CN100450976C - Method for preparing positioning iron red crystal glaze - Google Patents
Method for preparing positioning iron red crystal glaze Download PDFInfo
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- CN100450976C CN100450976C CNB2007100183854A CN200710018385A CN100450976C CN 100450976 C CN100450976 C CN 100450976C CN B2007100183854 A CNB2007100183854 A CN B2007100183854A CN 200710018385 A CN200710018385 A CN 200710018385A CN 100450976 C CN100450976 C CN 100450976C
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Abstract
The present invention discloses a preparation method for positioning ferreous crystal; the preparation of the base glaze is that: potassic feldspar, quartz, kaoline, ocher, steatite, limestone and bone ash are mixed with ferric oxide for grilling; the proportion of the glaze slurry is 1.6-1.7 g/cm3; the preparation method of the crystal core is that: kaoline is mixed with ferric oxide for grilling and calcining and cooling to become grain powder; and then crystal core is pre-buried in the position for the blank body to form the crystal flower; the size Phi of the preburied hole is about 1mm; the quantity and distribution are adjusted according to the actual requirement; the base glaze is put on the ceramic blank body preburied with crystal core evenly; the thickness of the glaze level is controlled on 0.7-1.0mm; the semi finished product of the ceramic glaze is baked to the maximum temperature with oxidation blaze, and then is cooled into the room temperature. The present invention uses the common ceramic raw material and the positioning crystal measure to produce the positioning ferreous crystal glaze, which solves the shortcoming that the size and the distribution for the ferreous crystal flower is hard to be controlled; the method is a stable preparation method with simple process technical, wide baking temperature range, good stability, without needing middle temperature heat preservation; the produce cost is much lower.
Description
Technical field
The invention belongs to the stupalith field, be specifically related to a kind of preparation method of positioning iron red crystal glaze.
Background technology
Along with growth in the living standard, people are also more and more higher to the demand grade of decorative ceramics, very big variation has taken place in modern's aesthetic consciousness, and people no longer appreciate those complicated numerous and jumbled works, but are more attracted by extremely uncomplicated, the simple and unadorned and generous form of the original art of the mankind.
To be crystalline glaze in the Song dynasty begin to burn iron makes, and the tea set that forms a kind of characteristic decorates, and famous have kinds such as oil droplet, the writing brush made of rabbit's hair, francolin spot at that time, is the earliest one of crystalline glaze product in the world.Iron red crystal glaze (iron oxide red fancy glaze) is the category of crystalline glaze as iron, its glaze is the pea size on the umbrinaceous background color, the discrete red crystallization of circle, make whole goods present unique beautiful outward appearance, just as a bunch bunch red plum that bursts forth, rich and gaudy and do not show poor taste, have on the high artistry to be worth.Its appearance once caused the attention on domestic and international ceramic boundary.But because its crystalline range is narrower; Firing condition harshness, and often be difficult for again controlling artificially that crystalline distributes and quantity in the glaze makes the stability and the repeated extreme difference of this series products; Brought difficulty to commercialization production, so that this series products can only rest on the position of showpiece for a long time.
Summary of the invention
The objective of the invention is to overcome the deficiencies in the prior art, provide a kind of preparation technology simple, enlarged the maturing range of iron red crystal glaze, improved its stability and repeated, easy realization of industrialization is produced, and the preparation method of the lower positioning iron red crystal glaze of manufacturing cost.
For achieving the above object, the technical solution used in the present invention is: by mass percentage with the potassium felspar sand of 40-45%, the quartz of 10-15%, the kaolin of 5-8%, the loess of 5-8%, the talcum of 8-10%, the Wingdale of 5-6%, the bone ash of 12-15% and 7-12% ferric oxide mix, and are finely ground to 250 orders, glaze slip proportion 1.6-1.7g/cm
3
2) nucleus agent preparation method: by mass percentage with the ferric oxide mixing of the kaolin of 30-70% and 30-70%, ball milling, 1270-1300 ℃ of calcining, be ground into the particle about 1mm after the cooling;
3) the nucleus agent is embedded in base substrate and need forms on the crystalline position, pre-buried via hole exists
About, the quantity and the adjustment voluntarily as required that distributes;
4) parent glaze is evenly bestowed on the ceramic body that is embedded with the nucleus agent, the glaze layer thickness is controlled at 0.7-1.0mm and obtains work in-process;
5) work in-process are burnt till with oxydizing flame under 1270 ℃-1300 ℃, be incubated and naturally cool to room temperature after 10-30 minute and get final product.
