CN1305979A - Composite leaf fertilizer and its preparing process - Google Patents
Composite leaf fertilizer and its preparing process Download PDFInfo
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- CN1305979A CN1305979A CN 01107174 CN01107174A CN1305979A CN 1305979 A CN1305979 A CN 1305979A CN 01107174 CN01107174 CN 01107174 CN 01107174 A CN01107174 A CN 01107174A CN 1305979 A CN1305979 A CN 1305979A
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Abstract
A composite leaf fertilizer is prepared from xanthohunic acid, amino acid solution, compounds of macro elements, medium elements and trace elements, complexing agent and wet penetrability through proportional mixing, reaction at a certain temp for a certain time and regulating acidity. Its advantages include low energy consumption, stable system, quick absorption, high fertility and high effect on improving quality and increasing yield.
Description
The present invention relates to composite foliage fertilizer and preparation method.
By retrieval, number of patent application is 97119485.8 Chinese invention patent, its denomination of invention " compound fulvic-acid liquid fertilizer ", and the mutual proportioning between its compound classification composition is: yellow humic acid 3～5; Feather casing amino acid solution 3～5; Nitrogen, phosphorus, potassium (chemical fertilizer) and boron, iodine (little fertilizer) compound liquid: 100; Zinc, copper, iron, manganese, magnesium, cobalt, molybdenum (little fertilizer) chelating liquid: 5～6.Its preparation method is made up of three parts: nitrogen, phosphorus, potassium (chemical fertilizer) and boron, the preparation of iodine (little fertilizer) compound liquid, and two sections controls of temperature of reaction were respectively 90 ℃, 60 minutes and 70 ℃, 40 minutes; Zinc, copper, iron, manganese, magnesium, cobalt, the preparation of molybdenum (little fertilizer) chelating liquid, temperature is 90 ℃～95 ℃, 2.5～3 hours time; Yellow humic acid, feather casing amino acid solution, ammoniacal liquor, the preparation of complexing agent mixed solution, temperature is 70 ℃, 0.5 hour; With this three partially mixed product that obtains.The content of its moderate-element and trace compound is low, only is 5%～6%, preparation method's complexity, and temperature high 95 ℃～70 ℃, the reaction times reaches 280～310 minutes, the energy consumption height.
The purpose of this invention is to provide a kind of composite foliage fertilizer and preparation method; not only compound classification composition is many, comprehensive nutrition, content height; and complex system is stable, can make plant leaf surface fully absorb nutritive element, can obviously suppress the disease that plant produces because of nutritional deficiency disease; the disease resistance ability is strong; drought-enduring, promote protein synthesis, vigorous, the well developed root system of plant strain growth, flower and fruit protecting and increasing production; improved the quality of crop, the preparation process energy consumption is low.
Purpose of the present invention is achieved through the following technical solutions:
Composite foliage fertilizer comprises following component and weight percent:
Moderate-element and trace compound 10～35
Urea 3～10
Aminoacids solution 5～25
Xanthohumic acid 2～8
Potassium hydroxide 2～8
Complexing agent 2～10
Wetting and penetrating agent 0.5～2.5
Clear water 35～55
Select at least a or multiple compound compositions among moderate-element Ca, Mg, S, the Cl, two or more compound compositions at least among trace elements zn, Fe, Cu, Mn, Mo, B, Sr, the Co, the total amount of compound of moderate-element and trace element is controlled at 10～35%;
Complexing agent comprises sodium ethylene diamine tetracetate, tartrate, trimethylenedinitrilo-tertraacetic acid, citric acid, heptonic acid, selects two or more complexing agents therein, and its overall control is 2%～10%;
Wetting and penetrating agent comprises nonionogenic tenside, anion surfactant and amphoterics, as polyoxyethylene groups ether in ninth of the ten Heavenly Stems phenol ether-10, aliphatic alcohol polyethenoxy base ether, polyoxyethylenated alcohol sodium sulfate, Sodium dodecylbenzene sulfonate, butyl a kind of apple sodium sulfonate etc., select two kinds therein, its overall control is 0.5%～2.5%;
The preparation method of composite foliage fertilizer, carry out in the following order:
Add clear water in the acid tolerance response container, stir, add aminoacids solution, urea, 20 ℃～40 ℃ of controlled temperature stirred 20～30 minutes;
The compound, the complexing agent that add moderate-element and trace element successively, 40 ℃～60 ℃ of control reaction temperature, 40～60 minutes time;
Transfer PH5～7 with potassium hydroxide and xanthohumic acid, continue reaction 20～30 minutes;
Adding wetting and penetrating agent mixed 30～60 minutes;
The equal continuously stirring of above-mentioned whole process.
