CN1633856A - Preparation and uses of specific medicine for killing influenza virus and bacteria through crystal volatilization - Google Patents
Preparation and uses of specific medicine for killing influenza virus and bacteria through crystal volatilization Download PDFInfo
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- CN1633856A CN1633856A CN 200410100875 CN200410100875A CN1633856A CN 1633856 A CN1633856 A CN 1633856A CN 200410100875 CN200410100875 CN 200410100875 CN 200410100875 A CN200410100875 A CN 200410100875A CN 1633856 A CN1633856 A CN 1633856A
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Abstract
Disclosed is a virus-eradicating factor which is prepared through mixing, dissolving and crystallizing, the disclosed medicine produces no residue and can eradicate the influenza virus, epidemic encephalitis viruses, pneumonia viruses, SARS viruses, typhoid viruses, Staphylococcus aureus legionaires and more than thirty common fungus. The invention provides a volatilization crystal form air sterilization agent.
Description
Technical field:
The invention belongs to sterile products, relate in particular to a kind of preparation and application of crystal volatilization killing influenza virus bacterium specific drug of air killing influenza virus.
Technical background:
Domestic and international known sterilization product only has liquid-type, smoke-type, ozone-type, evaporation type, ultraviolet line style at present, these sterile products are contact bactericidal actions, can not be in the crowd is dense the air bacterium flu-prevention communicate illness of dynamically killing the virus continuously, the people must leave the scene during disinfection, there is not the delicate fragrance air to drive peculiar smell, also environment is caused secondary pollution, have the shortcomings such as excitant, corrosivity, use inconvenience.
Summary of the invention:
For overcome existing sterile products can not be in the crowd is dense continuously the air Active sterilization kill the virus flu-prevention communicate illness, excitant, corrosivity, contaminative, use inconvenience, do not have the delicate fragrance air to drive the shortcomings such as peculiar smell.
The objective of the invention is to develop, develop a kind of preparation and application of crystal volatilization killing influenza virus bacterium specific drug of the crystal-type high effect nontoxic that volatilizees, it is characterized in that, the sterilization of crystal shape, natural crystal with volatility kill the virus anti-influenza, do not stay residue, never go bad, do not stimulate, burn into does not drive peculiar smell, fresh air, environment is not caused secondary pollution. Be applied to various air-conditionings, automobile, electric fan, scent device, sterilizer, bacteria-suppressing device, freshener, anion oxygen bar, steam air heater, steamer, aircraft, train, wardrobe, clothes, handicraft, artificial flower, family, hospital, kindergarten, school, hotel, trick and can accomplish to kill continuously all infective virus and the fresh airs such as air epidemic encephalitis, influenza, Legionella, pneumonia, hepatitis in holding institute, office, public place etc. the crowd is dense.
The technical solution adopted for the present invention to solve the technical problems is:
Preparation and the application of crystal volatilization killing influenza virus bacterium specific drug of the present invention, it is characterized in that, plant isatis root, flea body, garlic, the Chinese bulbul, the capsule of weeping forsythia, Herba Andrographitis extract respectively the bacterial activity factor crystal composition that kills the virus, and prepare caryophyllus oil or (other sesame oil, essential oil), mould inhibitor, stabilizing agent, nano-silver powder or (other metal nano powder) mixed dissolution crystallisation by cooling again and become product.
1, plant isatis root, folium isatidis are extracted viricidal process for purification: isatis root, folium isatidis → pulverizing → boiling water boiling is carried the powdery calcium hydroxide of 3 times → extract → adding leaf weight 13%, stir evenly, leave standstill 50mih, filtration → filtered fluid is transferred pH5.5-6 with hydrochloric acid, adds leaf weight 1.5% active carbon, and 15mih is boiled in heating, filter, the istain of indigo glycosides amount 58% (53%-61%) is heated to and boils in the quite clean scavenging solution of purification → scavenging solution, adding, behind the logical dioxy carbon 6mim, drip 20% hydrochloric acid 140ml, continue heating, logical dioxy carbon 20mih, let cool, filter → precipitation → washing neutrality → drying → crystallization.
2, plant Herba Andrographitis extracts the process for purification of sterilization factors: Herba Andrographitis → pulverizing → ethanol cold soaking → alcohol leaching liquid → active carbon, reflux decolour, while hot suction filtration → filtrate recycling ethanol → slowly add water → crystallization → suction filtration → crystal.
