CN1329831A - Disinfectant and its preparing process - Google Patents
Disinfectant and its preparing process Download PDFInfo
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- CN1329831A CN1329831A CN 00119124 CN00119124A CN1329831A CN 1329831 A CN1329831 A CN 1329831A CN 00119124 CN00119124 CN 00119124 CN 00119124 A CN00119124 A CN 00119124A CN 1329831 A CN1329831 A CN 1329831A
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Abstract
A disinfectant is prepared from 14 Chinese-medicinal materials including cloves, senecio, pulsatilla root, red sage root, etc through crushing, proportioning, extracting in water, adding matrine, deposition in alcohol, recovering alcohol, decolouring and dispensing. Its advantages are broad spectrum (including bacteria, fungus, virus, protozoon, spirochaete, etc), high effect, no irritation to skin and mucosa, and convenient application.
Description
The present invention is a kind of disinfectant and production method thereof, belongs to tcm field.
The existing medicament that also has some to play the sterilizing effect, as clean your the moon etc., but its narrow application range, and medicinal effects is also not exclusively fully up to expectations.
The object of the present invention is to provide a kind of safe in utilization, evident in efficacy, disinfectant applied widely and production method thereof.
Purpose of the present invention is implemented by following technical scheme: it is made up of by, frutus cnidii, the red sage root, Semen Hydnocarpi, kitchen garden, Chinese violet, Asian puccoon, evodia lepta, the coptis, the bletilla striata, golden cypress, honeysuckle, giant knotweed, Banlangen, isatis root and the bark of ash cloves, climbing groundsel, the Chinese pulsatilla, chenopodium ambrosiodies, Da Ye.
Shared percentage by weight, cloves are 4.3%-5.5%, climbing groundsel is 4.16%-5.37%, the Chinese pulsatilla is 4.1%6-5.37%, chenopodium ambrosiodies is 4.16%-5.2%, Da Ye is by being 6%-7.9%, frutus cnidii is 4.3%-5.5%, the red sage root is 4.16-5.5%, Semen Hydnocarpi is 4.16%-5.5%, kitchen garden is 4.2%-5.37%, Chinese violet is 3.6%-4.7%, Asian puccoon is 3.6%-4.7%, evodia lepta is 3.6%-4.7%, the coptis is 4.3%-5.5%, the bletilla striata is 3.6%-4.7%, golden cypress is 4.16%-5.5%, honeysuckle is 4.3%-5.37%, giant knotweed is 3.6%-4.7%, Banlangen is 12%-15.4%, isatis root is 3.6%-4.56%, the bark of ash is 3.6%-4.7%.
The production method of disinfectant is: (1) Chinese medicine is pulverized: select the clean dry Chinese herbal medicine of high-quality: cloves, climbing groundsel, the Chinese pulsatilla, chenopodium ambrosiodies, Da Ye are pulverized by, frutus cnidii, the red sage root, Semen Hydnocarpi, kitchen garden, Chinese violet, Asian puccoon, evodia lepta, the coptis, the bletilla striata, golden cypress, honeysuckle, giant knotweed, isatis root and the bark of ash, its granularity 10-40 orders are waited to prepare burden in the container of packing into; (2) batching: crushing Chinese medicine, according to prescription data, accurate proportioning and weighing; (3) water extracts: will join measured Chinese herbal medicine and pack in the steam heated multipotency extracting cylinder of chuck, and add the water of 4-10 times of weight of material simultaneously, heating was boiled 30-60 minutes, collected volatile oil simultaneously; Emit leaching liquid and be a water in storage tank, add the water of 3-8 times of weight of material again, heating was boiled 20-50 minutes, collected volatile oil simultaneously; Emit leaching liquid and be secondary water in storage tank, add the water of 2-7 times of weight of material again, heating was boiled 10-40 minutes, collected volatile oil simultaneously, and emitting leaching liquid is that three water are in storage tank; Three merging extracts, 2/4-3/4 of evaporation and concentration to three time extraction amount of water is the traditional Chinese medicine extraction concentrate; (4) add Banlangen: adding the Banlangen output in the traditional Chinese medicine extraction concentrate is 12%-15.4%, and heating was boiled 20-60 minutes, then cooling; (5) alcohol precipitation: the medicine that added Banlangen extracts concentrate and puts into settling tank and add 85-95% ethanol that concentrates 3-7 times of liquid measures and stir and leave standstill 22-28 hours.(6) ethanol reclaims: extract the alcohol precipitation supernatant and put into the logical vapour heating recovery ethanol of ethanol recycling can interlayer to 3/4-1/2 of supernatant amount, emit the refining liquid that contracts deeply; (7) decolouring, preparation: will make with extra care concentrate and put into steam-jacked kettle and add refining 0.8-1.2% the active carbon that concentrates liquid measure, heating is boiled and was stirred 20-60 minutes, filter with link-suspended basket centrifuge, add entry in the filtrate and extract the muddy hair oil of collecting, add aquae destillata (or ionized water) again to the output volume requirement, add 0.8-1.2% hydrochloric acid and regulate PH to 5-10, left standstill 32-44 hours, filter, promptly get disinfectant stoste.
