CN1626062A - 丝皂条及其制备方法 - Google Patents
丝皂条及其制备方法 Download PDFInfo
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- CN1626062A CN1626062A CNA2004100479934A CN200410047993A CN1626062A CN 1626062 A CN1626062 A CN 1626062A CN A2004100479934 A CNA2004100479934 A CN A2004100479934A CN 200410047993 A CN200410047993 A CN 200410047993A CN 1626062 A CN1626062 A CN 1626062A
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- sericin
- skin
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- 239000000344 soap Substances 0.000 title claims abstract description 16
- 238000000034 method Methods 0.000 title claims description 10
- 238000004519 manufacturing process Methods 0.000 title 1
- 108010013296 Sericins Proteins 0.000 claims abstract description 10
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 17
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 15
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 12
- 239000000835 fiber Substances 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 241000255791 Bombyx Species 0.000 claims description 4
- 239000010775 animal oil Substances 0.000 claims description 3
- 238000011084 recovery Methods 0.000 claims 1
- 238000010257 thawing Methods 0.000 claims 1
- 230000007794 irritation Effects 0.000 abstract 1
- 239000002075 main ingredient Substances 0.000 abstract 1
- 239000000843 powder Substances 0.000 description 10
- 238000004140 cleaning Methods 0.000 description 5
- 235000011187 glycerol Nutrition 0.000 description 5
- 239000000047 product Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- 101100117236 Drosophila melanogaster speck gene Proteins 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 108010022355 Fibroins Proteins 0.000 description 2
- 235000001014 amino acid Nutrition 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- 238000012925 biological evaluation Methods 0.000 description 2
- 239000002537 cosmetic Substances 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 230000036556 skin irritation Effects 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000255789 Bombyx mori Species 0.000 description 1
- 206010048768 Dermatosis Diseases 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 208000003351 Melanosis Diseases 0.000 description 1
- 241000283973 Oryctolagus cuniculus Species 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 230000001154 acute effect Effects 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007799 dermal corrosion Effects 0.000 description 1
- 235000015872 dietary supplement Nutrition 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- -1 hydrogen sodium oxide Chemical class 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 239000010773 plant oil Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 208000017520 skin disease Diseases 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 231100000022 skin irritation / corrosion Toxicity 0.000 description 1
- 229910001948 sodium oxide Inorganic materials 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/044—Hydroxides or bases
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07K—PEPTIDES
- C07K14/00—Peptides having more than 20 amino acids; Gastrins; Somatostatins; Melanotropins; Derivatives thereof
- C07K14/435—Peptides having more than 20 amino acids; Gastrins; Somatostatins; Melanotropins; Derivatives thereof from animals; from humans
- C07K14/43504—Peptides having more than 20 amino acids; Gastrins; Somatostatins; Melanotropins; Derivatives thereof from animals; from humans from invertebrates
