CN117653582A - Acne-removing shampoo composition containing sweet wormwood herb extract, preparation and application - Google Patents
Acne-removing shampoo composition containing sweet wormwood herb extract, preparation and application Download PDFInfo
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- CN117653582A CN117653582A CN202410144516.7A CN202410144516A CN117653582A CN 117653582 A CN117653582 A CN 117653582A CN 202410144516 A CN202410144516 A CN 202410144516A CN 117653582 A CN117653582 A CN 117653582A
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- sweet wormwood
- acne
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- 239000000284 extract Substances 0.000 title claims abstract description 149
- 239000000203 mixture Substances 0.000 title claims abstract description 116
- 239000002453 shampoo Substances 0.000 title claims abstract description 53
- 208000002874 Acne Vulgaris Diseases 0.000 title claims abstract description 44
- 206010000496 acne Diseases 0.000 title claims abstract description 44
- 235000001405 Artemisia annua Nutrition 0.000 title claims abstract description 43
- 240000000011 Artemisia annua Species 0.000 title claims abstract description 43
- 238000002360 preparation method Methods 0.000 title claims abstract description 30
- BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 claims abstract description 58
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- OQLKNTOKMBVBKV-UHFFFAOYSA-N hexamidine Chemical compound C1=CC(C(=N)N)=CC=C1OCCCCCCOC1=CC=C(C(N)=N)C=C1 OQLKNTOKMBVBKV-UHFFFAOYSA-N 0.000 claims abstract description 30
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- BTSZTGGZJQFALU-UHFFFAOYSA-N piroctone olamine Chemical class NCCO.CC(C)(C)CC(C)CC1=CC(C)=CC(=O)N1O BTSZTGGZJQFALU-UHFFFAOYSA-N 0.000 claims abstract description 30
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- 239000001522 artemisia absinthium l. herb extract Substances 0.000 claims description 28
- 229940119569 wormwood extract Drugs 0.000 claims description 28
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- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 2
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- QPJVMBTYPHYUOC-UHFFFAOYSA-N methyl benzoate Chemical compound COC(=O)C1=CC=CC=C1 QPJVMBTYPHYUOC-UHFFFAOYSA-N 0.000 description 20
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- LXAHHHIGZXPRKQ-UHFFFAOYSA-N 5-fluoro-2-methylpyridine Chemical group CC1=CC=C(F)C=N1 LXAHHHIGZXPRKQ-UHFFFAOYSA-N 0.000 description 10
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- 239000003921 oil Substances 0.000 description 7
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- 239000004480 active ingredient Substances 0.000 description 6
- 235000008582 Pinus sylvestris Nutrition 0.000 description 5
- 239000001839 pinus sylvestris Substances 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 4
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- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
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- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
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- MTZQAGJQAFMTAQ-UHFFFAOYSA-N ethyl benzoate Chemical compound CCOC(=O)C1=CC=CC=C1 MTZQAGJQAFMTAQ-UHFFFAOYSA-N 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
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- 239000004615 ingredient Substances 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
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- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 description 1
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- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
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- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 1
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- 125000000400 lauroyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
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Abstract
The invention belongs to the technical field of cosmetics, and particularly relates to an acne-removing shampoo composition containing sweet wormwood herb extract, and preparation and application thereof. The shampoo composition is prepared from azelaic acid, piroctone olamine salt, hexamidine di (hydroxyethyl sulfonic acid) salt, sweet wormwood herb extract, red pine leaf extract, behenyl trimethylammonium methyl sulfate, PPG-26-butanol polyether-26, laurocapram, skin conditioning agent, surfactant, humectant, emollient, thickener, softener, preservative, chelating agent, pH regulator and water, and has excellent acne removing effect, and can effectively inhibit secretion of scalp grease and endow scalp with refreshing effect.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to an acne-removing shampoo composition containing sweet wormwood herb extract, and preparation and application thereof.
Background
Folliculitis and acne are main factors causing acnes, and acnes on the scalp often cause skin to be itchy, induce infection, cause red, swollen and itchy skin, possibly run into running water, seriously affect human health and bring about adverse effects on the appearance of the human body.
