CN1695870A - Electron beam welding method of adding transition layer into compound between metals of titanium aluminium alloy - Google Patents
Electron beam welding method of adding transition layer into compound between metals of titanium aluminium alloy Download PDFInfo
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- CN1695870A CN1695870A CN 200510010088 CN200510010088A CN1695870A CN 1695870 A CN1695870 A CN 1695870A CN 200510010088 CN200510010088 CN 200510010088 CN 200510010088 A CN200510010088 A CN 200510010088A CN 1695870 A CN1695870 A CN 1695870A
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Abstract
An electronic beam welding method of Ti-Al alloy by adding transmission layer to generate intermetallic compound includes thermally treating the Ti-Al alloy to be welded for eliminating stress, chemically and physically cleaning the surfaces of TiAl alloy and metallic foil, filling the metallic foil in the seam to be welded, preheating by electronic beam, microalloying by electronic beam, and natural cooling.
Description
Technical field:
What the present invention relates to is the welding technology field of compound between metals of titanium aluminium alloy.
Background technology:
Metallic bond in existing titanium aluminium (TiAl) alloy crystal and covalent bond coexistence, make the high-temperature behavior of its intensity that has metal concurrently and pottery, and producing high specific strength, specific modulus, good non-oxidizability, creep resistance etc. therefrom, these advantages make it demonstrate good prospects for application as aero-engine and automobile heat resistant structure material.Want this type of alloy of successful Application will inevitably involve the secondary operations (as weldability) of alloy in the production reality.From present present Research as can be seen, the connection of Intermatallic Ti-Al compound self and with being connected of other metals, mainly be connected to the master with solid phase.Although characteristics and the superiority with himself compared in soldering, diffusion welding (DW) with melting welding, but also there is its intrinsic defective in it, lower as strength of joint, heat resistance is relatively poor, and owing to adopt lap joint morely, increase the consumption of mother metal and the weight of structure, thereby also become the research focus of recent welding field at the research of the melting welding interconnection technique of this intermetallic compound.The subject matter that also has electron beam welding to show in the TiAl alloy connects is easily to produce solid-state crackle, for reducing the sensitiveness of joint to crackle, just must take suitable preheat temperature, preheat temperature is high more, the heat affected area cooling rate is low more, joint crackle tendency is more little, but can not avoid the generation of joint underbead crack all the time.Also have TiAl intermetallic compound argon arc to weld in the recovery project of being everlasting and use, the normal method that adopts is to adopt superhigh temperature preheating (more than 800 ℃) before weldering, and has worsened working environment, and then has improved labour intensity, has reduced welding efficiency.And the mechanical strength of weld seam is starkly lower than mother metal at this moment, must improve the intensity of joint by suitable post weld heat treatment technology.
Summary of the invention:
The objective of the invention is in order to overcome in existing titanium aluminium (TiAl) the alloy welding, existing needs superhigh temperature preheating, joint inside easily cracks, postwelding needs heat treatment, the welding point mechanical strength is low problem before the weldering, and then a kind of compound between metals of titanium aluminium alloy electro-beam welding method that adds transition zone is provided.Its welding method step is: a, the heat treatment that removes stress-removal before titanium-aluminium alloy to be welded welded, and heating-up temperature is 600 ℃～700 ℃, temperature retention time is 1.5h～3h; B, physics and soak cleaning are carried out in the weld surface of titanium-aluminium alloy to be welded, the surface of metal forming, the thickness of metal forming is 30 μ m～1000 μ m; C, metal forming is arranged between the weld seam, and clamps; D, be 5 * 10 in vacuum
-2Pa～5 * 10
-4Under the condition of Pa, scan preheating or defocus preheating with the electron beam butt welded seam, the preheating number of times is 1 time～4 times; E, be 5 * 10 in vacuum
-2Pa～5 * 10
-4Under the condition of Pa, be that 2500mA～2700mA, accelerating potential are 40kV～60kV, to quicken electric current be that the electron beam butt welded seam of 10mA～30mA carries out microalloying and handles with focus current; F, original position naturally cool to room temperature.The present invention under vacuum condition with in high temperature preheating (about 500 ℃) back just can weld titanium-aluminium alloy, the inside of its welding point does not have that crackle, weld appearance are level and smooth, the mechanical strength of welding point is suitable with the mechanical strength of mother metal, and is useful for the various terminal form of welding.It also has simple, the manageable advantage of step, and can suppress the hot tearing and the cold cracking phenomenon of such alloy.
