CN100347136C - Microelement type composite foliage fertilizer and its preparation method - Google Patents
Microelement type composite foliage fertilizer and its preparation method Download PDFInfo
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Abstract
The present invention discloses a kind of microelement type complex foliage fertilizer and its preparation method. The described foliage fertilizer is formed from fulvic acid, sodium salicylate, alginic acid composite solution, special-purpose composite adjuvant and composite microelement solution (solution A and solution B), in which said solution A is made up by dissolving 100-150kg of citric acid in 250L of water with 60-80deg.C, then successively adding 100-150kg of FeSO4.7H2O, 50-100kg of CuSO4.5H2O, 20-50kg of MnCl2.6H2O and 250-300kg of Zn(NO3)2.7H2O, and the solution B is made up by dissolving 50-100kg of boric acid in 100 L of water with 40-60deg.C, then adding 20-50kg of potassium hydroxide, making them be fully reacted and regulating pH value to 5-6. Its preparation method includes the following steps: adding the solution B into the solution A, stirring them, adding 100-150kg of urea, adding 30-80L of fulvic acid, sodium salicylate and alginic acid composite solution, adding 1kg of sodium hydrogen sulfite and 20-50L of special-purpose adjuvant, regulating pH value to 3-3.5, then adding water to 1000L.
Description
One, technical field
The present invention is a kind of preparation method of microelement type composite foliage fertilizer, and this foliage fertilizer is a kind ofly can strengthen the fruit tinting strength, improves the microelement type composite foliage fertilizer of the sugar content of fruit.
Two, background technology
Fertilizer after the dilution dissolving is sprayed directly on the fertilizing method of plant leaf surface leaf dressing.Leaf dressing is one of fertilizing method of using always of peasant.Foliage fertilizer has characteristics such as nutrition absorption is fast, utilization rate of fertilizer is high, easy to operate.Along with the development of agriculture production, leaf dressing has become an important well stimulation.
The nutrition supply of fruit tree and the quality of fruit quality have confidential relation, and correct fertilising is to influence one of most important factor of fruit quality.Nutrient excess or deficiency all can produce adverse influence to fruits output and quality; Inharmonious if nourish and grow with reproductive growth, will cause the index of relevant qualities such as fruit taste, nutrition, color and luster, storage and processing to descend, even multiple physiological disturbance takes place easily.A large amount of studies confirm that, the coordinated balance supply of nutrient is to increase the yield of fruit and the important foundation of quality.Compare with general crop, the fruit tree leaf wax layer is thicker, is unfavorable for the nutrient absorbing utilization.General microelement type foliar nutrient exists that nutrients ratio is unreasonable, specific aim is poor, fertilizer is not easy to cause the not high shortcoming of nutrition absorption efficient attached to blade surface.The present invention is directed to the physilogical characteristics of fruit tree leaf and absorb the nutrition rule, by trace element chelated, blade mount technology, in conjunction with other organic uses, prepare not only and can strengthen the fruit color ability, improve the sugar content of fruit and can increase fruits output, improve the foliar nutrient of fruit tree resistance.
Indexs such as the coloring degree of fruit and pulp sugar degree, the important indicator of fruit commercial grade often, these indexs have often determined the price that fruit is sold, and generally, improve a commercial grade and just can improve selling price 2-3 one-tenth.Therefore, the excellent fruit of bright-colored mouthfeel is the target that production practice are pursued.
Three, summary of the invention
One of purpose of the present invention provides and a kind ofly can strengthen the fruit tinting strength, improves the microelement type composite foliage fertilizer of the sugar content of fruit.
Two of purpose of the present invention provides a kind of preparation method of microelement type composite foliage fertilizer.
