CN100424050C - Dextroglucose plants organic nutrient solution and producing technique - Google Patents
Dextroglucose plants organic nutrient solution and producing technique Download PDFInfo
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- CN100424050C CN100424050C CNB200710017479XA CN200710017479A CN100424050C CN 100424050 C CN100424050 C CN 100424050C CN B200710017479X A CNB200710017479X A CN B200710017479XA CN 200710017479 A CN200710017479 A CN 200710017479A CN 100424050 C CN100424050 C CN 100424050C
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- dextroglucose
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- 238000000034 method Methods 0.000 title claims abstract description 21
- 235000015097 nutrients Nutrition 0.000 title claims description 22
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims abstract description 105
- 238000003756 stirring Methods 0.000 claims abstract description 26
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 23
- 238000004519 manufacturing process Methods 0.000 claims abstract description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 19
- 239000007788 liquid Substances 0.000 claims abstract description 14
- 238000002156 mixing Methods 0.000 claims abstract description 9
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid group Chemical class C(CC(O)(C(=O)O)CC(=O)O)(=O)O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 77
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 44
- 239000008121 dextrose Substances 0.000 claims description 42
- 238000006243 chemical reaction Methods 0.000 claims description 39
- 239000002509 fulvic acid Substances 0.000 claims description 39
- PUKLDDOGISCFCP-JSQCKWNTSA-N 21-Deoxycortisone Chemical compound C1CC2=CC(=O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@@](C(=O)C)(O)[C@@]1(C)CC2=O PUKLDDOGISCFCP-JSQCKWNTSA-N 0.000 claims description 35
- FCYKAQOGGFGCMD-UHFFFAOYSA-N Fulvic acid Natural products O1C2=CC(O)=C(O)C(C(O)=O)=C2C(=O)C2=C1CC(C)(O)OC2 FCYKAQOGGFGCMD-UHFFFAOYSA-N 0.000 claims description 35
- 229940095100 fulvic acid Drugs 0.000 claims description 35
- 235000015165 citric acid Nutrition 0.000 claims description 28
- 239000012752 auxiliary agent Substances 0.000 claims description 27
- 239000004202 carbamide Substances 0.000 claims description 22
- 238000006386 neutralization reaction Methods 0.000 claims description 14
- 239000001508 potassium citrate Substances 0.000 claims description 11
- QEEAPRPFLLJWCF-UHFFFAOYSA-K potassium citrate (anhydrous) Chemical compound [K+].[K+].[K+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O QEEAPRPFLLJWCF-UHFFFAOYSA-K 0.000 claims description 11
- 230000002829 reductive effect Effects 0.000 claims description 11
- 239000002904 solvent Substances 0.000 claims description 11
- 235000015870 tripotassium citrate Nutrition 0.000 claims description 11
- 235000013305 food Nutrition 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 9
- PRPINYUDVPFIRX-UHFFFAOYSA-N 1-naphthaleneacetic acid Chemical compound C1=CC=C2C(CC(=O)O)=CC=CC2=C1 PRPINYUDVPFIRX-UHFFFAOYSA-N 0.000 claims description 7
- 150000001413 amino acids Chemical class 0.000 claims description 7
- 150000007523 nucleic acids Chemical class 0.000 claims description 7
- 102000039446 nucleic acids Human genes 0.000 claims description 7
- 108020004707 nucleic acids Proteins 0.000 claims description 7
- AXKBOWBNOCUNJL-UHFFFAOYSA-M sodium;2-nitrophenolate Chemical group [Na+].[O-]C1=CC=CC=C1[N+]([O-])=O AXKBOWBNOCUNJL-UHFFFAOYSA-M 0.000 claims description 7
- 235000013343 vitamin Nutrition 0.000 claims description 7
- 239000011782 vitamin Substances 0.000 claims description 7
- 229930003231 vitamin Natural products 0.000 claims description 7
- 229940088594 vitamin Drugs 0.000 claims description 7
- 150000003722 vitamin derivatives Chemical class 0.000 claims description 7
- 238000004090 dissolution Methods 0.000 claims description 6
- 238000005516 engineering process Methods 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- 230000035484 reaction time Effects 0.000 claims description 5
- 230000000694 effects Effects 0.000 abstract description 18
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 abstract 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 abstract 1
- 239000002671 adjuvant Substances 0.000 abstract 1
- 229940059741 aqua care Drugs 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 239000004021 humic acid Substances 0.000 abstract 1
- 230000000149 penetrating effect Effects 0.000 abstract 1
- 229960001031 glucose Drugs 0.000 description 38
- 241000196324 Embryophyta Species 0.000 description 27
- 239000000243 solution Substances 0.000 description 27
- 239000000047 product Substances 0.000 description 25
- 239000007921 spray Substances 0.000 description 8
