CN103922832A - Water-soluble fertilizer containing humic acid and production process of water-soluble fertilizer - Google Patents

Water-soluble fertilizer containing humic acid and production process of water-soluble fertilizer Download PDF

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Publication number
CN103922832A
CN103922832A CN201410191255.0A CN201410191255A CN103922832A CN 103922832 A CN103922832 A CN 103922832A CN 201410191255 A CN201410191255 A CN 201410191255A CN 103922832 A CN103922832 A CN 103922832A
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China
Prior art keywords
water
humic acid
parts
soluble fertilizer
macroelement
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Pending
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CN201410191255.0A
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Chinese (zh)
Inventor
朱春雷
秦彬彬
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JIANGSU GUYI AGRICULTURAL SCIENCE AND TECHNOLOGY Co Ltd
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JIANGSU GUYI AGRICULTURAL SCIENCE AND TECHNOLOGY Co Ltd
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Priority to CN201410191255.0A priority Critical patent/CN103922832A/en
Publication of CN103922832A publication Critical patent/CN103922832A/en
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Abstract

The invention discloses a water-soluble fertilizer containing humic acid. The fertilizer comprises, by weight, 75-80 parts of potassium humate powder, 70-75 parts of urea, 96.5-100 parts of monopotassium phosphate, 130-135 parts of potassium nitrate and the balance water. A production process includes the steps that solutions are mixed after pH values and temperatures of the material solutions are adjusted to be approximate, reaction time is about one hour, sampling and analysis are carried out, after the product is verified to be qualified, the product is led into a settling tank through an injection pump and stays in the settling tank for 48 hours, sampling is carried out again, and a supernatant is packaged and put in storage after being verified to be qualified. The water-soluble fertilizer containing the humic acid can quickly supplement a large number of elements and the humic acid necessary to crops, promotes fertilizer absorption, utilization and transformation, enhances photosynthesis, promotes the crops to grow and develop, enhances resistance of the crops, improves the yield of the crops, improves quality of agricultural products and facilitates yield increase and income increase.