Greasy hair can cause excessive secretion of oil on scalp, block pores, and easily cause dandruff. The pores are blocked by grease, so that scalp cannot breathe normally, and dandruff is generated; scalp itch is easily caused by hair oil passing, scalp balance is lost due to accumulation of grease, scalp is stimulated, and then the scalp is scratched for a long time to damage the scalp, and even inflammation is caused; hair greasiness can cause hair follicle blockage, affect the growth cycle of hair, and lead the hair to become sparse and easy to fall off; the grease can also make the hair become sticky, increase friction between the hairs and accelerate the occurrence of alopecia.
Although the existing shampoo products are various, few shampoo products truly effective in inhibiting scalp acne and effectively controlling scalp grease are available. Therefore, there is a need to provide a shampoo composition which is effective in removing acne and which is also effective in controlling scalp oil.
Disclosure of Invention
The invention provides a technical scheme for solving the technical problems, and the technical scheme of the invention covers an acne-removing shampoo composition containing sweet wormwood herb extract, and preparation and application thereof. The acne-removing shampoo composition provided by the invention can effectively remove acnes, can effectively inhibit scalp grease secretion, and gives the scalp a fresh and comfortable experience.
The shampoo composition is prepared from azelaic acid, piroctone olamine salt, hexamidine di (hydroxyethyl sulfonic acid) salt, sweet wormwood herb extract, red pine leaf extract, behenyl trimethylammonium methyl sulfate, PPG-26-butanol polyether-26, laurocapram, skin conditioning agent, surfactant, humectant, emollient, thickener, softener, preservative, chelating agent, pH regulator and water, and has excellent acne removing effect, and can effectively inhibit secretion of scalp grease and endow scalp with refreshing effect. Wherein, the components such as azelaic acid, sweet wormwood extract, red pine leaf extract and the like endow the composition with excellent acne removing effect, and especially the combination of the sweet wormwood extract and the red pine leaf extract can obviously enhance the acne removing effect of the scalp; ingredients such as piroctone olamine salt, hexamidine bis (isethionate) salt, etc., impart excellent antidandruff effects to the composition; the combination of the behentrimethylammonium methyl sulfate and the PPG-26-butanol polyether-26 can lead the active ingredients to be effectively delivered and exert effects on scalp and hairy roots, so that the acne removing and scalp grease controlling effects of the composition are more excellent; skin conditioning agents, moisturizers, emollients and the like are effective in caring scalp; the softener imparts a softening effect to the hair.
On the one hand, the acne-removing shampoo composition containing the sweet wormwood herb extract comprises the following components in percentage by mass: 0.01-1.5% azelaic acid, 0.05-0.9% piroctone olamine, 0.01-0.09% hexamidine bis (isethionic acid) salt, 0.1-3% sweet wormwood extract, 0.1-2.5% red pine leaf extract, 0.2-4% behenyl trimethyl ammonium methyl sulfate, 0.2-3.5% PPG-26-butanol polyether-26, 0.01-0.7% laurocapram, 1-8% skin conditioning agent, 0.5-9% surfactant, 3-10% humectant, 3-12% emollient, 0.1-3% thickener, 0.1-2% softener, 0.05-0.5% preservative, 0.01-1% chelating agent, 0.01-2% pH regulator and 30-80% water.
Preferably, the azelaic acid is present in the composition in an amount of 0.01%, 0.02%, 0.05%, 0.1%, 0.2%, 0.3%, 0.5%, 1%, 1.5% or a range between any two values.
Preferably, the piroctone olamine salt is used in the composition in an amount of 0.05%, 0.06%, 0.08%, 0.1%, 0.2%, 0.3%, 0.5%, 0.9% or a range between any two values.
Preferably, the hexamidine bis (isethionic acid) salt is used in the composition in an amount of 0.01%, 0.02%, 0.03%, 0.05%, 0.07%, 0.08%, 0.09% or a range between any two values.