- 201000010099 disease Diseases 0.000 description 7
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 7
- 230000035764 nutrition Effects 0.000 description 7
- 235000016709 nutrition Nutrition 0.000 description 7
- 239000000126 substance Substances 0.000 description 6
- 239000008399 tap water Substances 0.000 description 6
- 235000020679 tap water Nutrition 0.000 description 6
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 5
- 229910052700 potassium Inorganic materials 0.000 description 5
- 239000011591 potassium Substances 0.000 description 5
- 230000003381 solubilizing effect Effects 0.000 description 5
- 241001465754 Metazoa Species 0.000 description 4
- 210000004027 cell Anatomy 0.000 description 4
- 239000003337 fertilizer Substances 0.000 description 4
- 238000001784 detoxification Methods 0.000 description 3
- 230000004060 metabolic process Effects 0.000 description 3
- 230000000050 nutritive effect Effects 0.000 description 3
- 230000029553 photosynthesis Effects 0.000 description 3
- 238000010672 photosynthesis Methods 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- 229930091371 Fructose Natural products 0.000 description 2
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 241000227653 Lycopersicon Species 0.000 description 2
- 235000007688 Lycopersicon esculentum Nutrition 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- 240000006365 Vitis vinifera Species 0.000 description 2
- 235000014787 Vitis vinifera Nutrition 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 229960002737 fructose Drugs 0.000 description 2
- 239000008103 glucose Substances 0.000 description 2
- 230000012010 growth Effects 0.000 description 2
- JARKCYVAAOWBJS-UHFFFAOYSA-N hexanal Chemical compound CCCCCC=O JARKCYVAAOWBJS-UHFFFAOYSA-N 0.000 description 2
- 230000036039 immunity Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000007246 mechanism Effects 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- 239000008107 starch Substances 0.000 description 2
- 239000003053 toxin Substances 0.000 description 2
- 231100000765 toxin Toxicity 0.000 description 2
- 235000019154 vitamin C Nutrition 0.000 description 2
- 239000011718 vitamin C Substances 0.000 description 2
- RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 description 1
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- 208000004880 Polyuria Diseases 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- 229930003268 Vitamin C Natural products 0.000 description 1
- 235000009754 Vitis X bourquina Nutrition 0.000 description 1
- 235000012333 Vitis X labruscana Nutrition 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- LPQOADBMXVRBNX-UHFFFAOYSA-N ac1ldcw0 Chemical compound Cl.C1CN(C)CCN1C1=C(F)C=C2C(=O)C(C(O)=O)=CN3CCSC1=C32 LPQOADBMXVRBNX-UHFFFAOYSA-N 0.000 description 1
- 238000005903 acid hydrolysis reaction Methods 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- -1 aldehyde radical Chemical class 0.000 description 1
- GZCGUPFRVQAUEE-SLPGGIOYSA-N aldehydo-D-glucose Chemical group OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O GZCGUPFRVQAUEE-SLPGGIOYSA-N 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 229910052785 arsenic Inorganic materials 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 210000001185 bone marrow Anatomy 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 229910052793 cadmium Inorganic materials 0.000 description 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 1
- 239000000496 cardiotonic agent Substances 0.000 description 1
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- 239000012530 fluid Substances 0.000 description 1
- 239000013505 freshwater Substances 0.000 description 1
- 125000002791 glucosyl group Chemical group C1([C@H](O)[C@@H](O)[C@H](O)[C@H](O1)CO)* 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 210000002751 lymph Anatomy 0.000 description 1
- 239000002075 main ingredient Substances 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 230000009965 odorless effect Effects 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
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- 208000007578 phototoxic dermatitis Diseases 0.000 description 1
- 230000008635 plant growth Effects 0.000 description 1
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Images
Abstract
The invention discloses an organic nourishing liquid of dextroglucose plant and manufacturing technique, which comprises the following steps: adding potassium hydroxide into autoclave with water; adding citrate to neutralize; cooling below 60 deg.c; adding aquacare; stirring under normal temperature; adding biochemical humic acid; adding dextroglucose and adjuvant; stirring; blending evenly; obtaining the product with strong activity and penetrating property.
