CN1685839A - Preparation of volatile crystalline virus bacteria formaldehyde controller and application method - Google Patents
Preparation of volatile crystalline virus bacteria formaldehyde controller and application method Download PDFInfo
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- CN1685839A CN1685839A CN 200510065418 CN200510065418A CN1685839A CN 1685839 A CN1685839 A CN 1685839A CN 200510065418 CN200510065418 CN 200510065418 CN 200510065418 A CN200510065418 A CN 200510065418A CN 1685839 A CN1685839 A CN 1685839A
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Abstract
A volatile air disinfecting-detoxicating agent in the form of crystal for killing virus and bacteria, decomposing formaldehyde, benzene and CO2, and refreshing air is prepared from 3 Chinese-medicinal materials including rhubarb.
Description
Technical field:
The invention belongs to the preparation of disinfectant products, relate in particular to the preparation and the application method of the volatile crystalline virus bacteria formaldehyde controller that a plant material makes
Technical background:
Domestic and international known sterilization product has only liquid-type at present, smoke-type, the ozone type, evaporation type, the ultraviolet line style, the photocatalyst type, the formaldehyde aerosol type, the benzene aerosol type, formaldehyde benzene solid type, these products are contact effects, can not be in the crowd is dense continuously air dynamically kill the virus, remove formaldehyde, remove benzene, the infection prevention disease, the people must leave the scene during disinfection, there is not fresh air to drive the peculiar smell effect, also environment is caused secondary pollution, there is excitant, corrosivity, formaldehyde in addition, the benzene solid type also leaves residue, remove formaldehyde, remove benzene, kill the virus, bacterium is not obvious, practicality is not strong, during use to shortcomings such as the user make troubles.
Summary of the invention:
In order to overcome above existing thimerosal, remove formaldehyde, to remove benzaldehyde product.Can not in the crowd is dense, the dynamic sterilization of air continuously kill the virus, remove formaldehyde, remove benzene, excitant, corrosivity, contaminative, use inconvenience, not have fresh air to drive shortcomings such as peculiar smell.
The objective of the invention is to develop, develop a kind of preparation and application method of volatile crystalline virus bacteria formaldehyde controller of crystallization crystal volatilization type high effect nontoxic, it is characterized in that, the crystallization crystal shape, can volatilize naturally kill the virus, sterilize, remove formaldehyde, remove benzene, service time is long, do not stay residue, never go bad, do not stimulate, burn into does not drive peculiar smell, fresh air, environment is not caused secondary pollution.Virus bacteria formaldehyde controller is applied to various air-conditionings, automobile, electric fan, the drifting fragrance device, sterilization machine, antibacterial device, negative from the oxygen bar, steam air heater, steamer, aircraft, train, wardrobe, clothes, handicraft, artificial flower, family, hospital, school, the hotel, trick is held institute, office, public place etc., volatile crystalline virus bacteria formaldehyde controller is fitted in various electrical equipment, in the automobile, can accomplish in the crowd is dense that air is dynamically killed epidemic encephalitis continuously, influenza, pneumonia, all infective virus such as hepatitis reach and remove formaldehyde, remove benzene, purify air.
