CN1769245A - Oil drop glaze preparation method - Google Patents
Oil drop glaze preparation method Download PDFInfo
- Publication number
- CN1769245A CN1769245A CN 200510096003 CN200510096003A CN1769245A CN 1769245 A CN1769245 A CN 1769245A CN 200510096003 CN200510096003 CN 200510096003 CN 200510096003 A CN200510096003 A CN 200510096003A CN 1769245 A CN1769245 A CN 1769245A
- Authority
- CN
- China
- Prior art keywords
- glaze
- slip
- mixture
- glaze slip
- adds
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Glass Compositions (AREA)
- Adornments (AREA)
Abstract
The invention provides a method for preparation of a drop glaze, which contains: mixing potash feldspar, terminus earth, talc, red lead oxide, vanadic anhydride, manganese oxide, ferric oxide and copper oxide; adding carboxymethyl cellulose as a paste regulator and grinding, sifting by 220 meshes sifter to prepare slip glaze; coating the surface of dry billet of pottery with the slip glaze, drying; putting the dried billet into a electric stove, keeping temperature for 0.5-2 hours in 1160-1220Deg. C in air oxidizing atmosphere or H2 and CO reducing atmosphere; cooling down naturally to the room temperature. The invention is characterized in that drop glaze can be prepared in a low temperature and a wide sintering temperature; the technique is simple to control, is repeatable and suitable for kinds of pottery billet; the usage of ferric oxide raw material, and there is no need of adding bone ash and P2O5; it can prepare golden and silver drop glaze, and the drop on the glaze has uniform size and distribution, and the glaze is smooth.
Description
Technical field
The present invention relates to a kind of preparation method of oil-spot glaze.
Background technology
Oil-spot glaze is one of a famous and precious glaze kind in China Southern Song Dynasty period, mainly originates in Fujian and builds peace kiln, Jiangxi Chien ware, belongs to temmoku series glaze with the writing brush made of rabbit's hair, tea dust etc., be that iron is crystalline glaze, ancient title " oil droplet pearl " also claims " rain drop glaze ", is called the oil droplet temmoku in the world.Its glaze characteristics are to reveal many dots that silver gray or ochreous have metalluster that have in the glaze of black come-up, as " pitch-dark night sky Stem and leaf of Hongkong Pavetta ", " contain tea and dodge golden light, be filled with water and dodge silver-colored light ", have also spilt oil drop on the water surface as calmness.Simple and honest, dignified, simple because of its color and luster, unique decorative effect is arranged, have long enjoyed a good reputation in the world, be loved by the people.
Oil-spot glaze have " mystery of the strange pottery of China " and saying.Be regarded as famous and precious porcelain at all times, especially in Japan, a chi bottle cun broad-mouthed receptacle for holding liquid is considered as supreme product, and tender tea leaves bowl small handless wine cup is sighed and is the treasure of generation not.Even the fragment that also has oil-spot glaze also with emerald green the saying of gold with valency.Oil-spot glaze at Chinese origin in the Tang Dynasty, maturation and Song dynasty.Shandong Boshan (modern Zibo City) oil-spot glaze is the most famous.Reportedly, be provided with porcelain storehouse, Qingzhou the Northern Song Dynasty.Oil-spot glaze is listed in tribute, pays tribute the emperor.When foreign countries pay tribute, king Song with it as the gift of giving as security back.But it is lost after the Yuan Dynasty because of chaos caused by war.The Republic of China so far, particularly after the foundation of new China, potteries artist in various places once did a large amount of recovery research work, obtained certain effect, but the situation that the good recipe difficulty is looked for, elaboration is rare thoroughly changes yet, the historical and cultural heritage that this is precious has been close to lost.