Description of drawings:
Fig. 1 is the relative position structural representation between titanium-aluminium alloy to be welded, metal forming and the electron beam in the specific embodiment one.
The specific embodiment:
The specific embodiment one: in conjunction with Fig. 1 present embodiment is described, its welding method step is: a, the heat treatment that removes stress-removal before titanium-aluminium alloy to be welded welded, and heating-up temperature is 600 ℃～700 ℃, temperature retention time is 1.5h～3h; B, physics cleaning and soak cleaning are carried out in the surface of the weld surface of titanium-aluminium alloy to be welded, metal forming, the thickness of metal forming is 30 μ m～1000 μ m; C, metal forming is arranged between the weld seam, and clamps; D, be 5 * 10 in vacuum
-2Pa～5 * 10
-4Under the condition of Pa, scan preheating or defocus preheating with the electron beam butt welded seam, the preheating number of times is 1 time～4 times; E, be 5 * 10 in vacuum
-2Pa～5 * 10
-4Under the condition of Pa, be that 2500mA～2700mA, accelerating potential are 40kV～60kV, to quicken electric current be that the electron beam butt welded seam of 10mA～30mA carries out microalloying and handles with focus current; F, original position naturally cool to room temperature.Described physics cleaning can select for use abrasive paper for metallograph to polish step by step; Soak cleaning can be selected HF, HNO for use
3And H
2The mixed liquor of O cleans.
The specific embodiment two: the chemical composition of metal forming is made up of one or more mixing in titanium, the β phase stabilizing element in the step b of the specific embodiment one described welding method; Above-mentioned β phase stabilizing element comprises molybdenum, chromium, vanadium, niobium or manganese.
The specific embodiment three: the sweep waveform of electron beam scanning preheating is the symmetric figure waveform in the steps d of the specific embodiment one described welding method.The sweep waveform of electron beam scanning preheating can be selected square wave or sine wave for use.
The specific embodiment four: to carry out the speed that microalloying handles be 4mm/s～20mm/s to the electron beam butt welded seam in the step e of the specific embodiment one described welding method.
The specific embodiment five: the heat treatment that the difference of the present embodiment and the specific embodiment one is its welding method step a, remove stress-removal before titanium-aluminium alloy to be welded is welded, heating-up temperature is 620 ℃, temperature retention time is 2h; B, physics cleaning and soak cleaning are carried out in the surface of the weld surface of titanium-aluminium alloy to be welded, metal forming, the thickness of metal forming is 100 μ m; E, be 1 * 10 in vacuum
-2Under the condition of Pa, be that 2590mA, accelerating potential are 45kV, to quicken electric current be that the electron beam butt welded seam of 15mA carries out microalloying and handles with focus current.Other condition is identical with the specific embodiment one with step.
The specific embodiment six: the heat treatment that the difference of the present embodiment and the specific embodiment one is its welding method step a, remove stress-removal before titanium-aluminium alloy to be welded is welded, heating-up temperature is 650 ℃, temperature retention time is 2.4h; B, physics cleaning and soak cleaning are carried out in the surface of the weld surface of titanium-aluminium alloy to be welded, metal forming, the thickness of metal forming is 500 μ m; E, be 5 * 10 in vacuum
-3Under the condition of Pa, be that 2650mA, accelerating potential are 50kV, to quicken electric current be that the electron beam butt welded seam of 20mA carries out microalloying and handles with focus current.Other condition is identical with the specific embodiment one with step.
The specific embodiment seven: the heat treatment that the difference of the present embodiment and the specific embodiment one is its welding method step a, remove stress-removal before titanium-aluminium alloy to be welded is welded, heating-up temperature is 690 ℃, temperature retention time is 2.8h; B, physics cleaning and soak cleaning are carried out in the surface of the weld surface of titanium-aluminium alloy to be welded, metal forming, the thickness of metal forming is 900 μ m; E, be 1 * 10 in vacuum
-3Under the condition of Pa, be that 2690mA, accelerating potential are 55kV, to quicken electric current be that the electron beam butt welded seam of 25mA carries out microalloying and handles with focus current.Other condition is identical with the specific embodiment one with step.