The technical solution adopted for the present invention to solve the technical problems is:
The preparation of volatile crystalline virus bacteria formaldehyde controller of the present invention and application method, it is characterized in that, form by long celestial grass, rheum officinale, the extract of smelling grass, folium isatidis several plant, extract is with long celestial grass, rheum officinale, smells the powder of grass, folium isatidis pulverizing, extract through soaking with alcohol respectively, filter, concentrate, form, be equipped with again in the extract caryophyllus oil (or sweet osmanthus, rose or the like sesame oil and essential oil), mould inhibitor (preservative), stabilizing agent, nano-silver powder (or other Nano metal powder) fully stirring and dissolving be mixed and made into the virus and bacteria jinx.The weight ratio of active ingredient is long celestial grass, rheum officinale, smells grass, folium isatidis=3: 1: 2.1: 1, and caryophyllus oil 10-20%, mould inhibitor 31-73%, stabilizer comprises 13-35%, nano metal titanium valve 0.2-3%, it is 18 hours that extract soaks extraction time.Add adjuvant and mix stirring and dissolving inflow polypropylene plastics (PP) or vinyon box crystallisation by cooling.The box that polypropylene plastic box (PP) or other material are made, the volatile crystalline virus bacteria formaldehyde controller box is not of uniform size, shape differs, the ventilation hole shape differs, box can be made into circle, square, flat, semicircle or the like shape, be equipped with in the box various odor types sterilization, remove formaldehyde, to remove the crystallization crystal of benzene fragrant and tasteless type kills the virus, sterilization, remove formaldehyde, remove the crystal of benzene.Volatile crystalline virus bacteria formaldehyde controller is applied to various air-conditioning viricidal and antibacterials and removes formaldehyde, when removing benzene, puts into 15-10000 and restrain a box to air-conditioning inlet and outlet place or overanxious net or plug-in card, two-sided gluing.Wire hook hangs the central air-conditioning inlet and outlet, be used for the indoor viricidal and antibacterial of automobile remove formaldehyde, when removing benzene, put into 10-10000 restrain a box to air conditioning for automobiles air outlet place or medium other seat of overanxious net volatilize naturally.Be used for electric fan, drifting fragrance device, sterilization machine, antibacterial device, oxygen bar, viricidal and antibacterial removes formaldehyde, when removing benzene, puts into 10-10000 and restrain a box.Put into 10-600 when being used for wardrobe, clothing kitchen, suitcase, bookcase viricidal and antibacterial and restrain 1 box except that formaldehyde, except that benzene.
Volatile crystalline virus bacteria formaldehyde controller is through toxicology neasuring, and small white mouse per os LD50 is 2396 milligrams of kilograms, and the AMLS test belongs to positive, and the long term toxicity test proof does not have phenomenons such as carcinogenic, teratogenesis, mutagenesis, so nontoxic to people and animals.
After volatile crystalline virus bacteria formaldehyde controller is used, through, no burn into free from extraneous odour better, fragrance, air viricidal and antibacterial rate 96% with long-acting fruits of chemical disinfection contrast its drug effect of discovery such as peroxide chlorine, chlorine dioxide, clorox, Peracetic acid, sodium dichloro cyanurates.Contact viricidal and antibacterial rate 100%.
After volatile crystalline virus bacteria formaldehyde controller is used, water-soluble active methylenes compound through disclosing with Chinese patent publication number 1032047, sulfanilic acid and the mould mixing formula of urea that publication number 1104657 discloses, the tea powder that publication number 1298911 discloses, the hydrazide kind compound that publication number 1404891 discloses, triethanolamine and Sodium Metabisulfite mixing formula that publication number 1413750 discloses, the Tea Polyphenols that publication number 1425725 discloses, the natural canella extract that publication number 1431258 discloses, and the urea and the ammonium chloride mixing formula of U.S. Patent number 5108621 disclosures, the poly imonium that the patent No. 5317071 discloses, urea and cyclodextrin that the patent No. 60012741 discloses, urea that the patent No. 6043405 discloses and polyethylene imonium prescription, modified zeolite that Application No. 20010012820 discloses or molecular sieve or the like solution or powder-type formaldehyde are eliminated product, with formaldehyde catching agent, remover, scavenger etc., the product that remover and formaldehyde reaction form may be poisonous, absorption, decomposing formaldehyde, the benzene weak effect, also leave residue, easily cause secondary pollution, and may cause damage handling article such as furniture surface.Contrast finds that its drug effect reaches 1-2, no residue, no burn into free from extraneous odour, fragrance, photocatalysis is arranged, remove formaldehyde rate 97%, removes benzene rate 99%.