Description

Containing humic acid water-soluble fertilizer and production technique thereof
Technical field
The present invention relates to a kind of humic acid water-soluble fertilizer and production technique thereof of containing, be applicable to rice and wheat, beans, greengrocery, fruits, greenweed, nursery stock class etc.
Background technology
Fertilizer is the direct or indirect supply body of the required nutrient of plant growth, has improvement soil property, improves the function of crop yield and quality.But common fertilizer can not be dissolved in the water completely, can not directly be absorbed by the root system of crop and blade face, effective specific absorption of crop is low, and fertilizer efficiency is slow.A large amount of or the excessive chemical fertilizer of using, not only cause soil fertility utilization ratio low, nutrient is unbalanced, soil compaction, the problems such as soil microbial community is unbalance, and causing the series of environmental problems such as environmental pollution, nutrition accumulation, the loss that chemical fertilizer brings aspect environmental pollution is in recent years up to 1,000 hundred million yuan.
Summary of the invention
The object of the invention is in order to overcome above deficiency, provide a kind of containing humic acid water-soluble fertilizer and production technique thereof, this fertilizer contains n p k nutrition element and humic acids.Humic acids has multiple functional group, can be combined with many kinds of substance, has good biological activity, can play the effect of tensio-active agent.The surface tension of its metal-salt of humic acids is lower than the surface tension of water, and humic acids and applicable agriculture chemical compounding, can play and strengthen drug effect and fall hypotoxic effect, to agricultural chemicals, can produce obvious dispersion and emulsifying effectiveness, improves the dissolving power of solubility agricultural chemicals.Apply after this fertilizer, can promote fertilizer absorb, utilize and transform, promote crop growth, strengthen crop anti-adversity energy, improve crop yield, improve agricultural product quality, be conducive to increasing both production and income.
The present invention is achieved through the following technical solutions: a kind of containing humic acid water-soluble fertilizer, the raw material that it comprises following weight part: potassium fulvate powder: 75-80 part, urea: 70-75 part, potassium primary phosphate: 96.5-100 part, saltpetre: 130-135 part, all the other are water.
Containing humic acid water-soluble fertilizer, specifically comprise the following raw material of preparation by weight percentage: potassium fulvate powder: 77 parts, urea: 71 parts, potassium primary phosphate: 96.5 parts, saltpetre: 135 parts, all the other are water.
Contain macroelement and humic acids containing humic acid water-soluble fertilizer, wherein macroelement comprises nitrogen, phosphorus, potassium, content>=50g/L of N wherein, P 2o 5content>=50g/L, K 2content>=100g/L of O, content>=30 g/L of humic acids.
A production technique containing humic acid water-soluble fertilizer, comprises the steps:
(A), preparation composite humic acid solution: be stored in after compound potassium fulvate powder in feed bin measures by gauger and be discharged in reactor, in mixing tank, there are agitator and electrical heated pipings, the water that adds the spinner-type flowmeter of flowing through, 77 parts, potassium fulvate powder, 77 parts, water, pass into electrically heated mix and blend and dissolve, be made into the humic acid solution of w (N) 20%~23%, whipping temp is 60-70 ℃;
(B), preparation macroelement saturated solution: be stored in after chelated iron in feed bin measures by gauger and be discharged in reactor, add water, 71 parts, urea, potassium primary phosphate: 96.5 parts, saltpetre: 135 parts, water, 302.5 part, pass into electrically heated mix and blend and dissolve, be made into macroelement saturated solution, whipping temp is 60-70 ℃;
(C) composite humic acid solution, macroelement saturated solution that, first two steps prepare are sent in end reaction still by water pump, passing into electrically heated mix and blend dissolves, at approximately 1 hour chelatropic reaction of 70-80 ℃ of process, finally add through metering water in tempering tank, wherein the mass ratio of composite humic acid solution, macroelement saturated solution, water is: 0.56:2.19:7.25, what make mixes the water-soluble fertilizer of liquid composite humic acid macroelement, with squirt pump, import slurry tank after 48 hours, resampling detects qualified rear supernatant liquor packing warehouse-in.
The present invention compared with prior art has the following advantages: contain humic acid water-soluble fertilizer (macroelement type): via blade face epidermis, infiltrate or directly absorption of root fertilising, participate in protein synthesis, promote plant growth, middle without transforming waste, fertilizer efficiency is fast, promote chlorophyll synthetic, strengthen photosynthesis, the symptoms such as " unreal, leaflet, flat grain, deformities " that effectively control causes because of boron deficiency zinc, nontoxic, be green food, pollution-free vegetable, the ideal of Organic farming is with fertile;
Used containing after humic acid water-soluble fertilizer and had advantages of:
(1), promote growth, early flowering: to germinateing, yield positive results, have the magical effect of catalysis, the plump gloss of newborn branches and leaves increases disease drag, and branch bar is strong;
(2), quality-improving, ahead of time harvest: thoroughly improve fruit quality, the fruit sugar of forming is part high, sweet close good to eat, and the loose full fragrant attractive in appearance of fruit type is ripe ahead of time more than 14 days;
(3), disease and insect resistance, improve product: newborn branches and leaves are plump, gloss, and disease and pest drag is increased; Branch bar is strong, tall and straight, grows vigorous, enhances metabolism and extends the age of tree, can prevent shedding, malformed fruit, and the amount of gathering is increased to the growth limit.
embodiment:
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, and this embodiment only, for explaining the present invention, does not form limiting the scope of the present invention.
Containing a humic acid water-soluble fertilizer, the raw material that it comprises following weight part: potassium fulvate powder: 75-80 part, urea: 70-75 part, potassium primary phosphate: 96.5-100 part, saltpetre: 130-135 part, all the other are water.
Containing humic acid water-soluble fertilizer, specifically comprise the following raw material of preparation by weight percentage: potassium fulvate powder: 77 parts, urea: 71 parts, potassium primary phosphate: 96.5 parts, saltpetre: 135 parts, all the other are water.
Contain macroelement and humic acids containing humic acid water-soluble fertilizer, wherein macroelement comprises nitrogen, phosphorus, potassium, content>=50g/L of N wherein, P 2o 5content>=50g/L, K 2content>=100g/L of O, content>=30 g/L of humic acids.
A production technique containing humic acid water-soluble fertilizer, comprises the steps:
(A), preparation composite humic acid solution: be stored in after compound potassium fulvate powder in feed bin measures by gauger and be discharged in reactor, in mixing tank, there are agitator and electrical heated pipings, the water that adds the spinner-type flowmeter of flowing through, 77 parts, potassium fulvate powder, 77 parts, water, pass into electrically heated mix and blend and dissolve, be made into the humic acid solution of w (N) 20%~23%, whipping temp is 60-70 ℃;
(B), preparation macroelement saturated solution: be stored in after chelated iron in feed bin measures by gauger and be discharged in reactor, add water, 71 parts, urea, potassium primary phosphate: 96.5 parts, saltpetre: 135 parts, water, 302.5 part, pass into electrically heated mix and blend and dissolve, be made into macroelement saturated solution, whipping temp is 60-70 ℃;
(C) composite humic acid solution, macroelement saturated solution that, first two steps prepare are sent in end reaction still by water pump, passing into electrically heated mix and blend dissolves, at approximately 1 hour chelatropic reaction of 70-80 ℃ of process, finally add through metering water in tempering tank, wherein the mass ratio of composite humic acid solution, macroelement saturated solution, water is: 0.56:2.19:7.25, what make mixes the water-soluble fertilizer of liquid composite humic acid macroelement, with squirt pump, import slurry tank after 48 hours, resampling detects qualified rear supernatant liquor packing warehouse-in.
Total mixing time of material is 1.5-2h, separate unit reactor throughput >2. 5t/h, and yearly capacity can reach 3000-5000 ton.
Main production equipments is as following table:
Production unit Specification Quantity
Coal firing boiler (electrostatic precipitation) 5 cubes 1
High-level storage groove (feed bin) 1 cube 6
Gauger 0.2 kilogram of precision 6
Jet pump ? 4
Spinner-type flowmeter 5 liters/min 6
Enamel reaction still (mixing tank) 5000L 4
Stainless steel slurry tank 5000L 2
Platform scale, electronic scale 100 kilograms, 3 kilograms Each 2
Liquid-filling machine 5-1000 milliliter A set of
Code jetting device ? 1
Case sealer ? 1
Using method containing humic acid water-soluble fertilizer: spray: in plant growths optimum period (tillering phase, jointing stage, boot stage, filling stage) such as paddy rice, wheats, be watered dilution 500-800 and doubly carry out foliage-spray, can spray 2-3 time the time of infertility, spray 10-15 day/time interval, can suitably adjust extension rate according to crop different growing and growth of cereal crop seedlings quality; Drip irrigation: be watered dilution 500-800 in plant growth optimum period and doubly carry out drip irrigation, the amount that need to supplement according to crop during drip irrigation and the amount that can bear are used, general each mu 40ml.During use, avoid mixed with strong basicity agricultural chemicals and other fertilizer; Be stored in cool place, dry, ventilation; The time that sprays generally carries out before fine day 10:00 or after 16:00, should not use at noon or under hot conditions; Spray rear chance rain drop erosion, should respray to mend and execute; Within the quality guaranteed period, (certainly produce from 24 months) used, and as placed, the long period (still within the quality guaranteed period) produces muddiness or crystal is separated out, and after should shaking up, is watered and sprays; According to the principle of crop regulation of fertilizer requirement and fertilization compositions based on earth measurement, under local agrotechnique department instructs because soil is used because of climate science because of seedling.