Description
Technical field
The present invention relates to a kind of organic nutrition of plant liquid and production technique thereof, be specifically related to a kind of Dextroglucose plants organic nutrient solution and production technique thereof.
Background technology
Promote the dominant mechanism of plant-growth: the one, keep Premeabilisation of cells and press, the 2nd, promote photosynthesis.Photosynthesis of plants is to be undertaken by green body at leaf inner cell or tender stem superficial cell, carries out photosynthetic cell and makes organic factory just as one, and it absorbs water from root, absorbs CO from pore
2, producing organism is glucose and byproduct O
2, satisfy metabolism and the energy requirement of plant, promote photosynthesis, make body more healthy and stronger.
Dextrose is D (+) glucose, be distributed widely in seed, leaf, root, flower and the fruit of plant and the blood of animal, lymph liquid, bone marrow fluid in, be indispensable nutritive substance in the animals and plants vital movement.It can participate in metabolic processes directly in the animals and plants body, be the main source of body institute energy requirement, is photosynthetic promotor.The chemical structure of dextrose belongs to hexanal monose, chemical formula C
6H
12O
6, white crystal or powder, odorless, soluble in water, 146 ℃ of fusing points, proportion 1.544, the basic structure formula is CH
2OH (CHOH)
4CHO, structural formula is:
Have reductibility and dextrorotation photosensitiveness, in printing and dyeing, process hides, the industry of system mirror, be used as reductive agent; As nutrition agent, cardiac stimulant, diuresis detoxifcation etc., its detoxification mainly is to promote liver detoxification medically.
Summary of the invention
The object of the present invention is to provide a kind of Dextroglucose plants organic nutrient solution and production technique thereof, it has solved, and dextrose only is used for animal extra-nutrition, disease-resistant toxicide technical problem in the background technology.
Technical solution of the present invention is:
A kind of Dextroglucose plants organic nutrient solution, contain by weight percentage:
(1) 19.7～35.2% water;
(2) 12～15% dextroses;
(3) 10～13% potassium hydroxide; Described potassium hydroxide is 〉=90% potassium hydroxide;
(4) 11～14% citric acids; Described citric acid is 99% citric acid;
(5) 7.5～20% biochemical fulvic acids; Described biochemical fulvic acid is 〉=30% biochemical fulvic acid;
(6) 18～22% urea;
(7) 0.2～0.4% auxiliary agents; Described auxiliary agent is selected from sodium nitrophenolate, amino acid, nucleic acid, Nafusaku or VITAMIN, or is selected from wherein two to four kinds mixture.
Above-mentioned Dextroglucose plants organic nutrient solution, best composition by weight percentage contains:
(1) 19.7% water;
(2) 15% dextroses;
(3) 11% potassium hydroxide;
(4) 13% citric acids;
(5) 20% biochemical fulvic acids;
(6) 20% urea;
(7) 0.3% auxiliary agents.
Above-mentioned dextrose can adopt the technical grade dextrose; Described potassium hydroxide can adopt 〉=90% industrial goods potassium hydroxide; Described citric acid can adopt the food grade citric acid; Described biochemical fulvic acid can adopt 〉=30% biochemical fulvic acid liquid.
A kind of first kind of technology of producing above-mentioned Dextroglucose plants organic nutrient solution may further comprise the steps:
(1) dissolving: water is added in the reactor, slowly add potassium hydroxide under stirring, solvent temperature is controlled at below 50 ℃;
(2) neutralization: slowly add citric acid, carry out neutralization reaction, temperature of reaction is controlled between 65～75 ℃, reacts 45～60 minutes, generates Tripotassium Citrate;
(3) mixed dissolution: when temperature is reduced to below 60 ℃, add urea, be stirred to dissolving;
(4) chelating: under the normal temperature, add biochemical fulvic acid liquid while stirring, chelatropic reaction 15 ± 5 minutes;
(5) dissolving: add dextrose, be stirred to dissolving;
(6) chelating: add the auxiliary agent chelatropic reaction, be stirred to dissolving, mixing gets finished product.