The beneficial effect of the invention:
The preparation of volatile crystalline virus bacteria formaldehyde controller and using method are nontoxic, efficient, long-acting by various tests, wide spectrum, stifling kill the virus, bacterium, remove formaldehyde, remove characteristics such as benzene, no pesticide resistance.Virus bacteria formaldehyde controller can be killed viruses such as coronavirus in the air, the white Salmonella of Cray, staphylococcus aureus, Legionella, pneumobacillus, epidemic meningitis virus, SARS virus, typhoid fever virus, cholera virus, influenza virus, Escherichia coli, Candida albicans.Can also the special efficacy decomposing formaldehyde, benzene, nitrogen oxide, sulphur dioxide, carbonic acid gas.Can kill the common moulds of kind more than 30 such as aspergillus flavus, aspergillus fumigatus, Penicillium citrinum again significant killing action is arranged.
Volatile crystalline virus bacteria formaldehyde controller and existing disinfectant, remove the formaldehyde technology and compare: 1, overcome domestic and international known sterile products liquid-type, smoke-type, ozone type, ultraviolet line style, photocatalyst type, disinfection technologies such as formaldehyde aerosol type can not be in the crowd is dense continuously air dynamically kill the virus, remove formaldehyde, infection prevention disease, the people must leave the scene during disinfection.2, broken through the public place the crowd is dense in continuously the dynamic kill virus of air, remove formaldehyde, remove benzene and remove, purify air and drive peculiar smell, kill the infection, breeding, propagation of the various pathogenic bacteria in the room air, popular key technology strongly.3, solved a difficult problem that does not have crystal with volatility type air sterillization sterilization over the past thousands of years, removes formaldehyde, removes benzene, purifies air.4, realized not being subjected to that seasonal effect is killed the virus, sterilization, removed formaldehyde, remove benzene, purify air.5, broken through 35 gram crystal can volatilize naturally sterilization, remove formaldehyde, remove benzene, practical 1-2, and do not stay the new invention of the fresh air of residue, have vast market prospect.
Preparation technology's flow process:
1, mould inhibitor preparation: get maleic anhydride and methyl alcohol in 93: 29 ratio (weight ratio) the input retort, keep stirring with 45 rev/mins, esterification is carried out with methyl alcohol in maleic anhydride dissolving back, when temperature rises to 950 ℃, with cooling water retort is cooled off, keeping reaction temperature between 30-750 ℃, 3 hours, be cooled to room temperature, obtain the maleic acid methyl esters.To react the gained monomethyl maleate and place reaction pot, and add ethyl acetate, the ratio of monomethyl maleate and ethyl acetate is 1: 3, add again maleic acid methyl esters weight 1%, concentrated hydrochloric acid, keep 50 rev/mins of stirrings, finish after 6 hours.Use water quench in the isomate process, the isomerization reaction temperature is controlled at about 510 ℃.The mould inhibitor major part is separated out with precipitation form, by centrifugation (3000 rev/mins), gets mould inhibitor in centrifugal 7 minutes, uses water quench in the isomate process, and the isomerization reaction temperature is controlled at about 500 ℃.Wherein contain ethyl acetate approximately, place 45 ℃ of left and right sides baking ovens, vacuum drying gets mould inhibitor after 1 hour, add mould inhibitor, ethanol again, and Ma Xiancao oil 0.6-1.3% keeps 30 rev/mins of stirrings, and cold filtration is finished after about 35-56 ℃ 3 hours.Place 25-30 ℃ of left and right sides baking oven, vacuum drying gets mould inhibitor
2, long celestial grass, rheum officinale, smell grass, folium isatidis (screening, flushing) → 2, pulverize → 3, soak extract 16 hours → 4 distillations 1-3 hour → 5, filtrations → filtrate concentrated → 6, add people's auxiliary material caryophyllus oil or (essential oil), mould inhibitor, stabilizing agent, the nano metal titanium fully mixes and has dissolved inflow polypropylene plastics or vinyon box → 7 crystallisation by cooling → 8 volatile crystalline virus bacteria formaldehyde controllers.
The various plant monomer liquid of technological process mix to concentrate by 6 and prepare
Embodiment 1:
Long celestial grass 300 grams
Rheum officinale 100 grams
Smell grass 310 grams
Folium isatidis 100 grams
Caryophyllus oil 65 grams (or other sesame oil and essential oil), mould inhibitor (preservative) 351 grams, stabilizing agent 113 grams, nano metal titanium 3 grams are made 500 gram volatile crystalline virus bacteria formaldehyde controllers by aforementioned technology.
