CN112661562A - Water soluble foliage water flush fertilizer and its production method - Google Patents
Water soluble foliage water flush fertilizer and its production method Download PDFInfo
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Abstract
The invention provides a water-soluble foliar water flush fertilizer and a manufacturing method thereof, belonging to the technical field of fertilizers. The invention comprises medical stone, sodium hydroxide, humic acid urea, chitosan, compound amino acid, polyaspartic acid, amino acid chelating liquid, nano silicon magnesium powder, rooting agent, penetrant, vitamin B, Chinese herbal medicine residues and trace element mixture, wherein the trace element mixture comprises the following components in parts by weight: monopotassium phosphate, ammonium molybdate, ferrous sulfate, magnesium sulfate, zinc sulfate, copper sulfate and zinc oxide. The fertilizer has the advantages that the absorption and utilization of crops to major, medium and trace elements are enhanced, and the utilization rate of the fertilizer in the season is improved by over 75 percent; can quickly supplement trace elements which are lacked in soil and crops, regulate the balance relation between reproductive growth and vegetative growth of the crops, enhance the pollen activity and pollination capability of the crops, ensure that the crops have high fruit yield and full seeds, and effectively solve the physiological diseases of poor development, strange diseases, flower falling, fruit melting, empty and flat seeds and the like of the crops by more than 85 percent.
Description
Technical Field
The invention relates to the technical field of fertilizers, in particular to a water-soluble foliar water flush fertilizer and a manufacturing method thereof.
Background
The water-soluble fertilizer is a compound fertilizer containing nitrogen, phosphorus, potassium, calcium, magnesium, trace elements, amino acid, humic acid, alginic acid and the like, which can be completely dissolved in water. The fertilizer is divided into a solid water-soluble fertilizer and a liquid water-soluble fertilizer from the form, and is divided into a macroelement water-soluble fertilizer, a secondary element water-soluble fertilizer, a microelement water-soluble fertilizer, an amino acid-containing water-soluble fertilizer, a humic acid-containing water-soluble fertilizer, an organic water-soluble fertilizer and the like from the nutrient content.
Nowadays, water-soluble fertilizer is used as a novel fertilizer, compared with the traditional fertilizer, the water-soluble fertilizer has various formulas and very flexible application method, can be irrigated by soil, can make the roots of plants contact with the fertilizer comprehensively, and can effectively absorb various nutrient elements; the fertilizer can also be sprayed on the leaf surfaces and enters the interior of the plant through leaf surface pores, so that the absorption and utilization rate of the fertilizer is improved; the water soluble fertilizer is a quick-acting fertilizer, has comprehensive nutrient elements, can be produced according to the fertilizer requirement characteristics of different crops, and is a special water soluble fertilizer for various crops such as vegetables, fruit trees, flowers, grains, cotton, oils and the like sold in the market.
The existing water-soluble fertilizer has relatively single effect, and is mainly applied by a soil application or surface application method, different raw materials and proportions in the fertilizer greatly influence the absorption efficiency of the fertilizer, different application modes have different effects and action mechanisms on the growth of crops, and the composition, proportion and application mode of nutrient elements in the fertilizer are unreasonable, so that the crop yield cannot be improved, and the crop yield is reduced due to low utilization rate of the fertilizer; moreover, the existing water-soluble fertilizer cannot simultaneously have the effects of increasing the yield, resisting diseases and insect pests, preventing dysplasia and improving the absorption efficiency of trace, medium and large elements.
Disclosure of Invention
The technical problem to be solved by the invention is as follows:
the existing water-soluble foliar water flush fertilizer cannot simultaneously have multiple effects of increasing yield, resisting diseases and insect pests, preventing dysplasia and improving the absorption efficiency of trace, medium and large elements.