In first kind of production technique of above-mentioned Dextroglucose plants organic nutrient solution, the solvent temperature of described adding potassium hydroxide is controlled at below 50 ℃, is to control by the amount of control adding potassium hydroxide; The temperature of reaction of described adding citric acid is advisable to be controlled at more than 65 ℃; During described adding urea, be advisable when reducing to 50 ℃ with temperature; The chelatropic reaction time of described adding biochemical fulvic acid was advisable with 15 minutes; The stirring and dissolving time of described adding dextrose and auxiliary agent was advisable with 15 minutes respectively.
In first kind of production technique of above-mentioned Dextroglucose plants organic nutrient solution, described finished product was advisable to continue stirring reaction after all raw material adds in 45 minutes.
A kind of second kind of production technique of producing above-mentioned Dextroglucose plants organic nutrient solution may further comprise the steps:
(1) dissolving: water is added in the reactor, slowly add potassium hydroxide under stirring, solvent temperature is controlled at below 50 ℃;
(2) neutralization: slowly add citric acid, carry out neutralization reaction, temperature of reaction is controlled between 65～75 ℃, reacts 45～60 minutes, generates Tripotassium Citrate;
(3) mixed dissolution: when temperature is reduced to below 60 ℃, add urea, be stirred to dissolving, get I solution;
(4) dissolving: water is added in the reactor, add 50% biochemical fulvic acid powder, be stirred to dissolving fully, get II solution;
(5) chelating: II solution is added in the I solution stirring and evenly mixing;
(6) dissolving: add dextrose, be stirred to dissolving;
(7) chelating: add auxiliary agent, be stirred to dissolving, mixing gets finished product.
In second kind of production technique of above-mentioned Dextroglucose plants organic nutrient solution, the solvent temperature of described adding potassium hydroxide is controlled at below 50 ℃, is to control by the amount of control adding potassium hydroxide; The temperature of reaction of described adding citric acid is advisable to be controlled at 65 ℃; During described adding urea, be advisable when reducing to 50 ℃ with temperature; The chelatropic reaction time of described adding biochemical fulvic acid powder was advisable with 15 minutes; Described II solution adds the churning time of I solution and was advisable with 15 minutes; The stirring and dissolving time of described adding dextrose and auxiliary agent was advisable with 15 minutes respectively.
In second kind of production technique of above-mentioned Dextroglucose plants organic nutrient solution, described finished product was advisable to continue stirring reaction after all raw material adds in 45 minutes.
The present invention has the following advantages:
1. the prescription of product complements each other, and is scientific and reasonable.
(1) dextrose plant is had high nutrition and disease-resistant detoxification, and himself has no side effect as the main ingredient of plant water-soluble fertilizer.
(2) dextrose is as the organic nutrient solution for cultivating of plant, and is inexpensive, good water solubility, organic content height.
(3) sugariness of dextrose is lower, does water soluble fertilizer dilution back and does not have sweet taste substantially, can not attract the ant insect pest.
(4) the chelating pardon of other nutritive substances such as organic acid such as dextrose and biochemical fulvic acid, urea, Tripotassium Citrate, phosphoric acid is good.Is the Tripotassium Citrate compatibility with dextrose with having organic potassium source anticorrosion, anti-oxidant and that chelating is good, and easy the to be corrupt spoilage problems of dextrose can be readily solved.
2. effects such as the nutrition of product, disease-resistant, detoxifcation are comprehensive, and effect is remarkable.Because dextrose has the effect of quick extra-nutrition, disease-resistant strong sprout and detoxifcation to plant, take root chelating and trophicity of biochemical fulvic acid disease-resistant is preferable, Tripotassium Citrate has quick-acting preservative property and trophicity, the present invention combines dextrose, biochemical fulvic acid and Tripotassium Citrate and constitutes water soluble fertilizer with urea, effects such as therefore nutrition, disease-resistant, detoxifcation more comprehensively, more remarkable effect.
