CN1268556A - 含有钼化合物、酚盐和二芳基胺的润滑剂 - Google Patents
含有钼化合物、酚盐和二芳基胺的润滑剂 Download PDFInfo
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- CN1268556A CN1268556A CN00102596A CN00102596A CN1268556A CN 1268556 A CN1268556 A CN 1268556A CN 00102596 A CN00102596 A CN 00102596A CN 00102596 A CN00102596 A CN 00102596A CN 1268556 A CN1268556 A CN 1268556A
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Abstract
Description
组分 | 油#1 | 油#2 | 油#3 | 油#4 | 油#5 | 油#6 | 油#7 | 油#8 | 油#9 | 油#10 | 油#11 | 油#12 | 油#13 | 油#14 | 油#15 | 油#16 |
预混油 | 97 | 97 | 97 | 97 | 97 | 97 | 97 | 97 | 97 | 97 | 97 | 97 | 97 | 97 | 97 | 97 |
在预混油中的二苯胺 | 0.3 | 0.3 | 0.3 | 0.3 | 0.3 | 0.3 | 0.3 | 0.3 | 0.3 | 0.3 | 0.3 | 0.3 | 0.3 | 0.3 | 0 | 0 |
低TBN磺酸钙 | 0.9 | 0.5 | 0.5 | 0 | 0.4 | 0.9 | 1.4 | 0.5 | 1.0 | 0.7 | 0.9 | 1.0 | 0.5 | 0.5 | 0.5 | 0.7 |
高TBN磺酸钙 | 0.6 | 0.9 | 1.0 | 1.7 | 1.7 | 0.6 | 0.6 | 1.0 | 1.0 | 1.4 | 0.6 | 0.3 | 1.0 | 0.9 | 1.0 | 1.4 |
磺酸镁 | 0.9 | 1.2 | 0 | 0 | 0 | 0.9 | 0.9 | 0 | 0 | 0 | 0.9 | 0.9 | 0 | 0 | 0 | 0 |
苯酚钙 | 0 | 0 | 1.0 | 1.0 | 0.5 | 0 | 0 | 1.0 | 1.0 | 0.5 | 0 | 0 | 1.0 | 1.0 | 1.0 | 0.5 |
高碱性磺酸钠 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0.2 | 0 | 0.2 | 0 | 0 |
环烷酸酮 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0.25 | 0 | 0.25 | 0 | 0 | 0 |
钼化合物 | 0 | 0 | 0 | 0 | 0 | 0.25 | 0 | 0.25 | 0 | 0.125 | 0 | 0 | 0 | 0 | 0.25 | 0.125 |
操作油 | 0.6 | 0.4 | 0.5 | 0.3 | 0.4 | 0.35 | 0.10 | 0.25 | 0 | 0.28 | 0.35 | 0.6 | 0.2 | 0.6 | 0.25 | 0.28 |
氧化开始温度℃ | 油#1 | 油#2 | 油#3 | 油#4 | 油#5 | 油#6 | 油#7 | 油#8* | 油#9 | 油#10* | 油#11 | 油#12 | 油#13 | 油#14 | 油#15 | 油#16 |
#1 | 204.7 | 205.6 | 211.7 | 209.2 | 208.9 | 214.2 | 206.1 | 219.3 | 211.9 | 214.9 | 209.8 | 206.9 | 212.7 | 214.3 | 200.3 | 196.0 |
#2 | 207.3 | 206.7 | 211.4 | 212.1 | 208.2 | 213.9 | 205.4 | 218.8 | 211.2 | 216.0 | 209.0 | 206.4 | 211.4 | 212.2 | 200.3 | 196.6 |
#3 | 205.0 | 206.1 | 211.5 | 211.5 | 206.8 | 214.0 | 205.6 | 218.2 | 212.2 | 212.4 | 209.7 | 207.0 | 211.3 | 209.3 | 197.9 | 195.4 |
#4 | 204.3 | … | … | 212.0 | … | … | … | … | … | 211.6 | … | … | 211.3 | 211.1 | … | … |
平均 | 205.3 | 206.1 | 211.5 | 211.2 | 208.0 | 214.0 | 205.7 | 218.8 | 211.8 | 213.7 | 209.5 | 206.8 | 211.7 | 211.7 | 199.5 | 196.0 |
时间min | 油#1 | 油#2 | 油#3 | 油#4 | 油#5 | 油#6 | 油#7 | 油#8*+ | 油#9+ | 油#10* | 油#11 | 油#12 | 油#13 | 油#14 | 油#15 | 油#16 |
