CN101298402B - Compound fertilizer and preparation thereof - Google Patents
Compound fertilizer and preparation thereof Download PDFInfo
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- CN101298402B CN101298402B CN2008101109843A CN200810110984A CN101298402B CN 101298402 B CN101298402 B CN 101298402B CN 2008101109843 A CN2008101109843 A CN 2008101109843A CN 200810110984 A CN200810110984 A CN 200810110984A CN 101298402 B CN101298402 B CN 101298402B
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- fertilizer
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- fulvic acid
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Abstract
The invention discloses a compound fertilizer and a preparation method thereof. The main effective component contents (weight percentage) of the compound fertilizer are as follows: 1.5 to 2.0 percent of BcFA, 20 to 25 percent of NPK, 8 to 10 percent of organic matters, 0.3 to 0.5 percent of NaHm and KHm as well as 0.3 percent of Sanmate. The compound fertilizer of the invention has the three effects of bio-fertilizer, bio-pesticide and bio-growth adjusting, being capable of reducing agriculture manufacture cost, increasing crop output and playing the roles of slow release and decomposing residual to the pesticide.
Description
Technical field
The present invention relates to a kind of agricultural fertilizer, specifically relate to a kind of compound manure of biochemical fulvic acid and preparation method thereof.
Background technology
Xanthohumic acid (FA) is a kind of component in the humic acids (HA), accounts for about 5%.It is to be extracted and form through High Temperature High Pressure, strong acid and strong base by peat, low-calorie coal.(Biotechnology Fulvic Acid, be called for short BFA), be the material of a kind of class sapropelitic xanthohumic acid of producing with biotechnology of developing in recent years, contain organonitrogen phosphorus potassium (NPK) than GOOD TASTE, poly-basic organic acid, abundant nucleic acid, vitamin B group, vitamins C, inositol, trace element, amino acid and the active unknown factor.Humic acids or xanthohumic acid that it can replace extracting from coal are used for base manure, foliage fertilizer, have biological farming fertilizer, biological pesticide, biological growth adjusting three efficacy.
Traditional base manure mostly is inorganic chemical fertilizer greatly, and nitrogenous phosphorus potassium applies that nitrogen is easy to volatilization behind the soil in these fertilizer, and phosphorus potassium element is fixed, plant absorbing utilization only 20～30%, increase fertilizer amount after, peasant's production cost increases.
Summary of the invention
Technical problem to be solved by this invention provides a kind of compound manure that has biological farming fertilizer, biological pesticide, biological growth adjusting effect, can use chemical fertilizer, agricultural chemicals no longer separately, this compound manure can reduce agriculture production cost, increase crop yield, agricultural chemicals is had slowly-releasing and degrade residual function.
Compound manure of the present invention mainly contains effective component content following (weight percent):
The content of described biochemical fulvic acid is preferably 1.5%; The content of described nitrogen phosphorus potassium is preferably 25%.
Described organic matter is careless carbon.
The preparation process of making the liquid composite fertilizer of compound manure of the present invention is:
A. carry out proportioning according to following weight: 1000 kilograms in water, biochemical fulvic acid content are 15% 280 kilograms of the thick tail powders of biochemical fulvic acid, 220 kilograms in urea, 160 kilograms of monoammonium phosphates, 180 kilograms of vitriolate of tartar, 300 kilograms of natural pond liquid, 3 kilograms of derosal, 12.5 kilograms of Sodium salts humic acidss, 12.5 kilograms of potassium humates;
B. the thick tail powder of biochemical fulvic acid is thrown in 65 ℃ water, to soak and carried out the melt cinder separation after 48 hours, after separation, add good urea, monoammonium phosphate, vitriolate of tartar, derosal, Sodium salts humic acids and the potassium humate mixing stirring of proportioning in the liquid of gained and promptly get liquid composite fertilizer.