Technique effect of the present invention
1. this composite foliage fertilizer is owing to contain xanthohumic acid, aminoacids solution, major element, moderate-element, trace element and promote complexing agent and the wetting agent that fertilizer absorbs, can obviously suppress the disease that plant produces because of nutritional deficiency disease, has drought resistance function, and promotion root system development, protein synthesis, diseases prevention, resistance against diseases are strong.Use this product, can effectively prevent and treat " admirable in all its details " disease, anthrax etc. of blossom-end rot, bacterial wilt of ginger, rice blast and watermelon of verticillium, the capsicum of butt rot, the eggplant of hot pickled mustard tube; As hot pickled mustard tube butt rot having taken place, sprays this product immediately and recover normal after 5 days; Rained heavily more than 20 day in October, 2000 continuously in the Zhanjiang City, Guangdong Province, all vegetable melon and fruits that sprayed this product in September are all survived, and the vegetables of not spraying this product step back at water and die mostly;
2. owing to adopted multiple complexing agent, wetting and penetrating agent, prevented that each nutritive element from tangerine being taken place resist, increased the synergy between each element, absorbed soon the fertilizer efficiency height.As at lettuce planting experimental field in prosperous this composite foliage fertilizer that sprays for a long time, only after 26 hours with the control group in the plot relatively, be and rise appreciably; Soak after the balsam pear kind sowing and do not contrast with this product seed soaking with this product, test-results is as follows:
Not seed soaking of time seed soaking
Bud ratio 80% did not sprout in 5 days
Bud all sprouted in 8 days, and no worm bud ratio 50% has small worm.
3. this composite foliage fertilizer contains the various plants necessary nutritive element of growing, and can satisfy different plants and same kind of plant in the demand of different growing stages to nutritive element.It is a kind of organic and inorganic complex fertilizer, can increase production, guarantee the quality, and can cultivate soil fertility again, helps agricultural sustainable development.As spraying with this product at watermelon plantation seedling stage, transplanting phase, prosperous long-term and expanding stage, effectively prevented the generation of " admirable in all its details " disease and anthrax etc., solved the difficult problem of watermelon continuous cropping, in the plantation of continuous cropping ground, every mu is increased production 100～150 jin, the sugariness of watermelon increases, and anti-storage, and deposit the flooring did not have bad fruit in 55 days;
4. control reaction temperature of the present invention is at 30 ℃～60 ℃, and 110～180 minutes time, energy consumption is low.
This composite foliage fertilizer can be widely used in cultivations of plants such as paddy rice, vegetables, melon and fruit, flowers, tobacco, anise, Chinese prickly ash, has disease resistance, increasing both production and income, raising crops quality, and remarkable in economical benefits has popularizing application prospect widely.
Embodiment 1
The component of composite foliage fertilizer and weight percent:
Boric acid 4
Ammonium molybdate 2
Zinc Sulphate Heptahydrate 6
Manganese sulfate monohydrate 5
Cupric chloride 2
Iron vitriol 4
Strontium nitrate 1
Magnesium sulfate heptahydrate 3
Nitrocalcite 3
Aminoacids solution 5
Urea 5
Sodium ethylene diamine tetracetate 4
Tartrate 3
Potassium hydroxide 4～8
Xanthohumic acid 2～6
Polyoxyethylene nonylphenyl ether-10 1
Aliphatic alcohol polyethenoxy base ether 1
Clear water 40.