The present invention utilizes conventional ceramic raw material, and utilization location crystallization means have made positioning iron red crystal glaze, has solved the size and the distribution of the brilliant flower of iron oxide red, realized stable preparation method, because technology is simple, wide, the good stability of firing range, temperature insulation in need not, production cost is lower.
Embodiment
Embodiment 1: by mass percentage with 40% potassium felspar sand, and 15% quartz, 5% kaolin, 5% loess, 10% talcum, 5% Wingdale, 13% bone ash and 7% ferric oxide mix, and are finely ground to 250 orders, glaze slip proportion 1.6g/cm
3Nucleus agent preparation method: by mass percentage with the ferric oxide mixing of 30% kaolin and 70%, ball milling, 1270 ℃ of calcinings, be ground into the particle about 1mm after the cooling; The nucleus agent is embedded in base substrate need forms on the crystalline position, pre-buried via hole exists usually
About, the quantity and the adjustment voluntarily as required that distributes; Parent glaze is evenly bestowed on the ceramic body that is embedded with the nucleus agent, and the glaze layer thickness is controlled at 0.7mm and obtains work in-process; Work in-process are burnt till with oxydizing flame under 1270 ℃, be incubated and naturally cool to room temperature after 20 minutes and get final product.
Embodiment 2: by mass percentage with 45% potassium felspar sand, and 10% quartz, 6% kaolin, 6% loess, 8% talcum, 5% Wingdale, 12% bone ash and 8% ferric oxide mix, and are finely ground to 250 orders, glaze slip proportion 1.7g/cm
3Nucleus agent preparation method: by mass percentage with the ferric oxide mixing of 50% kaolin and 50%, ball milling, 1290 ℃ of calcinings, be ground into the particle about 1mm after the cooling; The nucleus agent is embedded in base substrate need forms on the crystalline position, pre-buried via hole exists usually
About, the quantity and the adjustment voluntarily as required that distributes; Parent glaze is evenly bestowed on the ceramic body that is embedded with the nucleus agent, and the glaze layer thickness is controlled at 0.9mm and obtains work in-process; Work in-process are burnt till with oxydizing flame under 1290 ℃, be incubated and naturally cool to room temperature after 30 minutes and get final product.
Embodiment 3: by mass percentage with 42% potassium felspar sand, and 12% quartz, 8% kaolin, 5% loess, 8% talcum, 6% Wingdale, 12% bone ash and 7% ferric oxide mix, and are finely ground to 250 orders, glaze slip proportion 1.7g/cm
3Nucleus agent preparation method: by mass percentage with the ferric oxide mixing of 70% kaolin and 30%, ball milling, 1280 ℃ of calcinings, be ground into the particle about 1mm after the cooling; The nucleus agent is embedded in base substrate need forms on the crystalline position, pre-buried via hole exists usually
About, the quantity and the adjustment voluntarily as required that distributes; Parent glaze is evenly bestowed on the ceramic body that is embedded with the nucleus agent, and the glaze layer thickness is controlled at 0.8mm and obtains work in-process; Work in-process are burnt till with oxydizing flame under 1280 ℃, be incubated and naturally cool to room temperature after 10 minutes and get final product.
Embodiment 4: by mass percentage with 40% potassium felspar sand, and 10% quartz, 5% kaolin, 8% loess, 8% talcum, 5% Wingdale, 15% bone ash and 9% ferric oxide mix, and are finely ground to 250 orders, glaze slip proportion 1.6g/cm
3Nucleus agent preparation method: by mass percentage with the ferric oxide mixing of 40% kaolin and 60%, ball milling, 1300 ℃ of calcinings, be ground into the particle about 1mm after the cooling; The nucleus agent is embedded in base substrate need forms on the crystalline position, pre-buried via hole exists usually
About, the quantity and the adjustment voluntarily as required that distributes; Parent glaze is evenly bestowed on the ceramic body that is embedded with the nucleus agent, and the glaze layer thickness is controlled at 1.0mm and obtains work in-process; Work in-process are burnt till with oxydizing flame under 1300 ℃, be incubated and naturally cool to room temperature after 15 minutes and get final product.
Embodiment 5: by mass percentage with 40% potassium felspar sand, and 10% quartz, 5% kaolin, 6% loess, 9% talcum, 6% Wingdale, 12% bone ash and 12% ferric oxide mix, and are finely ground to 250 orders, glaze slip proportion 1.7g/cm
3Nucleus agent preparation method: by mass percentage with the ferric oxide mixing of 60% kaolin and 40%, ball milling, 1280 ℃ of calcinings, be ground into the particle about 1mm after the cooling; The nucleus agent is embedded in base substrate need forms on the crystalline position, pre-buried via hole exists usually
About, the quantity and the adjustment voluntarily as required that distributes; Parent glaze is evenly bestowed on the ceramic body that is embedded with the nucleus agent, and the glaze layer thickness is controlled at 1.0mm and obtains work in-process; Work in-process are burnt till with oxydizing flame under 1280 ℃, be incubated and naturally cool to room temperature after 25 minutes and get final product.