These and other purpose of the present invention will realize by following technical proposals:
Microelement type composite foliage fertilizer of the present invention is made up of xanthohumic acid+sodium salicylate+Lalgine composite solution, special compound additive, solution B and sodium bisulfite.Is the preparation unit with 1000L, the preparation method of microelement type composite foliage fertilizer is: weighing 100-150Kg citric acid is dissolved in 250L 60-80 ℃ the water, dissolves in FeSO successively
47H
2O 100-150Kg, CuSO
45H
2O 50-100Kg, MnCl
26H
2O 20-50Kg, Zn (NO
3)
27H
2O 250-300Kg is mixed with solution A; Weighing 50-100Kg boric acid is dissolved in 100L 40-60 ℃ the water, adds 20-50Kg potassium hydroxide then, and fully reaction is regulated the pH value to 5-6, adds solution A then, stirs, and adds urea 100-150Kg again, promptly obtains solution B; Add 30-80L xanthohumic acid+sodium salicylate+Lalgine composite solution, sodium bisulfite 1Kg, special compound additive 20-50L in solution B, the pH value is transferred to 3-3.5, water is settled to 1000L, promptly makes the microelement type composite foliage fertilizer of 1000L.
Further, microelement type composite foliage fertilizer of the present invention is made up of xanthohumic acid+sodium salicylate+Lalgine composite solution, special compound additive, solution B and sodium bisulfite.Is the preparation unit with 1000L, the preparation method of microelement type composite foliage fertilizer is: weighing 100-140Kg citric acid is dissolved in 250L 60-80 ℃ the water, dissolves in FeSO successively
47H
2O 100-140Kg, CuSO
45H
2O 50-90Kg, MnCl
26H
2O 20-40Kg, Zn (NO
3)
27H
2O 250-290Kg is mixed with solution A; Weighing 50-90Kg boric acid is dissolved in 100L 40-60 ℃ the water, adds 20-40Kg potassium hydroxide then, and fully reaction is regulated the pH value to 5-6, adds solution A then, stirs, and adds urea 100-140Kg again, promptly obtains solution B.Add 30-80L xanthohumic acid+sodium salicylate+Lalgine composite solution, sodium bisulfite 1Kg, special compound additive 20-50L in solution B, the pH value is transferred to 3-3.5, water is settled to 1000L, promptly makes the microelement type composite foliage fertilizer of 1000L.
What can select is that microelement type composite foliage fertilizer of the present invention is made up of xanthohumic acid+sodium salicylate+Lalgine composite solution, special compound additive, solution B and sodium bisulfite.Is the preparation unit with 1000L, the preparation method of microelement type composite foliage fertilizer is: weighing 120-140Kg citric acid is dissolved in 250L 60-80 ℃ the water, dissolves in FeSO successively
47H
2O120-140Kg, CuSO
45H
2O 60-90Kg, MnCl
26H
2O 30-40Kg, Zn (NO
3)
27H
2O260-290Kg is mixed with solution A; Weighing 60-90Kg boric acid is dissolved in 100L 40-60 ℃ the water, adds 30-40Kg potassium hydroxide then, and fully reaction is regulated the pH value to 5-6, adds solution A then, stirs, and adds urea 120-140Kg again, promptly obtains solution B.Add 30-80L xanthohumic acid+sodium salicylate+Lalgine composite solution, sodium bisulfite 1Kg, special compound additive 20-50L in solution B, the pH value is transferred to 3-3.5, water is settled to 1000L, promptly makes the microelement type composite foliage fertilizer of 1000L.
In the preparation method of microelement type composite foliage fertilizer of the present invention, the preparation method of xanthohumic acid+sodium salicylate+Lalgine composite solution is: water content is no more than 6% the levigate 20-40 of mistake of peat composed of rotten mosses mesh sieve, add 1% citric acid solution, mix and to leave standstill 24 hours, then with the nitric acid of 10-20% concentration in 1: 10 ratio thorough mixing in reactor, maintain the temperature at 80-100 ℃, stir after 40-60 minute, be cooled to normal temperature, filtering separation, filtrate is xanthohumic acid solution.Every liter of xanthohumic acid solution adds 30-50 gram sodium salicylate, stirs after 20-30 minute, adds 15-20 gram Lalgine.Promptly make xanthohumic acid+sodium salicylate+Lalgine composite solution.