- C07K14/43563—Peptides having more than 20 amino acids; Gastrins; Somatostatins; Melanotropins; Derivatives thereof from animals; from humans from invertebrates from insects
- C07K14/43586—Peptides having more than 20 amino acids; Gastrins; Somatostatins; Melanotropins; Derivatives thereof from animals; from humans from invertebrates from insects from silkworms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/14—Shaping
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/384—Animal products
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- Zoology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Insects & Arthropods (AREA)
- Tropical Medicine & Parasitology (AREA)
- Toxicology (AREA)
- Gastroenterology & Hepatology (AREA)
- Biochemistry (AREA)
- Biophysics (AREA)
- Genetics & Genomics (AREA)
- Medicinal Chemistry (AREA)
- Molecular Biology (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Inorganic Chemistry (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
- Detergent Compositions (AREA)
- Peptides Or Proteins (AREA)
Abstract
本发明公开了一种以来自泰国丝的丝胶蛋白为主要成分的皮肤清洁用品，该丝胶蛋白与皂质中的各种成分相混合，所述皮肤清洁用品包括甘油皂和硬皂。本发明的产品使用安全，有助于滋养皮肤，使皮肤光滑柔软。本产品无刺激性，因此不同性别和年龄的人均可使用。
Description
技术领域
本发明涉及一种以丝蛋白为主要成分的皮肤清洁用品。
背景技术
丝粉是由丝纤维和蚕茧成分制成的。日本于1987年首次制出了可食用的野生丝粉，并随后于1989年将它开发用于化妆品。1997年，泰国Sisaket省的农业部桑树研究中心率先对丝粉进行了研究。由来自NangNoi Sisaket 1号品种蚕的丝纤维制得了这种不溶性丝粉。根据这项研究，已经发现丝粉含有16-18种氨基酸。根据该研究报告，已经发现这种丝粉具有皮肤吸湿效果，并能防止皮肤被紫外线灼伤，从而防止皮肤受到日晒伤害，并防止在皮肤上形成雀斑和黑斑。已经发现所制备的丝粉具有多种性能，例如抗氧化活性，并能杀灭导致皮肤疾病的微生物。根据这些性能，可将丝粉开发成为例如药物、化妆品和食品增补剂等保健品。
发明内容
本发明的目的是利用富含氨基酸和维生素E的丝粉的优点，将丝粉与本发明的具有杀菌作用的皮肤清洁用品混合，有助于滋养皮肤并增添魅力。
本发明涉及一种以丝蛋白为主要成分的皮肤清洁用品。经常使用本发明的皮肤清洁产品有助于滋养和软化皮肤，减少黑斑。本发明的皮肤清洁用品包括，例如，一种半透明的甘油皂条和一种淡黄色并具有香气的硬皂条。
本发明涉及一种丝清洁组合物，该丝清洁组合物包含丝胶蛋白。
具体实施方式
制备泰国丝皂条的方法包括以下步骤：
1.由泰国丝制备丝胶蛋白
1.1在干净的水中浸泡丝纤维或蚕茧。丝纤维或蚕茧与水的重量比为1∶20。
1.2将原料煮沸，在高压釜中提取25～30分钟，条件为110～120℃，压力不超过14磅/英寸2。
1.3用筛眼不小于220目的过滤器过滤所得溶液，然后浓缩，溶液中残留有所需使用浓度的丝胶残余物，或者可以将其在用于制皂前干燥并消毒。
2.本发明的丝清洁用品组合物包含：
1)0.01重量％～20.00重量％的来自泰国丝的丝胶蛋白
2)2.00重量％～20.00重量％的氢氧化钠或氢氧化钾
3)1.00重量％～30.00重量％的甘油(对于甘油产品)，或
4)20.00重量％～75.00重量％的植物或动物油脂(对于硬产品)
5)补足为100重量％的水
6)微量香料(根据需要而定)
制备甘油皂条的方法：
1)融化甘油组分；
2)在水中溶解氢氧化钠或氢氧化钾组分并加热；
3)将溶于水的泰国丝的丝胶蛋白和香料分别加入(1)中，充分搅拌，直至得到均质的混合物；
4)使皂质固化形成模具的形状。
制备硬皂条的方法
1)融化植物或动物油脂组分；
2)将氢氧化钠或氢氧化钾组分溶于水并加热，然后缓慢加入(1)中；
3)分别将溶于水的泰国丝的丝胶蛋白和香料加入(1)中，充分搅拌，直至得到均质的混合物；
4)使皂质固化形成模具的形状。
3.泰国丝皂的质量检查
根据《化学物质检验OECD规程(1992)》的第404部分“急性皮肤刺激/腐蚀”(OECD Guideline for the Testing of Chemicals，1992，Sec.404Acute dermal irritation/corrosions)和ISO 10993-10(1995)《医疗器械的生物学评估(Biological evaluation of medical devices)》的第10部分“刺激和过敏试验”，通过皮肤刺激试验检查泰国丝皂。
该泰国丝皂对实验兔的皮肤没有刺激(在10％重量/体积浓度下进行试验)。
Claims (7)
1.从泰国丝热回收丝胶蛋白的方法，其特征在于，将丝纤维或蚕茧与水以1∶20的重量比混合，然后在110～120℃下加热。
2.如权利要求1所述的方法，其中，在不超过14磅/英寸2的压力下实施所述加热步骤。
3.如权利要求1或2所述的方法，其中，所述加热时间为25～30分钟。
4.一种丝清洁组合物，该丝清洁组合物含有：
- 0.01重量％～20.00重量％的如权利要求1～3任一项所述的方法回收的丝胶蛋白；和
- 2.00重量％～20.00重量％的氢氧化钠或氢氧化钾。
5.如权利要求4所述的组合物，其中选择性地含有(a)1.00重量％～30.00重量％的甘油，或(b)20.00重量％～75.00重量％的植物或动物油脂。
6.如权利要求4或5的组合物，其中，选择性地加入水至100重量％，并根据需要加入微量香料。
7.制备丝皂的方法，该方法包括以下步骤：
—融化如权利要求5所述的任何组分；
—将所得溶液与如权利要求4所述的氢氧化钠或氢氧化钾混合；
—将所得产物与事先溶于水的丝胶蛋白混合，然后搅拌至均质的混合物；和
—使所得均质的混合物成形为所设计的形状。
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| TH088023 | 2003-12-11 | ||
| TH088023 | 2003-12-11 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1626062A true CN1626062A (zh) | 2005-06-15 |
| CN100566697C CN100566697C (zh) | 2009-12-09 |
Family
ID=34651622
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2004100479934A Expired - Lifetime CN100566697C (zh) | 2003-12-11 | 2004-06-14 | 丝皂条及其制备方法 |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US7314851B2 (zh) |
| JP (2) | JP5395317B2 (zh) |
| CN (1) | CN100566697C (zh) |