The invention adopts the technical scheme for solving the technical problems that:
the water-soluble foliar water flush fertilizer is characterized by being prepared from the following raw materials in parts by weight: 30-50 parts of medical stone, 15-25 parts of sodium hydroxide, 20-40 parts of humic acid urea, 15-20 parts of chitosan, 5-10 parts of compound amino acid, 1-5 parts of polyaspartic acid, 2-5 parts of amino acid chelating liquid, 1-3 parts of nano silicon magnesium powder, 1-5 parts of rooting agent, 2-3 parts of penetrant, 0.1-0.3 part of vitamin B, 3-5 parts of Chinese herbal medicine residues and 20-30 parts of trace element mixture, wherein the trace element mixture comprises: 1.5-2 parts of monopotassium phosphate, 3-5 parts of ammonium molybdate, 2-5 parts of ferrous sulfate, 2-5 parts of magnesium sulfate, 2-3 parts of zinc sulfate, 1-3 parts of copper sulfate and 1-2 parts of zinc oxide.
Optionally, the feed additive is prepared from the following raw materials in parts by weight: 30-45 parts of medical stone, 20-25 parts of sodium hydroxide, 30-40 parts of humic acid urea, 15-20 parts of chitosan, 8-10 parts of compound amino acid, 3-5 parts of polyaspartic acid, 3-4 parts of amino acid chelating liquid, 1.5-2.5 parts of nano silicon magnesium powder, 3-4 parts of rooting agent, 2-3 parts of penetrating agent, 0.1-0.3 part of vitamin B, 4-5 parts of Chinese herbal medicine residues and 25-30 parts of trace element mixture, wherein the trace element mixture comprises: 1.5-2 parts of monopotassium phosphate, 3-5 parts of ammonium molybdate, 2-4 parts of ferrous sulfate, 3-5 parts of magnesium sulfate, 2-3 parts of zinc sulfate, 2-3 parts of copper sulfate and 1-2 parts of zinc oxide.
The preparation method of the water-soluble foliar water flush fertilizer is characterized by comprising the following steps:
(1) adding animal hoof and horn or hair into 25-35% sulfuric acid, hydrolyzing at 110 ℃ for 1-2 hours to generate amino acid, then adding lime to neutralize until the pH value is 6.0-6.8, adding 3-4 parts by weight of hydroxymethyl cellulose into 15 parts by weight of hydrolysis solution, adding 1-2 parts by weight of ferrous sulfate and 3-4 parts by weight of ammonium molybdate to dissolve, and reacting at 90-105 ℃ for 5-6 hours to obtain amino acid chelating solution for later use;
(2) taking 7-10 parts of water-soluble humic acid, 20-30 parts of urea and 15-25 parts of water-soluble potash fertilizer, putting the water-soluble humic acid and the urea in a reaction kettle according to a proportion, controlling the temperature at 110-130 ℃, stirring for 30-40 minutes to generate humic acid urea, then putting the water-soluble potash fertilizer in the reaction kettle according to a proportion, controlling the temperature at 85-95 ℃, stirring for 20-30 minutes, cooling, drying, caking and crushing to obtain powdery humic acid urea;
(3) drying chitosan at 70-80 deg.C, and pulverizing to 80 mesh;
(4) weighing the following raw materials in parts by weight: 30-50 parts of medical stone, 15-25 parts of sodium hydroxide, 20-40 parts of humic acid urea, 15-20 parts of chitosan, 5-10 parts of compound amino acid, 1-5 parts of polyaspartic acid, 2-5 parts of amino acid chelating liquid, 1-3 parts of nano silicon magnesium powder, 1-5 parts of rooting agent, 2-3 parts of penetrant, 0.1-0.3 part of vitamin B, 3-5 parts of Chinese herbal medicine residues and 20-30 parts of trace element mixture, wherein the trace element mixture comprises: 1.5-2 parts of monopotassium phosphate, 3-5 parts of ammonium molybdate, 2-5 parts of ferrous sulfate, 2-5 parts of magnesium sulfate, 2-3 parts of zinc sulfate, 1-3 parts of copper sulfate and 1-2 parts of zinc oxide;
(5) mixing the medical stone weighed in the step (4) with sodium hydroxide, and calcining at the high temperature of 1200-2000 ℃ for 0.5-3 hours to obtain medical stone silicon crystal salt;
(6) mixing the humic acid urea, the amino acid chelating solution and the trace element mixture weighed in the step (4) with the medical stone silicon crystal salt weighed in the step (5) at the temperature of 60-70 ℃ to obtain a first mixture;
(7) and (4) adding the chitosan, the compound amino acid, the polyaspartic acid, the nano silicon magnesium powder, the rooting agent, the penetrating agent, the vitamin B and the Chinese herbal medicine residues weighed in the step (4) into the first mixture obtained in the step (6), mixing at 40-50 ℃, cooling, agglomerating and crushing to obtain the water-soluble foliar fertilization fertilizer.