In the preparation method of microelement type composite foliage fertilizer of the present invention, the preparation method of special compound additive is: trolamine, glycine, sucrose fatty ester were mixed according to 10: 5: 1, add 2 parts of OP-10 then in mixed solution.
The application method of microelement type composite foliage fertilizer of the present invention is that the 800-1000 times of leaf dressing of fertilizer liquid dilute with water that will prepare used.
In the present invention, utilize trace element to combine the synergy that the back produces with some organic substances, reach the purpose that improves fruit quality.Use has trace element builts such as the auxiliary agent that promotes the blade face nutrient absorption capability and boron, zinc, iron, manganese, again in conjunction with the natural extract material of biologically active as materials such as xanthohumic acid, Whitfield's ointment and Lalgines.Determine proiprietary formula by a large amount of field tests, preparation not only can strengthen the fruit color ability, improves the sugar content of fruit and can increase fruits output, improves the foliar nutrient of fruit tree resistance.
The present invention can improve the moistening and penetrating power of microelement type composite foliage fertilizer on the plant leaf surface, improves utilization rate of fertilizer.In time replenish the micro-element nutrition that needs in the growth and development of fruit tree critical period, the multiple spot demonstration test shows: not only can effectively promote fruit color, improve the sugar content of fruit in the application of fruit trees such as apple, grape, peach, and can improve output.
Blending process of the present invention is simple, low production cost, economic benefit and obvious social benefit.
The all raw material of Shi Yonging etc. all is conventional uses in the present invention, can buy from market, refers in particular to as non-, and all amount, per-cents are weight unit.
Below in conjunction with embodiment the present invention is carried out concrete description.As known by the technical knowledge, the present invention can realize by other the embodiment that does not break away from its spirit or essential feature.Therefore, following embodiment with regard to each side, all just illustrates, and is not only.All within the scope of the present invention or the change that is equal in the scope of the present invention all be included in the invention.
Four, embodiment
Embodiment 1
Take by weighing raw material in following ratio, and preparation:
1, the preparation of xanthohumic acid+sodium salicylate+Lalgine composite solution: water content is no more than the levigate 20-40 of mistake of 6% peat composed of rotten mosses mesh sieve, add 1% citric acid solution, mix and left standstill 24 hours, then with the nitric acid of 10-20% concentration in 1: 10 ratio thorough mixing in reactor, maintain the temperature at 80-100 ℃, stir after 40-60 minute, be cooled to normal temperature, filtering separation, filtrate are xanthohumic acid solution.Every liter of xanthohumic acid solution adds 35 gram sodium salicylates, stirs after 20-30 minute, adds 16 gram Lalgines, is to be xanthohumic acid+sodium salicylate+Lalgine composite solution.
2, the preparation of special compound additive: trolamine, glycine, sucrose fatty ester were mixed according to 10: 5: 1, in mixed solution, add 2 parts of OP-10 then, stir, be mixed with special compound additive.
3, weighing 110Kg citric acid is dissolved in 250L 60-80 ℃ the water, dissolves in FeSO successively
47H
2O 110Kg, CuSO
45H
2O 60Kg, MnCl
26H
2O 30Kg, Zn (NO
3)
27H
2O260Kg is mixed with solution A.
4,60Kg boric acid is dissolved in 100L 40-60 ℃ the water, adds 25Kg potassium hydroxide then, fully reaction is regulated the pH value to 5-6, adds solution A then, stirs, and adds urea 110Kg again, promptly obtains solution B.
5, in solution B, add eight 45L xanthohumic acid+sodium salicylates+Lalgine composite solution, special compound additive 25L, sodium bisulfite 1Kg transfers to 3-3.5 with the pH value, and water is settled to 1000L then.