3 plant garlics are extracted the process for purification of sterilization factors volatile oil: add thermal distillation in garlic → pulverizing → paraffin oil bath and extract the absolute ether extraction → ether solution of the turbid liquid in 5h → extract → standing separation → yellow oil → upper strata → adding 1/3 amount → recovery ether → merging → galic essential oil.
4, the plant capsule of weeping forsythia extracts the process for purification of crystal sterilization factors: a small amount of Paris white of capsule of weeping forsythia powder → mix, adding poach and carry 3 times, each 3 hours → filtration → filtrate → decompression distillation → medicinal extract → 5 times → extract → reduced pressure concentration of alcohol immersion → residue → be dissolved in is in the hot water → and magnesia mixes thoroughly → 2 times → concentrated placement → filtration → crystallization → drying → crystalline solid of solids → alcohol extract
5, the plant Chinese bulbul is extracted the process for purification of crystal sterilization factors: Chinese bulbul herb pulverizings → steam distillation → add sodium chloride is saturated to be concentrated → crystallization with chloroform jolting 8 times → chloroform solution → pressure reducing and steaming chloroform → residue → be dissolved in the ethanol that boils → filtration → ethanol
6, plant flea body extracts the process for purification of crystal sterilization factors: flea body powder 500g → 5 times → leachate → thin film evaporation of 95% alcohol immersion is to 200ml, decompression recycling ethanol, adding 2 times of amount 20% salt fully stirs, placement is spent the night, filtration → filtrate → sediment → 3 times → acid liquid → sodium carbonate of ether washing alkalizes to pH9～10, it is saturated to add sodium chloride, chloroform extraction is to inanimate object reaction → extract → anhydrous sodium sulfate drying, chloroform → brown paste → extracted by ether → precipitation → ether layer → acetone crystallization is reclaimed in decompression distillation.
4, mould inhibitor prepares the esterification synthetic method:
This reaction is to carry out in an esterifier of being furnished with rectifying column, in esterifier, add fumaric acid, methyl alcohol and catalyst by a certain percentage, startup heat riser and agitator rise to uniform temperature and carry out back flow reaction, and the water that produces and the methyl alcohol of effusion enter in the rectifying column that links to each other with reactor and separates. The methyl alcohol that is steamed by the rectifying column top is back in the reactor again, and the moisture that reaction generates is by the regularly discharging of rectifying column bottom. Reaction is poured reactant liquor in the flask that fills cold water into after finishing, and uses Na2CO
3Solution is neutralized to neutrality, more after filtration, washing, dry mould inhibitor.
5, produce the method for nano-silver powder:
Silver nitrate → obtain solution → activation → adding ammonia → adding hydrogen peroxide → reaction → precipitation → filtration → washing → 180 ℃ drying → nano-silver powder.
Preparation and the application of 6 crystal volatilization killing influenza virus bacterium specific drugs, the technological process of production:
Plant isatis root crystal, Herba Andrographitis crystal, Chinese bulbul crystal, flea body crystal, capsule of weeping forsythia crystal, galic essential oil, caryophyllus oil, mould inhibitor, stabilizing agent mix → decompression dissolving → crystallisation by cooling → Nano Silver → mix and blend dissolving inflow polypropylene plastic box (PP) or vinyon box crystallisation by cooling, crystal volatilization killing influenza virus bacterium specific drug. The box that the powder charge plastic casing adopts polypropylene plastics (PP) or other material to make, medicine box is not of uniform size, shape differs, the fragrance outlet hole shape differs, box can be made into circle, square, flat, semicircle etc. shape, and it is fragrant and without the odor type crystal that kills the virus that the sterilization crystallization crystal of various odor types is housed in the box. Crystal volatilization killing influenza virus bacterium specific drug when being used for the air-conditioning viricidal and antibacterial, being put into 10-5000 and is restrained a box to air-conditioning inlet and outlet place or overanxious net. When being used for the anti-flu of car room viricidal and antibacterial, put into 1000 gram 1 boxes or 9000 grams, 1 box to central air-conditioning inlet and outlet place, put into that 10-5000 restrains a box to the vehicle air conditioning outlet place or volatilize naturally in other seat. Put into 10-1000 and restrain a box for electric fan, scent device, sterilizer, bacteria-suppressing device, oxygen bar. Put into 5-100 for wardrobe, clothing kitchen, suitcase, bookcase etc. and restrain 1 box.