3. product activity, taking root property, drought resistance and perviousness are strong.
Biochemical fulvic acid is the small molecules that contains nutritive substances such as amino acid, nucleic acid, VITAMIN, with mother liquor and the skeleton of biochemical fulvic acid as product, makes product activity, taking root property, drought resistance and keep the osmotic pressure effect of cell better.
The quick-acting of product and strong sprout effect remarkable.
Adding a large amount of organic nitrogenous fertilizers in prescription is urea and auxiliary agent, make product quick-acting and strong sprout more remarkable effect, be beneficial to increasing both production and income, improve plant quality.
5. Product Green environmental protection.
Because the main raw material of formula for a product is to adopt food grade materials, so the harmful element index of product is significantly less than national standard, as: arsenic, cadmium, mercury etc. detect real data respectively below 2mg/kg.
6. produce low-cost, pollution-free.
Production technology optimization need not to add reaction heat, has saved the energy, greatly reduces production cost, and does not have " three wastes " discharging in producing.
Description of drawings
Fig. 1 is a production method schematic flow sheet of the present invention.
Fig. 2 is the test-results figure of product of the present invention to fruit sugar, vitamins C and acid content influence.
Fig. 3 is the test-results figure of product toxin immunity of the present invention.
Embodiment
The weight percent of the present invention's prescription is as follows:
Water 19.7～35.2%,
Dextrose 12～15%,
Potassium hydroxide 10～13%,
Citric acid 11～14%,
Biochemical fulvic acid 7.5～20%,
Urea 18～22%,
Auxiliary agent 0.2～0.4%.
Wherein, dextrose is good to adopt the technical grade dextrose, also can adopt high-purity glucose; Potassium hydroxide is 〉=90% potassium hydroxide, specifically can adopt industrial goods; Citric acid is 99% food grade citric acid; Biochemical fulvic acid is advisable to adopt 〉=30% biochemical fulvic acid liquid, is good to adopt 〉=50% biochemical fulvic acid liquid; Auxiliary agent can adopt a kind of of sodium nitrophenolate, amino acid, nucleic acid, Nafusaku, VITAMIN etc. or any two to multiple mixture.
Embodiment by weight percentage is as follows for product of the present invention:
Water 35.2 26.6 29 32 24
Dextrose 12 14 12 13 15
Potassium hydroxide 12 13 11 11 10
Citric acid 13 13 12 12 11
Biochemical fulvic acid 7.5 14 15.8 10.7 17.8
Urea 20 19 18 21 22
Auxiliary agent 0.3 0.4 0.2 0.3 0.2
The embodiment 1 of production technique of the present invention is as follows:
(1) solubilizing reaction: get tap water and add in the reactor, slowly add technical grade potassium hydroxide under stirring.Control adds the amount of potassium hydroxide, makes solvent temperature below 50 ℃.
(2) neutralization reaction: slowly add the food grade citric acid, carry out neutralization reaction, temperature of reaction is controlled between 65～75 ℃, reacts 45～60 minutes, generates Tripotassium Citrate.
(3) mixed dissolution: when temperature is reduced to below 60 ℃, add urea, be stirred to dissolving.Dissolved urea has utilized preceding reaction heat.
(4) chelatropic reaction: under the normal temperature, added biochemical fulvic acid liquid chelatropic reaction 15 ± 5 minutes.Add biochemical fulvic acid liquid in the back, temperature of reaction is low, can guarantee the activity, nutrition of biochemical fulvic acid etc.
(5) solubilizing reaction: add the food grade dextrose, be stirred to dissolving.Add dextrose in the back, temperature of reaction is low, can guarantee the activity of dextrose.
(6) chelatropic reaction: add the auxiliary agent chelatropic reaction, be stirred to dissolving, mixing gets finished product.
The specific embodiment of production technique embodiment 1 of the present invention:
(1) the 197kg tap water is added in the reactor, slowly add technical grade potassium hydroxide 120kg under stirring, the control feeding quantity makes reactor temperature below 50 ℃.
(2) slowly add 99% food grade citric acid 130kg, carry out neutralization reaction; Temperature of reaction should be controlled between 65～75 ℃, and the reaction times is 45 minutes, generates Tripotassium Citrate.