Embodiment 2
Take by weighing raw material in following ratio, and preparation:
1, the preparation of xanthohumic acid+sodium salicylate+Lalgine composite solution: water content is no more than the levigate 20-40 of mistake of 6% peat composed of rotten mosses mesh sieve, add 1% citric acid solution, mix and left standstill 24 hours, then with the nitric acid of 10-20% concentration in 1: 10 ratio thorough mixing in reactor, maintain the temperature at 80-100 ℃, stir after 40-60 minute, be cooled to normal temperature, filtering separation, filtrate are nitro xanthohumic acid solution.Every liter of xanthohumic acid solution adds 40 gram sodium salicylates, stirs after 20-30 minute, adds 17 gram Lalgines, is to be xanthohumic acid+sodium salicylate+Lalgine composite solution.
2, the preparation of special compound additive: trolamine, glycine, sucrose fatty ester were mixed according to 10: 5: 1, in mixed solution, add 2 parts of OP-10 then, stir, be mixed with special compound additive.
3, weighing 125Kg citric acid is dissolved in 250L 60-80 ℃ the water, dissolves in FeSO successively
47H
2O 120Kg, CuSO
45H
2O 70Kg, MnCl
26H
2O 35Kg, Zn (NO
3)
27H
2O280Kg is mixed with solution A.
4,75Kg boric acid is dissolved in 100L 40-60 ℃ the water, adds 35Kg potassium hydroxide then, fully reaction is regulated the pH value to 5-6, adds solution A then, stirs, and adds urea 125Kg again, promptly obtains solution B.
5, in solution B, add 60L xanthohumic acid+sodium salicylate+Lalgine composite solution, composite assistant 35L, sodium bisulfite 1Kg transfers to 3-3.5 with the pH value, and water is settled to 1000L then.
Embodiment 3
Take by weighing raw material in following ratio, and preparation:
1, the preparation of xanthohumic acid+sodium salicylate+Lalgine composite solution: water content is no more than the levigate 20-40 of mistake of 6% peat composed of rotten mosses mesh sieve, add 1% citric acid solution, mix and left standstill 24 hours, then with the nitric acid of 10-20% concentration in 1: 10 ratio thorough mixing in reactor, maintain the temperature at 80-100 ℃, stir after 40-60 minute, be cooled to normal temperature, filtering separation, filtrate are xanthohumic acid solution.Every liter of xanthohumic acid solution adds 45 gram sodium salicylates, stirs after 20-30 minute, adds 18 gram Lalgines, is to be xanthohumic acid+sodium salicylate+Lalgine composite solution.
2, the preparation of special compound additive: trolamine, glycine, sucrose fatty ester were mixed according to 10: 5: 1, in mixed solution, add 2 parts of OP-10 then, stir, be mixed with special compound additive.
3, weighing 140Kg citric acid is dissolved in 250L 60-80 ℃ the water, dissolves in FeSO successively
47H
2O 130Kg, CuSO
45H
2O 90Kg, MnCl
26H
2O 45Kg, Zn (NO
3)
27H
2O290Kg is mixed with solution A.
4,90Kg boric acid is dissolved in 100L 40-60 ℃ the water, adds 45Kg potassium hydroxide then, fully reaction is regulated the pH value to 5-6, adds solution A then, stirs, and adds urea 135Kg again, promptly obtains solution B.
5, in solution B, add 75L xanthohumic acid+sodium salicylate+Lalgine composite solution, composite assistant 45L, sodium bisulfite 1Kg transfers to 3-3.5 with the pH value, and water is settled to 1000L then.
Five, the active research of microelement type composite foliage fertilizer liquid
1, special compound additive is to the influence of blade face nutrition absorption
For verifying that special-purpose composite assistant utilizes apple to carry out the Foliage Absorption test to the influence of blade face nutrition absorption effect in the microelement type foliar nutrient.