90 | 17.9 | 16.7 | 2.2 | 3.8 | 1.6 | 0.4 | 12.7 | 0.70.4 | 0.91.4 | 0.3 | 3.4 | 15.1 | 1.2 | 5.7 | 9.9 | 5.5 |
120 | 19.3 | 21.4 | 12.9 | 16.3 | 9.8 | 4.7 | 16.6 | 0.61.3 | 4.32.9 | 0.9 | 4.0 | 17.0 | 8.1 | 12.3 | 11.7 | 15.7 |
150 | 19 | 21.6 | 13.2 | 15.9 | 15.6 | 3.9 | 16.3 | 1.10.9 | 8.96.8 | 1.0 | 15.4 | 20.0 | 11.3 | 18.4 | 13.8 | 18.1 |
180 | 19 | 21.2 | 12.3 | 16.4 | 13.4 | 6.7 | 18.5 | 2.01.1 | 11.811.3 | 3.9 | 12.4 | 18.8 | 11.6 | 15.2 | 16.8 | 17.0 |
试验 | 油#17 | 油#18* |
CMOT-时间min | ||
90 | 2.1 | 1.8 |
120 | 2.1 | 1.7 |
150 | 2.9 | 1.7 |
180 | 16.5 | 2.0 |
1M-PC沉积物测定值 | 300.3 | 156.6 |
组分 | 油#17 | 油#18* | 油#19* | 油#20 |
分散剂 | 3.57 | 3.76 | 3.76 | 4.18 |
去垢剂 | 0.743 | 0.89 | 0.89 | 1.06 |
抗磨剂 | 0.588 | 0.7 | 0.7 | 0.65 |
抗氧剂(二芳基胺除外) | 0.336 | 0.45 | 0.45 | 0.42 |
破乳剂、硅酮、防锈剂、稀释剂 | 0.341 | 0.343 | 0.39 | 0.31 |
VI改性剂/PPD | 11.0 | 9.1 | 9.1 | 7.79 |
基油 | 81.99 | 83.4 | 83.4 | 84.5 |
苯酚钙 | 0.756 | 0.58 | 0.58 | 0.44 |
二芳基胺 | 0.676 | 0.61 | 0.61 | 0.65 |
钼 | ||||
辛酸钼 | … | … | 0.12 | … |
MolyvanTM855 | … | 0.167 | … | … |
1M-PC试验参数 | 油#17 | 油#18* | 油#19* | 油#20 |
第一道环槽充满,% | 60 | 35 | 56 | 13 |
WTD | 300.3 | 156.6 | 239 | 272.5 |
环侧间隙损失,mm | 0.013 | 0 | 0 | 0 |
合格/不合格 | 不合格 | 合格 | 合格 | 不合格 |
试验参数 | 油#18 | 合格范围 |
平均挺杆面磨损(高度),μm | 6.88 | 4-8 |
平均挺杆重量损失,g | -0.025 | 通常为负值 |
平均球窝磨损,μm | 6.67 | 不是好的鉴别因素 |
平均内衬磨损,μm | 2.49 | 1-2.6 |
第一道活塞环平均磨损,mg | 7.7 | 未报告 |
第二道活塞环平均磨损,mg | 38.2 | 未报告 |
连杆轴承平均重量损失,mg | 1.8 | 4-17 |
未称重活塞沉积物额定值,缺点 | 89.6 | 70-120 |
进气阀/排气阀沉积物平均额定值,缺点 | 9.3 | 8.4-9.7取决于阀杆密封 |
排气阀平均凹入,μm | 60 | 5-350取决于阀杆密封 |
粘度增加,KV在100℃ | -7.26% | 约增加4% |
所用油Pb在EOT,ppm | 3 | 0-5 |
所用油Fe在EOT,ppm | 10 | 8-9 |
所用油Cu在EOT,ppm | 32 | 能够热交换钝化 |
总碱值下降,按D4739测定 | 1.55 | 多数油下降3个单位 |
总酸值增加,按D664-87测定 | 0.45 | 多数油增加约1个单位 |
试验参数 | 油#18的数值 | 允许限度 |
轴承重量损失 | 15.6mg | 40mg最大 |
新油粘度 | 14.09 | |
粘度在10hr | 13.05 | 按级别定(Stay in Grade) |
20hr | 12.70 | 按级别定 |
30hr | 12.72 | 按级别定 |
40hr | 12.62 | 按级别定 |
合格/不合格 | 合格 |
组分 | 油#21 | 油#22* | 油#23 | 油#24* |
苯酚钙 | 2.3 | 2.3 | 2.3 | 2.3 |
非二芳基胺抗氧剂 | 0.8 | 0.8 | 0.5 | 0.5 |
二芳基胺 | 0.4 | 0.4 | 0.4 | 0.4 |
MolyvanTM 855 | … | 0.167 | … | 0.167 |
参数 | 油#21 | 油#22* | 油#23 | 油#24* |
Panel沉积物(mg) | 247 | 55 | 533 | 319 |
试验参数 | 油#18 | 可接受的限度 |
粘度增至375%的小时数 | 70.8 | 64最小 |
平均淤渣 | 9.49 | 9.2最小 |
平均积炭 | 8.78 | 8.9最小 |
环面积炭 | 5.19 | 3.5最小 |
凸轮和挺杆磨损,平均,μm | 17.2 | 30最大 |