Optionally, the vitamin B includes vitamin B1, vitamin B6, and vitamin B12.
Optionally, the vitamin B is prepared from the following components in parts by mass: 0.03-0.06 part of vitamin B1, 0.03-0.06 part of vitamin B6 and 0.01-0.05 part of vitamin B12.
Optionally, the Chinese herbal medicine residue is residue of cortex moutan, folium artemisiae argyi, honeysuckle, coptis chinensis, radix sophorae flavescentis and fructus meliae.
Compared with the prior art, the invention has the beneficial effects that:
carboxyl and phenolic hydroxyl functional groups contained in the water-soluble foliar water flush fertilizer have strong ion exchange and adsorption and decomposition capabilities, can effectively inhibit the activity of urease, reduce the urea loss and improve the urea fertilizer efficiency; the activity of phosphorus in the soil can be improved, the fixation of phosphorus in the soil is inhibited, and the absorption and utilization of phosphorus by crops are promoted; the medical stone can absorb and store nitrogen, phosphorus and potassium ions, improve the available quick-acting nitrogen, phosphorus and potassium content of crops, and meet the requirements of strong stems, fullness and maturity of crops;
the humic acid fertilizer contains an amino acid chelating agent and humic acid, and can carry out a chelating reaction with insoluble trace elements to generate a humic acid trace element chelate, so that the absorption and utilization of crops on large, medium and trace elements are enhanced, and the utilization rate of the fertilizer in the season is improved by over 75 percent; the fertilizer can quickly supplement trace elements which are lacked in soil and crops, adjust the balance relation between reproductive growth and vegetative growth of the crops, enhance the pollen activity and pollination capability of the crops, ensure that the fruit yield of the crops is high and the seeds are full, and effectively solve over 85 percent of physiological diseases such as poor development, strange diseases, flower falling, fruit melting, empty and flat seeds of the crops; the chitosan in the invention has good effect on the development, growth and expansion of the root tuber of the crop, and can not generate adverse effect on the crop after being used;
the compound amino acid and the polyaspartic acid in the invention contain active peptide chains, and can fully activate various functional enzymes in soil and crops, thereby forming nitrogen fixation enzyme, and leading the roots and leaves of the crops to have the effect of fixing and recycling free nitrogen in the air;
the Chinese herbal medicine residues are mostly taken from roots, stems, leaves, flowers, fruits and skins of plants, contain rich nutrient substances, still contain a large amount of various nutrient substances such as nitrogen, phosphorus, potassium and the like required by the growth of crops after being decocted, are fermented and sterilized, are used in a matrix and can provide nutrient components for the crops;
the polymeric amino acid, the polyaspartic acid, the humic acid, the rooting agent and the penetrating agent have the effects of catalysis, adsorption, decomposition, permeation, diffusion and chelation, not only can permeate the roots of crops through carbohydrates in the crops, but also can rapidly permeate, conduct and diffuse nutrient elements on plant fibers and reproductive organs so as to protect the crop plants from being damaged by germs and pests and to promote the robust growth, can also stimulate the activity of reproductive cells and the activity of enzymes, promotes the generation of fruit organs and improves the utilization rate of the carbohydrates;
the organic matter is used as a main material, and the medical stone, urea, ammonium molybdate and other chemical fertilizers are compounded, so that the soil hardening cannot be caused after long-term repeated use, and the organic matter has a remarkable effect in the water and fertilizer propulsion integration technology in China.
Detailed Description
In order to make the aforementioned and other objects, features and advantages of the present invention comprehensible, embodiments accompanied with figures are described in detail below.