Special compound additive is by liking the preparation of technical division of fertile (Beijing) agrotechnique company limited, and the best working concentration in blade face is 50mg/L.Test is carried out in Wang Qu orchard, color town, Beijing's Shunyi District south, and apple variety is the Fuji apple, the age of tree 5 years, and the fruit tree seeding row spacing is 3 * 5m, establishes 3 processing: A, foliage-spray clear water (ck) altogether; B, the common trace element solution of foliage-spray (ck); C, foliage-spray contain the trace element solution (CS1) of 50mg/L special compound additive.
Every strain sprays the 6L diluent.Contain Fe, Mn, Cu, Zn, B concentration is 50mg/kg.
As table 1, apple blade critical surface tension value is low, and spray liquid is not easy on the blade face wetting, and blade face nutrition absorption effect is obvious not as general crop.When not adding special compound additive, blade is few to trace elements absorbed, and wherein blade does not have notable difference to absorption and the contrast of Cu.After adding special compound additive, blade obviously improves various trace elements absorbed.The special compound additive that this invention is described can significantly improve fruit tree leaf to the trace elements absorbed ability.
Table 1, to the influence of apple blade nutrient content (mg/kg)
| Handle | Fe | Mn | Cu | Zn | B |
| A B C | 118.2c 125.1b 148.6a | 23.2c 30.6b 42.13a | 4.3c 5.1b 6.35a | 9.2c 15.7b 23.2a | 46.8c 70.3b 78.7a |
2, microelement type composite foliage fertilizer is to promoting the influence of fruit color, increase sugar degree
Table 2 is the influences to fruit qualities such as apple, peach, grapes.As seen from Table 2: the processing of use microelement type composite foliage fertilizer has significantly increased the content of fruit soluble solid, has reduced fruit acidity, increases colourity.Because this processing equilibrium provides micro-element nutrition, not only can improve the light and the ability to function of blade, and help the generation and the transportation of carbohydrate, to improving fruit qualities such as apple, peach, grape obvious effects is arranged all.
Six, effect of increasing production analysis
2003-2006 has carried out simultaneous test on Shaanxi Province's apple, Hebei province's grape and peach produce, the result is as follows:
1, test design:
Apple and peach are adopted pair test, establish 3 processing, 4 repetitions, and each selects the fruit tree of 12 strain upgrowth situation basically identicals, and bar shaped is arranged.The grape harvest plot experiment is established 3 processing, 4 repetitions, 4 * 10 square metres of areas.
Handle 1, microelement type composite foliage fertilizer.Handle 2, common trace elements leaf fertilizer (conventional contrast).Handle 3, CK (blank clear water contrast).
2, using method:
First fruit phase, expanding stage at apple use 800-1000 times of liquid, the each 6L of every strain; Use 800-1000 times of liquid, the each 6L of every strain in the young fruit period of peach, painted phase; Veraison 800-1000 times of liquid of the young fringe phase of grape and swollen fruit uses every mu of each 3-5L.
3, result:
Yield result is carried out variance analysis and PLSD check, comparative result such as table 3.