Advantage of the present invention is: this disinfectant to various common disease substances, comprise that bacterium, fungi, virus, protozoon, conveyor screw etc. all have remarkable killing and inhibitory action, to skin, non-stimulated, the no allergy of mucous membrane, the application safety effect is remarkable, and usage is easy.
The invention will be further described below in conjunction with drawings and Examples:
Fig. 1 is the technological process of production figure of disinfectant.
Embodiment:
Embodiment 1: cloves 32 grams, climbing groundsel 32 grams, the Chinese pulsatilla 31 grams, chenopodium ambrosiodies 31 grams, Da Ye are by 45 grams, frutus cnidii 32 grams, the red sage root 31 grams, Semen Hydnocarpi 31 grams, kitchen garden 32 grams, Chinese violet 27 grams, Asian puccoon 27 grams, evodia lepta 27 grams, the coptis 32 grams, the bletilla striata 27 grams, golden cypress 31 grams, honeysuckle 32 grams, giant knotweed 27 grams, Banlangen 90 grams, isatis root 27 grams and the bark of ash 27 grams, and gross weight is 33.55kg.
Technological process prepares disinfectant as shown in Figure 1, produce and implement to select the dry Chinese medicinal herbs of various high-qualitys for use according to the prescription raw material variety, as mentioned above: cloves 32 grams, climbing groundsel 32 grams, the Chinese pulsatilla 31 grams, chenopodium ambrosiodies 31 grams, Da Ye is by 45 grams, frutus cnidii 32 grams, the red sage root 31 grams, Semen Hydnocarpi 31 grams, kitchen garden 32 grams, Chinese violet 27 grams, Asian puccoon 27 grams, evodia lepta 27 grams, the coptis 32 grams, the bletilla striata 27 grams, golden cypress 31 grams, honeysuckle 32 grams, giant knotweed 27 grams, isatis root 27 grams and the bark of ash 27 grams, be ground into 30 purpose powders, kind and quantity according to prescription are prepared burden, add in 250 liters of omnipotent extractors, add ordinary tap water 134kg, heating was boiled 30-60 minutes, collect volatile oil aqueous solution 34kg simultaneously in basin, emit an extract 100kg and put into the leaching liquid basin, add running water 100kg in the omnipotent extractor again, heating was boiled 20-60 minutes, collect volatile oil aqueous solution 20kg simultaneously, emit secondary raffinate 80kg, merge and put into the leaching liquid basin.Add running water 67kg in the omnipotent extractor again, heating was boiled 10-40 minutes, collected simultaneously and pressed volatile oil aqueous solution 17kg, went into out extract 50kg No. three times in basin, merged and put into the leaching liquid basin, and No. three times the extract amalgamation liquid amounts to 230kg.Add the concentration tank heating and be concentrated into volume 150kg, add Banlangen 4.5kg while hot, fully heated and stirred is even, and heating was boiled 20 minutes, was cooled to room temperature.The traditional Chinese medicine extraction concentrate 150kg that will add total alkali, put into settling tank and add 85-95% ethanol 450kg, stir, left standstill 22 hours, draw upper strata clear ethanol liquid 550kg and add the ethanol recycling can, the logical vapour heating recovery ethanol of interlayer is to refining concentrate 138kg, adds to add active carbon 1.3kg heating in the steam folder pot and boil to stir and filtered with tripod pendulum type batch centrifugal in 20 minutes, the volatile oil aqueous solution 70kg that extracting in water is collected in the filtrate adds aquae destillata (or ionized water) again to 500kg.Adding 0.8% hydrochloric acid transfers PH6-10 to leave standstill to filter in 32 hours and promptly gets disinfection stoste.