Claims (7)
1, a kind of compound between metals of titanium aluminium alloy electro-beam welding method that adds transition zone, the welding method step that it is characterized in that it is: a, the heat treatment that removes stress-removal before titanium-aluminium alloy to be welded welded, heating-up temperature is 600 ℃～700 ℃, and temperature retention time is 1.5h～3h; B, physics cleaning and soak cleaning are carried out in the surface of the weld surface of titanium-aluminium alloy to be welded, metal forming, the thickness of metal forming is 30 μ m～1000 μ m; C, metal forming is arranged between the weld seam, and clamps; D, be 5 * 10 in vacuum
-2Pa～5 * 10
-4Under the condition of Pa, scan preheating or defocus preheating with the electron beam butt welded seam, the preheating number of times is 1 time～4 times; E, be 5 * 10 in vacuum
-2Pa～5 * 10
-4Under the condition of Pa, be that 2500mA～2700mA, accelerating potential are 40kV～60kV, to quicken electric current be that the electron beam butt welded seam of 10mA～30mA carries out microalloying and handles with focus current; F, original position naturally cool to room temperature.
2, a kind of compound between metals of titanium aluminium alloy electro-beam welding method that adds transition zone according to claim 1 is characterized in that the chemical composition of metal forming among the step b of welding method is made up of one or more mixing in titanium, the β phase stabilizing element.
3, a kind of compound between metals of titanium aluminium alloy electro-beam welding method that adds transition zone according to claim 1 is characterized in that the sweep waveform of electron beam scanning preheating in the steps d of welding method is the symmetric figure waveform.
4, a kind of compound between metals of titanium aluminium alloy electro-beam welding method that adds transition zone according to claim 1 is characterized in that it is 4mm/s～20mm/s that electron beam butt welded seam among the step e of welding method carries out the speed that microalloying handles.
5, a kind of compound between metals of titanium aluminium alloy electro-beam welding method that adds transition zone according to claim 1, the welding method step that it is characterized in that it is: a, the heat treatment that removes stress-removal before titanium-aluminium alloy to be welded welded, heating-up temperature is 620 ℃, and temperature retention time is 2h; B, physics cleaning and soak cleaning are carried out in the surface of the weld surface of titanium-aluminium alloy to be welded, metal forming, the thickness of metal forming is 100 μ m; E, be 1 * 10 in vacuum
-2Under the condition of Pa, be that 2590mA, accelerating potential are 45kV, to quicken electric current be that the electron beam butt welded seam of 15mA carries out microalloying and handles with focus current.
6, a kind of compound between metals of titanium aluminium alloy electro-beam welding method that adds transition zone according to claim 1, the welding method step that it is characterized in that it is: a, the heat treatment that removes stress-removal before titanium-aluminium alloy to be welded welded, heating-up temperature is 650 ℃, and temperature retention time is 2.4h; B, physics cleaning and soak cleaning are carried out in the surface of the weld surface of titanium-aluminium alloy to be welded, metal forming, the thickness of metal forming is 500 μ m; E, be 5 * 10 in vacuum
-3Under the condition of Pa, be that 2650mA, accelerating potential are 50kV, to quicken electric current be that the electron beam butt welded seam of 20mA carries out microalloying and handles with focus current.
7, a kind of compound between metals of titanium aluminium alloy electro-beam welding method that adds transition zone according to claim 1, the welding method step that it is characterized in that it is: a, the heat treatment that removes stress-removal before titanium-aluminium alloy to be welded welded, heating-up temperature is 690 ℃, and temperature retention time is 2.8h; B, physics cleaning and soak cleaning are carried out in the surface of the weld surface of titanium-aluminium alloy to be welded, metal forming, the thickness of metal forming is 900 μ m; E, be 1 * 10 in vacuum
-3Under the condition of Pa, be that 2690mA, accelerating potential are 55kV, to quicken electric current be that the electron beam butt welded seam of 25mA carries out microalloying and handles with focus current.