Preferably, the sweet wormwood herb extract is used in the composition in an amount of 0.2-3%, 0.3-3%, 0.4-2.8%, 0.5-2.8% or 0.5-2.5%.
Preferably, the Pinus sylvestris leaf extract is used in an amount of 0.2-2.5%, 0.3-2.5%, 0.4-2.2%, 0.5-2.2% or 0.5-2% in the composition.
Preferably, in order to further enhance the acne removing effect of the composition, the mass ratio of the sweet wormwood extract to the red pine leaf extract is (1-2): 1. (1-1.8): 1. (1-1.6): 1. (1.1-1.6): 1 or (1.2-1.6): 1.
preferably, the behenyl trimethylammonium methylsulfate is used in an amount of 0.3-4%, 0.4-4%, 0.5-4%, 0.6-4%, 0.8-3.8% or 1-3.7% in the composition.
Preferably, the PPG-26-butanol polyether-26 is used in an amount of 0.3-3.5%, 0.4-3.5%, 0.5-3.2%, 0.5-3% or 0.6-3% in the composition.
Preferably, in order to further increase the acne removing and scalp grease secretion controlling effects of the composition, the mass ratio of the behenyl trimethylammonium methylsulfate to the PPG-26-butanol polyether-26 is (0.8-1.5): 1. (0.85-1.45): 1. (0.9-1.45): 1. (0.9-1.4): 1 or (1-1.4): 1.
preferably, the laurocapram is used in the composition in an amount of 0.01%, 0.02%, 0.05%, 0.08%, 0.1%, 0.2%, 0.3%, 0.4%, 0.5%, 0.6%, 0.7% or in a range between any two values.
Preferably, the skin conditioning agent is present in the composition in an amount of 1.5-8%, 2-8%, 2.5-8%, 3-7.5%, 4-7.5% or 4.5-7.5%. The skin conditioner comprises at least one of fructus forsythiae extract, radix et rhizoma Rhei extract, scutellariae radix extract, coptidis rhizoma extract, rhizoma paridis extract, caulis Lonicerae extract, and herba Taraxaci extract.
Preferably, the surfactant is used in the composition in an amount of 1-9%, 1.2-9%, 1.5-9%, 2-8.5%, 2.5-8% or 3-8%. The surfactant comprises at least one of sodium lauroyl oat amino acid, cocamidopropyl PG-dimethyl ammonium chloride phosphate and cocamidopropyl betaine.
Preferably, the humectant is present in the composition in an amount of 4-10%, 5-10%, 5.5-10%, 6-9.5%, 6.5-9.5% or 7-9%. The humectant comprises at least one of glycerol, 1, 2-butanediol, beta-glucan, 1, 2-propylene glycol, betaine and sorbitol.
Preferably, the emollient is present in the composition in an amount of 4-12%, 5-12%, 5.5-12%, 6-11%, 6.5-11% or 7-11%. The emollient comprises at least one of grape seed oil, jojoba oil, polydimethylsiloxane, camellia oil, sweet almond oil, caprylic/capric glyceride.
Preferably, the thickener is used in the composition in an amount of 0.2-3%, 0.3-3%, 0.4-3%, 0.5-2.8%, 0.6-2.5% or 0.6-2%. The thickener comprises at least one of sodium chloride, xanthan gum, carrageenan, polyacrylate, alginate, cellulose and derivatives thereof.
Preferably, the softener is used in an amount of 0.2 to 2%, 0.3 to 2%, 0.4 to 2%, 0.5 to 2%, 0.6 to 1.8%, or 0.6 to 1.5% in the composition. The softener comprises a polyquaternium.
Preferably, the preservative is used in the composition in an amount of 0.07-0.5%, 0.08-0.5%, 0.09-0.5%, 0.1-0.5%, 0.2-0.5% or 0.25-0.45%. The preservative comprises at least one of phenoxyethanol, methyl benzoate, ethyl benzoate and benzoate.
Preferably, the chelating agent is used in the composition in an amount of 0.02-1%, 0.05-1%, 0.1-1%, 0.2-1%, 0.3-1% or 0.35-0.85%. The chelating agent comprises at least one of EDTA and its salts, and citrate.