The preparation process of making the solid-state composite fertilizer of compound manure of the present invention is:
A. carry out proportioning according to following weight: 3 kilograms of derosal, 300 kilograms of five water calcium superphosphate, 80 kilograms in bicarbonate of ammonia, biochemical fulvic acid content are 15% 225 kilograms of the thick tail powders of biochemical fulvic acid, 160 kilograms in urea, monoammonium phosphate 120 kg, 90 kilograms of vitriolate of tartar, 60 kilograms in careless carbon, 12.5 kilograms of Sodium salts humic acidss, 12.5 kilograms of potassium humates;
B. after the five water calcium superphosphate that a proportioning is good set by step being mixed stirring with bicarbonate of ammonia, promptly get powdery composite fertilizer again with after the proportioning good thick tail powder of biochemical fulvic acid, urea, monoammonium phosphate, vitriolate of tartar, careless carbon, derosal, Sodium salts humic acids and the potassium humate mixing stirring.
Gained slag charge when further, the thick tail powder of biochemical fulvic acid of making powdery composite fertilizer carries out the melt cinder separation for making in the liquid composite fertilizer process.
Biochemical fulvic acid is a fertilizer synergistic agent, include plant-growth needed almost all amino acid, nitrogen, phosphorus, potassium, trace element, VITAMIN and multiple enzyme, carbohydrate, and material such as nucleic acid, but the needed nitrogen of one season crop, phosphorus, potassium content is often not enough.The present invention has done hundreds of time tests to the ratio of the required nitrogen phosphorus potassium of all kinds of crops, adjusts for hundreds of times, has finally determined the ratio of the azophoska of adding, to replenish the demand of crop.
Biochemical fulvic acid is a pesticide synergistic agent, and the present invention forms mixture by adding the fungicide carbendazim of absorption in the high-efficiency low-toxicity with biochemical fulvic acid.This mixture is by strengthening growing way and the resistance against diseases of plant self, and the change of the permeation of pair cell and to the slowly-releasing and the synergistic function of agricultural chemicals, the sick worm of various plants is all demonstrated good preventive and therapeutic effect, and not only sterilization is disease-resistant, separates remains of pesticide but also release.This mixture can be saved pesticide dosage 1/2～2/3 to slowly-releasing, synergy and the degrade residual function of agricultural chemicals, improves drug effect more than 50%, and the farm crop economic characters are improved, and quality improves, remarkable in economical benefits.
Growth regulator belongs to the hormone category, but biochemical fulvic acid does not contain any hormone, and various plants yield stimulant such as its effect and growth hormone, phytokinin, dormin are similar, and growth and development of plant is played comprehensive adjusting control action kou, promotes growth; It does not belong to the meta-bolites of plant yet, does not participate in metabolic process directly yet, but quickens the metabolism of multiple material in the plant materials by the promoter action that pair cell is breathed.
Embodiment below in conjunction with embodiment is described in further detail the present invention, but this should be interpreted as that the scope of the above-mentioned theme of the present invention only limits to following embodiment.Do not breaking away under the above-mentioned technological thought situation of the present invention, various replacements or change according to ordinary skill knowledge and customary means are made include within the scope of the invention.
Embodiment
Embodiment one
280 kilograms of thick tail powders of biochemical fulvic acid (biochemical fulvic acid content is 15%) are soaked in 65 ℃ 1000 kilograms water carry out melt cinder after 48 hours and separate, in liquid, add 220 kilograms in urea, 160 kilograms of monoammonium phosphates, 180 kilograms of vitriolate of tartar, 300 kilograms of natural pond liquid, 3 kilograms of derosal, 12.5 kilograms of Sodium salts humic acidss, potassium humate mixes stirring for 12.5 kilograms and promptly gets liquid composite fertilizer, and this liquid state composite fertilizer mesophytization xanthohumic acid content is about 2.0%.
With 300 kilograms of five water calcium superphosphate mix with 80 kilograms in bicarbonate of ammonia stir after, be 90 kilograms of 15% 225 kilograms of the thick tail powders of biochemical fulvic acid, 160 kilograms in urea, monoammonium phosphate 120 kg, vitriolate of tartar with biochemical fulvic acid content again, 60 kilograms in grass carbon, 3 kilograms of derosal, after mixing stirring, 12.5 kilograms of Sodium salts humic acidss, 12.5 kilograms of potassium humates promptly get powdery composite fertilizer.
