CN1188505C - 生产洗涤组合物的方法 - Google Patents
生产洗涤组合物的方法 Download PDFInfo
- Publication number
- CN1188505C CN1188505C CNB971816093A CN97181609A CN1188505C CN 1188505 C CN1188505 C CN 1188505C CN B971816093 A CNB971816093 A CN B971816093A CN 97181609 A CN97181609 A CN 97181609A CN 1188505 C CN1188505 C CN 1188505C
- Authority
- CN
- China
- Prior art keywords
- powder
- raw material
- composition
- detergent
- mixing tank
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 52
- 238000000034 method Methods 0.000 title claims abstract description 51
- 239000003599 detergent Substances 0.000 title claims abstract description 24
- 238000004519 manufacturing process Methods 0.000 title abstract description 12
- 230000008569 process Effects 0.000 title abstract description 10
- 239000000843 powder Substances 0.000 claims abstract description 71
- 238000002156 mixing Methods 0.000 claims abstract description 37
- 239000002245 particle Substances 0.000 claims abstract description 34
- 238000005520 cutting process Methods 0.000 claims abstract description 14
- 239000011149 active material Substances 0.000 claims abstract description 13
- 239000007788 liquid Substances 0.000 claims abstract description 12
- 239000002243 precursor Substances 0.000 claims abstract description 8
- 238000003756 stirring Methods 0.000 claims abstract description 6
- 239000002994 raw material Substances 0.000 claims description 21
- 239000011236 particulate material Substances 0.000 claims description 19
- 238000001035 drying Methods 0.000 claims description 17
- 238000005507 spraying Methods 0.000 claims description 14
- 239000000463 material Substances 0.000 claims description 12
- 230000009471 action Effects 0.000 abstract description 2
- 239000007858 starting material Substances 0.000 abstract 3
- 229910021536 Zeolite Inorganic materials 0.000 description 17
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 17
- 239000010457 zeolite Substances 0.000 description 17
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 15
- 238000004140 cleaning Methods 0.000 description 13
- 238000009826 distribution Methods 0.000 description 13
- 238000005406 washing Methods 0.000 description 13
- 101710108306 Bifunctional dihydroflavonol 4-reductase/flavanone 4-reductase Proteins 0.000 description 12
- 101710170824 Dihydroflavonol 4-reductase Proteins 0.000 description 12
- 239000002253 acid Substances 0.000 description 11
- 235000019832 sodium triphosphate Nutrition 0.000 description 9
- 239000007787 solid Substances 0.000 description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
- 101710194948 Protein phosphatase PhpP Proteins 0.000 description 8
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 description 8
- 239000000047 product Substances 0.000 description 8
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 7
- 238000000280 densification Methods 0.000 description 7
- 239000011521 glass Substances 0.000 description 7
- 238000005469 granulation Methods 0.000 description 7
- 230000003179 granulation Effects 0.000 description 7
- 229910052700 potassium Inorganic materials 0.000 description 7
- 239000011591 potassium Substances 0.000 description 7
- 239000002002 slurry Substances 0.000 description 6
- 238000001694 spray drying Methods 0.000 description 6
- 238000001816 cooling Methods 0.000 description 5
- 238000002474 experimental method Methods 0.000 description 5
- 150000002632 lipids Chemical class 0.000 description 5
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
- 239000002671 adjuvant Substances 0.000 description 4
- 230000008901 benefit Effects 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 238000013517 stratification Methods 0.000 description 4
- 125000000217 alkyl group Chemical group 0.000 description 3
- 239000002131 composite material Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- MZSDGDXXBZSFTG-UHFFFAOYSA-M sodium;benzenesulfonate Chemical compound [Na+].[O-]S(=O)(=O)C1=CC=CC=C1 MZSDGDXXBZSFTG-UHFFFAOYSA-M 0.000 description 3
- 239000004094 surface-active agent Substances 0.000 description 3