Example 1
The water-soluble foliar water flush fertilizer is prepared from the following raw materials in parts by weight: 30 parts of medical stone, 20 parts of sodium hydroxide, 30 parts of humic acid urea, 15 parts of chitosan, 8 parts of compound amino acid, 3 parts of polyaspartic acid, 3 parts of amino acid chelating liquid, 1.5 parts of nano silicon magnesium powder, 3 parts of rooting agent, 2 parts of penetrating agent, 0.1 part of vitamin B, 3 parts of Chinese herbal medicine dregs and 25 parts of trace element mixture, wherein the trace element mixture comprises: 1.5 parts of monopotassium phosphate, 3 parts of ammonium molybdate, 2 parts of ferrous sulfate, 3 parts of magnesium sulfate, 2 parts of zinc sulfate, 2 parts of copper sulfate and 1 part of zinc oxide.
Example 2
The water-soluble foliar water flush fertilizer is prepared from the following raw materials in parts by weight: 45 parts of medical stone, 25 parts of sodium hydroxide, 40 parts of humic acid urea, 20 parts of chitosan, 10 parts of compound amino acid, 5 parts of polyaspartic acid, 4 parts of amino acid chelating liquid, 2.5 parts of nano silicon magnesium powder, 4 parts of rooting agent, 3 parts of penetrating agent, 0.3 part of vitamin B, 5 parts of Chinese herbal medicine dregs and 30 parts of trace element mixture, wherein the trace element mixture comprises: 2 parts of monopotassium phosphate, 5 parts of ammonium molybdate, 4 parts of ferrous sulfate, 5 parts of magnesium sulfate, 3 parts of zinc sulfate, 3 parts of copper sulfate and 2 parts of zinc oxide.
Example 3
The water-soluble foliar water flush fertilizer is prepared from the following raw materials in parts by weight: 40 parts of medical stone, 23 parts of sodium hydroxide, 35 parts of humic acid urea, 18 parts of chitosan, 9 parts of compound amino acid, 4 parts of polyaspartic acid, 4 parts of amino acid chelating liquid, 2 parts of nano silicon magnesium powder, 4 parts of rooting agent, 3 parts of penetrating agent, 0.2 part of vitamin B, 4 parts of Chinese herbal medicine dregs and 12 parts of trace element mixture, wherein the trace element mixture comprises: 2 parts of monopotassium phosphate, 4 parts of ammonium molybdate, 3 parts of ferrous sulfate, 4 parts of magnesium sulfate, 3 parts of zinc sulfate, 3 parts of copper sulfate and 1.5 parts of zinc oxide.
Example 4
The preparation method of the water-soluble foliar fertilization fertilizer comprises the following steps of proportioning the raw materials in parts by weight in the embodiment 3:
(1) adding animal hoof and horn or hair into 25% sulfuric acid, hydrolyzing at 100 ℃ for 1 hour to generate amino acid, then adding lime to neutralize until the pH value is 6.0, adding 3-4 parts by weight of hydroxymethyl cellulose into 15 parts by weight of hydrolysis solution, adding 1 part of ferrous sulfate and 3 parts of ammonium molybdate to dissolve, and reacting at 90 ℃ for 5 hours to obtain amino acid chelate solution for later use;
(2) taking 7 parts of water-soluble humic acid, 20 parts of urea and 15 parts of water-soluble potash fertilizer, putting the water-soluble humic acid and the urea in a reaction kettle according to a proportion, controlling the temperature at 110 ℃, stirring for 30 minutes to generate humic acid urea, then putting the water-soluble potash fertilizer in the reaction kettle according to a proportion, controlling the temperature at 85 ℃, stirring for 20 minutes, cooling, drying, caking and crushing to obtain powdery humic acid urea;
(3) drying chitosan at 70 ℃, and crushing to 80 meshes for later use;
(4) weighing the following raw materials in parts by weight: 30 parts of medical stone, 15 parts of sodium hydroxide, 20 parts of humic acid urea, 15 parts of chitosan, 5 parts of compound amino acid, 1 part of polyaspartic acid, 2 parts of amino acid chelating liquid, 1 part of nano silicon magnesium powder, 1 part of rooting agent, 2 parts of penetrating agent, 0.1 part of vitamin B, 3 parts of Chinese herbal medicine dregs and 20 parts of trace element mixture, wherein the trace element mixture comprises: 1.5 parts of monopotassium phosphate, 3 parts of ammonium molybdate, 2 parts of ferrous sulfate, 2 parts of magnesium sulfate, 2 parts of zinc sulfate, 1 part of copper sulfate and 1 part of zinc oxide;