Embodiment two
200 kilograms of thick tail powders of biochemical fulvic acid (biochemical fulvic acid content is 15%) are soaked in 65 ℃ 1000 kilograms water carry out melt cinder after 48 hours and separate, in liquid, add 180 kilograms in urea, 140 kilograms of monoammonium phosphates, 140 kilograms of vitriolate of tartar, 300 kilograms of natural pond liquid, 3 kilograms of derosal, 12.5 kilograms of Sodium salts humic acidss, potassium humate mixes stirring for 12.5 kilograms and promptly gets liquid composite fertilizer, and the liquid composite fertilizer of gained mesophytization xanthohumic acid content is for being about 1.5%.
With 300 kilograms of five water calcium superphosphate mix with 80 kilograms in bicarbonate of ammonia stir after, be 15% the thick tail powder of biochemical fulvic acid 120 kg, 180 kilograms in urea, 140 kilograms of monoammonium phosphates, 140 kilograms of vitriolate of tartar again with biochemical fulvic acid content, 60 kilograms in grass carbon, 3 kilograms of derosal, after mixing stirring, 12.5 kilograms of Sodium salts humic acidss, 12.5 kilograms of potassium humates promptly get powdery composite fertilizer.
Embodiment three
225 kilograms of thick tail powders of biochemical fulvic acid (biochemical fulvic acid content is 15%) are soaked in 65 ℃ 1000 kilograms water carry out melt cinder after 48 hours and separate, in liquid, add 190 kilograms in urea, 140 kilograms of monoammonium phosphates, 150 kilograms of vitriolate of tartar, 300 kilograms of natural pond liquid, 3 kilograms of derosal, 12.5 kilograms of Sodium salts humic acidss, potassium humate mixes stirring for 12.5 kilograms and promptly gets liquid composite fertilizer, and the liquid composite fertilizer of gained mesophytization xanthohumic acid content is about 1.75%.
With 300 kilograms of five water calcium superphosphate mix with 80 kilograms in bicarbonate of ammonia stir after, be 15% 130 kilograms of the thick tail powders of biochemical fulvic acid, 200 kilograms in urea, 150 kilograms of monoammonium phosphates, 160 kilograms of vitriolate of tartar again with biochemical fulvic acid content, 60 kilograms in grass carbon, 3 kilograms of derosal, after mixing stirring, 12.5 kilograms of Sodium salts humic acidss, 12.5 kilograms of potassium humates promptly get powdery composite fertilizer.
The test situation that the present invention is used for production practice:
One, compound manure of the present invention is carried out manure trial at fruit tree pears, loquat, grape
1. test fertilizer type: compound manure of the present invention, conventional fertilizer
2. basic condition experimental field: four groups of test arrangements in Longquanyi District Xing Long town Qi dragon village
2.1 the grape experiment kind is huge peak, householder Wang Zhi China, and 0.9 mu of area, belongs to the tree that bears fruit that grows up at 5 years field planting time;
2.2 pear tree test kind is an abundance of water, 0.8 mu of area, householder Wang Zhi China, 6 years field planting time;
2.3 loquat test kind is big five-pointed star, 1.3 mu of areas, and 4 years field planting time, the householder is for plain English.
More than three field pieces cultivations all adopt the high railway carriage or compartment of the common zanjon of local area mode, pear tree, loquat mu is planted 110 strains, grape mu is planted about 400 strains, it is medium that level of management belong to the whole district.
3. mode is handled and method: adopt with field simultaneous test mode, each Tree Species Selection is representative, 1 of the field piece of growth basically identical, pears and grape experiment are with compound manure bulk application of the present invention once, spray foliage fertilizer 2 times, loquat sprays foliage fertilizer (because of test time missed base manure time of application).Time and consumption that the contrast part uses conventional fertilizer to use by peasant household's custom carry out.