Shanghai silicate institute once analyzed the chemical constitution of Song dynasty oil-spot glaze, and its chemical constitution generally is in following scope: Fe
2O
3Content 4～8%, the content 6～9% of CaO, the content of MgO is more than 2%, Al
2O
3Content be no more than 20%, in addition should be by a little P
2O
5Deng.[Li Jiazhi etc. Ancient Chinese is for the ceramic science technological contribution. Shanghai: Shanghai Science Press, 1988] therefore, people have adopted diverse ways and prescription on above basis, also prepared oil-spot glaze.For example people such as Guo Qiang adds an amount of bone ash as the phase-splitting agent on conventional ceramic raw mineral materials system-based, in 1230-1250 ℃ temperature range, burn till, imitation Song-Dynasty-style typeface black oil-spot glaze [Guo Qiang, EXPERIMENT OF IMITATING OIL-DROP GLAZE, Chinese pottery have been prepared, 2000 (5): 13] [Guo Qiang, Study on Glazed Porcelain in Zibo, ceramic research, 1996, (1), 10-5].Wang Jinfeng [Wang Jinfeng; Liu Weijie; Liu Baohua; Li Zhi's great waves. the development of imitative Southern Song Dynasty oil-spot glaze. ceramic engineering .2001 (12)]; Miu Songlan [Miu Songlan, horse brilliance, money literary composition China. the research of oil-spot glaze manufacture craft. Chinese pottery industry .2002 (4)] etc. the people adopt similar method, also prepared oil-spot glaze.
Yet, have following limitation in the present method of reporting for preparing oil-spot glaze.The first, all adopt SiO
2-Al
2O
3-Fe
2O
3-CaO-MgO-K
2O-Na
2O-P
2O
5Glaze becomes sub-system, wherein P
2O
5Be main phase-splitting raw material, lack P
2O
5Glaze then be difficult to form the oil droplet effect, promptly enable to produce oil droplet and also be difficult to the size of control oil droplet and distribute, influence the decorative effect of oil droplet; The second, present preparation temperature is higher, generally could produce oil droplet more than 1230 ℃, and firing range is very narrow, and is very responsive to temperature, and general upper and lower temperature difference is no more than 20 ℃, otherwise can not form the oil droplet effect, therefore is difficult to realize suitability for industrialized production; The 3rd, the method control ratio of present prepared oil-spot glaze is difficult, and particularly the oil droplet effect is to very responsive to atmosphere and glazing thickness; The 4th, present oil-spot glaze preparation method can only prepare silver-colored oil droplet, is difficult to prepare polishes and drips.
Summary of the invention
The objective of the invention is to overcome the shortcoming of above-mentioned prior art, provide a kind of technology controlling and process simple, good reproducibility and under lower temperature and in the wide temperature range, can prepare the preparation method of the oil-spot glaze of golden and silver color oil droplet.
For achieving the above object, the preparation method that the present invention adopts is: at first by mass percentage the potassium felspar sand of 69-70%, the Jiepai clay of 7-9%, the talcum of 2.2-2.6%, the lead oxide red of 14.5-15.5%, the Vanadium Pentoxide in FLAKES of 0.8-2%, the manganese oxide of 0-0.6%, the ferric oxide of 3-3.4% and the cupric oxide of 0-1.5% are mixed and made into mixture; Press mixture: mill ball: the mass ratio of water=1: 2: 0.8 adds in the shredder, and the carboxymethyl cellulose that adds mixture quality per-cent 0.1～0.3% simultaneously grinds as the slip conditioning agent, grinds to finish back mistake 220 mesh sieves and make glaze slip; Glaze slip is applied to ceramic dry body surface, and the coat-thickness of control glaze slip is 0.3-1.5mm, then 40-80 ℃ of oven dry down; Glazing base substrate after the oven dry is put into electric furnace, in 1160-1220 ℃ temperature range, at atmospheric oxidation atmosphere or H
2, down insulation 0.5-2 hour of CO reducing atmosphere; Get final product to room temperature behind the naturally cooling.
The present invention can prepare oil-spot glaze in the firing range of lower temperature and broad; And technology controlling and process is simple, and good process repeatability all is suitable for various ceramic bodies, adopts atmospheric oxidation atmosphere or H
2, the CO reducing atmosphere burns till all and can obtain oil-spot glaze, glaze is insensitive to temperature, firing atmosphere and glazing thickness, easily control; The raw iron oxide material consumption is few, and does not need to add bone ash and introduce P
2O
5Can prepare golden oil-spot glaze and silver color oil-spot glaze, and on the glaze oil droplet size be evenly distributed, glaze is level and smooth, good decorating effect.