This product is through toxicology neasuring, and the small white mouse LD50 of passing through mouth is 6196.3 milligrams of kilograms, and the AMLS test belongs to positive, and the long term toxicity test proof does not have the phenomenons such as carcinogenic, teratogenesis, mutagenesis, so nontoxic to people and animals.
After the practicality of this product, through and the contrast of the chemical disinfections such as peroxide chlorine, chlorine dioxide, clorox, Peracetic acid, sodium dichloro cyanurate find its drug effect continuation, effect is stronger, without the burn into free from extraneous odour.
The beneficial effect of the invention:
Crystal volatilization killing influenza virus bacterium specific drug is characterized in that having brute force and kills influenza virus in the air, epidemic meningitis virus, pneumonia germ, SARS virus, typhoid fever germ, cholera bacteria, Escherichia coli, staphylococcus aureus, white and read the viruses such as coccus, Legionella. Can also kill the common moulds of kind more than 30 such as aspergillus flavus, aspergillus fumigatus, Penicillium citrinum significant killing action is arranged. Compare with existing disinfectant products technology: 1, overcome the disinfection technologies such as domestic and international known sterile products liquid-type, smoke-type, ozone-type, ultraviolet line style can not be in the crowd is dense the air infection prevention disease of dynamically killing the virus continuously, the people must leave the scene during disinfection. 2, broken through the public place the crowd is dense in continuously the dynamic kill virus of air, drive peculiar smell, strongly kill the infection, breeding, propagation of the various pathogenic bacteria in the room air, popular key technology. 3, solved a difficult problem that does not have over the past thousands of years crystal-type air sterillization sterilization. Realized not being subjected to the seasonal effect viricidal and antibacterial, 19 restrain the sterilization 3 years of naturally volatilizing, and do not stay residue. Can fully reconcile body immunity, tranquilization and refreshment, easypro through sensible, influenza, flu, the various rhinitis that can effectively prevent the infection of the upper respiratory tract to cause, multiple transmissible disease in migraine and general headache and the air.
Implementation:
Embodiment 1:
Isatis root crystal 15 grams, flea body crystal 13 grams, garlic oil 50ml, Chinese bulbul crystal 11 grams, capsule of weeping forsythia crystal 13 grams, Herba Andrographitis crystal 11 grams. Caryophyllus oil 73 grams (or Chinese mugwort oil), mould inhibitor (anticorrisive agent) 353 grams, stabilizing agent 183 grams, nano-silver powder 1 gram mix and blend dissolving flows into polypropylene plastics (PP) or vinyon box crystallisation by cooling, obtained 500 gram crystal volatilization killing influenza virus bacterium specific drugs.
Embodiment 2:
Get embodiment 1 prepared crystal volatilization killing influenza virus bacterium specific drug 500 gram 1 boxes or 9000 grams, 1 box and put into central air-conditioning air outlet, air inlet, restrain 1 box with 15-1000, put into air-conditioner air outlet or air inlet at 10 squares of indoor 30 minutes sterilizing rate 81-99%. Germ rate 99.9% was killed in the contact sterilization in 1-15 minute
Embodiment 3:
When getting the prepared crystal volatilization killing influenza virus bacterium specific drug of embodiment 1 and being used for the car room viricidal and antibacterial, put into that 10-1000 restrains a box to the vehicle air conditioning outlet place or volatilize naturally in other seat.
Embodiment 4:
Get embodiment 1 made crystal volatilization killing influenza virus bacterium specific drug 500 and restrain, dilute 300 times, carry out dipping for 53 sheep, without any reaction, and the hair color light is pure white, disturbs without mosquitos and flies with rear sheep, tracing observation shows after the dipping, and sheep occurs without vermin after bathing.