4. fertilization time and consumption
4.1 compound manure base manure is determined amount of application according to tree vigo(u)r, the age of tree, the pears strain is executed 0.5 kilogram, and the grape strain is executed 0.15 kilogram, before fertilization time is rudiment; The foliage fertilizer time of spraying is the best fruiting period, sprays 7～10 days pitch times twice
4.2 contrast fertilization time and rate of fertilizer application: from the Spring Festival to fruit picking, pear tree fertilising 3 times, 0.5 kilogram in urea is executed in average every strain, 2 kilograms in phosphate fertilizer (calcium superphosphate), 0.5 kilogram in bicarbonate of ammonia, 2 kilograms of compound potassium sulfate fertilizers, 0.25 kilogram of potassium primary phosphate, 0.08 kilogram of luxuriant green rich board foliage fertilizer 5 times; Grape 3 times, 0.15 kilogram in urea is executed in average every strain, 0.75 kilogram in phosphate fertilizer (calcium superphosphate), 0.25 kilogram in bicarbonate of ammonia, 0.4 kilogram of compound potassium sulfate fertilizer, 0.025 kilogram of potassium primary phosphate, 0.02 kilogram of luxuriant green rich board foliage fertilizer 3 times; Loquat sprays once luxuriant green rich board foliage fertilizer.
5. investigation content and method
According to different tests, take the content of different investigation methods.Each is handled and respectively selects 10 strains as the fixed point investigation.
The loquat test: time on-test is fruit expanding period, only executes foliage fertilizer, and investigation content is loquat fallen leaves number, takes out and send out the young sprout number of blade;
The pear tree test: the investigation pears fruit number, the young sprout number of blade, mean fruit weight;
Grape experiment: investigation is taken out and is sent out a branch amount, leaf area, fruit ear and the amount of giving birth to; Measure heavy, the soluble solid of its fruit single (fringe) during fruit maturation.
6. test-results
Can promote young sprout to take out to send out that showing as young sprout, to take out the speed of sending out fast, many, long behind this fertilizer 6.1 use, blade is many and the leaf look dark green, and loquat, the comparison of pears young sprout blade be according to increase by 4.3～5.0 leaves, 1 of grape branch increase.
6.2 promote blade to increase, leaf area strengthens, and photosynthesis is strengthened, dry-matter accumulation increases, and the comparison of grape leaf area is according to increasing by 48.09 square centimeters.
6.3 prolong the leaf growth phase, postpone leaf senile, keep the healthy and strong growth of tree body, the comparison of loquat individual plant fallen leaves according to few 12.3 leaves.
6.4 the tree bulk-growth is coordinated, and is balanced in nutrition, really increases, and the pear tree individual plant really comparison according to increasing by 22.5, and the comparison of grape individual plant flower fringe is according to many 4 fringes.
6.5 raising output promotes to increase income.Use loquat, pears, the grape single fruit (fringe) of this fertilizer to compare heavily respectively according to increasing by 6.9 grams, amplification is respectively 10.55%, 46.67% and 12.16%.Stay under the situation of fruit number in existing cultivation technique control, can improve output, thereby make Increase Income of Peasant Households.
6.6 soluble solid matter increases, and has improved quality.Pears solid substance matter improves 2 percentage points; Grape solid substance matter improves 0.8 percentage point, has improved fruit quality and local flavor.
Detailed results is seen attached list.
6.7 saving cost.According to test market price in period, pear tree experimental control part mu is thrown 698 yuan of fertilizer costs, and compound manure mu drops into 445 yuan, and comparison is according to saving 253 yuan of costs.
7. conclusion
By test, confirmed that this fertilizer has security and good result in grape, pear tree, loquat etc. fruit tree, can promote bud differentiation, young sprout is taken out and is sent out neatly, is improving the fruit rate, strengthens the plant resistance, improves fruit quality, improves commodity.Therefore, popularizations of can in suitable zone, demonstrating of this fertilizer, the suggestion consumption, the fruit tree pears of growing up, loquat are executed 0.5～1 kilogram according to how many strains of staying fruit to measure, and the grape strain is executed 0.1～0.2 kilogram.