Preferably, the pH adjustor is used in the composition in an amount of 0.02-1.8%, 0.05-1.6%, 0.1-1.5%, 0.2-1.5%, 0.3-1.4% or 0.4-1.2%. The pH regulator is at least one of acetic acid, citric acid, tartaric acid, lactic acid, sodium hydroxide, potassium hydroxide, sodium carbonate, potassium carbonate, sodium bicarbonate and potassium bicarbonate.
Preferably, the water is used in the composition in an amount of 30%, 35%, 40%, 45%, 50%, 55%, 60%, 65%, 70%, 75%, 80% or in a range between any two of the above values.
In another aspect, the invention provides a method for preparing the composition comprising the step of mixing the raw materials.
Preferably, the preparation method comprises the following steps:
step 1: adding water into a container, heating, adding thickener, surfactant, behenyl trimethyl ammonium methyl sulfate, PPG-26-butanol polyether-26, piroctone olamine salt, hexamidine di (hydroxyethyl sulfonate), azelaic acid, laurocapram, humectant, emollient and softener, and stirring;
step 2: cooling, adding skin conditioner, herba Artemisiae Annuae extract, folium Pini extract, antiseptic, chelating agent, and pH regulator, stirring, and sterilizing to obtain the composition.
Preferably, the heating temperature of the step 1 is 40-80 ℃, 45-80 ℃, 50-75 ℃ or 55-70 ℃.
Preferably, the temperature of the step 2 is 10-38deg.C, 15-37deg.C, 20-35deg.C or 25-32deg.C.
Preferably, the stirring speeds of the steps 1 and 2 can be 20-3000 rpm, 50-2000 rpm, 60-1000 rpm or 80-600 rpm, respectively.
Preferably, the stirring time of each of the steps 1,2 may be 0.1 to 8 hours, 0.2 to 7 hours, 0.3 to 5 hours or 0.4 to 3 hours, respectively.
In another aspect, the invention also provides the use of said composition for the preparation of hair cosmetics.
Advantageous effects
The shampoo composition is prepared from azelaic acid, piroctone olamine salt, hexamidine di (hydroxyethyl sulfonic acid) salt, sweet wormwood herb extract, red pine leaf extract, behenyl trimethylammonium methyl sulfate, PPG-26-butanol polyether-26, laurocapram, skin conditioning agent, surfactant, humectant, emollient, thickener, softener, preservative, chelating agent, pH regulator and water, and has excellent acne removing effect, and can effectively inhibit secretion of scalp grease and endow scalp with refreshing effect. Wherein, the components such as azelaic acid, sweet wormwood extract, red pine leaf extract and the like endow the composition with excellent acne removing effect, and especially the combination of the sweet wormwood extract and the red pine leaf extract can obviously enhance the acne removing effect of the scalp; ingredients such as piroctone olamine salt, hexamidine bis (isethionate) salt, etc., impart excellent antidandruff effects to the composition; the combination of the behentrimethylammonium methyl sulfate and the PPG-26-butanol polyether-26 can lead the active ingredients to be effectively delivered and exert effects on scalp and hairy roots, so that the acne removing and scalp grease controlling effects of the composition are more excellent; skin conditioning agents, moisturizers, emollients and the like are effective in caring scalp; the softener imparts a softening effect to the hair.
The shampoo composition provided by the invention has the advantages that the acne-removing cure rate reaches 40% and the effective rate reaches 95% after being used for 5 times, and the shampoo composition prepared by the invention has the efficient acne-removing effect and gives the user excellent experience.
The combination of the sweet wormwood extract and the Pinus sylvestris leaf extract in the shampoo composition system can obviously increase the acne removing effect of the composition, and the sweet wormwood extract and the Pinus sylvestris leaf extract have synergistic interaction in promoting the acne removing effect of the composition. And when the dosage ratio of the two is (1-2): when the content is within the range of 1, the obtained shampoo composition has better acne removing effect.
