CN1494513A - 纳米级粉末的制备方法 - Google Patents

纳米级粉末的制备方法 Download PDF

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Publication number
CN1494513A
CN1494513A CNA028059131A CN02805913A CN1494513A CN 1494513 A CN1494513 A CN 1494513A CN A028059131 A CNA028059131 A CN A028059131A CN 02805913 A CN02805913 A CN 02805913A CN 1494513 A CN1494513 A CN 1494513A
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solution
reaction
stator
settling vessel
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CN1210207C (zh
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周英彦
高首山
李红霞
王开明
李晓奇
李莉香
温传庚
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Anshan University of Science and Technology
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Anshan University of Science and Technology
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B3/00—Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G1/00—Methods of preparing compounds of metals not covered by subclasses C01B, C01C, C01D, or C01F, in general
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S977/00—Nanotechnology
    • Y10S977/70—Nanostructure
    • Y10S977/773—Nanoparticle, i.e. structure having three dimensions of 100 nm or less
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S977/00—Nanotechnology
    • Y10S977/70—Nanostructure
    • Y10S977/773—Nanoparticle, i.e. structure having three dimensions of 100 nm or less
    • Y10S977/775—Nanosized powder or flake, e.g. nanosized catalyst
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S977/00—Nanotechnology
    • Y10S977/70—Nanostructure
    • Y10S977/773—Nanoparticle, i.e. structure having three dimensions of 100 nm or less
    • Y10S977/775—Nanosized powder or flake, e.g. nanosized catalyst
    • Y10S977/776—Ceramic powder or flake
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S977/00—Nanotechnology
    • Y10S977/70—Nanostructure
    • Y10S977/773—Nanoparticle, i.e. structure having three dimensions of 100 nm or less
    • Y10S977/775—Nanosized powder or flake, e.g. nanosized catalyst
    • Y10S977/777—Metallic powder or flake

Abstract

本发明公开了一种制备纳米级粉末的制备方法，包括：(a)提供能快速反应生成沉淀的A、B两种反应物溶液；(b)将A、B溶液分别连续送入具有定子和转子的处于运转状态的混合反应沉淀器中；(c)将从反应沉淀器连续流出的含沉淀浆料进行后处理。该方法能使纳米粒子的粒径大小可调控，粒度均匀、分散性好、产量高、工艺简单、消耗少。采用该方法，可生产各种金属、氧化物、氢氧化物、盐、磷化物和硫化物、有机化合物纳米级粉末。

Description

PCT国内申请，说明书已公开。

Claims (1)

  1. PCT国内申请，权利要求书已公开。
CNB028059131A 2001-03-07 2002-03-05 纳米级粉末的制备方法 Expired - Fee Related CN1210207C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CN01106279A CN1373083A (zh) 2001-03-07 2001-03-07 一种尺寸可控的纳米粉体制备方法
CN01106279.7 2001-03-07

Publications (2)

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CN1494513A true CN1494513A (zh) 2004-05-05
CN1210207C CN1210207C (zh) 2005-07-13

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CN01106279A Pending CN1373083A (zh) 2001-03-07 2001-03-07 一种尺寸可控的纳米粉体制备方法
CNB028059131A Expired - Fee Related CN1210207C (zh) 2001-03-07 2002-03-05 纳米级粉末的制备方法

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CN01106279A Pending CN1373083A (zh) 2001-03-07 2001-03-07 一种尺寸可控的纳米粉体制备方法

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US (1) US7211230B2 (zh)
EP (1) EP1371610A1 (zh)
JP (1) JP2004533912A (zh)
KR (1) KR100621675B1 (zh)
CN (2) CN1373083A (zh)
CA (1) CA2439485A1 (zh)
IL (2) IL157778A0 (zh)
WO (1) WO2002070409A1 (zh)

