面5种组分在一21装有700g珠的分散罐中于10m/s下分散2小时,之后加入剩余组分 | |
Tegokat 219催化剂(81%的二甲苯中)(Goldschmidt TIBGmbH) | 13.4 |
溶剂混合物二甲苯/MPA/BuAc 1∶1∶1 | 76.2 |
原料 | 初始质量,g |
AlkydalF681粘合剂(75%的石油溶剂中)(BayerAG) | 280.0 |
KRONOS2065二氧化钛(KRONOS Int.) | 300.0 |
溶剂:石油溶剂 | 90.0 |
将上面3种组分在一分散罐中在冷却下于18m/s下分散30分钟,然后与以下组分混合,并搅拌 | |
AlkydalF681粘合剂(75%的石油溶剂中)(BayerAG) | 255.8 |
Nuodex Ca干燥器(5%)(Elementis Specialties,Inc.) | 2.0 |
Nuodex Zr干燥器(12%)(Elementis Specialties,Inc.) | 3.0 |
Nuodex Co干燥器(6%)(Elementis Specialties,Inc.) | 3.2 |
Ascinin R 55防结皮剂(Borchers) | 0.8 |
分散树脂 | 碳黑膏剂(S/U) | 细分配(μm) | 亮度值L* |
对比例C3 | U | n/a | n/a |
对比例C4 | U | n/a | n/a |
对比例C5 | U | n/a | n/a |
对比例C6 | U | n/a | n/a |
1 | S | <10μm | 56.8 |
2 | S | <12μm | 55.4 |
5 | S | <10μm | 54.2 |
6 | S | <8μm | 54.1 |
12 | S | <12μm | 55.8 |
18 | S | <10μm | 54.7 |
分散树脂 | 亮度值L* |
1 | 59.8 |
2 | 60.7 |
5 | 61.0 |
7 | 59.7 |
9 | 60.3 |
15 | 60.8 |
18 | 61.2 |
Claims (9)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102005004024A DE102005004024A1 (de) | 2005-01-28 | 2005-01-28 | Polyether/Polyester enthaltende Dispergierharze |
DE102005004024.1 | 2005-01-28 |
Publications (2)
Publication Number | Publication Date |
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CN1820834A true CN1820834A (zh) | 2006-08-23 |
CN100545192C CN100545192C (zh) | 2009-09-30 |
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CNB2006100062978A Active CN100545192C (zh) | 2005-01-28 | 2006-01-25 | 包括聚醚/聚酯的分散树脂 |
Country Status (8)
Country | Link |
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US (1) | US8202935B2 (zh) |
EP (1) | EP1685895B1 (zh) |
JP (1) | JP2006206902A (zh) |
CN (1) | CN100545192C (zh) |
BR (1) | BRPI0600200A (zh) |
CA (1) | CA2529678C (zh) |
DE (1) | DE102005004024A1 (zh) |
DK (1) | DK1685895T3 (zh) |
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- 2005-01-28 DE DE102005004024A patent/DE102005004024A1/de not_active Withdrawn
- 2005-12-09 CA CA2529678A patent/CA2529678C/en not_active Expired - Fee Related
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2006
- 2006-01-12 JP JP2006004669A patent/JP2006206902A/ja active Pending
- 2006-01-14 EP EP06000768A patent/EP1685895B1/de active Active
- 2006-01-14 DK DK06000768.9T patent/DK1685895T3/da active
- 2006-01-25 CN CNB2006100062978A patent/CN100545192C/zh active Active
- 2006-01-26 US US11/341,253 patent/US8202935B2/en active Active
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Also Published As
Publication number | Publication date |
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EP1685895A2 (de) | 2006-08-02 |
DE102005004024A1 (de) | 2006-08-03 |
EP1685895A3 (de) | 2012-04-04 |
CA2529678A1 (en) | 2006-07-28 |
JP2006206902A (ja) | 2006-08-10 |
BRPI0600200A (pt) | 2006-09-19 |
US8202935B2 (en) | 2012-06-19 |
CA2529678C (en) | 2013-03-26 |
US20060183815A1 (en) | 2006-08-17 |
DK1685895T3 (da) | 2013-06-17 |
EP1685895B1 (de) | 2013-03-13 |
CN100545192C (zh) | 2009-09-30 |
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