(3) when temperature is reduced to 50 ℃, add 200kg urea, be stirred to dissolving fully.
(4) be cooled to normal temperature naturally, add 30% biochemical fulvic acid liquid 200kg while stirring, chelatropic reaction 15 minutes.
(5) add 150kg dextrose, stirring and dissolving 15 minutes; Add the 3kg auxiliary agent again, this auxiliary agent is selected from sodium nitrophenolate, amino acid, nucleic acid, Nafusaku or VITAMIN, or is selected from the mixture of wherein any two to four kinds of arbitrary proportions, stirring and dissolving 15 minutes.
(6) after all raw material added, restir reaction 45 minutes got product.
The embodiment 2 of production technique of the present invention is as follows:
(1) solubilizing reaction: get tap water and add in the reactor, slowly add technical grade potassium hydroxide under stirring.Control adds the amount of potassium hydroxide, makes solvent temperature below 50 ℃.
(2) neutralization reaction: slowly add the food grade citric acid, carry out neutralization reaction, temperature of reaction is controlled between 65～75 ℃, reacts 45～60 minutes, generates Tripotassium Citrate.
(3) mixed dissolution: when temperature is reduced to below 60 ℃, add urea, be stirred to dissolving, get I solution.
(4) solubilizing reaction: get tap water and add in another reactor, stir adding 80% biochemical fulvic acid powder down, be stirred to dissolving fully, get II solution.
(5) chelatropic reaction: II solution is added in the I solution, stirred 15 minutes.
(6) solubilizing reaction: add dextrose, be stirred to dissolving.
(7) chelatropic reaction: add the auxiliary agent chelatropic reaction, be stirred to dissolving, mixing gets finished product.
The specific embodiment of production technique embodiment 2 of the present invention:
(1) get the 200kg tap water and add in the reactor, slowly add 120kg technical grade potassium hydroxide under stirring, solvent temperature is controlled at below 50 ℃.
(2) slowly add 130kg food grade citric acid, carry out neutralization reaction, temperature of reaction is controlled at 65 ℃, reacts 60 minutes, generates Acidum Citricum potassium.
(3) when temperature is reduced to below 60 ℃, add 200kg urea, stirred 20 minutes, get I solution.
(4) get the 152kg tap water and add in another reactor, stir adding 75kg80% biochemical fulvic acid powder down, be stirred to dissolving fully, get II solution.
(5) II solution is added in the I solution, stirred 15 minutes.
(6) add the 120kg dextrose, be stirred to dissolving.
(7) add the 3kg auxiliary agent, this auxiliary agent is selected from sodium nitrophenolate, amino acid, nucleic acid, Nafusaku or VITAMIN, or is selected from the mixture of wherein any two to four kinds of arbitrary proportions, and stirring reaction 45 minutes gets finished product.
Dextrose in the production technique embodiment 1 of the present invention and 2 can also can be produced through root enzyme or interior spore enzyme diastatic action by starch by starch through hydrochloric acid or dilute sulphuric acid hydrolysis and make
Main component of the present invention is the organonitrogen potassium that contains dextrose and biochemical fulvic acid, and suitable component index is: organonitrogen 〉=100g/L, organic potassium 〉=100g/L, biochemical fulvic acid 〉=40g/L, dextrose 〉=160g/L, auxiliary agent 〉=4g/L.Wherein, organonitrogen is in N, and organic potassium is with K
2O meter, biochemical fulvic acid is in HA, and dextrose is in organic matter, and auxiliary agent contains one or more of sodium nitrophenolate, amino acid, nucleic acid, Nafusaku, VITAMIN etc.
Newly build the strong grape experiment of think of garden at the Xi'an Baqiao District, adopt product of the present invention that the grapevine of swollen fruit phase has been carried out continuous three spraying tests, test-results proves: the organic nutrition of plant liquid of dextrose and preparation thereof is obvious to improving fruit sugar content, Vitamin C content and reducing the acid content effect, the adding of dextrose increases the activity intensity of plant materials endoenzyme, thereby metabolism is vigorous.Referring to accompanying drawing 2.