Embodiment
Embodiment 1: at first by mass percentage 69% potassium felspar sand, 9% Jiepai clay, 2.2% talcum, 14.5% lead oxide red, 0.8% Vanadium Pentoxide in FLAKES, 3% ferric oxide and 1.5% cupric oxide are mixed and made into mixture; Press mixture: mill ball: the mass ratio of water=1: 2: 0.8 adds in the shredder, and the carboxymethyl cellulose that adds mixture quality per-cent 0.1% simultaneously grinds as the slip conditioning agent, grinds to finish back mistake 220 mesh sieves and make glaze slip; Glaze slip is applied to ceramic dry body surface, and the coat-thickness of control glaze slip is 0.3mm, then 40 ℃ of oven dry down; Glazing base substrate after the oven dry is put into electric furnace, and in 1160 ℃ temperature range, insulation is 0.5 hour under atmospheric oxidation atmosphere; Can obtain the silver color oil-spot glaze to room temperature behind the naturally cooling.
Embodiment 2: at first by mass percentage 70% potassium felspar sand, 7% Jiepai clay, 2.6% talcum, 15% lead oxide red, 1.5% Vanadium Pentoxide in FLAKES, 0.6% manganese oxide, 3% ferric oxide and 0.3% cupric oxide are mixed and made into mixture; Press mixture: mill ball: the mass ratio of water=1: 2: 0.8 adds in the shredder, and the carboxymethyl cellulose that adds mixture quality per-cent 0.2% simultaneously grinds as the slip conditioning agent, grinds to finish back mistake 220 mesh sieves and make glaze slip; Glaze slip is applied to ceramic dry body surface, and the coat-thickness of control glaze slip is 0.8mm, then 80 ℃ of oven dry down; Glazing base substrate after the oven dry is put into electric furnace, in 1220 ℃ temperature range, at H
2Reducing atmosphere is incubated 1 hour down; Can obtain the silver color oil-spot glaze to room temperature behind the naturally cooling.
Embodiment 3: at first by mass percentage 69% potassium felspar sand, 8% Jiepai clay, 2.5% talcum, 15.5% lead oxide red, 2% Vanadium Pentoxide in FLAKES and 3% ferric oxide are mixed and made into mixture; Press mixture: mill ball: the mass ratio of water=1: 2: 0.8 adds in the shredder, and the carboxymethyl cellulose that adds mixture quality per-cent 0.3% simultaneously grinds as the slip conditioning agent, grinds to finish back mistake 220 mesh sieves and make glaze slip; Glaze slip is applied to ceramic dry body surface, and the coat-thickness of control glaze slip is 1.2mm, then 60 ℃ of oven dry down; Glazing base substrate after the oven dry is put into electric furnace, and in 1200 ℃ temperature range, insulation is 2 hours under the CO reducing atmosphere; Can obtain golden oil-spot glaze to room temperature behind the naturally cooling.
Embodiment 4: at first by mass percentage 69.5% potassium felspar sand, 7.5% Jiepai clay, 2.4% talcum, 15.2% lead oxide red, 1% Vanadium Pentoxide in FLAKES, 0.5% manganese oxide, 3.4% ferric oxide and 0.5% cupric oxide are mixed and made into mixture; Press mixture: mill ball: the mass ratio of water=1: 2: 0.8 adds in the shredder, and the carboxymethyl cellulose that adds mixture quality per-cent 0.2% simultaneously grinds as the slip conditioning agent, grinds to finish back mistake 220 mesh sieves and make glaze slip; Glaze slip is applied to ceramic dry body surface, and the coat-thickness of control glaze slip is 1.5mm, then 50 ℃ of oven dry down; Glazing base substrate after the oven dry is put into electric furnace, and in 1180 ℃ temperature range, insulation is 1.5 hours under atmospheric oxidation atmosphere; Can obtain golden oil-spot glaze to room temperature behind the naturally cooling.