Embodiment 2:
Get the prepared volatile crystalline virus bacteria formaldehyde controller of embodiment 1 500 gram 1 boxes or 10000 grams, 1 box with wire hook, hasp, plug-in card, two-sided gluing central air-conditioning air outlet, air inlet.Restrain 1 box with 15-10000, wire hook, hasp, plug-in card, two-sided gluing air-conditioner air outlet or air inlet place are at 10 squares of indoor 30 minutes sterilizing rates 99%.Killed germ rate 99.9%, drive cockroach 100% in contact sterilization 1-15 minute.
Embodiment 3
Get embodiment 1 prepared volatile crystalline virus bacteria formaldehyde controller and be used for the indoor viricidal and antibacterial of automobile, remove formaldehyde, when removing benzene, put into 10-1000 restrain a box to air conditioning for automobiles air outlet place or other seat volatilize naturally.Viricidal and antibacterial rate 96%, remove formaldehyde rate 97%, remove benzene rate 99%.
Embodiment 4:
Get embodiment 1 made volatile crystalline virus bacteria formaldehyde controller 500 and restrain, dilute 300 times, give 53 and exempt to carry out dipping, do not have any reaction with the back sheep, and the hair color light is pure white, no mosquitos and flies disturbs, tracing observation shows after the dipping, exempts from not have vermin after the bath and takes place.
Embodiment 5:
Get embodiment 1 made volatile crystalline virus bacteria formaldehyde controller 100-1000 and restrain a box, put into special bus air-conditioner air outlet test, viricidal and antibacterial rate 96%, remove formaldehyde rate 97%, remove benzene rate 99%.
Embodiment 6:
Get embodiment 1 prepared volatile crystalline virus bacteria formaldehyde controller 5 gram/boxes and put into wardrobe, clothing kitchen, suitcase, bookcase cockroach, insect killing rate 100% after 3 days respectively, remove formaldehyde rate 97%, remove benzene rate 99%.Viricidal and antibacterial rate 99.9%, clothes delicate fragrance is pleasant.
Embodiment 7:
Getting embodiment 1 prepared volatile crystalline virus bacteria formaldehyde controller allocates electric fan, drifting fragrance device, sterilization machine, antibacterial device, oxygen bar into and puts into 10-5000 and restrain a box.Air viricidal and antibacterial rate 96%, remove formaldehyde rate 97%, remove benzene rate 99%, drive cockroach 100%.
Claims (10)
1, the preparation of volatile crystalline virus bacteria formaldehyde controller and application method is characterized in that, grow celestial grass, rheum officinale, smell grass, folium isatidis, caryophyllus oil 12-25%, mould inhibitor (preservative) 31-73%, stabilizer comprises 13-35%, nanometer titanium 0.2-3%.
2, the preparation of volatile crystalline virus bacteria formaldehyde controller according to claim 1 and application method is characterized in that, mould inhibitor (preservative) 31-73%, stabilizer comprises 13-25%.
3, the preparation of volatile crystalline virus bacteria formaldehyde controller according to claim 1 and application method is characterized in that, the nanometer that metal materials such as titanium are made.
4, the preparation of volatile crystalline virus bacteria formaldehyde controller according to claim 1 and application method, it is characterized in that, the crystallization crystal shape of the various odor types that sesame oil such as cloves, sweet osmanthus, rose, jasmine or essential oil are mixed with, the color of crystal shape differs, odor type differs, and weight differs.
5, the preparation of volatile crystalline virus bacteria formaldehyde controller according to claim 1 and application method, it is characterized in that, the box that the dress crystal holder adopts polypropylene plastics (PP) or other material to make, box is not of uniform size, shape differs, the ventilation hole shape differs, and crystal holder can be made into circle, square, flat, semicircle or the like shape, viricidal and antibacterial is housed, removes formaldehyde, removes the fragrant and tasteless crystal of crystallization crystal of benzene.