(5) mixing the medical stone weighed in the step (4) with sodium hydroxide, and calcining at the high temperature of 1200 ℃ for 0.5 hour to obtain medical stone silicon crystal salt;
(6) mixing the humic acid urea, the amino acid chelating solution and the trace element mixture weighed in the step (4) with the medical stone silicon crystal salt weighed in the step (5) at the temperature of 60 ℃ to obtain a first mixture;
(7) and (4) adding the chitosan, the compound amino acid, the polyaspartic acid, the nano silicon magnesium powder, the rooting agent, the penetrating agent, the vitamin B and the Chinese herbal medicine residues weighed in the step (4) into the first mixture obtained in the step (6), mixing at 40 ℃, cooling, agglomerating and crushing to obtain the water-soluble foliar fertilization fertilizer.
Example 5
The preparation method of the water-soluble foliar fertilization fertilizer comprises the following steps of proportioning the raw materials in parts by weight in the embodiment 3:
(1) adding animal hoof and horn or hair into 30% sulfuric acid, hydrolyzing at 105 ℃ for 1.5 hours to generate amino acid, then adding lime to neutralize until the pH value is 6.4, adding 3.5 parts by weight of hydroxymethyl cellulose into 15 parts by weight of hydrolysis solution, adding 1.5 parts by weight of ferrous sulfate and 3.5 parts by weight of ammonium molybdate to dissolve, and reacting at 100 ℃ for 5.5 hours to obtain amino acid chelate solution for later use;
(2) taking 9 parts of water-soluble humic acid, 25 parts of urea and 20 parts of water-soluble potash fertilizer, putting the water-soluble humic acid and the urea in a reaction kettle in proportion, controlling the temperature at 120 ℃, stirring for 35 minutes to generate humic acid urea, then putting the water-soluble potash fertilizer in the reaction kettle in proportion, controlling the temperature at 90 ℃, stirring for 20-30 minutes, cooling, drying, caking and crushing to obtain powdery humic acid urea;
(3) drying chitosan at 75 ℃, and crushing to 80 meshes for later use;
(4) weighing the following raw materials in parts by weight: 40 parts of medical stone, 20 parts of sodium hydroxide, 30 parts of humic acid urea, 18 parts of chitosan, 8 parts of compound amino acid, 3 parts of polyaspartic acid, 4 parts of amino acid chelating liquid, 2 parts of nano silicon magnesium powder, 3 parts of rooting agent, 2.5 parts of penetrating agent, 0.2 part of vitamin B, 4 parts of Chinese herbal medicine dregs and 25 parts of trace element mixture, wherein the trace element mixture comprises: 1.8 parts of monopotassium phosphate, 4 parts of ammonium molybdate, 4 parts of ferrous sulfate, 4 parts of magnesium sulfate, 2.5 parts of zinc sulfate, 2 parts of copper sulfate and 1.5 parts of zinc oxide;
(5) mixing the medical stone weighed in the step (4) with sodium hydroxide, and calcining at the high temperature of 1600 ℃ for 2 hours to obtain medical stone silicon crystal salt;
(6) mixing the humic acid urea, the amino acid chelating solution and the trace element mixture weighed in the step (4) with the medical stone silicon crystal salt weighed in the step (5) at 65 ℃ to obtain a first mixture;
(7) and (4) adding the chitosan, the compound amino acid, the polyaspartic acid, the nano silicon magnesium powder, the rooting agent, the penetrating agent, the vitamin B and the Chinese herbal medicine residues weighed in the step (4) into the first mixture obtained in the step (6), mixing at 45 ℃, cooling, agglomerating and crushing to obtain the water-soluble foliar fertilization fertilizer.