Claims (4)

1. containing a humic acid water-soluble fertilizer, it is characterized in that: the raw material that it comprises following weight part: potassium fulvate powder: 75-80 part, urea: 70-75 part, potassium primary phosphate: 96.5-100 part, saltpetre: 130-135 part, all the other are water.
2. according to claim 1 containing humic acid water-soluble fertilizer, it is characterized in that: it comprises the following raw material of preparation by weight percentage: potassium fulvate powder: 77 parts, urea: 71 parts, potassium primary phosphate: 96.5 parts, saltpetre: 135 parts, all the other are water.
3. according to claim 1 containing humic acid water-soluble fertilizer, it is characterized in that: it contains macroelement and humic acids, wherein macroelement comprises nitrogen, phosphorus, potassium, content>=50g/L of N wherein, P 2o 5content>=50g/L, K 2content>=100g/L of O, content>=30 g/L of humic acids.
4. containing a production technique for humic acid water-soluble fertilizer, it is characterized in that: comprise the steps:
(A), preparation composite humic acid solution: be stored in after compound potassium fulvate powder in feed bin measures by gauger and be discharged in reactor, in mixing tank, there are agitator and electrical heated pipings, the water that adds the spinner-type flowmeter of flowing through, 77 parts, potassium fulvate powder, 77 parts, water, pass into electrically heated mix and blend and dissolve, be made into the humic acid solution of w (N) 20%~23%, whipping temp is 60-70 ℃;
(B), preparation macroelement saturated solution: be stored in after chelated iron in feed bin measures by gauger and be discharged in reactor, add water, 71 parts, urea, potassium primary phosphate: 96.5 parts, saltpetre: 135 parts, water, 302.5 part, pass into electrically heated mix and blend and dissolve, be made into macroelement saturated solution, whipping temp is 60-70 ℃;
(C) composite humic acid solution, macroelement saturated solution that, first two steps prepare are sent in end reaction still by water pump, passing into electrically heated mix and blend dissolves, at approximately 1 hour chelatropic reaction of 70-80 ℃ of process, finally add through metering water in tempering tank, wherein the mass ratio of composite humic acid solution, macroelement saturated solution, water is: 0.56:2.19:7.25, what make mixes the water-soluble fertilizer of liquid composite humic acid macroelement, with squirt pump, import slurry tank after 48 hours, resampling detects qualified rear supernatant liquor packing warehouse-in.
CN201410191255.0A 2014-05-08 2014-05-08 Water-soluble fertilizer containing humic acid and production process of water-soluble fertilizer Pending CN103922832A (en)