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 2
- 229920002125 Sokalan® Polymers 0.000 description 2
- 235000010724 Wisteria floribunda Nutrition 0.000 description 2
- 238000004220 aggregation Methods 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 125000001931 aliphatic group Chemical group 0.000 description 2
- 125000000129 anionic group Chemical group 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- -1 for example Chemical compound 0.000 description 2
- 238000006386 neutralization reaction Methods 0.000 description 2
- 230000003472 neutralizing effect Effects 0.000 description 2
- 230000001737 promoting effect Effects 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 238000007127 saponification reaction Methods 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 description 2
- 235000017550 sodium carbonate Nutrition 0.000 description 2
- 230000003068 static effect Effects 0.000 description 2
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical group C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- VCUFZILGIRCDQQ-KRWDZBQOSA-N N-[[(5S)-2-oxo-3-(2-oxo-3H-1,3-benzoxazol-6-yl)-1,3-oxazolidin-5-yl]methyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C1O[C@H](CN1C1=CC2=C(NC(O2)=O)C=C1)CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F VCUFZILGIRCDQQ-KRWDZBQOSA-N 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 125000002947 alkylene group Chemical group 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- VJAGHZLYXAKQID-UHFFFAOYSA-N benzenesulfonic acid;potassium Chemical compound [K].OS(=O)(=O)C1=CC=CC=C1 VJAGHZLYXAKQID-UHFFFAOYSA-N 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 150000002191 fatty alcohols Chemical class 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- RBNPOMFGQQGHHO-UHFFFAOYSA-N glyceric acid Chemical compound OCC(O)C(O)=O RBNPOMFGQQGHHO-UHFFFAOYSA-N 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910017053 inorganic salt Inorganic materials 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- VSXGXPNADZQTGQ-UHFFFAOYSA-N oxirane;phenol Chemical compound C1CO1.OC1=CC=CC=C1 VSXGXPNADZQTGQ-UHFFFAOYSA-N 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- NFIYTPYOYDDLGO-UHFFFAOYSA-N phosphoric acid;sodium Chemical compound [Na].OP(O)(O)=O NFIYTPYOYDDLGO-UHFFFAOYSA-N 0.000 description 1
- 229920000058 polyacrylate Polymers 0.000 description 1
- 229920001444 polymaleic acid Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000004904 shortening Methods 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000003760 tallow Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 description 1
- ABDKAPXRBAPSQN-UHFFFAOYSA-N veratrole Chemical compound COC1=CC=CC=C1OC ABDKAPXRBAPSQN-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
- C11D17/065—High-density particulate detergent compositions
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
- Glanulating (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GBGB9625066.7A GB9625066D0 (en) | 1996-12-02 | 1996-12-02 | Process for the production of a detergent composition |
| GB9625066.7 | 1996-12-02 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1245530A CN1245530A (zh) | 2000-02-23 |
| CN1188505C true CN1188505C (zh) | 2005-02-09 |
Family
ID=10803825
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB971816093A Expired - Fee Related CN1188505C (zh) | 1996-12-02 | 1997-10-29 | 生产洗涤组合物的方法 |
Country Status (14)
| Country | Link |
|---|---|
| EP (1) | EP0942958B2 (de) |
| CN (1) | CN1188505C (de) |
| AR (1) | AR009644A1 (de) |
| AU (1) | AU721831B2 (de) |
| BR (1) | BR9714494A (de) |
| CA (1) | CA2273849C (de) |
| DE (1) | DE69709398T3 (de) |
| EA (1) | EA001453B1 (de) |
| ES (1) | ES2169882T3 (de) |
| GB (1) | GB9625066D0 (de) |
| ID (1) | ID22478A (de) |
| TR (1) | TR199901756T2 (de) |
| WO (1) | WO1998024876A1 (de) |
| ZA (1) | ZA979825B (de) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE69932827T2 (de) | 1998-08-20 | 2007-03-15 | The Procter & Gamble Company, Cincinnati | Verfahren zur herstellung von waschmittel unter einsatz von einem mittelschnellen mischer/verdichter |