Table 2, different treatment are to the influence of apple, peach, grape fruit quality
| Handle | Soluble solid (%) | Titratable acid (%) | Degree of staining | |
| Apple | Common foliar nutrient | 13.1 | 0.36 | 3 |
| Microelement type composite foliage fertilizer | 14.0 | 0.29 | 5 | |
| Grape | Common foliar nutrient | 15.2 | 0.41 | 4 |
| Microelement type composite foliage fertilizer | 17.3 | 0.36 | 5 | |
| Peach | Common foliar nutrient | 10.2 | 0.25 | 4 |
| Microelement type composite foliage fertilizer | 12.3 | 0.19 | 5 |
Table 3 microelement type composite foliage fertilizer is to the influence of fruits output
| Kind | Test site | Amount of increase in production (%) | The results of analysis of variance |
| Apple peach grape | Hanzhong City Hebei province, Shaanxi Province Shen Zhoushi Hebei province Zhangjiakou City | 12.9 13.6 14.7 | Difference is utmost point conspicuous level difference and is remarkable level difference and is utmost point conspicuous level |
Claims (3)
1, a kind of microelement type composite foliage fertilizer material is characterized in that being made up of xanthohumic acid+sodium salicylate+Lalgine composite solution, special compound additive, solution B and sodium bisulfite;
Wherein, the preparation method of xanthohumic acid+sodium salicylate+Lalgine composite solution is: water content is no more than 6% the levigate 20-40 of mistake of peat composed of rotten mosses mesh sieve, add 1% citric acid solution, mix and to leave standstill 24 hours, then with concentration be the nitric acid of 10-20% according to 1: 10 ratio thorough mixing in reactor, maintain the temperature at 80-100 ℃, stir after 40-60 minute, be cooled to normal temperature, filtering separation, filtrate is xanthohumic acid solution; Add 30-50 gram sodium salicylate in every liter of xanthohumic acid solution, stir after 20-30 minute, add 15-20 gram Lalgine, promptly get xanthohumic acid+sodium salicylate+Lalgine composite solution;
The preparation method of special compound additive is: trolamine, glycine, sucrose fatty ester were mixed according to 10: 5: 1, add 2 parts of OP-10 then in mixed solution, promptly get special compound additive;
The preparation method of solution B is: weighing 100-150Kg citric acid is dissolved in 250L60-80 ℃ the water, dissolves in FeSO successively
47H
2O 100-150Kg, CuSO
45H
2O50-100Kg, MnCl
26H
2O 20-50Kg, Zn (NO
3)
27H
2O 250-300Kg is mixed with solution A; 50-100Kg boric acid is dissolved in 100L 40-60 ℃ the water, adds 20-50Kg potassium hydroxide then, fully reaction is regulated pH value to 5-6; Add solution A then, stir, add urea 100-150Kg again, promptly obtain solution B;
In solution B, add xanthohumic acid+sodium salicylate+Lalgine composite solution 30-80L, sodium bisulfite 1Kg, special compound additive 20-50L transfers to 3-3.5 with the pH value, and water is settled to 1000L then, promptly makes the microelement type composite foliage fertilizer material.
2, microelement type composite foliage fertilizer material according to claim 1 is characterized in that: weighing 100-140Kg citric acid is dissolved in 250L 60-80 ℃ the water, dissolves in FeSO successively
47H
2O 100-140Kg, CuSO
45H
2O 50-90Kg, MnCl
26H
2O20-40Kg, Zn (NO
3)
27H
2O 250-290Kg is mixed with solution A; 50-90Kg boric acid is dissolved in 100L 40-60 ℃ the water, adds 20-40Kg potassium hydroxide then, fully reaction is regulated pH value to 5-6; Add solution A then, stir, add urea 100-140Kg again, promptly obtain solution B.
3, microelement type composite foliage fertilizer material according to claim 1 and 2 is characterized in that: weighing 120-140Kg citric acid is dissolved in 250L 60-80 ℃ the water, dissolves in FeSO successively
47H
2O 120-140Kg, CuSO
45H
2O 60-90Kg, MnCl
26H
2O 30-40Kg, Zn (NO
3)
27H
2O 260-290Kg is mixed with solution A; 60-90Kg boric acid is dissolved in 100L 40-60 ℃ the water, adds 30-40Kg potassium hydroxide then, fully reaction is regulated pH value to 5-6; Add solution A then, stir, add urea 120-140Kg again, promptly obtain solution B.
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| CN107459424B (en) * | 2017-08-08 | 2020-07-03 | 山东农业大学 | Application of sodium salicylate in improving chelating efficiency and stability of fulvic acid iron and improving method |
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| CN115385744A (en) * | 2022-09-13 | 2022-11-25 | 新疆益果生物科技有限责任公司 | Apple calcium alginate water-soluble leaf fertilizer for Xinjiang saline-alkali soil and preparation method thereof |
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