Claims (6)
1, a kind of preparation method of positioning iron red crystal glaze is characterized in that:
1) preparation of parent glaze: by mass percentage with the potassium felspar sand of 40-45%, the quartz of 10-15%, the kaolin of 5-8%, the loess of 5-8%, the talcum of 8-10%, the Wingdale of 5-6%, the bone ash of 12-15% and 7-12% ferric oxide mix, and are finely ground to 250 orders, glaze slip proportion 1.6-1.7g/cm
3
2) nucleus agent preparation method: by mass percentage with the ferric oxide mixing of the kaolin of 30-70% and 30-70%, ball milling, 1270-1300 ℃ of calcining, be ground into the particle about 1mm after the cooling;
3) the nucleus agent is embedded in base substrate and need forms on the crystalline position, pre-buried via hole exists
About, the quantity and the adjustment voluntarily as required that distributes;
4) parent glaze is evenly bestowed on the ceramic body that is embedded with the nucleus agent, the glaze layer thickness is controlled at 0.7-1.0mm, thereby obtains work in-process;
5) work in-process are burnt till with oxydizing flame under 1270 ℃-1300 ℃, be incubated and naturally cool to room temperature after 10-30 minute and get final product.
2, the preparation method of positioning iron red crystal glaze according to claim 1, it is characterized in that: by mass percentage with 40% potassium felspar sand, 15% quartz, 5% kaolin, 5% loess, 10% talcum, 5% Wingdale, 13% bone ash and 7% ferric oxide mix, and are finely ground to 250 orders, glaze slip proportion 1.6g/cm
3Nucleus agent preparation method: by mass percentage with the ferric oxide mixing of 30% kaolin and 70%, ball milling, 1270 ℃ of calcinings, be ground into the particle about 1mm after the cooling; The nucleus agent is embedded in base substrate need forms on the crystalline position, pre-buried via hole exists
About, the quantity and the adjustment voluntarily as required that distributes; Parent glaze is evenly bestowed on the ceramic body that is embedded with the nucleus agent, and the glaze layer thickness is controlled at 0.7mm and obtains work in-process; Work in-process are burnt till with oxydizing flame under 1270 ℃, be incubated and naturally cool to room temperature after 20 minutes and get final product.
3, the preparation method of positioning iron red crystal glaze according to claim 1, it is characterized in that: by mass percentage with 45% potassium felspar sand, 10% quartz, 6% kaolin, 6% loess, 8% talcum, 5% Wingdale, 12% bone ash and 8% ferric oxide mix, and are finely ground to 250 orders, glaze slip proportion 1.7g/cm
3Nucleus agent preparation method: by mass percentage with the ferric oxide mixing of 50% kaolin and 50%, ball milling, 1290 ℃ of calcinings, be ground into the particle about 1mm after the cooling; The nucleus agent is embedded in base substrate need forms on the crystalline position, pre-buried via hole exists
About, the quantity and the adjustment voluntarily as required that distributes; Parent glaze is evenly bestowed on the ceramic body that is embedded with the nucleus agent, and the glaze layer thickness is controlled at 0.9mm and obtains work in-process; Work in-process are burnt till with oxydizing flame under 1290 ℃, be incubated and naturally cool to room temperature after 30 minutes and get final product.
4, the preparation method of positioning iron red crystal glaze according to claim 1, it is characterized in that: at first by mass percentage with 42% potassium felspar sand, 12% quartz, 8% kaolin, 5% loess, 8% talcum, 6% Wingdale, 12% bone ash and 7% ferric oxide mix, and are finely ground to 250 orders, then glaze slip proportion 1.7g/cm
3Soak glaze; Nucleus agent preparation method: by mass percentage with the ferric oxide mixing of 70% kaolin and 30%, ball milling, 1280 ℃ of calcinings, be ground into the particle about 1mm after the cooling; The nucleus agent is embedded in base substrate need forms on the crystalline position, pre-buried via hole exists
About, the quantity and the adjustment voluntarily as required that distributes; Parent glaze is evenly bestowed on the ceramic body that is embedded with the nucleus agent, and the glaze layer thickness is controlled at 0.8mm and obtains work in-process; Work in-process are burnt till with oxydizing flame under 1280 ℃, be incubated and naturally cool to room temperature after 10 minutes and get final product.