| DE69925286T2 (de) * | 1998-09-18 | 2006-02-23 | The Procter & Gamble Company, Cincinnati | Kontinuierliches herstellungsverfahren für waschmittel |
| US6794354B1 (en) | 1998-09-18 | 2004-09-21 | The Procter & Gamble Company | Continuous process for making detergent composition |
| EP1115836A1 (de) * | 1998-09-25 | 2001-07-18 | The Procter & Gamble Company | Granulares waschmittel mit verbessertem aussehen und erhöhter löslichkeit |
| WO2000018874A1 (en) * | 1998-09-25 | 2000-04-06 | The Procter & Gamble Company | Granular detergent composition having improved appearance and solubility |
| JP2002528600A (ja) * | 1998-10-26 | 2002-09-03 | ザ、プロクター、エンド、ギャンブル、カンパニー | 外観と溶解性の改良された粒状洗剤組成物の製造方法 |
| US6951837B1 (en) | 1999-06-21 | 2005-10-04 | The Procter & Gamble Company | Process for making a granular detergent composition |
| US6767882B1 (en) | 1999-06-21 | 2004-07-27 | The Procter & Gamble Company | Process for producing coated detergent particles |
| EP1187902A1 (de) * | 1999-06-21 | 2002-03-20 | The Procter & Gamble Company | Verfahren zur herstellung von beschichteten tensidpartikeln |
| WO2020222996A1 (en) * | 2019-04-29 | 2020-11-05 | The Procter & Gamble Company | A process for making a laundry detergent composition |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB8626082D0 (en) * | 1986-10-31 | 1986-12-03 | Unilever Plc | Detergent powders |
| CA2001535C (en) * | 1988-11-02 | 1995-01-31 | Peter Willem Appel | Process for preparing a high bulk density granular detergent composition |
| GB9125035D0 (en) * | 1991-11-26 | 1992-01-22 | Unilever Plc | Detergent compositions and process for preparing them |
| GB9513327D0 (en) * | 1995-06-30 | 1995-09-06 | Uniliver Plc | Process for the production of a detergent composition |
-
1996
- 1996-12-02 GB GBGB9625066.7A patent/GB9625066D0/en active Pending
-
1997
- 1997-10-29 DE DE69709398T patent/DE69709398T3/de not_active Expired - Lifetime
- 1997-10-29 EP EP97950085A patent/EP0942958B2/de not_active Expired - Lifetime
- 1997-10-29 CN CNB971816093A patent/CN1188505C/zh not_active Expired - Fee Related
- 1997-10-29 BR BR9714494A patent/BR9714494A/pt not_active IP Right Cessation
- 1997-10-29 TR TR1999/01756T patent/TR199901756T2/xx unknown
- 1997-10-29 ID IDW990449A patent/ID22478A/id unknown
- 1997-10-29 ES ES97950085T patent/ES2169882T3/es not_active Expired - Lifetime
- 1997-10-29 WO PCT/EP1997/006073 patent/WO1998024876A1/en active IP Right Grant
- 1997-10-29 EA EA199900516A patent/EA001453B1/ru not_active IP Right Cessation
- 1997-10-29 CA CA002273849A patent/CA2273849C/en not_active Expired - Fee Related
- 1997-10-29 AU AU53168/98A patent/AU721831B2/en not_active Ceased
- 1997-10-31 ZA ZA979825A patent/ZA979825B/xx unknown
- 1997-11-28 AR ARP970105599A patent/AR009644A1/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP0942958B1 (de) | 2001-12-19 |
| ZA979825B (en) | 1999-04-30 |
| ES2169882T3 (es) | 2002-07-16 |
| DE69709398T3 (de) | 2007-04-19 |
| CN1245530A (zh) | 2000-02-23 |
| EP0942958B2 (de) | 2006-12-13 |
| AU721831B2 (en) | 2000-07-13 |
| GB9625066D0 (en) | 1997-01-22 |
| CA2273849C (en) | 2007-04-10 |
| EP0942958A1 (de) | 1999-09-22 |
| CA2273849A1 (en) | 1998-06-11 |
| TR199901756T2 (xx) | 1999-11-22 |
| BR9714494A (pt) | 2000-03-21 |
| WO1998024876A1 (en) | 1998-06-11 |
| DE69709398D1 (de) | 2002-01-31 |
| EA199900516A1 (ru) | 2000-02-28 |
| AU5316898A (en) | 1998-06-29 |
| ID22478A (id) | 1999-10-21 |
| DE69709398T2 (de) | 2002-06-20 |
| AR009644A1 (es) | 2000-04-26 |
| EA001453B1 (ru) | 2001-04-23 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C56 | Change in the name or address of the patentee |
Owner name: UNILEVER N.V. Free format text: FORMER NAME: UNILEVER NV |
|
| CP01 | Change in the name or title of a patent holder |
Address after: Rotterdam Patentee after: Unilever N. V. Address before: Rotterdam Patentee before: Unilever NV |
|
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20050209 Termination date: 20131029 |