| MY (1) | MY140104A (zh) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109266470A (zh) * | 2018-09-20 | 2019-01-25 | 重庆丝玛帛科技有限公司 | 一种具有清洁功能的纤维制品 |
| CN110257198A (zh) * | 2019-07-25 | 2019-09-20 | 安徽省农业科学院蚕桑研究所 | 一种以天然丝胶蛋白原液制备洁面皂的方法 |
| CN111793533A (zh) * | 2020-07-18 | 2020-10-20 | 广东茂名健康职业学院 | 一种草本精华蚕丝皂及其制备方法 |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1931702B1 (en) | 2005-10-05 | 2013-01-02 | Commonwealth Scientific And Industrial Research Organisation | Silk proteins |
| EA201270304A1 (ru) | 2009-08-26 | 2012-09-28 | Коммонвелт Сайнтифик Энд Индастриэл Рисерч Организэйшн | Способы получения шелковой пасты |
| US10098674B2 (en) | 2009-10-22 | 2018-10-16 | Nuvasive, Inc. | System and method for posterior cervical fusion |
| WO2011050140A1 (en) | 2009-10-22 | 2011-04-28 | Blue Fury Consulting, L.L.C. | Posterior cervical fusion system and techniques |
| JP6317258B2 (ja) | 2011-11-16 | 2018-04-25 | コモンウェルス サイエンティフィック アンド インダストリアル リサーチ オーガナイゼーション | コラーゲン様絹遺伝子 |
| AU2013239320B2 (en) | 2012-03-26 | 2018-11-01 | Commonwealth Scientific And Industrial Research Organisation | Silk polypeptides |
| CN111278421B (zh) * | 2017-10-25 | 2022-12-09 | 联合利华知识产权控股有限公司 | 包含结构化水相和丝胶蛋白的组合物 |
| WO2019101524A1 (en) * | 2017-11-21 | 2019-05-31 | Unilever N.V. | A personal care composition comprising sericin |
| WO2019115172A1 (en) * | 2017-12-12 | 2019-06-20 | Unilever N.V. | A stable personal care composition |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5573702A (en) * | 1993-11-22 | 1996-11-12 | Colgate-Palmolive Co. | Liquid cleaning compositions with grease release agent |
| JP2615440B2 (ja) * | 1995-01-27 | 1997-05-28 | 農林水産省蚕糸・昆虫農業技術研究所長 | 絹フィブロイン微粉末の製造方法 |
| JPH1029909A (ja) * | 1996-02-28 | 1998-02-03 | Shinko Silk:Kk | セリシンペプチド溶液及びその製造方法 |
| JP3610358B2 (ja) * | 1996-11-08 | 2005-01-12 | セーレン株式会社 | 抗酸化剤 |
| JPH11131318A (ja) * | 1997-10-30 | 1999-05-18 | Kyoto Prefecture | セリシンの分離回収方法 |
| JP3362778B2 (ja) * | 1999-06-03 | 2003-01-07 | 独立行政法人農業生物資源研究所 | 結晶性絹超微粉末の製造方法 |
| JP3716293B2 (ja) * | 1999-08-02 | 2005-11-16 | 日清紡績株式会社 | セリシンの抽出方法 |
| JP2001106794A (ja) * | 1999-10-05 | 2001-04-17 | Mochida Shoko Kk | セリシン含有高分子含水ゲル及びその製造方法 |
| JP4677078B2 (ja) * | 2000-06-14 | 2011-04-27 | 株式会社相生発酵 | 皮膚癌予防剤 |
| JP2002226897A (ja) * | 2001-02-05 | 2002-08-14 | Chozo Hirao | オレイン酸石鹸及びその製造方法、並びに抗酸化剤及びその製造方法 |
| US6706675B1 (en) * | 2002-08-30 | 2004-03-16 | The Dial Corporation | Translucent soap bar composition and method of making the same |
| DE10241597B4 (de) * | 2002-09-07 | 2004-09-16 | Scs Skin Care Systems Gmbh | Seifenzubereitung mit Luftblasen |
-
2004
- 2004-06-07 US US10/862,893 patent/US7314851B2/en active Active
- 2004-06-11 JP JP2004173361A patent/JP5395317B2/ja not_active Expired - Lifetime
- 2004-06-11 MY MYPI20042254A patent/MY140104A/en unknown
- 2004-06-14 CN CNB2004100479934A patent/CN100566697C/zh not_active Expired - Lifetime
-
2011
- 2011-05-18 JP JP2011111099A patent/JP2011201901A/ja active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109266470A (zh) * | 2018-09-20 | 2019-01-25 | 重庆丝玛帛科技有限公司 | 一种具有清洁功能的纤维制品 |
| CN110257198A (zh) * | 2019-07-25 | 2019-09-20 | 安徽省农业科学院蚕桑研究所 | 一种以天然丝胶蛋白原液制备洁面皂的方法 |
| CN110257198B (zh) * | 2019-07-25 | 2021-02-09 | 安徽省农业科学院蚕桑研究所 | 一种以天然丝胶蛋白原液制备洁面皂的方法 |
| CN111793533A (zh) * | 2020-07-18 | 2020-10-20 | 广东茂名健康职业学院 | 一种草本精华蚕丝皂及其制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JP2005171218A (ja) | 2005-06-30 |
| JP5395317B2 (ja) | 2014-01-22 |
| CN100566697C (zh) | 2009-12-09 |
| US20050130857A1 (en) | 2005-06-16 |
| JP2011201901A (ja) | 2011-10-13 |
| US7314851B2 (en) | 2008-01-01 |
| MY140104A (en) | 2009-11-30 |
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