5, the preparation method of positioning iron red crystal glaze according to claim 1, it is characterized in that: at first by mass percentage with 40% potassium felspar sand, 10% quartz, 5% kaolin, 8% loess, 8% talcum, 5% Wingdale, 15% bone ash and 9% ferric oxide mix, and are finely ground to 250 orders, then glaze slip proportion 1.6g/cm
3Soak glaze; Nucleus agent preparation method: by mass percentage with the ferric oxide mixing of 40% kaolin and 60%, ball milling, 1300 ℃ of calcinings, be ground into the particle about 1mm after the cooling; The nucleus agent is embedded in base substrate need forms on the crystalline position, pre-buried via hole exists
About, the quantity and the adjustment voluntarily as required that distributes; Parent glaze is evenly bestowed on the ceramic body that is embedded with the nucleus agent, and the glaze layer thickness is controlled at 1.0mm and obtains work in-process; Work in-process are burnt till with oxydizing flame under 1300 ℃, be incubated and naturally cool to room temperature after 15 minutes and get final product.
6, the preparation method of positioning iron red crystal glaze according to claim 1, it is characterized in that: at first by mass percentage with 40% potassium felspar sand, 10% quartz, 5% kaolin, 6% loess, 9% talcum, 6% Wingdale, 12% bone ash and 12% ferric oxide mix, and are finely ground to 250 orders, then glaze slip proportion 1.7g/cm
3Soak glaze; Nucleus agent preparation method: by mass percentage with the ferric oxide mixing of 60% kaolin and 40%, ball milling, 1280 ℃ of calcinings, be ground into the particle about 1mm after the cooling; The nucleus agent is embedded in base substrate need forms on the crystalline position, pre-buried via hole exists
About, the quantity and the adjustment voluntarily as required that distributes; Parent glaze is evenly bestowed on the ceramic body that is embedded with the nucleus agent, and the glaze layer thickness is controlled at 1.0mm and obtains work in-process; Work in-process are burnt till with oxydizing flame under 1280 ℃, be incubated and naturally cool to room temperature after 25 minutes and get final product.
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| Application Number | Priority Date | Filing Date | Title |
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| CNB2007100183854A CN100450976C (en) | 2007-07-31 | 2007-07-31 | Method for preparing positioning iron red crystal glaze |
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| CNB2007100183854A CN100450976C (en) | 2007-07-31 | 2007-07-31 | Method for preparing positioning iron red crystal glaze |
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| CN100450976C true CN100450976C (en) | 2009-01-14 |
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Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101624297B (en) * | 2009-08-07 | 2011-11-09 | 陕西科技大学 | Preparation method for tea dust temmoku glaze |
| CN102173869B (en) * | 2011-01-19 | 2013-02-27 | 江苏高淳陶瓷股份有限公司 | Preparation method of non-ferrous tea dust crystalline glaze |
| CN104446659A (en) * | 2014-12-01 | 2015-03-25 | 王桂忠 | Iron oxide oil-drop transmutation glaze |
| CN105218166A (en) * | 2015-10-23 | 2016-01-06 | 张昭 | Self-cleaning mirror face ceramics glaze of hydrophobic and preparation method thereof |
| CN105693091B (en) * | 2016-01-20 | 2018-05-15 | 福建省德化县鸿芳陶瓷有限公司 | Sapporo color ceramic and its Sapporo color ceramic preparation process |
| CN107619188A (en) * | 2017-10-25 | 2018-01-23 | 西安文理学院 | A kind of ceramic glaze and preparation method thereof |
| CN109627051A (en) * | 2018-12-30 | 2019-04-16 | 鲁山县段店花瓷非物质文化遗产开发有限公司 | The production method of tea set |
| CN110510989A (en) * | 2019-07-06 | 2019-11-29 | 福建省乐普陶板制造有限公司 | A kind of crystalline glaze ceramic plate and preparation method thereof |
| CN113860924B (en) * | 2021-09-28 | 2023-05-02 | 福建省德化博龙陶瓷有限公司 | Under-glaze green thorn over-glaze safflower ceramic and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1769245A (en) * | 2005-09-08 | 2006-05-10 | 陕西科技大学 | Oil drop glaze preparation method |
| CN1887809A (en) * | 2006-07-24 | 2007-01-03 | 胡天霏 | Bright red underglaze color, overglaze and their prepn process |
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- 2007-07-31 CN CNB2007100183854A patent/CN100450976C/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1769245A (en) * | 2005-09-08 | 2006-05-10 | 陕西科技大学 | Oil drop glaze preparation method |
| CN1887809A (en) * | 2006-07-24 | 2007-01-03 | 胡天霏 | Bright red underglaze color, overglaze and their prepn process |
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