Example 6
The preparation method of the water-soluble foliar fertilization fertilizer comprises the following steps of proportioning the raw materials in parts by weight in the embodiment 3:
(1) adding animal hoof and horn or hair into 35% sulfuric acid, hydrolyzing at 110 ℃ for 2 hours to generate amino acid, then adding lime to neutralize until the pH value is 6.8, adding 4 parts by weight of hydroxymethyl cellulose into 15 parts by weight of hydrolysis solution, adding 2 parts by weight of ferrous sulfate and 4 parts by weight of ammonium molybdate to dissolve, and reacting at 105 ℃ for 6 hours to obtain amino acid chelate solution for later use;
(2) taking 10 parts of water-soluble humic acid, 30 parts of urea and 25 parts of water-soluble potash fertilizer, putting the water-soluble humic acid and the urea in a reaction kettle in proportion, controlling the temperature at 130 ℃, stirring for 40 minutes to generate humic acid urea, then putting the water-soluble potash fertilizer in the reaction kettle in proportion, controlling the temperature at 95 ℃, stirring for 30 minutes, cooling, drying, caking and crushing to obtain powdery humic acid urea;
(3) drying chitosan at 80 ℃, and crushing to 80 meshes for later use;
(4) weighing the following raw materials in parts by weight: 50 parts of medical stone, 25 parts of sodium hydroxide, 40 parts of humic acid urea, 20 parts of chitosan, 10 parts of compound amino acid, 5 parts of polyaspartic acid, 5 parts of amino acid chelating liquid, 3 parts of nano silicon magnesium powder, 5 parts of rooting agent, 3 parts of penetrating agent, 0.3 part of vitamin B, 5 parts of Chinese herbal medicine dregs and 30 parts of trace element mixture, wherein the trace element mixture comprises the following components in parts by weight: 2 parts of monopotassium phosphate, 5 parts of ammonium molybdate, 5 parts of ferrous sulfate, 5 parts of magnesium sulfate, 3 parts of zinc sulfate, 3 parts of copper sulfate and 2 parts of zinc oxide;
(5) mixing the medical stone weighed in the step (4) with sodium hydroxide, and calcining at the high temperature of 2000 ℃ for 3 hours to obtain medical stone silicon crystal salt;
(6) mixing the humic acid urea, the amino acid chelating solution and the trace element mixture weighed in the step (4) with the medical stone silicon crystal salt weighed in the step (5) at 70 ℃ to obtain a first mixture;
(7) and (4) adding the chitosan, the compound amino acid, the polyaspartic acid, the nano silicon magnesium powder, the rooting agent, the penetrating agent, the vitamin B and the Chinese herbal medicine residues weighed in the step (4) into the first mixture obtained in the step (6), mixing at 50 ℃, cooling, agglomerating and crushing to obtain the water-soluble foliar fertilization fertilizer.
The water-soluble foliar fertilization fertilizer prepared in all the embodiments is black and gray powder, elements are well released, no pesticide residue is left, when the water-soluble foliar fertilization fertilizer is used, 40 kilograms of water is added into every 500 grams of the fertilizer, the fertilizer is soaked for 24 hours, the fertilizer is stirred for 3 minutes and then is reprecipitated, and clear liquid is poured into a sprayer and is sprayed on the foliage of crops according to different types of agricultural products.
Application example 1
The invention relates to the influence of a water-soluble foliar water flush fertilizer on potatoes.
Potato cultivation land: ziqihaer city, black dragon Jiang province.
The fertilizing method comprises the following steps: the six groups of embodiments are mixed with water, soaked and dissolved according to the dosage of 500 g/mu, and the leaf application is carried out twice after one heart of six leaves, and meanwhile, a clear water control group is arranged.