The preparation of composite foliage fertilizer is carried out in the following order:
Add clear water in the acid tolerance response container, start stirring, add aminoacids solution, urea, 30 ℃ ± 5 ℃ of controlled temperature stirred 20 minutes;
Add compound, the complexing agent of moderate-element and trace element successively, control 55 ℃ ± 5 ℃ of its temperature, 60～90 minutes time;
Transfer PH5～7 with potassium hydroxide and xanthohumic acid;
Adding wetting and penetrating agent mixed 30～60 minutes;
The equal continuously stirring of above-mentioned whole process.
Present embodiment is applicable to Chinese cabbage group, solanaceous vegetables and melon vegetables etc.
Embodiment 2
The component of composite foliage fertilizer and weight percent:
Boric acid 3
Ammonium molybdate 2
Zinc Sulphate Heptahydrate 3
Manganese sulfate monohydrate 3
Cupric sulfate pentahydrate 3
Iron vitriol 3
Magnesium sulfate heptahydrate 3
Nitrocalcite 4
Aminoacids solution 10
Urea 5
Sodium ethylene diamine tetracetate 3
Tartrate 2.5
Potassium hydroxide 4～7
Xanthohumic acid 3～7
Polyoxyethylene nonylphenyl ether-10 0.6
Aliphatic alcohol polyethenoxy base ether 0.6
Clear water 44.3.The preparation of composite foliage fertilizer is with embodiment 1.Present embodiment is applicable to melon or fruit type crops.
The component and the weight percent of embodiment 3 composite foliage fertilizers:
Boric acid 3
Ammonium molybdate 0.5
Zinc Sulphate Heptahydrate 2
Manganese sulfate monohydrate 2
Cupric sulfate pentahydrate 1
Iron vitriol 1
Vitriolate of tartar 3
Magnesium sulfate heptahydrate 2
Nitrocalcite 4
Aminoacids solution 20
Urea 4
Sodium ethylene diamine tetracetate 2.5
Citric acid 1.5
Potassium hydroxide 2～5
Xanthohumic acid 5～7
Fatty alcohol-polyoxyethylene ether sulfuric acid 0.5
Sodium
Aliphatic alcohol polyethenoxy base ether 0.5
Clear water 43.5.The preparation method of composite foliage fertilizer is with embodiment 1.
Present embodiment is applicable to green vegetable class and root vegetable.
Embodiment 4
The component of composite foliage fertilizer and weight percent:
Boric acid 1
Ammonium molybdate 1
Zinc Sulphate Heptahydrate 10
Manganese sulfate monohydrate 2
Cupric sulfate pentahydrate 1
Iron vitriol 1
Magnesium sulfate heptahydrate 2
Potassium primary phosphate 2
Nitrocalcite 2
Aminoacids solution 15
Urea 4
Sodium ethylene diamine tetracetate 3
Citric acid 2
Potassium hydroxide 3～7
Xanthohumic acid 4～7
Sodium dodecylbenzene sulfonate 1.0
Sodium butylnaphthalenesulfonate 0.5
Clear water 43.5.
The composite foliage fertilizer preparation method of present embodiment is undertaken by embodiment 1, and different is to add potassium primary phosphate before transferring PH, stirs 20 minutes.
Present embodiment is applicable to rice standing grain class.
Claims (7)
1. a composite foliage fertilizer is characterized in that this composite foliage fertilizer comprises following component and weight percent:
Moderate-element and trace compound 10～35
Urea 3～10
Aminoacids solution 5～25
Xanthohumic acid 2～8
Potassium hydroxide 2～8
Complexing agent 2～10
Wetting and penetrating agent 0.5～2.5
Clear water 35～55
Select at least a or multiple compound among moderate-element Ca, Mg, S, the Cl, two or more compounds at least among trace elements zn, Fe, Cu, Mn, Mo, B, Sr, the Co, the overall control of the compound of moderate-element and trace element is 10～35%;
Complexing agent comprises sodium ethylene diamine tetracetate, tartrate, trimethylenedinitrilo-tertraacetic acid, citric acid, heptonic acid, selects two or more complexing agents therein, and its overall control is 2%～10%;
Wetting and penetrating agent comprises nonionogenic tenside, anion surfactant and amphoterics, selects two kinds therein, and its overall control is 0.5%～2.5%.