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Cited By (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104193460A (en) * 2014-08-22 2014-12-10 江苏谷熠农业科技有限公司 Water-soluble fertilizer containing major elements and production technique thereof
CN104402652A (en) * 2014-11-20 2015-03-11 柳州市源晨农副产品有限公司 Special fertilizer for grape culture
CN104788176A (en) * 2015-03-30 2015-07-22 安徽金农生态农业科技发展有限公司 Water-soluble quick-acting drip irrigation fertilizer
CN105110861A (en) * 2015-08-07 2015-12-02 安徽省文胜生物工程股份有限公司 Water-soluble organic-inorganic compounded fertilizer and preparation method therefor
CN105130676A (en) * 2015-07-03 2015-12-09 河南晋开化工投资控股集团有限责任公司 Liquid fertilizer for resisting drought and preserving moisture and fertility and preparation method thereof
CN105315059A (en) * 2014-07-31 2016-02-10 陕西扬晨新材料科技有限公司 Humic acid containing water-soluble fertilizer and preparation method therefor
CN105837330A (en) * 2016-04-05 2016-08-10 宁夏共享生物化工有限公司 Humic acid-containing water-soluble fertilizer specially used for melons and fruits, and preparation method thereof
CN106045782A (en) * 2016-06-06 2016-10-26 江门市智虎实业有限公司 Water-soluble fertilizer containing humic acid and preparation method of water-soluble fertilizer
CN106614728A (en) * 2016-11-30 2017-05-10 山东理工大学 Preparation and application of wheat pollution-free maturation-accelerating suspending agent
CN106614727A (en) * 2016-11-30 2017-05-10 山东理工大学 Preparation and application of pollution-free corn ripening suspending agent
CN107473875A (en) * 2017-10-23 2017-12-15 山东普金肥料有限公司 A kind of slow-release suspension liquid composite fertilizer and preparation method thereof
CN110922261A (en) * 2019-11-26 2020-03-27 云南中翼鼎东投资集团生物科技开发有限公司 Water-soluble fertilizer containing humic acid and major elements and preparation method thereof
CN111484364A (en) * 2020-03-10 2020-08-04 湖南玖恪环境工程有限公司 Foliar fertilizer for reducing cadmium in rice and application method and application thereof
CN111995483A (en) * 2020-09-09 2020-11-27 山西绿丰肥业有限公司 Water-soluble fertilizer capable of effectively improving nutrients of crops and preparation method thereof
CN113307688A (en) * 2021-06-24 2021-08-27 山东万物新农业科技有限公司 Production and application method of spray fertilizer for increasing yield, improving quality and increasing efficiency by saving chemical fertilizer and pesticide for crops by 50% and 30%
CN113354471A (en) * 2021-06-24 2021-09-07 湖北宜施壮农业科技有限公司 Compound fertilizer for flying application and preparation method thereof
CN113416108A (en) * 2021-08-02 2021-09-21 大理洱海生物肥业有限公司 Preparation method of liquid organic fertilizer for potatoes
CN113439519A (en) * 2021-06-24 2021-09-28 山东万物新农业科技有限公司 Topdressing fertilizer production and application method for crop topdressing-free fertilizer, pesticide saving by 30%, yield increasing, quality improving and efficiency increasing
CN113717000A (en) * 2021-08-26 2021-11-30 云南省化工研究院有限公司 Combined fertilizer and use method thereof

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EP0926113A1 (en) * 1997-12-24 1999-06-30 Dante C. Dizon Biostimulant type fertilizer for various crops and method of use thereof
CN101570456A (en) * 2008-10-22 2009-11-04 新疆农垦科学院农业新技术推广服务中心 Water soluble humic acid multi-element solid fertilizer and production method thereof
CN101928174A (en) * 2010-08-23 2010-12-29 杭州绿叶科技有限公司 Humic acid water-soluble fertilizer
CN102173945A (en) * 2011-02-17 2011-09-07 山东省农业科学院农业资源与环境研究所 Water-soluble fertilizer containing urea humate and preparation method thereof
CN102757292A (en) * 2012-05-17 2012-10-31 新疆农垦科学院农业新技术推广服务中心 Water-soluble microbial multi-element solid fertilizer