Stoste through can, is used the CO sterilization after the exterior and interior packing after quality testing is qualified, become the disinfectant formal product.
Embodiment 2: cloves 41 grams, climbing groundsel 40 grams, the Chinese pulsatilla 40 grams, chenopodium ambrosiodies 39 grams, Da Ye are by 59 grams, frutus cnidii 41 grams, the red sage root 41 grams, Semen Hydnocarpi 41 grams, kitchen garden 40 grams, Chinese violet 35 grams, Asian puccoon 35 grams, evodia lepta 35 grams, the coptis 41 grams, the bletilla striata 35 grams, golden cypress 41 grams, honeysuckle 40 grams, giant knotweed 35 grams, Banlangen 115 grams, isatis root 34 grams and the bark of ash 35 grams, and gross weight is 43.41kg.
Technological process prepares disinfectant as shown in Figure 1, produce and implement to select the dry Chinese medicinal herbs of various high-qualitys for use according to producing the prescription raw material variety, as mentioned above: cloves 41 grams, climbing groundsel 40 grams, the Chinese pulsatilla 40 grams, chenopodium ambrosiodies 39 grams, Da Ye is by 59 grams, frutus cnidii 41 grams, the red sage root 41 grams, Semen Hydnocarpi 41 grams, kitchen garden 40 grams, Chinese violet 35 grams, Asian puccoon 35 grams, evodia lepta 35 grams, the coptis 41 grams, the bletilla striata 35 grams, golden cypress 41 grams, honeysuckle 40 grams, giant knotweed 35 grams, isatis root 34 grams and the bark of ash 35 grams, be ground into 30 purpose powders, prepare burden according to the kind quantity of producing prescription, add in the omnipotent extractor of 250L, add running water 348kg, heating was boiled 60 minutes, collect volatilization oil-water fluid 60kg simultaneously, basin is emitted extract 200kg No. one time, put into the leaching liquid basin, add running water 260kg in the omnipotent extractor again, heating was boiled 40 minutes, collect volatile oil aqueous solution 50kg simultaneously in basin, emit secondary raffinate 180kg, merge and put into the leaching liquid basin, add running water 174kg in the omnipotent extractor again, heating was boiled 30 minutes, collect volatile oil aqueous solution 40kg simultaneously in basin, emit extract 100kg No. three times, merge and put into the leaching liquid basin, No. three extracts merge and amount to 480kg, add concentration tank, heating is concentrated into volume 200kg, add Banlangen 5.75kg while hot, fully heated and stirred is even, and heating is boiled and was cooled to room temperature in 40 minutes.To add the traditional Chinese medicine extraction concentrate 200kg of total alkali, and put into settling tank and add 95%, ethanol 800kg stirs, and leaves standstill 28 hours.Draw upper strata clear ethanol liquid 700kg, add the ethanol recycling can, the logical vapour heating of interlayer, reclaim ethanol to refining concentrate 175kg, add in the steam-jacked kettle, add active carbon 1.75kg heating and boil, stirred 30 minutes, filter with link-suspended basket centrifuge, the volatile oil aqueous solution 150kg that extracting in water is collected in the filtrate adds aquae destillata (or ionized water) again to 500kg, add 1% hydrochloric acid accent PH6-9, left standstill 44 hours, and filtered, promptly get disinfectant stoste.
Stoste is after quality testing is qualified, and through can, exterior and interior packing CO sterilization becomes the disinfectant formal product.
Claims (3)
1, a kind of disinfectant is characterized in that it is made up of by, frutus cnidii, the red sage root, Semen Hydnocarpi, kitchen garden, Chinese violet, Asian puccoon, evodia lepta, the coptis, the bletilla striata, golden cypress, honeysuckle, giant knotweed, Banlangen, isatis root and the bark of ash cloves, climbing groundsel, the Chinese pulsatilla, chenopodium ambrosiodies, Da Ye.