Newly build fixed point booth vegetable base in the Xi'an, adopt product of the present invention that the booth tomato has been carried out product and spray the toxin immunity test, spray observation in back 24 hours: find that the leaf roll phenomenon appears in tomato 2#, 3#, especially 3# is the most serious.Spray that the leaf roll phenomenon fades away after 3 days, restore normal growth, and spray the back leaf and turn green, big, thick, effect is remarkable, and especially the 3# growing way is best.The leaf roll phenomenon appears in 2#, 3#, and especially 3# is obvious, is because sodium nitrophenolate and the temporary transient murder by poisoning of these two kinds growths of naphthylacetic acid auxiliary agent initial stages appearance in the product.Carry out the spraying test second time after 10 days.It is serious to spray back 24 hours 3# leaf rolls, immediately 3# is handled afterwards, promptly sprays respectively with clear water, 4#, 5# respectively.Handle and observed in back 24 hours: 4# sprays at the experimental plot of 3# leaf roll piece leaf roll and disappears immediately; The 3# leaf roll ground leaf roll of fresh water spraying still part exists; 5# sprays 3# leaf roll remission effect not obvious.This phenomenon proves absolutely: dextrose is to the detoxicating functions of plant.The test sample composition is seen accompanying drawing 3.The present invention to the detoxifcation mechanism of plant is: the aldehyde radical in the dextrose molecule can reduce some toxicants, and a plurality of hydroxyls in its molecule can be with the esterification of toxicity acidic substance.
Evidence: dextrose to the plant foliage top dressing, has the effect of quick extra-nutrition, disease-resistant strong sprout and detoxifcation as the main component of plant nutrition liquid.
Claims (9)
1. Dextroglucose plants organic nutrient solution, the composition of its weight percent is:
(1) 19.7～35.2% water;
(2) 12～15% dextroses;
(3) 10～13% potassium hydroxide; Described potassium hydroxide is 〉=90% potassium hydroxide;
(4) 11～14% citric acids; Described citric acid is 99% citric acid;
(5) 7.5～20% biochemical fulvic acids; Described biochemical fulvic acid is 〉=30% biochemical fulvic acid;
(6) 18～22% urea;
(7) 0.2～0.4% auxiliary agents; Described auxiliary agent is selected from sodium nitrophenolate, amino acid, nucleic acid, Nafusaku or VITAMIN, or is selected from wherein two to four kinds mixture.
2. Dextroglucose plants organic nutrient solution according to claim 1 is characterized in that: the composition of its weight percent is:
(1) 19.7% water;
(2) 15% dextroses;
(3) 11～13% potassium hydroxide;
(4) 13% citric acids;
(5) 20% biochemical fulvic acids;
(6) 20% urea;
(7) 0.3% auxiliary agents.
3. Dextroglucose plants organic nutrient solution according to claim 1 and 2 is characterized in that: described dextrose is the technical grade dextrose; Described potassium hydroxide is 〉=90% industrial goods potassium hydroxide; Described citric acid is the food grade citric acid; Described biochemical fulvic acid is 〉=30% biochemical fulvic acid liquid.
4. technology of producing the described Dextroglucose plants organic nutrient solution of claim 1 may further comprise the steps:
(1) dissolving: water is added in the reactor, slowly add potassium hydroxide under stirring, solvent temperature is controlled at below 50 ℃:
(2) neutralization: slowly add citric acid, carry out neutralization reaction, temperature of reaction is controlled between 65～75 ℃, reacts 45～60 minutes, generates Tripotassium Citrate;
(3) mixed dissolution: when temperature is reduced to below 60 ℃, add urea, be stirred to dissolving;
(4) chelating: under the normal temperature, add biochemical fulvic acid liquid while stirring, chelatropic reaction 15 ± 5 minutes;
(5) dissolving: add dextrose, be stirred to dissolving;
(6) chelating: add the auxiliary agent chelatropic reaction, be stirred to dissolving, mixing gets finished product.
5. the production technique of Dextroglucose plants organic nutrient solution according to claim 4, it is characterized in that: the solvent temperature of described adding potassium hydroxide is controlled at below 50 ℃, is to control by the amount that control adds potassium hydroxide; The temperature of reaction of described adding citric acid is controlled at 65 ℃; During described adding urea, be when temperature is reduced to 50 ℃, to carry out; The chelatropic reaction time of described adding biochemical fulvic acid is 15 minutes; The stirring and dissolving time of described adding dextrose and auxiliary agent was respectively 15 minutes.