Compound manure pilot survey table
Two, with compound manure of the present invention on vegetables
Demonstrate on pumpkin, cucumber, wild cabbage, radish vegetables, test equates with fertile cost with conventional cultivation with fertile cost design.Radish mu is thrown 190 yuan of compound manure valencys of the present invention, and plant strain growth is good, and blade is light green, and drought-resistant ability is strong; Cucumber mu is thrown 260 yuan in compound manure, the plant strain growth stalwartness, and upright blade is light green, and drought resistance is strong, and precocious 3～5 days, fruit bar shaped and quality made moderate progress; Pumpkin mu is thrown 165 yuan in compound manure, the tendril stalwartness, and leaf is light green, and drought-resistant ability is strong, and fruit marketability is good, meat powder, sweet, ripening stage basically identical; Wild cabbage mu is thrown 260 yuan, and the leaf look light green, robust growth.
Three, investigate compound manure degrading pesticide residues function of the present invention
Beijing area tomato, romaine lettuce test nitrate content test result show, after executing behind the compound manure of the present invention 160 kilograms of significantly low five water calcium superphosphate of nitrate average content and mixing stirring with 80 kilograms in bicarbonate of ammonia, be 15% 280 kilograms of the thick tail powders of biochemical fulvic acid, 220 kilograms in urea, 160 kilograms of monoammonium phosphates, 180 kilograms of vitriolate of tartar again with biochemical fulvic acid content, 60 kilograms in grass carbon, 3 kilograms of derosal, after mixing stirring, 12.5 kilograms of Sodium salts humic acidss, 12.5 kilograms of potassium humates promptly get powdery composite fertilizer.In waiting nutrient chemical fertilizer disposition, wherein, the tomato nitrate content reduces by 9.5%, and romaine lettuce reduces by 8.1%.
The nitrate average content of using compound manure processing of the present invention in the Chinese cabbage test of Shandong is 416.6mg/kg, and the average content of using chemical fertilizer is 764.6mg/kg.
Four, the compound manure of the present invention effect of improving the soil
Experiment and demonstration data according to Beijing, Shandong, use compound manure of the present invention and improved the soil organism, full nitrogen and available phosphorus content, respectively handling the soil analysis result before Tongzhou District, Beijing tomato test results shows, the soil organism that compound manure of the present invention is handled, full nitrogen and available phosphorus be respectively 1.34%, O.106% and 82.4mg/kg, then be respectively 1.16%, 0.087% and 78.3mg/kg Deng what the nutrient chemical fertilizer was handled, three indexs all are higher than to use and wait the processing of nutrient chemical fertilizer.
Five, the effect of compound manure foliage fertilizer of the present invention aspect the control soybean cyst nematode
Heilongjiang Province's soy bean test shows that the soybean per plant cyst roundworm number that does not use successive planting agent to handle is 5.3, and the nematode number of dressing seed with compound manure of the present invention is 1.7.
Six, compound manure foliage fertilizer of the present invention is to the effect of cotton wilt
2 field tests of Shandong Dongying show that the cotton wilt sickness rate of foliage-spray compound manure of the present invention is respectively 2.4% and 0, and the rate of delivering that the spray clear water is handled is respectively 8.7% and 8.1%; 2 demonstration pilot projects in Woyang, Anhui also show same result, model field and contrast field occurring degree significant difference.
Claims (4)
1. a compound manure is characterized in that, the main effective constituent of described compound manure by weight percentage, content is as follows:
2. a kind of compound manure according to claim 1 is characterized in that, the content of described biochemical fulvic acid is 1.5%.
3. a kind of compound manure according to claim 1 is characterized in that, the content of described nitrogen phosphorus potassium is 25%.