2. composite foliage fertilizer according to claim 1 is characterized in that the component and the weight percent of this composite foliage fertilizer:
Boric acid 4
Ammonium molybdate 2
Zinc Sulphate Heptahydrate 6
Manganese sulfate monohydrate 5
Cupric chloride 2
Iron vitriol 4
Strontium nitrate 1
Magnesium sulfate heptahydrate 3
Nitrocalcite 3
Aminoacids solution 5
Urea 5
Sodium ethylene diamine tetracetate 4
Tartrate 3
Potassium hydroxide 4～8
Xanthohumic acid 2～6
Polyoxyethylene nonylphenyl ether-10 1
Aliphatic alcohol polyethenoxy base ether 1
Clear water 40.
3. composite foliage fertilizer according to claim 1 is characterized in that the component and the weight percent of this composite foliage fertilizer:
Boric acid 4
Ammonium molybdate 2
Zinc Sulphate Heptahydrate 3
Manganese sulfate monohydrate 3
Cupric sulfate pentahydrate 3
Iron vitriol 3
Magnesium sulfate heptahydrate 3
Nitrocalcite 4
Aminoacids solution 10
Urea 5
Sodium ethylene diamine tetracetate 3
Tartrate 2.5
Potassium hydroxide 4～7
Xanthohumic acid 3～7
Polyoxyethylene nonylphenyl ether-10 0.6
Aliphatic alcohol polyethenoxy base ether 0.6
Clear water 44.3.
4. composite foliage fertilizer according to claim 1 is characterized in that the component and the weight percent of this composite foliage fertilizer:
Boric acid
Ammonium molybdate 0.5
Zinc Sulphate Heptahydrate 2
Manganese sulfate monohydrate 2
Cupric sulfate pentahydrate 1
Iron vitriol 1
Vitriolate of tartar 3
Magnesium sulfate heptahydrate 2
Nitrocalcite 4
Aminoacids solution 20
Urea 4
Sodium ethylene diamine tetracetate 2.5
Citric acid 1.5
Potassium hydroxide 2～5
Xanthohumic acid 5～7
Aliphatic alcohol polyethenoxy base ether 0.5
Polyoxyethylenated alcohol sodium sulfate 0.5
Clear water 43.5.
5. composite foliage fertilizer according to claim 1 is characterized in that the component and the weight percent of this composite foliage fertilizer:
Boric acid 1
Ammonium molybdate 1
Zinc Sulphate Heptahydrate 10
Manganese sulfate monohydrate 2
Cupric sulfate pentahydrate 1
Iron vitriol 1
Magnesium sulfate heptahydrate 2
Potassium primary phosphate 2
Nitrocalcite 2
Aminoacids solution 15
Urea 4
Sodium ethylene diamine tetracetate 3
Citric acid 2
Potassium hydroxide 3～7
Xanthohumic acid 4～7
Sodium dodecylbenzene sulfonate 1.0
Sodium butylnaphthalenesulfonate 0.5
Clear water 43.5.
6. the preparation method of a composite foliage fertilizer is characterized in that this preparation method carries out in the following order:
In the acid tolerance response container, add clear water, ceaselessly stir, add aminoacids solution, urea, 20 ℃～40 ℃ of controlled temperature, 20～30 minutes time;
Add compound, the complexing agent of moderate-element and trace element successively, control 40 ℃～60 ℃ of its temperature of reaction, 40～60 minutes time;
With PH5～7 that potassium hydroxide and xanthohumic acid are transferred above-mentioned solution, continue reaction 20～30 minutes;
Adding wetting and penetrating agent mixed 30～60 minutes;
The equal continuously stirring of above-mentioned whole process.