The combination of the behenyl trimethyl ammonium methyl sulfate and the PPG-26-butanol polyether-26 in the shampoo composition can mutually promote so that the acne-removing active ingredients are effectively delivered and exert an effect on the scalp, and the acne-removing effect of the composition is more excellent. And the mass ratio of the two is (0.8-1.5): 1, the acne-removing effect of the shampoo composition is more remarkable.
The shampoo composition provided by the invention has the scalp grease reduction rate of 42.5% after being used for 10 times continuously and 59.2% after being used for 20 times continuously, and can effectively inhibit scalp grease secretion and endow the scalp with fresh and comfortable experience.
The combination of the behenyl trimethylammonium methyl sulfate and the PPG-26-butanol polyether-26 in the shampoo composition can mutually promote so that the oil control active ingredient is effectively delivered and exerts an effect on the scalp, and the composition has better effect of controlling scalp oil secretion. The mass ratio of the behenyl trimethyl ammonium methyl sulfate to the PPG-26-butanol polyether-26 in the composition of the invention reaches (0.8-1.5): within the range of 1, the shampoo composition has the best effect of controlling scalp grease secretion.
Detailed Description
The effects of the present invention will be more clearly shown by the following description of the present invention.
The detailed information of the sources of the raw materials of the specific embodiment of the invention is as follows:
piroctone olamine salt: hubei is emerging for changing new material technology limited company; hexamidine bis (isethionic acid) salt: hubei is emerging for changing new material technology limited company; extract of sweet wormwood: long Sha Hepu biotechnology limited; extract of Pinus sylvestris leaf: shenzhen, ruiyite Biotechnology Co., ltd; behenyl trimethylammonium methylsulfate: wuhank Mike Biomedicine technologies Co., ltd; PPG-26-butanol polyether-26: henan kang Wang Biotechnology Co., ltd; laurocapram: shanghai Miclin Biochemical technologies Co., ltd; fructus forsythiae extract: shanghai Xinkai medicine technologies Co., ltd; rhubarb extract: the chemical company of the martial arts, yaohuang, inc.; radix Scutellariae extract: hubei Baoling chemical technology Co., ltd; extract of coptis chinensis: shaanxi, inc. of pharmaceutical chemical industry; extract of paris polyphylla: waterly Biotech Co., ltd; honeysuckle stem extract: wuhan Puluofu Biotech Co., ltd; dandelion extract: wuhan Fuxin chemical Co., ltd; sodium lauroyl oat amino acid: wuhank Mike Biomedicine technologies Co., ltd; cocamidopropyl PG-dimethyl ammonium chloride phosphate: wuhank Mike Biomedicine technologies Co., ltd; cocamidopropyl betaine: mountain eastern Ammi chemical technology Co., ltd; beta-glucan: duckweed Biotechnology Co., ltd; sorbitol: shandong Xin Tar chemical Co., ltd; grape seed oil: jiangxi Baolin natural perfume Co., ltd; jojoba oil: jiangxi Baolin natural perfume Co., ltd; camellia oil: wuhan Hua Xiangke Jietexilate Co., ltd; sweet almond oil: wuhan Bei Leshe biomedical technologies inc; xanthan gum: guangdong Hongyou biotechnology Co Ltd; polyquaternium-7: starfish environmental protection technology Co.Ltd in the cloud and floating city; polyquaternium-22: wuhank Mike Biomedicine technologies Co.