2, a kind of disinfectant according to claim 1, it is characterized in that shared percentage by weight, cloves is 4.3%-5.5%, climbing groundsel is 4.16%-5.37%, the Chinese pulsatilla is 4.1%6-5.37%, chenopodium ambrosiodies is 4.16%-5.2%, Da Ye is by being 6%-7.9%, frutus cnidii is 4.3%-5.5%, the red sage root is 4.16-5.5%, Semen Hydnocarpi is 4.16%-5.5%, kitchen garden is 4.2%-5.37%, Chinese violet is 3.6%-4.7%, Asian puccoon is 3.6%-4.7%, evodia lepta is 3.6%-4.7%, the coptis is 4.3%-5.5%, the bletilla striata is 3.6%-4.7%, golden cypress is 4.16%-5.5%, honeysuckle is 4.3%-5.37%, giant knotweed is 3.6%-4.7%, Banlangen is 12%-15.4%, isatis root is 3.6%-4.56%, the bark of ash is 3.6%-4.7%.
3, the production method of disinfectant according to claim 1, it is characterized in that: (1) Chinese medicine is pulverized: select the clean dry Chinese herbal medicine of high-quality: cloves, climbing groundsel, the Chinese pulsatilla, chenopodium ambrosiodies, Da Ye are pulverized by, frutus cnidii, the red sage root, Semen Hydnocarpi, kitchen garden, Chinese violet, Asian puccoon, evodia lepta, the coptis, the bletilla striata, golden cypress, honeysuckle, giant knotweed, isatis root and the bark of ash, its granularity 10-40 orders are waited to prepare burden in the container of packing into; (2) batching: crushing Chinese medicine, according to prescription data, accurate proportioning and weighing; (3) water extracts: will join measured Chinese herbal medicine and pack in the steam heated multipotency extracting cylinder of chuck, and add the water of 4-10 times of weight of material simultaneously, heating was boiled 30-60 minutes, collected volatile oil simultaneously; Emit leaching liquid and be a water in storage tank, add the water of 3-8 times of weight of material again, heating was boiled 20-50 minutes, collected volatile oil simultaneously; Emit leaching liquid and be secondary water in storage tank, add the water of 2-7 times of weight of material again, heating was boiled 10-40 minutes, collected volatile oil simultaneously, and emitting leaching liquid is that three water are in storage tank; Three merging extracts, 2/4-3/4 of evaporation and concentration to three time extraction amount of water is the traditional Chinese medicine extraction concentrate; (4) add Banlangen: adding the Banlangen output in the traditional Chinese medicine extraction concentrate is 12%-15.4%, and heating was boiled 20-60 minutes, then cooling; (5) alcohol precipitation: the medicine that added Banlangen extracts concentrate and puts into settling tank and add 85-95% ethanol that concentrates 3-7 times of liquid measures and stir and leave standstill 22-28 hours.(6) ethanol reclaims: extract the alcohol precipitation supernatant and put into the logical vapour heating recovery ethanol of ethanol recycling can interlayer to 3/4-1/2 of supernatant amount, emit the refining liquid that contracts deeply; (7) decolouring, preparation: will make with extra care concentrate and put into steam-jacked kettle and add refining 0.8-1.2% the active carbon that concentrates liquid measure, heating is boiled and was stirred 20-60 minutes, filter with link-suspended basket centrifuge, add entry in the filtrate and extract the muddy hair oil of collecting, add aquae destillata (or ionized water) again to the output volume requirement, add 0.8-1.2% hydrochloric acid and regulate PH to 5-10, left standstill 32-44 hours, filter, promptly get disinfectant stoste.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB001191241A CN1138476C (en) | 2000-06-17 | 2000-06-17 | Disinfectant and its preparing process |
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| CNB001191241A CN1138476C (en) | 2000-06-17 | 2000-06-17 | Disinfectant and its preparing process |