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Cited By (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100450694C (en) * | 2006-11-21 | 2009-01-14 | 宁波江丰电子材料有限公司 | A vacuum electron beam welding method |
| CN100462178C (en) * | 2007-06-18 | 2009-02-18 | 哈尔滨工业大学 | Compound control method for heat cycle of electron beam welding TiAl / TC4 heterogeneous materials |
| CN101811222A (en) * | 2010-05-20 | 2010-08-25 | 西安航天远征流体控制股份有限公司 | Method for welding titanium anode slot |
| CN101890570A (en) * | 2010-06-18 | 2010-11-24 | 哈尔滨工业大学 | Electron-beam welding method for aluminum alloy and steel based on intermediate layer isolation control |
| CN101690991B (en) * | 2009-10-14 | 2011-07-27 | 重庆理工大学 | Ultrasonic auxiliary vacuum electron beam welding method of aluminum and aluminum alloy |
| CN102133683A (en) * | 2011-01-28 | 2011-07-27 | 晋西工业集团有限责任公司 | Aluminium alloy vacuum welding forming method of rocket bomb stabilizing device |
| CN102229019A (en) * | 2011-04-28 | 2011-11-02 | 中国航空工业集团公司北京航空材料研究院 | Argon arc welding method suitable for TiAl-based alloy material and titanium alloy |
| CN102371430A (en) * | 2010-08-25 | 2012-03-14 | 北京有色金属研究总院 | Electron beam welding method suitable for injection-molded 7000-series aluminum alloy |
| CN102649192A (en) * | 2012-04-28 | 2012-08-29 | 西安航天动力机械厂 | Method of vacuum electron beam butt welding in condition of superstandard assembling clearance |
| CN103273205A (en) * | 2013-04-24 | 2013-09-04 | 哈尔滨工业大学 | Method for electron beam composite instant liquid phase diffusion bonding of GH4169 high-temperature alloy |
| CN104439676A (en) * | 2014-11-24 | 2015-03-25 | 中国核动力研究设计院 | CLF-1 thick steel plate electron beam welding process |
| CN104907657A (en) * | 2015-05-28 | 2015-09-16 | 航天材料及工艺研究所 | TiAl/TC4 electronic-beam melting-brazing method with addition of alloy middle layer |
| CN107552961A (en) * | 2017-10-19 | 2018-01-09 | 上海交通大学 | A kind of method of LASER BEAM WELDING TiAl alloy |
| CN108262579A (en) * | 2017-10-27 | 2018-07-10 | 南京理工大学 | The dissimilar material joining joint structure and preparation method of toughening transition |
| CN108406076A (en) * | 2018-01-14 | 2018-08-17 | 哈尔滨工业大学（威海） | A kind of high-density alloy electron beam welding packing material and method |
| CN109483037A (en) * | 2018-12-22 | 2019-03-19 | 山西汾西重工有限责任公司 | The one step welding method of aluminium alloy thick plate vacuum electron beam of gas hole defect can be overcome |
| CN109483146A (en) * | 2018-10-15 | 2019-03-19 | 中国航发北京航空材料研究院 | A method of repairing Intermatallic Ti-Al compound casting defect |
| CN110039169A (en) * | 2019-04-30 | 2019-07-23 | 中国船舶重工集团公司第七二五研究所 | A kind of titanium-aluminum dissimilar metal electro-beam welding method |
| CN110142495A (en) * | 2019-06-05 | 2019-08-20 | 哈尔滨工业大学 | A kind of titanium-aluminium alloy electro-beam welding method reducing base material dilution rate |
| CN110142496A (en) * | 2019-06-05 | 2019-08-20 | 哈尔滨工业大学 | A kind of TiAl/Ti adding Y shape middle layer3Al electron beam welding method for dissimilar materials |
| CN110653477A (en) * | 2019-09-29 | 2020-01-07 | 南京航空航天大学 | Electron beam welding process for improving aluminum-lithium alloy weld joint forming and improving joint quality |
| CN113020769A (en) * | 2021-02-05 | 2021-06-25 | 江苏京沂电器有限公司 | Electron beam welding method for producing manganin shunt |
| CN115609133A (en) * | 2022-11-17 | 2023-01-17 | 河北宇天材料科技有限公司 | Welding method for improving tensile strength of aluminum alloy weld joint |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0163018A3 (en) * | 1981-04-30 | 1988-02-10 | Nissan Motor Co., Ltd. | Method of welding titanium alloy parts with an insert member consisting essentially of 0 to 3% by weight of aluminium and the balance of titanium |
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- 2005-06-16 CN CNB2005100100886A patent/CN100358666C/en not_active Expired - Fee Related
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| CN100450694C (en) * | 2006-11-21 | 2009-01-14 | 宁波江丰电子材料有限公司 | A vacuum electron beam welding method |
| CN100462178C (en) * | 2007-06-18 | 2009-02-18 | 哈尔滨工业大学 | Compound control method for heat cycle of electron beam welding TiAl / TC4 heterogeneous materials |