Embodiment 5:
Get embodiment 1 made crystal volatilization killing influenza virus bacterium specific drug 100-1000 and restrain a box, put into special bus air-conditioner air outlet result of the test, air disinfection rate (30-60 minute) is respectively 87%-99%
Embodiment 6:
Get embodiment 1 prepared crystal volatilization killing influenza virus bacterium specific drug 5 gram/boxes and put into respectively wardrobe, clothing kitchen, suitcase, bookcase cockroach, Pest killing rate 100% after 3 days, clothes delicate fragrance is pleasant.
Embodiment 7:
Getting embodiment 1 prepared crystal volatilization killing influenza virus bacterium specific drug puts into 10-1000 and restrains a box for electric fan, scent device, sterilizer, bacteria-suppressing device, freshener, anion oxygen bar.
Crystal volatilization killing influenza virus bacterium specific drug and other disinfectants (or sterilization method) compare:
| Trade name | Contact sterilization power | Air continues sterilizing power | Security, environment, peculiar smell | Corrosivity | Excitant |
| Crystal volatilization killing influenza virus bacterium specific drug | Extremely strong | Nature volatilization power is extremely strong, and residue is not stayed in the sterilization of air dynamic continuance | The pure and fresh fragrance of nontoxic, indoor environment, invigorating, security, environment | Nothing | Nothing |
| Chlorine dioxide | By force | Without continuing sterilizing power | Form the carcinogenic substances such as chloroform, produce secondary pollution, chlorine smell | By force | By force |
| Chlorine | By force | Without continuing sterilizing power | Form the carcinogenic substances such as chloroform, produce secondary pollution, chlorine smell | By force | Extremely strong |
| Clorox | Generally | Without continuing sterilizing power | Form the carcinogenic substances such as chloroform, produce secondary pollution, stink | By force | By force |
| Peracetic acid | By force | Without continuing sterilizing power | Safety, secondary pollution | Extremely strong | By force |
| Aldehyde disinfectant (glutaraldehyde class) | Stronger | Without continuing sterilizing power | May produce the Skin Cell pathology, must under unmanned condition, sterilize, produce the secondary pollution environment, | A little less than | By force |
| Sodium dichloro cyanurate | By force | Without continuing sterilizing power | Form the carcinogenic substances such as chloroform, produce secondary pollution, stink | By force | By force |
| Sym-closene | By force | Without continuing sterilizing power | Form the carcinogenic substances such as chloroform, produce secondary pollution, stink | By force | By force |
| Ozone | By force | Can not continuation | Environmental friendliness may produce the Skin Cell pathology, must sterilize stink under unmanned condition | A little less than | Stronger |
| Disinfection by ultraviolet light | Stronger | Can not continuation | Must under unmanned condition, sterilize. | Nothing | Nothing |
Claims (10)
1, preparation and the application of crystal volatilization killing influenza virus bacterium specific drug, it is characterized in that, isatis root crystal, flea body crystal, garlic oil, Chinese bulbul crystal, capsule of weeping forsythia crystal, Chinese mugwort oil or caryophyllus oil 12-25%, mould inhibitor (anticorrisive agent) 21-71%, stabilizing agent accounts for 13-35%, nano-silver powder 1-2%.
2, preparation and the application of crystal volatilization killing influenza virus bacterium specific drug according to claim 1 is characterized in that, mould inhibitor (anticorrisive agent) 21-71%, and stabilizing agent accounts for 13-25%.
3, preparation and the application of crystal volatilization killing influenza virus bacterium specific drug according to claim 1 is characterized in that the nanometer that the metal materials such as zinc, titanium, silver are made.
4, preparation and the application of crystal volatilization killing influenza virus bacterium specific drug according to claim 1, it is characterized in that, the crystallization crystal shape of the various odor types that the sesame oil such as cloves, sweet osmanthus, rose, jasmine or essential oil are mixed with is fragrant, the color of crystal shape differs, odor type differs, and weight differs.
5, preparation and the application of crystal volatilization killing influenza virus bacterium specific drug according to claim 1, it is characterized in that, the box that the powder charge plastic casing adopts polypropylene plastics (PP) or other material to make, medicine box is not of uniform size, shape differs, the fragrance outlet hole shape differs, and the crystal pomander can be made into circle, square, flat, semicircle etc. shape, be equipped with in the box various odor types kill the anti-flu of germ crystallization crystal fragrant and without odor type kill the virus, anti-influenza crystal.