凸轮和挺杆磨损,最大μm | 38 | 64最大 |
合格/不合格 | 磨损合格 |
油#25 | 油#26 | 油#27* | |
分散剂 | 9.6 | 9.6 | 9.583 |
去垢剂 | 0.66 | 1.06 | 0.659 |
抗磨剂 | 1.45 | 1.45 | 1.447 |
辅助抗氧剂 | 0.8 | 0.8 | 0.799 |
硅酮/稀释剂 | 0.59 | 0.59 | 0.591 |
VI改进剂/PPD | 6.15 | 6.15 | 6.139 |
基油 | |||
矿物油 | 56.05 | 55.55 | 55.957 |
聚α-烯烃 | 22 | 22 | 21.963 |
苯酚钙 | 2.3 | 2.3 | 2.296 |
二芳基胺 | 0.4 | 0.5 | 0.399 |
钼 | |||
MolyvanTM855 | … | … | 0.167 |
1P试验参数 | 油#25试验#1 | 油#25试验#2 | 油#25试验#3 | 油#26 | 油#27* | 限度 |
沉积物总重 | 390.6 | … | … | 384.8 | 268.3 | 350最大 |
顶槽碳 | 29.75 | … | … | 60.00 | 25.25 | 36最大 |
顶面碳 | 69.25 | … | … | 48.00 | 28 | 40最大 |
平均油耗g/h(0-360h) | 10.0 | … | … | 14.1 | 7.5 | 12.4最大 |
最终油耗g/h(312-360h) | 19.4 | … | … | 39.5 | 7.9 | 14.6最大 |
划痕,活塞,环,内衬 | 无 | … | … | 无 | 无 | 无 |
注解 | 不合格 | 因油耗过高未能完成试验 | 因油耗过高未能完成试验 | 不合格 | 合格 |
Claims (31)
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US09/281,747 US6174842B1 (en) | 1999-03-30 | 1999-03-30 | Lubricants containing molybdenum compounds, phenates and diarylamines |
US09/281747 | 1999-03-30 |
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US (1) | US6174842B1 (zh) |
EP (1) | EP1041134B1 (zh) |
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KR (1) | KR100356073B1 (zh) |
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JP3608805B2 (ja) | 1993-04-30 | 2005-01-12 | 東燃ゼネラル石油株式会社 | 潤滑油組成物 |
GB9318928D0 (en) | 1993-09-13 | 1993-10-27 | Exxon Research Engineering Co | Lubricant composition containing combination of antiwear and antioxidant additives |
EP0719312B1 (en) | 1993-09-13 | 1999-12-15 | Infineum USA L.P. | Lubricating compositions with improved antioxidancy |
JPH07286190A (ja) | 1994-03-31 | 1995-10-31 | Tonen Corp | 潤滑油組成物 |
JP3454593B2 (ja) * | 1994-12-27 | 2003-10-06 | 旭電化工業株式会社 | 潤滑油組成物 |
US5650381A (en) | 1995-11-20 | 1997-07-22 | Ethyl Corporation | Lubricant containing molybdenum compound and secondary diarylamine |
US5726133A (en) | 1996-02-27 | 1998-03-10 | Exxon Research And Engineering Company | Low ash natural gas engine oil and additive system |
US5736491A (en) * | 1997-01-30 | 1998-04-07 | Texaco Inc. | Method of improving the fuel economy characteristics of a lubricant by friction reduction and compositions useful therein |
US5840672A (en) | 1997-07-17 | 1998-11-24 | Ethyl Corporation | Antioxidant system for lubrication base oils |