TABLE 1 comparison of Water-soluble foliar Water-applied fertilizers to Potato growth in groups of examples 1, 2 and 3
| Plant height/cm | Stem thickness/cm | Yield/kg | |
| CK | 52 | 1.8 | 2435 |
| Example 1 | 59 | 2.1 | 3184 |
| Example 2 | 63 | 2.5 | 3658 |
| Example 3 | 67 | 2.3 | 3935 |
TABLE 2 comparison of Water-soluble foliar Water-applied fertilizers to Potato growth in groups of examples 4, 5 and 6
| Plant height/cm | Stem thickness/cm | Yield/kg | |
| CK | 52 | 1.8 | 2435 |
| Example 4 | 64 | 2.1 | 3849 |
| Example 5 | 63 | 2.1 | 3862 |
| Example 6 | 68 | 2.4 | 3967 |
As can be seen from tables 1 and 2, the water-soluble foliar fertilization fertilizer has obvious promotion effects on the growth and yield of potatoes, particularly has the yield increase of 62.9% to the maximum extent, and has better effect compared with the traditional fertilizer. As can be seen from table 1, the growth and yield of example 3 were increased most, indicating that the ratio of example 3 was optimal and the resulting effect was the best; as can be seen from table 2, the growth and yield of example 6 were maximized, indicating that the production method of example 6 is the most favorable and the most favorable results are obtained, compared to the production methods of examples 4 and 5.
Although the present disclosure has been described above, the scope of the present disclosure is not limited thereto. Various changes and modifications may be effected therein by one of ordinary skill in the pertinent art without departing from the spirit and scope of the present disclosure, and these changes and modifications are intended to be within the scope of the present disclosure.
Claims (5)
1. The water-soluble foliar water flush fertilizer is characterized by being prepared from the following raw materials in parts by weight: 30-50 parts of medical stone, 15-25 parts of sodium hydroxide, 20-40 parts of humic acid urea, 15-20 parts of chitosan, 5-10 parts of compound amino acid, 1-5 parts of polyaspartic acid, 2-5 parts of amino acid chelating liquid, 1-3 parts of nano silicon magnesium powder, 1-5 parts of rooting agent, 2-3 parts of penetrant, 0.1-0.3 part of vitamin B, 3-5 parts of Chinese herbal medicine residues and 20-30 parts of trace element mixture, wherein the trace element mixture comprises: 1.5-2 parts of monopotassium phosphate, 3-5 parts of ammonium molybdate, 2-5 parts of ferrous sulfate, 2-5 parts of magnesium sulfate, 2-3 parts of zinc sulfate, 1-3 parts of copper sulfate and 1-2 parts of zinc oxide.
2. The water-soluble foliar water flush fertilizer as claimed in claim 1, which is prepared from the following raw materials in parts by weight: 30-45 parts of medical stone, 20-25 parts of sodium hydroxide, 30-40 parts of humic acid urea, 15-20 parts of chitosan, 8-10 parts of compound amino acid, 3-5 parts of polyaspartic acid, 3-4 parts of amino acid chelating liquid, 1.5-2.5 parts of nano silicon magnesium powder, 3-4 parts of rooting agent, 2-3 parts of penetrating agent, 0.1-0.3 part of vitamin B, 4-5 parts of Chinese herbal medicine residues and 25-30 parts of trace element mixture, wherein the trace element mixture comprises: 1.5-2 parts of monopotassium phosphate, 3-5 parts of ammonium molybdate, 2-4 parts of ferrous sulfate, 3-5 parts of magnesium sulfate, 2-3 parts of zinc sulfate, 2-3 parts of copper sulfate and 1-2 parts of zinc oxide.