6, preparation and the application of crystal volatilization killing influenza virus bacterium specific drug according to claim 1, it is characterized in that, 5 gram 1 boxes or 1000 grams, 1 box are put into respectively killing pathogenic bacteria, cockroach, the insects such as wardrobe, clothing kitchen, suitcase, bookcase, make clothes leave delicate fragrance.
7, preparation and the application of crystal volatilization killing influenza virus bacterium specific drug according to claim 1, it is characterized in that, when air-conditioning uses, 100 gram 1 boxes or 9000 grams, 1 box are put into the central air-conditioning inlet and outlet, 10 gram 1 boxes or 1000 grams, 1 box are put into air-conditioner air outlet or other seat use such as air inlet, overanxious net.
8, preparation and the application of crystal volatilization killing influenza virus bacterium specific drug according to claim 1, it is characterized in that, when automobile uses, 10 gram 1 boxes or 5000 grams, 1 box are put into vehicle air conditioning outlet or air inlet, or put into other seat sterilization fresh air that naturally volatilizees.
9, preparation and the application of crystal volatilization killing influenza virus bacterium specific drug according to claim 1, it is characterized in that: 10 grams-1000 grams, one box is fitted in anti-influenza such as the bacterium of killing the virus in sterilizer, bacteria-suppressing device, freshener, anion oxygen bar, electric fan, the scent device etc., anti-flu, delicate fragrance air.
10, preparation and the application of crystal volatilization killing influenza virus bacterium specific drug according to claim 1, it is characterized in that, be applied to various air-conditionings, automobile, electric fan, sterilizer, bacteria-suppressing device, scent device, anion oxygen bar, steam air heater, steamer, aircraft, train, wardrobe, clothes, handicraft, artificial flower, family, hospital, kindergarten, school, hotel, trick and kill continuously infective virus sterilization and the delicate fragrance air such as epidemic encephalitis in the air, influenza, Legionella, pneumonia in holding institute, office, public place etc. the crowd is dense.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410100875 CN1633856A (en) | 2004-12-11 | 2004-12-11 | Preparation and uses of specific medicine for killing influenza virus and bacteria through crystal volatilization |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410100875 CN1633856A (en) | 2004-12-11 | 2004-12-11 | Preparation and uses of specific medicine for killing influenza virus and bacteria through crystal volatilization |
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| CN1633856A true CN1633856A (en) | 2005-07-06 |
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| CN 200410100875 Pending CN1633856A (en) | 2004-12-11 | 2004-12-11 | Preparation and uses of specific medicine for killing influenza virus and bacteria through crystal volatilization |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103039541A (en) * | 2012-12-28 | 2013-04-17 | 湖南奥能驰远节能科技有限公司 | Environmental-friendly automobile air conditioner and interior environment purification agent and preparation method thereof |
| CN104026150A (en) * | 2014-05-30 | 2014-09-10 | 湖南省轻工投资有限公司 | Composite liquid for preventing and killing avian influenza viruses and preparation method and application thereof |
| CN108094424A (en) * | 2017-12-30 | 2018-06-01 | 赣州市特可环保技术有限公司 | Kill the fumigation plant nanometer fat preparation method and application of air fungus infection virus |
-
2004
- 2004-12-11 CN CN 200410100875 patent/CN1633856A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103039541A (en) * | 2012-12-28 | 2013-04-17 | 湖南奥能驰远节能科技有限公司 | Environmental-friendly automobile air conditioner and interior environment purification agent and preparation method thereof |
| CN103039541B (en) * | 2012-12-28 | 2015-07-08 | 湖南奥能驰远节能科技有限公司 | Environmental-friendly automobile air conditioner and interior environment purification agent and preparation method thereof |
| CN104026150A (en) * | 2014-05-30 | 2014-09-10 | 湖南省轻工投资有限公司 | Composite liquid for preventing and killing avian influenza viruses and preparation method and application thereof |
| CN104026150B (en) * | 2014-05-30 | 2015-04-15 | 湖南省轻工投资有限公司 | Composite liquid for preventing and killing avian influenza viruses and preparation method and application thereof |
| CN108094424A (en) * | 2017-12-30 | 2018-06-01 | 赣州市特可环保技术有限公司 | Kill the fumigation plant nanometer fat preparation method and application of air fungus infection virus |
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