Embodiment 5: at first by mass percentage 69% potassium felspar sand, 8.5% Jiepai clay, 2.3% talcum, 14.8% lead oxide red, 1.2% Vanadium Pentoxide in FLAKES, 0.2% manganese oxide, 3.1% ferric oxide and 0.9% cupric oxide are mixed and made into mixture; Press mixture: mill ball: the mass ratio of water=1: 2: 0.8 adds in the shredder, and the carboxymethyl cellulose that adds mixture quality per-cent 0.1% simultaneously grinds as the slip conditioning agent, grinds to finish back mistake 220 mesh sieves and make glaze slip; Glaze slip is applied to ceramic dry body surface, and the coat-thickness of control glaze slip is 1.0mm, then 70 ℃ of oven dry down; Glazing base substrate after the oven dry is put into electric furnace, in 1210 ℃ temperature range, at H
2Reducing atmosphere is incubated 0.5 hour down; Can obtain golden oil-spot glaze to room temperature behind the naturally cooling.
Embodiment 6: at first by mass percentage 70% potassium felspar sand, 7.5% Jiepai clay, 2.2% talcum, 15.3% lead oxide red, 1% Vanadium Pentoxide in FLAKES, 0.4% manganese oxide, 3.3% ferric oxide and 0.3% cupric oxide are mixed and made into mixture; Press mixture: mill ball: the mass ratio of water=1: 2: 0.8 adds in the shredder, and the carboxymethyl cellulose that adds mixture quality per-cent 0.3% simultaneously grinds as the slip conditioning agent, grinds to finish back mistake 220 mesh sieves and make glaze slip; Glaze slip is applied to ceramic dry body surface, and the coat-thickness of control glaze slip is 0.5mm, then 55 ℃ of oven dry down; Glazing base substrate after the oven dry is put into electric furnace, and in 1170 ℃ temperature range, insulation is 2 hours under the CO reducing atmosphere; Can obtain golden oil-spot glaze to room temperature behind the naturally cooling.
Claims (7)
1, a kind of preparation method of oil-spot glaze is characterized in that:
1) at first by mass percentage the potassium felspar sand of 69-70%, the Jiepai clay of 7-9%, the talcum of 2.2-2.6%, the lead oxide red of 14.5-15.5%, the Vanadium Pentoxide in FLAKES of 0.8-2%, the manganese oxide of 0-0.6%, the ferric oxide of 3-3.4% and the cupric oxide of 0-1.5% are mixed and made into mixture;
2) press mixture: mill ball: the mass ratio of water=1: 2: 0.8 adds in the shredder, and the carboxymethyl cellulose that adds mixture quality per-cent 0.1～0.3% simultaneously grinds as the slip conditioning agent, grinds to finish back mistake 220 mesh sieves and make glaze slip;
3) glaze slip is applied to ceramic dry body surface, the coat-thickness of control glaze slip is 0.3-1.5mm, then 40-80 ℃ of oven dry down; Glazing base substrate after the oven dry is put into electric furnace, in 1160-1220 ℃ temperature range, at atmospheric oxidation atmosphere or H
2, down insulation 0.5-2 hour of CO reducing atmosphere; Get final product to room temperature behind the naturally cooling.
2, the preparation method of oil-spot glaze according to claim 1 is characterized in that: at first by mass percentage 69% potassium felspar sand, 9% Jiepai clay, 2.2% talcum, 14.5% lead oxide red, 0.8% Vanadium Pentoxide in FLAKES, 3% ferric oxide and 1.5% cupric oxide are mixed and made into mixture; Press mixture: mill ball: the mass ratio of water=1: 2: 0.8 adds in the shredder, and the carboxymethyl cellulose that adds mixture quality per-cent 0.1% simultaneously grinds as the slip conditioning agent, grinds to finish back mistake 220 mesh sieves and make glaze slip; Glaze slip is applied to ceramic dry body surface, and the coat-thickness of control glaze slip is 0.3mm, then 40 ℃ of oven dry down; Glazing base substrate after the oven dry is put into electric furnace, and in 1160 ℃ temperature range, insulation is 0.5 hour under atmospheric oxidation atmosphere; Get final product to room temperature behind the naturally cooling.