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CN1166448C (zh) * 2001-07-27 2004-09-15 鞍山钢铁学院 液相纳米粉体及纳米粒子聚集结构材料的制备方法
US20040154985A1 (en) * 2003-02-07 2004-08-12 Ferro Corporation Method and apparatus for producing particles via supercritical fluid processing
JP2005220435A (ja) * 2003-10-22 2005-08-18 Mitsuboshi Belting Ltd 金属ナノ粒子及び金属ナノ粒子分散液の製造方法
JP4558657B2 (ja) * 2006-01-31 2010-10-06 株式会社ワイエムシィ 微粒子生成装置及びマイクロチャネル基板
US8642123B1 (en) * 2006-03-22 2014-02-04 University Of South Florida Integration of ZnO nanowires with nanocrystalline diamond fibers
US8853116B2 (en) 2006-08-02 2014-10-07 Eestor, Inc. Method of preparing ceramic powders
CN101784484B (zh) * 2007-07-06 2013-07-17 M技术株式会社 陶瓷纳米粒子的制造方法
WO2009008390A1 (ja) * 2007-07-06 2009-01-15 M.Technique Co., Ltd. 金属微粒子の製造方法及びその金属微粒子を含む金属コロイド溶液
CN101784258B (zh) 2007-07-06 2013-07-17 M技术株式会社 生物摄取物微粒子及其制造方法、分散体、医药组成物
WO2009020188A1 (ja) 2007-08-09 2009-02-12 M.Technique Co., Ltd. 半導体微粒子の製造方法及びその微粒子
JPWO2009041274A1 (ja) 2007-09-27 2011-01-20 エム・テクニック株式会社 磁性体微粒子の製造方法、これにより得られた磁性体微粒子及び磁性流体、磁性体製品の製造方法
JP4399612B2 (ja) * 2007-11-09 2010-01-20 エム・テクニック株式会社 磁性体微粒子の製造方法、これにより得られた磁性体微粒子及び磁性流体、磁性体製品
JP4784623B2 (ja) * 2008-07-15 2011-10-05 株式会社豊田中央研究所 超微粒子の製造方法及び装置
KR101613318B1 (ko) * 2008-08-11 2016-04-18 프라이믹스 가부시키가이샤 도료의 제조방법 및 장치
JP5155840B2 (ja) * 2008-12-12 2013-03-06 三井金属鉱業株式会社 金属水酸化物の粒子の製造方法
CN102333724A (zh) * 2009-02-27 2012-01-25 埃斯托股份有限公司 用于氧化物粉末的湿化学共沉淀的反应管以及水热处理
KR101698762B1 (ko) * 2010-04-30 2017-01-23 삼성에스디아이 주식회사 리튬 전이금속 인산염의 제조방법
US9410065B2 (en) * 2013-01-29 2016-08-09 Halliburton Energy Services, Inc. Precipitated particles and wellbore fluids and methods relating thereto
US20140209393A1 (en) * 2013-01-29 2014-07-31 Halliburton Energy Services, Inc. Precipitated Particles and Wellbore Fluids and Methods Relating Thereto
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CN105655551B (zh) * 2016-01-05 2017-11-21 扬州大学 一种快速制备和分离无机纳米颗粒的方法
CN106390981A (zh) * 2016-09-19 2017-02-15 常州大学 一种稀土掺杂钛酸钡纳米粉光催化剂及其制备方法
CN107364849B (zh) * 2017-07-11 2019-10-01 南通大学 连续流立式平面型液相剪切装置
CN107311121A (zh) * 2017-07-21 2017-11-03 华北理工大学 一种制备纳米硒化铅的系统

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CN114853062A (zh) * 2022-03-28 2022-08-05 江西工陶院精细陶瓷有限公司 一种纳米级氧化锆粉体制备工艺

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JP2004533912A (ja) 2004-11-11
US7211230B2 (en) 2007-05-01
IL157778A0 (en) 2004-03-28
IL157778A (en) 2007-03-08
CN1210207C (zh) 2005-07-13
KR100621675B1 (ko) 2006-09-13
KR20040010602A (ko) 2004-01-31
WO2002070409A1 (fr) 2002-09-12
EP1371610A1 (en) 2003-12-17
CN1373083A (zh) 2002-10-09
CA2439485A1 (en) 2002-09-12
US20040115123A1 (en) 2004-06-17

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