| CN101690991B (en) * | 2009-10-14 | 2011-07-27 | 重庆理工大学 | Ultrasonic auxiliary vacuum electron beam welding method of aluminum and aluminum alloy |
| CN101811222A (en) * | 2010-05-20 | 2010-08-25 | 西安航天远征流体控制股份有限公司 | Method for welding titanium anode slot |
| CN101890570A (en) * | 2010-06-18 | 2010-11-24 | 哈尔滨工业大学 | Electron-beam welding method for aluminum alloy and steel based on intermediate layer isolation control |
| CN101890570B (en) * | 2010-06-18 | 2012-07-25 | 哈尔滨工业大学 | Electron-beam welding method for aluminum alloy and steel based on intermediate layer isolation control |
| CN102371430A (en) * | 2010-08-25 | 2012-03-14 | 北京有色金属研究总院 | Electron beam welding method suitable for injection-molded 7000-series aluminum alloy |
| CN102133683B (en) * | 2011-01-28 | 2013-04-24 | 晋西工业集团有限责任公司 | Aluminium alloy vacuum welding forming method of rocket bomb stabilizing device |
| CN102133683A (en) * | 2011-01-28 | 2011-07-27 | 晋西工业集团有限责任公司 | Aluminium alloy vacuum welding forming method of rocket bomb stabilizing device |
| CN102229019A (en) * | 2011-04-28 | 2011-11-02 | 中国航空工业集团公司北京航空材料研究院 | Argon arc welding method suitable for TiAl-based alloy material and titanium alloy |
| CN102229019B (en) * | 2011-04-28 | 2014-07-02 | 中国航空工业集团公司北京航空材料研究院 | Argon arc welding method suitable for TiAl-based alloy material and titanium alloy |
| CN102649192A (en) * | 2012-04-28 | 2012-08-29 | 西安航天动力机械厂 | Method of vacuum electron beam butt welding in condition of superstandard assembling clearance |
| CN102649192B (en) * | 2012-04-28 | 2014-07-09 | 西安航天动力机械厂 | Method of vacuum electron beam butt welding in condition of superstandard assembling clearance |
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| CN103273205B (en) * | 2013-04-24 | 2015-08-19 | 哈尔滨工业大学 | A kind of method of electron beam compound transient liquid phase bonding GH4169 high temperature alloy |
| CN104439676A (en) * | 2014-11-24 | 2015-03-25 | 中国核动力研究设计院 | CLF-1 thick steel plate electron beam welding process |
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| CN104907657A (en) * | 2015-05-28 | 2015-09-16 | 航天材料及工艺研究所 | TiAl/TC4 electronic-beam melting-brazing method with addition of alloy middle layer |
| CN107552961A (en) * | 2017-10-19 | 2018-01-09 | 上海交通大学 | A kind of method of LASER BEAM WELDING TiAl alloy |
| CN108262579A (en) * | 2017-10-27 | 2018-07-10 | 南京理工大学 | The dissimilar material joining joint structure and preparation method of toughening transition |
| CN108406076A (en) * | 2018-01-14 | 2018-08-17 | 哈尔滨工业大学（威海） | A kind of high-density alloy electron beam welding packing material and method |
| CN109483146A (en) * | 2018-10-15 | 2019-03-19 | 中国航发北京航空材料研究院 | A method of repairing Intermatallic Ti-Al compound casting defect |
| CN109483146B (en) * | 2018-10-15 | 2020-06-09 | 中国航发北京航空材料研究院 | Method for repairing defects of titanium-aluminum intermetallic compound casting |
| CN109483037A (en) * | 2018-12-22 | 2019-03-19 | 山西汾西重工有限责任公司 | The one step welding method of aluminium alloy thick plate vacuum electron beam of gas hole defect can be overcome |
| CN110039169A (en) * | 2019-04-30 | 2019-07-23 | 中国船舶重工集团公司第七二五研究所 | A kind of titanium-aluminum dissimilar metal electro-beam welding method |
| CN110039169B (en) * | 2019-04-30 | 2021-04-02 | 中国船舶重工集团公司第七二五研究所 | Electron beam welding method for titanium-aluminum dissimilar metal |
| CN110142495A (en) * | 2019-06-05 | 2019-08-20 | 哈尔滨工业大学 | A kind of titanium-aluminium alloy electro-beam welding method reducing base material dilution rate |
| CN110142496A (en) * | 2019-06-05 | 2019-08-20 | 哈尔滨工业大学 | A kind of TiAl/Ti adding Y shape middle layer3Al electron beam welding method for dissimilar materials |
| CN110653477A (en) * | 2019-09-29 | 2020-01-07 | 南京航空航天大学 | Electron beam welding process for improving aluminum-lithium alloy weld joint forming and improving joint quality |
| CN113020769A (en) * | 2021-02-05 | 2021-06-25 | 江苏京沂电器有限公司 | Electron beam welding method for producing manganin shunt |
| CN115609133A (en) * | 2022-11-17 | 2023-01-17 | 河北宇天材料科技有限公司 | Welding method for improving tensile strength of aluminum alloy weld joint |
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