CN1200040C - 一种有机-无机纳米碳酸钙活性混合物及其制备方法 - Google Patents
一种有机-无机纳米碳酸钙活性混合物及其制备方法 Download PDFInfo
- Publication number
- CN1200040C CN1200040C CN 03143174 CN03143174A CN1200040C CN 1200040 C CN1200040 C CN 1200040C CN 03143174 CN03143174 CN 03143174 CN 03143174 A CN03143174 A CN 03143174A CN 1200040 C CN1200040 C CN 1200040C
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- CN
- China
- Prior art keywords
- calcium carbonate
- nano
- organic
- nano calcium
- inorganic nano
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 title claims abstract description 88
- 229910000019 calcium carbonate Inorganic materials 0.000 title claims abstract description 57
- 239000000203 mixture Substances 0.000 title claims abstract description 45
- 238000000034 method Methods 0.000 title claims description 16
- 230000008569 process Effects 0.000 title description 7
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 18
- 239000002245 particle Substances 0.000 claims abstract description 16
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 14
- 239000003822 epoxy resin Substances 0.000 claims abstract description 11
- 238000007599 discharging Methods 0.000 claims abstract description 4
- 235000012204 lemonade/lime carbonate Nutrition 0.000 claims description 25
- 239000002105 nanoparticle Substances 0.000 claims description 22
- 239000004593 Epoxy Substances 0.000 claims description 15
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical group C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 claims description 15
- 238000002844 melting Methods 0.000 claims description 15
- 230000008018 melting Effects 0.000 claims description 15
- 238000010792 warming Methods 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 9
- 229920005989 resin Polymers 0.000 claims description 8
- 239000011347 resin Substances 0.000 claims description 8
- 125000003700 epoxy group Chemical group 0.000 claims description 7
- 235000021355 Stearic acid Nutrition 0.000 claims description 5
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 5
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 239000008117 stearic acid Substances 0.000 claims description 5
- QGBSISYHAICWAH-UHFFFAOYSA-N dicyandiamide Chemical compound NC(N)=NC#N QGBSISYHAICWAH-UHFFFAOYSA-N 0.000 claims description 4
- BBBUAWSVILPJLL-UHFFFAOYSA-N 2-(2-ethylhexoxymethyl)oxirane Chemical compound CCCCC(CC)COCC1CO1 BBBUAWSVILPJLL-UHFFFAOYSA-N 0.000 claims description 3
- YSUQLAYJZDEMOT-UHFFFAOYSA-N 2-(butoxymethyl)oxirane Chemical compound CCCCOCC1CO1 YSUQLAYJZDEMOT-UHFFFAOYSA-N 0.000 claims description 3
- CUFXMPWHOWYNSO-UHFFFAOYSA-N 2-[(4-methylphenoxy)methyl]oxirane Chemical compound C1=CC(C)=CC=C1OCC1OC1 CUFXMPWHOWYNSO-UHFFFAOYSA-N 0.000 claims description 3
- CMBRSAKTEQFDPC-UHFFFAOYSA-N 4,5-diethyl-1h-imidazole Chemical class CCC=1N=CNC=1CC CMBRSAKTEQFDPC-UHFFFAOYSA-N 0.000 claims description 3
- 229930185605 Bisphenol Natural products 0.000 claims description 3
- FQYUMYWMJTYZTK-UHFFFAOYSA-N Phenyl glycidyl ether Chemical compound C1OC1COC1=CC=CC=C1 FQYUMYWMJTYZTK-UHFFFAOYSA-N 0.000 claims description 3
- AWMVMTVKBNGEAK-UHFFFAOYSA-N Styrene oxide Chemical compound C1OC1C1=CC=CC=C1 AWMVMTVKBNGEAK-UHFFFAOYSA-N 0.000 claims description 3
- 229910052791 calcium Inorganic materials 0.000 claims description 3
- 239000011575 calcium Substances 0.000 claims description 3
- JDVIRCVIXCMTPU-UHFFFAOYSA-N ethanamine;trifluoroborane Chemical compound CCN.FB(F)F JDVIRCVIXCMTPU-UHFFFAOYSA-N 0.000 claims description 3
- 238000001125 extrusion Methods 0.000 claims description 3
- 239000011248 coating agent Substances 0.000 claims description 2
- 238000000576 coating method Methods 0.000 claims description 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 claims 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims 1
- 239000005642 Oleic acid Substances 0.000 claims 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 claims 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims 1
- 239000000463 material Substances 0.000 abstract description 23
- 238000002156 mixing Methods 0.000 abstract description 23
- 238000002360 preparation method Methods 0.000 abstract description 15
- 239000002114 nanocomposite Substances 0.000 abstract description 4
- 230000000630 rising effect Effects 0.000 abstract 2
- 239000003085 diluting agent Substances 0.000 abstract 1
- 239000004850 liquid epoxy resins (LERs) Substances 0.000 abstract 1
- 239000011148 porous material Substances 0.000 abstract 1
- 235000010216 calcium carbonate Nutrition 0.000 description 16
- 239000002131 composite material Substances 0.000 description 10
- 238000006116 polymerization reaction Methods 0.000 description 10
- 239000011159 matrix material Substances 0.000 description 9
- 239000004800 polyvinyl chloride Substances 0.000 description 7
- 229920000915 polyvinyl chloride Polymers 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 6
- 239000004594 Masterbatch (MB) Substances 0.000 description 5