3, the preparation method of oil-spot glaze according to claim 1 is characterized in that: at first by mass percentage 70% potassium felspar sand, 7% Jiepai clay, 2.6% talcum, 15% lead oxide red, 1.5% Vanadium Pentoxide in FLAKES, 0.6% manganese oxide, 3% ferric oxide and 0.3% cupric oxide are mixed and made into mixture; Press mixture: mill ball: the mass ratio of water=1: 2: 0.8 adds in the shredder, and the carboxymethyl cellulose that adds mixture quality per-cent 0.2% simultaneously grinds as the slip conditioning agent, grinds to finish back mistake 220 mesh sieves and make glaze slip; Glaze slip is applied to ceramic dry body surface, and the coat-thickness of control glaze slip is 0.8mm, then 80 ℃ of oven dry down; Glazing base substrate after the oven dry is put into electric furnace, in 1220 ℃ temperature range, at H
2Reducing atmosphere is incubated 1 hour down; Get final product to room temperature behind the naturally cooling.
4, the preparation method of oil-spot glaze according to claim 1 is characterized in that: at first by mass percentage 69% potassium felspar sand, 8% Jiepai clay, 2.5% talcum, 15.5% lead oxide red, 2% Vanadium Pentoxide in FLAKES and 3% ferric oxide are mixed and made into mixture; Press mixture: mill ball: the mass ratio of water=1: 2: 0.8 adds in the shredder, and the carboxymethyl cellulose that adds mixture quality per-cent 0.3% simultaneously grinds as the slip conditioning agent, grinds to finish back mistake 220 mesh sieves and make glaze slip; Glaze slip is applied to ceramic dry body surface, and the coat-thickness of control glaze slip is 1.2mm, then 60 ℃ of oven dry down; Glazing base substrate after the oven dry is put into electric furnace, and in 1200 ℃ temperature range, insulation is 2 hours under the CO reducing atmosphere; Get final product to room temperature behind the naturally cooling.
5, the preparation method of oil-spot glaze according to claim 1 is characterized in that: at first by mass percentage 69.5% potassium felspar sand, 7.5% Jiepai clay, 2.4% talcum, 15.2% lead oxide red, 1% Vanadium Pentoxide in FLAKES, 0.5% manganese oxide, 3.4% ferric oxide and 0.5% cupric oxide are mixed and made into mixture; Press mixture: mill ball: the mass ratio of water=1: 2: 0.8 adds in the shredder, and the carboxymethyl cellulose that adds mixture quality per-cent 0.2% simultaneously grinds as the slip conditioning agent, grinds to finish back mistake 220 mesh sieves and make glaze slip; Glaze slip is applied to ceramic dry body surface, and the coat-thickness of control glaze slip is 1.5mm, then 50 ℃ of oven dry down; Glazing base substrate after the oven dry is put into electric furnace, and in 1180 ℃ temperature range, insulation is 1.5 hours under atmospheric oxidation atmosphere; Get final product to room temperature behind the naturally cooling.
6, the preparation method of oil-spot glaze according to claim 1 is characterized in that: at first by mass percentage 69% potassium felspar sand, 8.5% Jiepai clay, 2.3% talcum, 14.8% lead oxide red, 1.2% Vanadium Pentoxide in FLAKES, 0.2% manganese oxide, 3.1% ferric oxide and 0.9% cupric oxide are mixed and made into mixture; Press mixture: mill ball: the mass ratio of water=1: 2: 0.8 adds in the shredder, and the carboxymethyl cellulose that adds mixture quality per-cent 0.1% simultaneously grinds as the slip conditioning agent, grinds to finish back mistake 220 mesh sieves and make glaze slip; Glaze slip is applied to ceramic dry body surface, and the coat-thickness of control glaze slip is 1.0mm, then 70 ℃ of oven dry down; Glazing base substrate after the oven dry is put into electric furnace, in 1210 ℃ temperature range, at H
2Reducing atmosphere is incubated 0.5 hour down; Get final product to room temperature behind the naturally cooling.