6. according to the production technique of claim 4 or 5 described Dextroglucose plants organic nutrient solutions, it is characterized in that: described finished product is after all raw material adds, and the restir reaction obtained in 45 minutes.
7. technology of producing the described Dextroglucose plants organic nutrient solution of claim 1 may further comprise the steps:
(1) dissolving: water is added in the reactor, slowly add potassium hydroxide under stirring, solvent temperature is controlled at below 50 ℃;
(2) neutralization: slowly add citric acid, carry out neutralization reaction, temperature of reaction is controlled between 65～75 ℃, reacts 45～60 minutes, generates Tripotassium Citrate;
(3) mixed dissolution: when temperature is reduced to below 60 ℃, add urea, be stirred to dissolving, get I solution;
(4) dissolving: water is added in the reactor, add the biochemical fulvic acid powder, be stirred to dissolving fully, get II solution;
(5) chelating: II solution is added in the I solution stirring and evenly mixing;
(6) dissolving: add dextrose, be stirred to dissolving;
(7) chelating: add auxiliary agent, be stirred to dissolving, mixing gets finished product.
8. the production technique of Dextroglucose plants organic nutrient solution according to claim 7, it is characterized in that: the solvent temperature of described adding potassium hydroxide is controlled at below 50 ℃, is to control by the amount that control adds potassium hydroxide; The temperature of reaction of described adding citric acid is controlled at 65 ℃; During described adding urea, be when temperature is reduced to 50 ℃, to carry out; The chelatropic reaction time of described adding biochemical fulvic acid is 15 minutes; The churning time that described II solution adds I solution is 15 minutes; The stirring and dissolving time of described adding dextrose and auxiliary agent was respectively 15 minutes.
9. according to the production technique of claim 7 or 8 described Dextroglucose plants organic nutrient solutions, it is characterized in that: described finished product is after all raw material adds, and the restir reaction obtained in 45 minutes.
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| CN107011156A (en) * | 2017-05-04 | 2017-08-04 | 江苏润普食品科技股份有限公司 | A kind of method of utilization citric acid and liquid potassium hydroxide synthesizing citric acid potassium |
| CN107286010A (en) * | 2017-07-27 | 2017-10-24 | 连云港树人科创食品添加剂有限公司 | A kind of preparation method of potassium citrate |
| CN107365201A (en) * | 2017-08-18 | 2017-11-21 | 苏州寿丰农业科技有限公司 | A kind of plant cultivation nutrient solution |
| CN112110762A (en) * | 2020-08-08 | 2020-12-22 | 河北玮祺农业发展科技有限公司 | Water-soluble fertilizer and production process thereof |
| CN112707760A (en) * | 2020-12-25 | 2021-04-27 | 刘柱 | Organic nutrition powder for promoting plant sweetening, coloring, yield increasing and disease resistance and preparation method thereof |
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| CN1196343A (en) * | 1997-04-17 | 1998-10-21 | 中国科学院化学研究所 | Compound plant nutrient solution and preparation method thereof |
| CN1305979A (en) * | 2001-02-23 | 2001-08-01 | 王镛先 | Composite leaf fertilizer and its preparing process |
| AU1836201A (en) * | 2000-02-08 | 2001-08-09 | Era Farming Company Pty Ltd, The | Biological fertiliser composition |
| CN1445202A (en) * | 2002-03-20 | 2003-10-01 | 王兴中 | Fertilizer for spraying on leaf surface with biologic raw materials as main material |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1196343A (en) * | 1997-04-17 | 1998-10-21 | 中国科学院化学研究所 | Compound plant nutrient solution and preparation method thereof |
| AU1836201A (en) * | 2000-02-08 | 2001-08-09 | Era Farming Company Pty Ltd, The | Biological fertiliser composition |
| CN1305979A (en) * | 2001-02-23 | 2001-08-01 | 王镛先 | Composite leaf fertilizer and its preparing process |
| CN1445202A (en) * | 2002-03-20 | 2003-10-01 | 王兴中 | Fertilizer for spraying on leaf surface with biologic raw materials as main material |
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