1. Preparation of shampoo compositions
1. Shampoo composition 1
The preparation method comprises the following raw materials in percentage by mass: 0.28% azelaic acid, 0.15% piroctone olamine, 0.05% hexamidine bis (isethionic acid) salt, 1.4% sweet wormwood extract, 1% red pine leaf extract, 3.6% behenyl trimethyl ammonium methyl sulfate, 3% ppg-26-butanol polyether-26, 0.2% laurocapram, 6.5% skin conditioning agent, 7.5% surfactant, 8% humectant, 6.2% emollient, 1.2% thickener, 1.8% softener, 0.4% preservative, 0.5% chelating agent, 0.6% ph adjuster and balance water;
the mass ratio of the sweet wormwood extract to the red pine leaf extract is 1.4:1, a step of;
the mass ratio of the behenyl trimethyl ammonium methyl sulfate to the PPG-26-butanol polyether-26 is 1.2:1, a step of;
the skin conditioner comprises 0.8% fructus forsythiae extract, 0.7% radix et rhizoma Rhei extract, 1% Scutellariae radix extract, 1% Coptidis rhizoma extract, 1% rhizoma paridis extract, 1% caulis Lonicerae extract and 1% herba Taraxaci extract; the surfactant is 2% sodium lauroyl oat amino acid, 2% cocamidopropyl PG-dimethyl ammonium chloride phosphate and 3.5% cocamidopropyl betaine; the humectant is 3% glycerol, 1%1, 2-butanediol, 0.5% beta-dextran, 1%1, 2-propylene glycol, 1.5% betaine and 1% sorbitol; the emollient is 1.2% grape seed oil, 2% jojoba oil, 1% oleum Camelliae Japonicae and 2% oleum Armeniacae amarum; the thickener is 0.6% sodium chloride and 0.6% xanthan gum; the softener comprises 0.9% of polyquaternium-7 and 0.9% of polyquaternium-22; the preservative is 0.2% phenoxyethanol and 0.2% methyl benzoate; the chelating agent is EDTA-disodium; the pH regulator is citric acid;
the preparation method comprises the following steps:
step 1: adding water into a container, heating to 65 ℃, then adding a thickening agent, a surfactant, behenyl trimethyl ammonium methyl sulfate, PPG-26-butanol polyether-26, piroctone olamine salt, hexamidine di (hydroxyethyl sulfonic acid) salt, azelaic acid, laurocapram, a humectant, an emollient and a softener, stirring for 0.5 hour at a stirring speed of 100 revolutions per minute, and uniformly stirring;
step 2: cooling to 25deg.C, adding skin conditioner, herba Artemisiae Annuae extract, folium Pini extract, antiseptic, chelating agent, and pH regulator, stirring at 80 rpm for 0.6 hr, stirring uniformly, and sterilizing to obtain composition 1.
2. Shampoo composition 2
The preparation method comprises the following raw materials in percentage by mass: 0.27% azelaic acid, 0.14% piroctone olamine, 0.06% hexamidine bis (isethionic acid) salt, 1.2% sweet wormwood extract, 1.2% red pine leaf extract, 3.3% behenyl trimethyl ammonium methyl sulfate, 3.3% ppg-26-butanol polyether-26, 0.3% laurocapram, 6.6% skin conditioning agent, 7% surfactant, 7.5% humectant, 6.5% emollient, 1.3% thickener, 1.7% softener, 0.45% preservative, 0.45% chelating agent, 0.55% ph adjuster and balance water;
the mass ratio of the sweet wormwood extract to the red pine leaf extract is 1:1;
the mass ratio of the behenyl trimethyl ammonium methyl sulfate to the PPG-26-butanol polyether-26 is 1:1;
the skin conditioner comprises 1% fructus forsythiae extract, 1% radix et rhizoma Rhei extract, 0.8% Scutellariae radix extract, 0.8% Coptidis rhizoma extract, 1.2% rhizoma paridis extract, 0.8% caulis Lonicerae extract and 1% herba Taraxaci extract; the surfactant is 2.5% of lauroyl oat amino acid sodium, 2.5% of cocamidopropyl PG-dimethyl ammonium chloride phosphate and 2% of cocamidopropyl betaine; the humectant is 2.5% glycerol, 1%1, 2-butanediol, 2% beta-glucan, 1%1, 2-propylene glycol and 1% betaine; the emollient is 1.5% grape seed oil, 1% jojoba oil, 1.5% camellia oil and 2.5% sweet almond oil; the thickener is xanthan gum; the softener is polyquaternium-7; the preservative is phenoxyethanol; the chelating agent is EDTA-disodium; the pH regulator is citric acid;
the preparation method comprises the following steps:
step 1: adding water into a container, heating to 63 ℃, then adding a thickening agent, a surfactant, behenyl trimethyl ammonium methyl sulfate, PPG-26-butanol polyether-26, piroctone olamine salt, hexamidine di (hydroxyethyl sulfonic acid) salt, azelaic acid, laurocapram, a humectant, an emollient and a softener, stirring for 0.6 hour at a stirring speed of 120 r/min, and uniformly stirring;
step 2: cooling to 28deg.C, adding skin conditioner, herba Artemisiae Annuae extract, folium Pini extract, antiseptic, chelating agent, and pH regulator, stirring at 100 rpm for 0.5 hr, stirring uniformly, and sterilizing to obtain composition 2.