7, the preparation method of oil-spot glaze according to claim 1 is characterized in that: at first by mass percentage 70% potassium felspar sand, 7.5% Jiepai clay, 2.2% talcum, 15.3% lead oxide red, 1% Vanadium Pentoxide in FLAKES, 0.4% manganese oxide, 3.3% ferric oxide and 0.3% cupric oxide are mixed and made into mixture; Press mixture: mill ball: the mass ratio of water=1: 2: 0.8 adds in the shredder, and the carboxymethyl cellulose that adds mixture quality per-cent 0.3% simultaneously grinds as the slip conditioning agent, grinds to finish back mistake 220 mesh sieves and make glaze slip; Glaze slip is applied to ceramic dry body surface, and the coat-thickness of control glaze slip is 0.5mm, then 55 ℃ of oven dry down; Glazing base substrate after the oven dry is put into electric furnace, and in 1170 ℃ temperature range, insulation is 2 hours under the CO reducing atmosphere; Get final product to room temperature behind the naturally cooling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100960030A CN100358842C (en) | 2005-09-08 | 2005-09-08 | Oil drop glaze preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100960030A CN100358842C (en) | 2005-09-08 | 2005-09-08 | Oil drop glaze preparation method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1769245A true CN1769245A (en) | 2006-05-10 |
| CN100358842C CN100358842C (en) | 2008-01-02 |
Family
ID=36750831
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2005100960030A Expired - Fee Related CN100358842C (en) | 2005-09-08 | 2005-09-08 | Oil drop glaze preparation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN100358842C (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100447110C (en) * | 2006-03-30 | 2008-12-31 | 霍镰泉 | Preparation method of dry glaze for pasedo-classic glazed tile |
| CN100450976C (en) * | 2007-07-31 | 2009-01-14 | 陕西科技大学 | Method for preparing positioning iron red crystal glaze |
| CN100453512C (en) * | 2006-03-30 | 2009-01-21 | 霍镰泉 | Dry glaze for pasedo-classic glazed tile |
| CN101306957B (en) * | 2008-07-03 | 2011-05-04 | 湖南省醴陵市楚华陶瓷实业有限公司 | Method of making archaic crystal fancy glaze |
| CN101759442B (en) * | 2010-01-08 | 2011-12-14 | 蔡奕洲 | Blue ceramic decorative porcelain glaze and preparation method thereof |
| CN104987045A (en) * | 2015-06-24 | 2015-10-21 | 史江伟 | Preparation process of greyness temmoku oil-spot glaze porcelain |
| CN106082982A (en) * | 2016-08-21 | 2016-11-09 | 宜兴爱宜艺术陶瓷有限公司 | A kind of boccaro polishes drips enameling method |
| CN106396385A (en) * | 2016-08-31 | 2017-02-15 | 福建省德化佳诚陶瓷有限公司 | Golden stripe tiger skin enameled container and manufacturing technology thereof |
| CN115838246A (en) * | 2022-12-27 | 2023-03-24 | 陕西科技大学 | Silver glaze and preparation method for firing silver glaze in reducing atmosphere |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1021836C (en) * | 1991-04-20 | 1993-08-18 | 中国科学院电工研究所 | Ion plating technology for titanium carbonitride coatings |
| CN1036516C (en) * | 1994-01-29 | 1997-11-26 | 邢良坤 | Hongtianmu glaze ceramic and producing method |
-
2005
- 2005-09-08 CN CNB2005100960030A patent/CN100358842C/en not_active Expired - Fee Related
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100447110C (en) * | 2006-03-30 | 2008-12-31 | 霍镰泉 | Preparation method of dry glaze for pasedo-classic glazed tile |
| CN100453512C (en) * | 2006-03-30 | 2009-01-21 | 霍镰泉 | Dry glaze for pasedo-classic glazed tile |
| CN100450976C (en) * | 2007-07-31 | 2009-01-14 | 陕西科技大学 | Method for preparing positioning iron red crystal glaze |