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| CN1329831A true CN1329831A (en) | 2002-01-09 |
| CN1138476C CN1138476C (en) | 2004-02-18 |
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| CNB001191241A Expired - Fee Related CN1138476C (en) | 2000-06-17 | 2000-06-17 | Disinfectant and its preparing process |
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| CN1301060C (en) * | 2003-07-29 | 2007-02-21 | 王丽华 | Plant Source non-public hazard biological insect repellant and preparing process |
| CN100333766C (en) * | 2003-11-26 | 2007-08-29 | 胡祥仁 | Medicine for treating dermatopathy and its preparing process |
| CN101861883A (en) * | 2009-04-16 | 2010-10-20 | 北京普瑞华康生物科技有限公司 | Plant disinfectant and preparation method thereof |
| CN101161077B (en) * | 2007-11-26 | 2010-12-08 | 倪建忠 | Four-effectiveness nuisance free agriculture chemicals and method of manufacturing the same |
| CN101496784B (en) * | 2009-03-13 | 2011-01-12 | 云南省药物研究所 | Chinese medicine shower lotion |
| CN102349992A (en) * | 2011-07-20 | 2012-02-15 | 王旋旋 | Medical skin disinfectant |
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| US20120156316A1 (en) * | 2002-09-04 | 2012-06-21 | Biomor Israel Ltd. | Biocompatible tea tree oil compositions |
| CN1301060C (en) * | 2003-07-29 | 2007-02-21 | 王丽华 | Plant Source non-public hazard biological insect repellant and preparing process |
| CN100333766C (en) * | 2003-11-26 | 2007-08-29 | 胡祥仁 | Medicine for treating dermatopathy and its preparing process |
| CN101161077B (en) * | 2007-11-26 | 2010-12-08 | 倪建忠 | Four-effectiveness nuisance free agriculture chemicals and method of manufacturing the same |
| CN101496784B (en) * | 2009-03-13 | 2011-01-12 | 云南省药物研究所 | Chinese medicine shower lotion |
| CN101513196B (en) * | 2009-04-07 | 2012-07-25 | 西南大学 | Traditional Chinese medicine extract for preventing hypertrophic Sclerotinia sclerotiorum |
| CN101861883A (en) * | 2009-04-16 | 2010-10-20 | 北京普瑞华康生物科技有限公司 | Plant disinfectant and preparation method thereof |
| CN101861883B (en) * | 2009-04-16 | 2013-04-03 | 北京普瑞华康生物科技有限公司 | Plant disinfectant and preparation method thereof |
| CN102349992B (en) * | 2011-07-20 | 2014-04-23 | 刘广真 | Medical skin disinfectant |
| CN102349992A (en) * | 2011-07-20 | 2012-02-15 | 王旋旋 | Medical skin disinfectant |
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| CN104383570A (en) * | 2014-11-26 | 2015-03-04 | 南京正宽医药科技有限公司 | Mixed disinfection type medical equipment disinfection cabinet |
| CN104645175A (en) * | 2015-03-13 | 2015-05-27 | 龚灿锋 | Traditional Chinese medicine disinfection liquid for clinical laboratory |
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| CN106421557A (en) * | 2016-10-28 | 2017-02-22 | 四川福方医疗器械有限公司 | Antimicrobial pharmaceutical composition |
| CN107306721A (en) * | 2017-06-12 | 2017-11-03 | 广西贵港市港北区鑫农桑蚕种养专业合作社 | A kind of green prevention and control method of tealeaves pest and disease damage |
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Owner name: NEI MENGGU ZHONGKANG BIOLOGY TECHNOLOGY CO., LTD. Free format text: FORMER OWNER: KUSHEN BIOCHEMICAL GROUP CO LTD, INNER MONGOLIAN AUTONOMOUS REGION Effective date: 20030118 |
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Effective date of registration: 20030118 Address after: 010051, No. 546 East Sea Road, Xincheng District, the Inner Mongolia Autonomous Region, Hohhot Applicant after: Zhongkang Biotechnology Co., Ltd. Address before: 010010, 9, Hebei street, East guard Town, Xincheng District, the Inner Mongolia Autonomous Region, Hohhot Applicant before: Kuh-seng Biochemical Group Co., Ltd., Nei Monggol |
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