6, the preparation of volatile crystalline virus bacteria formaldehyde controller according to claim 1 and application method, it is characterized in that, 5 gram 1 boxes or 1000 grams, 1 box are put into killing pathogenic bacteria, cockroach, insects such as wardrobe, clothing kitchen, suitcase, bookcase respectively, make clothes leave delicate fragrance.
7, the preparation of volatile crystalline virus bacteria formaldehyde controller according to claim 1 and application method is characterized in that, when air-conditioning uses, with 100 gram 1 boxes or 10000 grams, 1 box, put into the central air-conditioning inlet and outlet with the wire hook.With 10 gram 1 boxes or 10000 grams, 1 box, stick into air-conditioner air outlet or other seat use such as air inlet, overanxious net with plug-in card, double faced adhesive tape.At 10 squares of indoor 30 minutes sterilizing rates 99%.Killed germ rate 99.9%, drive cockroach 100% in contact sterilization 1-15 minute.
8, the preparation of volatile crystalline virus bacteria formaldehyde controller according to claim 1 and application method, it is characterized in that, be used for the indoor viricidal and antibacterial of automobile, remove formaldehyde, when removing benzene, put into 10-10000 and restrain a box, plug-in card to air conditioning for automobiles air outlet place or put into other seat and volatilize naturally.Viricidal and antibacterial rate 96%, remove formaldehyde rate 97%, remove benzene rate 99%.
9, the preparation of volatile crystalline virus bacteria formaldehyde controller according to claim 1 and application method, it is characterized in that, 10 grams-10000 grams, one box is fitted in sterilizer, antibacterial machine, delicate fragrance device, anion oxygen bar, electric fan, the drifting fragrance device etc., viricidal and antibacterial 96%, removes formaldehyde 97%, remove benzene 99%, drive cockroach 100%.
10, the preparation of volatile crystalline virus bacteria formaldehyde controller according to claim 1 and application method, it is characterized in that, be applied to various air-conditionings, automobile, electric fan, sterilization machine, antibacterial device, the drifting fragrance device, the anion oxygen bar, steam air heater, steamer, aircraft, train, wardrobe, clothes, handicraft, artificial flower, family, hospital, the kindergarten, school, the hotel, trick is held institute, office, epidemic encephalitis in the air is killed during the crowd is dense continuously in public places etc., influenza, Legionella, the sterilization of infective virus such as pneumonia, remove formaldehyde, remove benzene, drive cockroach and delicate fragrance air.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200510065418 CN1685839A (en) | 2005-04-01 | 2005-04-01 | Preparation of volatile crystalline virus bacteria formaldehyde controller and application method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN 200510065418 CN1685839A (en) | 2005-04-01 | 2005-04-01 | Preparation of volatile crystalline virus bacteria formaldehyde controller and application method |
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| CN1685839A true CN1685839A (en) | 2005-10-26 |
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| CN 200510065418 Pending CN1685839A (en) | 2005-04-01 | 2005-04-01 | Preparation of volatile crystalline virus bacteria formaldehyde controller and application method |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106190590A (en) * | 2016-09-19 | 2016-12-07 | 重庆工商大学 | A kind of plant essential oil formaldehyde remover and application thereof |
| CN109769868A (en) * | 2019-03-19 | 2019-05-21 | 上海延龙环保科技有限公司 | A kind of high efficiency air sterilizing plant society material and preparation method thereof |
| CN111632334A (en) * | 2020-06-17 | 2020-09-08 | 成都市图腾环保科技有限公司 | Disinfectant, and preparation method and application thereof |
-
2005
- 2005-04-01 CN CN 200510065418 patent/CN1685839A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106190590A (en) * | 2016-09-19 | 2016-12-07 | 重庆工商大学 | A kind of plant essential oil formaldehyde remover and application thereof |
| CN109769868A (en) * | 2019-03-19 | 2019-05-21 | 上海延龙环保科技有限公司 | A kind of high efficiency air sterilizing plant society material and preparation method thereof |
| CN111632334A (en) * | 2020-06-17 | 2020-09-08 | 成都市图腾环保科技有限公司 | Disinfectant, and preparation method and application thereof |
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