- 230000004048 modification Effects 0.000 description 5
- 230000002776 aggregation Effects 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000012986 modification Methods 0.000 description 4
- 229920000642 polymer Polymers 0.000 description 4
- 238000005054 agglomeration Methods 0.000 description 3
- 230000005540 biological transmission Effects 0.000 description 3
- 238000009472 formulation Methods 0.000 description 3
- 238000011065 in-situ storage Methods 0.000 description 3
- 229920002521 macromolecule Polymers 0.000 description 3
- 239000011858 nanopowder Substances 0.000 description 3
- -1 nonionogenic tenside Chemical class 0.000 description 3
- 230000035939 shock Effects 0.000 description 3
- 230000004913 activation Effects 0.000 description 2
- 238000007385 chemical modification Methods 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 1
- 238000005411 Van der Waals force Methods 0.000 description 1
- 230000004931 aggregating effect Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000007822 coupling agent Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 238000001746 injection moulding Methods 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 239000004530 micro-emulsion Substances 0.000 description 1
- 238000002715 modification method Methods 0.000 description 1
- 239000003607 modifier Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920001610 polycaprolactone Polymers 0.000 description 1
- 239000004632 polycaprolactone Substances 0.000 description 1
- 239000002861 polymer material Substances 0.000 description 1
- 239000013339 polymer-based nanocomposite Substances 0.000 description 1
- 230000005476 size effect Effects 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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- Compositions Of Macromolecular Compounds (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
Abstract
Description
Claims (6)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 03143174 CN1200040C (zh) | 2003-06-19 | 2003-06-19 | 一种有机-无机纳米碳酸钙活性混合物及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN 03143174 CN1200040C (zh) | 2003-06-19 | 2003-06-19 | 一种有机-无机纳米碳酸钙活性混合物及其制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN1468902A CN1468902A (zh) | 2004-01-21 |
CN1200040C true CN1200040C (zh) | 2005-05-04 |
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CN 03143174 Expired - Lifetime CN1200040C (zh) | 2003-06-19 | 2003-06-19 | 一种有机-无机纳米碳酸钙活性混合物及其制备方法 |
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CN (1) | CN1200040C (zh) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102251315B (zh) * | 2011-08-12 | 2013-08-21 | 江门市新会区新华胶丝厂 | 一种耐磨造纸网用聚酯单丝的制备方法 |
CN104028409B (zh) * | 2014-06-10 | 2016-06-22 | 陈曦 | 一种利用纳米碳酸钙吸附漆雾的方法 |
CN105111501B (zh) * | 2015-07-30 | 2018-05-01 | 杭州明鑫钙业有限公司 | 一种热塑性碳酸钙增韧粒子及其制备方法 |
CN106220892B (zh) * | 2016-08-16 | 2019-04-05 | 谭国权 | 环氧树脂固化包覆物及其制备方法 |
CN113113224A (zh) * | 2021-04-14 | 2021-07-13 | 中国科学院宁波材料技术与工程研究所 | 一种模压电感用软磁粉末的新型绝缘包覆方法 |
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2003
- 2003-06-19 CN CN 03143174 patent/CN1200040C/zh not_active Expired - Lifetime
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Publication number | Publication date |
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CN1468902A (zh) | 2004-01-21 |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: CHINA PUTIAN HANGZHOU HONGYAN ELECTRIC CO., LTD. Free format text: FORMER OWNER: HONGYAN ELECTRIC APPLIANCE CO., LTD., HANGZHOU Effective date: 20131203 |
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C56 | Change in the name or address of the patentee |
Owner name: HONGYAN ELECTRIC APPLIANCE CO., LTD., HANGZHOU Free format text: FORMER NAME: HONGYAN ELECTRICAL APPARATUS, HANGZHOU |
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COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 310013 HANGZHOU, ZHEJIANG PROVINCE TO: 311305 HANGZHOU, ZHEJIANG PROVINCE |
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CP03 | Change of name, title or address |
Address after: 310013 B building, Huahong building, 248 Tian Tian Shan Road, Zhejiang, Hangzhou Patentee after: HANGZHOU HONYAR ELECTRICAL Co.,Ltd. Address before: The three District of Hangzhou City, Zhejiang province 310012 Chui Qing Road No. 9 Patentee before: Hangzhou Swangoose Electrical Corp. |
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TR01 | Transfer of patent right |
Effective date of registration: 20131203 Address after: 311305, Zhejiang City, Hangzhou province Ling'an City Qingshan Lake Street Research Village (Ling'an Economic Development Zone) Patentee after: Hangzhou Hongyan Cable Co.,Ltd. Address before: 310013 B building, Huahong building, 248 Tian Tian Shan Road, Zhejiang, Hangzhou Patentee before: HANGZHOU HONYAR ELECTRICAL Co.,Ltd. |
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CX01 | Expiry of patent term |
Granted publication date: 20050504 |
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CX01 | Expiry of patent term |