3. The method for preparing the water-soluble foliar fertilization fertilizer according to claim 1, comprising the following steps:
(1) adding animal hoof and horn or hair into 25-35% sulfuric acid, hydrolyzing at 110 ℃ for 1-2 hours to generate amino acid, then adding lime to neutralize until the pH value is 6.0-6.8, adding 3-4 parts by weight of hydroxymethyl cellulose into 15 parts by weight of hydrolysis solution, adding 1-2 parts by weight of ferrous sulfate and 3-4 parts by weight of ammonium molybdate to dissolve, and reacting at 90-105 ℃ for 5-6 hours to obtain amino acid chelating solution for later use;
(2) taking 7-10 parts of water-soluble humic acid, 20-30 parts of urea and 15-25 parts of water-soluble potash fertilizer, putting the water-soluble humic acid and the urea in a reaction kettle according to a proportion, controlling the temperature at 110-130 ℃, stirring for 30-40 minutes to generate humic acid urea, then putting the water-soluble potash fertilizer in the reaction kettle according to a proportion, controlling the temperature at 85-95 ℃, stirring for 20-30 minutes, cooling, drying, caking and crushing to obtain powdery humic acid urea;
(3) drying chitosan at 70-80 deg.C, and pulverizing to 80 mesh;
(4) weighing the following raw materials in parts by weight: 30-50 parts of medical stone, 15-25 parts of sodium hydroxide, 20-40 parts of humic acid urea, 15-20 parts of chitosan, 5-10 parts of compound amino acid, 1-5 parts of polyaspartic acid, 2-5 parts of amino acid chelating liquid, 1-3 parts of nano silicon magnesium powder, 1-5 parts of rooting agent, 2-3 parts of penetrant, 0.1-0.3 part of vitamin B, 3-5 parts of Chinese herbal medicine residues and 20-30 parts of trace element mixture, wherein the trace element mixture comprises: 1.5-2 parts of monopotassium phosphate, 3-5 parts of ammonium molybdate, 2-5 parts of ferrous sulfate, 2-5 parts of magnesium sulfate, 2-3 parts of zinc sulfate, 1-3 parts of copper sulfate and 1-2 parts of zinc oxide;
(5) mixing the medical stone weighed in the step (4) with sodium hydroxide, and calcining at the high temperature of 1200-2000 ℃ for 0.5-3 hours to obtain medical stone silicon crystal salt;
(6) mixing the humic acid urea, the amino acid chelating solution and the trace element mixture weighed in the step (4) with the medical stone silicon crystal salt weighed in the step (5) at the temperature of 60-70 ℃ to obtain a first mixture;
(7) and (4) adding the chitosan, the compound amino acid, the polyaspartic acid, the nano silicon magnesium powder, the rooting agent, the penetrating agent, the vitamin B and the Chinese herbal medicine residues weighed in the step (4) into the first mixture obtained in the step (6), mixing at 40-50 ℃, cooling, agglomerating and crushing to obtain the water-soluble foliar fertilization fertilizer.
4. The method for manufacturing a water-soluble foliar fertilization fertilizer according to claim 3, wherein: the vitamin B comprises vitamin B1, vitamin B6 and vitamin B12.
5. The manufacturing method of the water-soluble foliar fertilization fertilizer as claimed in claim 4, wherein the vitamin B comprises the following components in parts by mass: 0.03-0.06 part of vitamin B1, 0.03-0.06 part of vitamin B6 and 0.01-0.05 part of vitamin B12.
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| CN107382569A (en) * | 2017-09-21 | 2017-11-24 | 阿米巴南京生物技术有限责任公司 | A kind of balanced type a great number of elements water-soluble fertilizer and preparation method |
| CN107512981A (en) * | 2017-09-30 | 2017-12-26 | 王意强 | Dual-purpose type fertilizer that a kind of foliage-spray and root punching are applied and its preparation method and application |
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| CN103467195A (en) * | 2013-09-03 | 2013-12-25 | 陕西大唐节能科技有限公司 | Nano silicon-magnesium-potassium water flush fertilizer and preparation method thereof |
| CN106831251A (en) * | 2017-03-01 | 2017-06-13 | 安徽六国化工股份有限公司 | A kind of full-service fluid fertilizer |
| CN107382569A (en) * | 2017-09-21 | 2017-11-24 | 阿米巴南京生物技术有限责任公司 | A kind of balanced type a great number of elements water-soluble fertilizer and preparation method |
| CN107512981A (en) * | 2017-09-30 | 2017-12-26 | 王意强 | Dual-purpose type fertilizer that a kind of foliage-spray and root punching are applied and its preparation method and application |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114133289A (en) * | 2021-12-14 | 2022-03-04 | 上海农乐生物制品股份有限公司 | Low-chlorine compound amino acid chelated multi-element metal element fertilizer and preparation method thereof |
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