4. according to claim 1 or 2 or 3 described a kind of compound manure, it is characterized in that described organic matter is careless carbon.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008101109843A CN101298402B (en) | 2007-07-30 | 2008-06-19 | Compound fertilizer and preparation thereof |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2007100924936A CN101125778A (en) | 2007-07-30 | 2007-07-30 | Composite fertilizer |
| CN200710092493.6 | 2007-07-30 | ||
| CN2008101109843A CN101298402B (en) | 2007-07-30 | 2008-06-19 | Compound fertilizer and preparation thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101298402A CN101298402A (en) | 2008-11-05 |
| CN101298402B true CN101298402B (en) | 2011-10-26 |
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Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
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| CNA2007100924936A Pending CN101125778A (en) | 2007-07-30 | 2007-07-30 | Composite fertilizer |
| CN2008101109843A Expired - Fee Related CN101298402B (en) | 2007-07-30 | 2008-06-19 | Compound fertilizer and preparation thereof |
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| Application Number | Title | Priority Date | Filing Date |
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| CNA2007100924936A Pending CN101125778A (en) | 2007-07-30 | 2007-07-30 | Composite fertilizer |
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Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101125778A (en) * | 2007-07-30 | 2008-02-20 | 罗安明 | Composite fertilizer |
| CN102531742B (en) * | 2010-12-31 | 2014-04-16 | 郭宗华 | Liquid fertilizer and preparation method thereof |
| CN102295487B (en) * | 2011-03-11 | 2013-07-10 | 山东远东国际生物化工股份有限公司 | Organic enveloped controlled-release compound fertilizer and preparation method thereof |
| CN103539564B (en) * | 2013-10-30 | 2015-03-18 | 孟树胜 | Seedling raising fertilizer |
| CN103708978B (en) * | 2013-12-25 | 2016-07-13 | 广西农战士高工效农业技术有限公司 | A kind of organic-inorganic pestsides synthesis sustained-controll-release fertiliser |
| CN103664409A (en) * | 2013-12-26 | 2014-03-26 | 黄蓉华 | Special fertilizer for grape |
| CN104447108B (en) * | 2014-11-21 | 2017-06-27 | 新疆慧尔农业集团股份有限公司 | A kind of humic acid drip irrigation special fertilizer and preparation method thereof |
| CN106699385A (en) * | 2016-12-28 | 2017-05-24 | 郑州阿波罗肥业有限公司 | Manntiol-Ca- and biochemical fulvic acid-containing special fertilizer for drought-resistant grape |
| CN113416105A (en) * | 2021-06-28 | 2021-09-21 | 华强化工集团股份有限公司 | Water-soluble fertilizer for increasing yield of cabbages and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1535938A (en) * | 2003-04-08 | 2004-10-13 | 上海中林生物技术有限公司 | Bio-chemical activity humic acid organic fertilizer |
| CN1853481A (en) * | 2005-04-27 | 2006-11-01 | 王国刚 | Compound chemcial reagent for preventing and treating cotton blight and use thereof |
| CN101125778A (en) * | 2007-07-30 | 2008-02-20 | 罗安明 | Composite fertilizer |
-
2007
- 2007-07-30 CN CNA2007100924936A patent/CN101125778A/en active Pending
-
2008
- 2008-06-19 CN CN2008101109843A patent/CN101298402B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1535938A (en) * | 2003-04-08 | 2004-10-13 | 上海中林生物技术有限公司 | Bio-chemical activity humic acid organic fertilizer |
| CN1853481A (en) * | 2005-04-27 | 2006-11-01 | 王国刚 | Compound chemcial reagent for preventing and treating cotton blight and use thereof |
| CN101125778A (en) * | 2007-07-30 | 2008-02-20 | 罗安明 | Composite fertilizer |
Non-Patent Citations (1)
| Title |
|---|
| 李善祥.腐植酸类物质与农药——研究应用与展望.《腐植酸》.2002,(第2期),17－25. * |
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| CN101125778A (en) | 2008-02-20 |
| CN101298402A (en) | 2008-11-05 |
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Assignee: Anhui Mengteer Fertilizer Industry Co., Ltd. Assignor: Luo Anming Contract record no.: 2012500000018 Denomination of invention: Compound fertilizer and preparation thereof Granted publication date: 20111026 License type: Exclusive License Open date: 20081105 Record date: 20120409 |
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