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Publication number Priority date Publication date Assignee Title
EP0926113A1 (en) * 1997-12-24 1999-06-30 Dante C. Dizon Biostimulant type fertilizer for various crops and method of use thereof
CN101570456A (en) * 2008-10-22 2009-11-04 新疆农垦科学院农业新技术推广服务中心 Water soluble humic acid multi-element solid fertilizer and production method thereof
CN101928174A (en) * 2010-08-23 2010-12-29 杭州绿叶科技有限公司 Humic acid water-soluble fertilizer
CN102173945A (en) * 2011-02-17 2011-09-07 山东省农业科学院农业资源与环境研究所 Water-soluble fertilizer containing urea humate and preparation method thereof
CN102757292A (en) * 2012-05-17 2012-10-31 新疆农垦科学院农业新技术推广服务中心 Water-soluble microbial multi-element solid fertilizer

Cited By (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105315059A (en) * 2014-07-31 2016-02-10 陕西扬晨新材料科技有限公司 Humic acid containing water-soluble fertilizer and preparation method therefor
CN104193460A (en) * 2014-08-22 2014-12-10 江苏谷熠农业科技有限公司 Water-soluble fertilizer containing major elements and production technique thereof
CN104402652A (en) * 2014-11-20 2015-03-11 柳州市源晨农副产品有限公司 Special fertilizer for grape culture
CN104788176A (en) * 2015-03-30 2015-07-22 安徽金农生态农业科技发展有限公司 Water-soluble quick-acting drip irrigation fertilizer
CN105130676A (en) * 2015-07-03 2015-12-09 河南晋开化工投资控股集团有限责任公司 Liquid fertilizer for resisting drought and preserving moisture and fertility and preparation method thereof
CN105110861A (en) * 2015-08-07 2015-12-02 安徽省文胜生物工程股份有限公司 Water-soluble organic-inorganic compounded fertilizer and preparation method therefor
CN105837330A (en) * 2016-04-05 2016-08-10 宁夏共享生物化工有限公司 Humic acid-containing water-soluble fertilizer specially used for melons and fruits, and preparation method thereof
CN106045782A (en) * 2016-06-06 2016-10-26 江门市智虎实业有限公司 Water-soluble fertilizer containing humic acid and preparation method of water-soluble fertilizer
CN106614728A (en) * 2016-11-30 2017-05-10 山东理工大学 Preparation and application of wheat pollution-free maturation-accelerating suspending agent
CN106614727A (en) * 2016-11-30 2017-05-10 山东理工大学 Preparation and application of pollution-free corn ripening suspending agent
CN107473875A (en) * 2017-10-23 2017-12-15 山东普金肥料有限公司 A kind of slow-release suspension liquid composite fertilizer and preparation method thereof
CN110922261A (en) * 2019-11-26 2020-03-27 云南中翼鼎东投资集团生物科技开发有限公司 Water-soluble fertilizer containing humic acid and major elements and preparation method thereof
CN111484364A (en) * 2020-03-10 2020-08-04 湖南玖恪环境工程有限公司 Foliar fertilizer for reducing cadmium in rice and application method and application thereof
CN111995483A (en) * 2020-09-09 2020-11-27 山西绿丰肥业有限公司 Water-soluble fertilizer capable of effectively improving nutrients of crops and preparation method thereof
CN113307688A (en) * 2021-06-24 2021-08-27 山东万物新农业科技有限公司 Production and application method of spray fertilizer for increasing yield, improving quality and increasing efficiency by saving chemical fertilizer and pesticide for crops by 50% and 30%
CN113354471A (en) * 2021-06-24 2021-09-07 湖北宜施壮农业科技有限公司 Compound fertilizer for flying application and preparation method thereof
CN113439519A (en) * 2021-06-24 2021-09-28 山东万物新农业科技有限公司 Topdressing fertilizer production and application method for crop topdressing-free fertilizer, pesticide saving by 30%, yield increasing, quality improving and efficiency increasing
CN113416108A (en) * 2021-08-02 2021-09-21 大理洱海生物肥业有限公司 Preparation method of liquid organic fertilizer for potatoes
CN113717000A (en) * 2021-08-26 2021-11-30 云南省化工研究院有限公司 Combined fertilizer and use method thereof

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Application publication date: 20140716