3. Shampoo composition 3
The preparation method comprises the following raw materials in percentage by mass: 0.28% azelaic acid, 0.15% piroctone olamine, 0.05% hexamidine bis (isethionic acid) salt, 2.4% red pine leaf extract, 3.6% behenyl trimethylammonium methylsulfate, 3% ppg-26-butanol polyether-26, 0.2% laurocapram, 6.5% skin conditioner, 7.5% surfactant, 8% humectant, 6.2% emollient, 1.2% thickener, 1.8% softener, 0.4% preservative, 0.5% chelating agent, 0.6% ph adjuster, and balance water;
the mass ratio of the behenyl trimethyl ammonium methyl sulfate to the PPG-26-butanol polyether-26 is 1.2:1, a step of;
the skin conditioner comprises 0.8% fructus forsythiae extract, 0.7% radix et rhizoma Rhei extract, 1% Scutellariae radix extract, 1% Coptidis rhizoma extract, 1% rhizoma paridis extract, 1% caulis Lonicerae extract and 1% herba Taraxaci extract; the surfactant is 2% sodium lauroyl oat amino acid, 2% cocamidopropyl PG-dimethyl ammonium chloride phosphate and 3.5% cocamidopropyl betaine; the humectant is 3% glycerol, 1%1, 2-butanediol, 0.5% beta-dextran, 1%1, 2-propylene glycol, 1.5% betaine and 1% sorbitol; the emollient is 1.2% grape seed oil, 2% jojoba oil, 1% oleum Camelliae Japonicae and 2% oleum Armeniacae amarum; the thickener is 0.6% sodium chloride and 0.6% xanthan gum; the softener comprises 0.9% of polyquaternium-7 and 0.9% of polyquaternium-22; the preservative is 0.2% phenoxyethanol and 0.2% methyl benzoate; the chelating agent is EDTA-disodium; the pH regulator is citric acid;
the preparation method comprises the following steps:
step 1: adding water into a container, heating to 65 ℃, then adding a thickening agent, a surfactant, behenyl trimethyl ammonium methyl sulfate, PPG-26-butanol polyether-26, piroctone olamine salt, hexamidine di (hydroxyethyl sulfonic acid) salt, azelaic acid, laurocapram, a humectant, an emollient and a softener, stirring for 0.5 hour at a stirring speed of 100 revolutions per minute, and uniformly stirring;
step 2: cooling to 25deg.C, adding skin conditioner, pinus sylvestris leaf extract, antiseptic, chelating agent, and pH regulator, stirring at 80 rpm for 0.6 hr, stirring uniformly, and sterilizing to obtain composition 3.