US6103674A (en) * | 1999-03-15 | 2000-08-15 | Uniroyal Chemical Company, Inc. | Oil-soluble molybdenum multifunctional friction modifier additives for lubricant compositions |
-
1999
- 1999-03-30 US US09/281,747 patent/US6174842B1/en not_active Expired - Lifetime
-
2000
- 2000-02-25 CA CA002299229A patent/CA2299229C/en not_active Expired - Fee Related
- 2000-03-03 SG SG200001185A patent/SG76648A1/en unknown
- 2000-03-08 AU AU20726/00A patent/AU758452B2/en not_active Ceased
- 2000-03-23 JP JP2000082058A patent/JP3507915B2/ja not_active Expired - Lifetime
- 2000-03-29 KR KR1020000016157A patent/KR100356073B1/ko not_active IP Right Cessation
- 2000-03-30 CN CNB001025961A patent/CN1175091C/zh not_active Expired - Lifetime
- 2000-03-30 EP EP00302646.5A patent/EP1041134B1/en not_active Expired - Lifetime
Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101235335B (zh) * | 2007-01-19 | 2015-01-28 | 雅富顿公司 | 高总碱值/低磷的经济的拖拉机超级通用油润滑剂 |
CN103642565B (zh) * | 2007-01-19 | 2015-09-09 | 雅富顿公司 | 高总碱值/低磷的经济的拖拉机超级通用油润滑剂 |
CN101236965B (zh) * | 2007-02-01 | 2011-05-11 | 瑞萨电子株式会社 | 半导体集成电路装置 |
CN102666819A (zh) * | 2009-12-24 | 2012-09-12 | 吉坤日矿日石能源株式会社 | 十字头型柴油机用气缸润滑油组合物 |
CN102666819B (zh) * | 2009-12-24 | 2013-09-11 | 吉坤日矿日石能源株式会社 | 十字头型柴油机用气缸润滑油组合物 |
CN102533362A (zh) * | 2012-01-09 | 2012-07-04 | 华东理工大学 | 一种无硫磷含钼抗氧剂及其制备方法和应用 |
CN102533362B (zh) * | 2012-01-09 | 2014-05-14 | 华东理工大学 | 一种无硫磷含钼抗氧剂及其制备方法和应用 |
CN109196079A (zh) * | 2016-07-13 | 2019-01-11 | 雪佛龙奥伦耐有限责任公司 | 含有抗氧化剂混合物的协同润滑油组合物 |
CN109196079B (zh) * | 2016-07-13 | 2022-04-05 | 雪佛龙奥伦耐有限责任公司 | 含有抗氧化剂混合物的协同润滑油组合物 |
CN107868108A (zh) * | 2016-09-28 | 2018-04-03 | 中国石油化工股份有限公司 | 一种有机钼盐及其制备方法 |
CN107868108B (zh) * | 2016-09-28 | 2021-04-06 | 中国石油化工股份有限公司 | 一种有机钼盐及其制备方法 |
Also Published As
Publication number | Publication date |
---|---|
EP1041134B1 (en) | 2019-05-08 |
KR100356073B1 (ko) | 2002-10-11 |
JP3507915B2 (ja) | 2004-03-15 |
EP1041134A3 (en) | 2001-09-19 |
JP2000290675A (ja) | 2000-10-17 |
SG76648A1 (en) | 2000-11-21 |
EP1041134A2 (en) | 2000-10-04 |
CA2299229A1 (en) | 2000-09-30 |
KR20000063052A (ko) | 2000-10-25 |
US6174842B1 (en) | 2001-01-16 |
CN1175091C (zh) | 2004-11-10 |
AU2072600A (en) | 2000-10-05 |
CA2299229C (en) | 2003-07-22 |
AU758452B2 (en) | 2003-03-20 |
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