7. the preparation method of composite foliage fertilizer according to claim 6 is characterized in that adding P contained compound after complex reaction, stirs 20～40 minutes.
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| CN 01107174 CN1305979A (en) | 2001-02-23 | 2001-02-23 | Composite leaf fertilizer and its preparing process |
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|---|---|---|---|
| CN 01107174 CN1305979A (en) | 2001-02-23 | 2001-02-23 | Composite leaf fertilizer and its preparing process |
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| CN100347136C (en) * | 2006-08-07 | 2007-11-07 | 爱沃(北京)农业技术有限公司 | Microelement type composite foliage fertilizer and its preparation method |
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| CN104447091A (en) * | 2014-12-03 | 2015-03-25 | 大新县科学技术情报研究所 | Special leaf fertilizer for kuding tea and production method thereof |
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| CN100347136C (en) * | 2006-08-07 | 2007-11-07 | 爱沃(北京)农业技术有限公司 | Microelement type composite foliage fertilizer and its preparation method |
| CN100424050C (en) * | 2007-03-09 | 2008-10-08 | 陕西汉唐环保农业有限公司 | Dextroglucose plants organic nutrient solution and producing technique |
| CN101182270B (en) * | 2007-10-22 | 2011-03-09 | 李海涛 | Organic acid inorganic salt complex agent for crop and preparation method thereof |
| CN101857472B (en) * | 2009-04-10 | 2013-07-03 | 董旭 | Foliar compound fertilizer and preparation method thereof |
| CN101717287B (en) * | 2009-11-26 | 2011-12-14 | 西北农林科技大学 | Grape nutrition-balanced foliar fertilizer and preparation method thereof |
| CN102276354A (en) * | 2011-06-28 | 2011-12-14 | 云南金星化工有限公司 | Foliar fertilizer with high activity organic acid and preparation process thereof |
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| CN103130559A (en) * | 2011-11-25 | 2013-06-05 | 施可丰化工股份有限公司 | Broad spectrum type leaf fertilizer |
| CN102491818B (en) * | 2011-12-07 | 2013-08-07 | 陈忠慧 | Fertilizer special for high-potassium rice and preparation method of fertilizer |
| CN102491818A (en) * | 2011-12-07 | 2012-06-13 | 陈忠慧 | Fertilizer special for high-potassium rice and preparation method of fertilizer |
| CN103113157A (en) * | 2013-02-01 | 2013-05-22 | 兰州熙瑞化工科技有限公司 | Slow-release water-retaining compound fertilizer composition |
| CN103113157B (en) * | 2013-02-01 | 2014-12-03 | 兰州熙瑞化工科技有限公司 | Slow-release water-retaining compound fertilizer composition |
| CN103242089A (en) * | 2013-05-07 | 2013-08-14 | 宁波致富宝生物科技有限公司 | Special polymicro liquid nitrogen leaf fertilizer for vegetable |
| CN103265364A (en) * | 2013-05-23 | 2013-08-28 | 苏州富通高新材料科技股份有限公司 | Nutritionally-balanced selenium-rich nutrient solution for cultivating chillies |
| CN103539575A (en) * | 2013-11-08 | 2014-01-29 | 南开大学 | Development method of special efficient fulvic acid liquid compound fertilizer for potatoes |
| CN104291942A (en) * | 2014-09-23 | 2015-01-21 | 石家庄瑞思达生物技术有限公司 | Drought-resistant foliar fertilizer for increasing yield, and preparation method and application thereof |
| CN104262007A (en) * | 2014-09-29 | 2015-01-07 | 高台县旺达绿禾肥业有限责任公司 | Whole water-soluble nitrogen fertilizer with relatively high pelletizing rate |
| CN104447091A (en) * | 2014-12-03 | 2015-03-25 | 大新县科学技术情报研究所 | Special leaf fertilizer for kuding tea and production method thereof |
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