| CN101306957B (en) * | 2008-07-03 | 2011-05-04 | 湖南省醴陵市楚华陶瓷实业有限公司 | Method of making archaic crystal fancy glaze |
| CN101759442B (en) * | 2010-01-08 | 2011-12-14 | 蔡奕洲 | Blue ceramic decorative porcelain glaze and preparation method thereof |
| CN104987045A (en) * | 2015-06-24 | 2015-10-21 | 史江伟 | Preparation process of greyness temmoku oil-spot glaze porcelain |
| CN106082982A (en) * | 2016-08-21 | 2016-11-09 | 宜兴爱宜艺术陶瓷有限公司 | A kind of boccaro polishes drips enameling method |
| CN106396385A (en) * | 2016-08-31 | 2017-02-15 | 福建省德化佳诚陶瓷有限公司 | Golden stripe tiger skin enameled container and manufacturing technology thereof |
| CN106396385B (en) * | 2016-08-31 | 2019-10-22 | 福建省德化佳诚陶瓷有限公司 | Golden spot tiger fur glaze porcelain and its manufacture craft |
| CN115838246A (en) * | 2022-12-27 | 2023-03-24 | 陕西科技大学 | Silver glaze and preparation method for firing silver glaze in reducing atmosphere |
Also Published As
| Publication number | Publication date |
|---|---|
| CN100358842C (en) | 2008-01-02 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN100358842C (en) | Oil drop glaze preparation method | |
| CN101786904B (en) | Color-changing glaze for metallic luster ceramics and preparation method thereof | |
| CN102731066B (en) | Porcelain with Junyu glaze and manufacturing method thereof | |
| CN108751718B (en) | Preparation process of relief oil drop jian cup | |
| CN112456802B (en) | Giant crystal particles capable of forming crystal flowers, dry particle combination, particles for ceramics, ceramics and preparation method of ceramics | |
| CN100360462C (en) | Glaze coloured decoration daily use poocelain and its production method | |
| CN105884197A (en) | Method for preparing series iron-series colored glaze from iron-ore slag and decoration method based on colored glaze | |
| CN102060571A (en) | Green glaze for domestic porcelain | |
| CN107010922B (en) | Preparation method of transmutation glaze purple sand fine pottery | |
| CN108484114B (en) | Glazed ceramic tile with high-content polishing waste and preparation method thereof | |
| CN105776866B (en) | Longquan celadon jasper green glaze, the green Longquan celadon of jasper and preparation method thereof | |
| CN110845252A (en) | Special blank large-particle combined digital cloth archaized brick and preparation method thereof | |
| CN114773033B (en) | Daily ceramic product with transparent glaze and preparation method thereof | |
| CN111995360A (en) | Manufacturing process of squama manis oil drop jian cup | |
| CN102633535B (en) | Method for preparing gemstone fancy glaze | |
| CN105218162B (en) | A kind of ceramet glaze and preparation method thereof | |
| CN100453009C (en) | Western tableware of iron and ceramic and its making process | |
| CN111233328B (en) | Lead-free metallic luster glaze, ceramic thereof and preparation method of lead-free metallic luster glaze | |
| CN110963781B (en) | Craft porcelain with glaze surface having raised particle effect and preparation method thereof | |
| CN102060572A (en) | Method for manufacturing ceramic weathered glaze | |
| CN112830679B (en) | Mixed gray glaze, preparation process and firing method of pottery thereof | |
| CN101367613B (en) | Red oil spot glaze and method of preparing ceramic product | |
| CN115286361A (en) | Preparation process of black hair jian calendula | |
| CN114573232A (en) | Tile-splitting glaze for ceramic tiles and method for preparing ceramic tiles | |
| CN110950536A (en) | Bronze-imitating artistic ceramic and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20080102 Termination date: 20100908 |