4. Shampoo composition 4
The preparation method comprises the following raw materials in percentage by mass: 0.28% azelaic acid, 0.15% piroctone olamine, 0.05% hexamidine bis (isethionic acid) salt, 2.4% sweet wormwood extract, 3.6% behenyl trimethyl ammonium methyl sulfate, 3% ppg-26-butanol polyether-26, 0.2% laurocapram, 6.5% skin conditioning agent, 7.5% surfactant, 8% humectant, 6.2% emollient, 1.2% thickener, 1.8% softener, 0.4% preservative, 0.5% chelating agent, 0.6% ph adjuster and balance water;
the mass ratio of the behenyl trimethyl ammonium methyl sulfate to the PPG-26-butanol polyether-26 is 1.2:1, a step of;
the skin conditioner comprises 0.8% fructus forsythiae extract, 0.7% radix et rhizoma Rhei extract, 1% Scutellariae radix extract, 1% Coptidis rhizoma extract, 1% rhizoma paridis extract, 1% caulis Lonicerae extract and 1% herba Taraxaci extract; the surfactant is 2% sodium lauroyl oat amino acid, 2% cocamidopropyl PG-dimethyl ammonium chloride phosphate and 3.5% cocamidopropyl betaine; the humectant is 3% glycerol, 1%1, 2-butanediol, 0.5% beta-dextran, 1%1, 2-propylene glycol, 1.5% betaine and 1% sorbitol; the emollient is 1.2% grape seed oil, 2% jojoba oil, 1% oleum Camelliae Japonicae and 2% oleum Armeniacae amarum; the thickener is 0.6% sodium chloride and 0.6% xanthan gum; the softener comprises 0.9% of polyquaternium-7 and 0.9% of polyquaternium-22; the preservative is 0.2% phenoxyethanol and 0.2% methyl benzoate; the chelating agent is EDTA-disodium; the pH regulator is citric acid;
the preparation method comprises the following steps:
step 1: adding water into a container, heating to 65 ℃, then adding a thickening agent, a surfactant, behenyl trimethyl ammonium methyl sulfate, PPG-26-butanol polyether-26, piroctone olamine salt, hexamidine di (hydroxyethyl sulfonic acid) salt, azelaic acid, laurocapram, a humectant, an emollient and a softener, stirring for 0.5 hour at a stirring speed of 100 revolutions per minute, and uniformly stirring;
step 2: cooling to 25deg.C, adding skin conditioner, herba Artemisiae Annuae extract, antiseptic, chelating agent, and pH regulator, stirring at 80 rpm for 0.6 hr, stirring uniformly, and sterilizing to obtain composition 4.
5. Shampoo composition 5
The preparation method comprises the following raw materials in percentage by mass: 0.28% azelaic acid, 0.15% piroctone olamine, 0.05% hexamidine bis (isethionic acid) salt, 0.8% sweet wormwood extract, 1.6% red pine leaf extract, 3.6% behenyl trimethyl ammonium methyl sulfate, 3% ppg-26-butanol polyether-26, 0.2% laurocapram, 6.5% skin conditioning agent, 7.5% surfactant, 8% humectant, 6.2% emollient, 1.2% thickener, 1.8% softener, 0.4% preservative, 0.5% chelating agent, 0.6% ph adjuster and balance water;
the mass ratio of the sweet wormwood extract to the red pine leaf extract is 0.5:1, a step of;
the mass ratio of the behenyl trimethyl ammonium methyl sulfate to the PPG-26-butanol polyether-26 is 1.2:1, a step of;
the skin conditioner comprises 0.8% fructus forsythiae extract, 0.7% radix et rhizoma Rhei extract, 1% Scutellariae radix extract, 1% Coptidis rhizoma extract, 1% rhizoma paridis extract, 1% caulis Lonicerae extract and 1% herba Taraxaci extract; the surfactant is 2% sodium lauroyl oat amino acid, 2% cocamidopropyl PG-dimethyl ammonium chloride phosphate and 3.5% cocamidopropyl betaine; the humectant is 3% glycerol, 1%1, 2-butanediol, 0.5% beta-dextran, 1%1, 2-propylene glycol, 1.5% betaine and 1% sorbitol; the emollient is 1.2% grape seed oil, 2% jojoba oil, 1% oleum Camelliae Japonicae and 2% oleum Armeniacae amarum; the thickener is 0.6% sodium chloride and 0.6% xanthan gum; the softener comprises 0.9% of polyquaternium-7 and 0.9% of polyquaternium-22; the preservative is 0.2% phenoxyethanol and 0.2% methyl benzoate; the chelating agent is EDTA-disodium; the pH regulator is citric acid;
the preparation method comprises the following steps:
step 1: adding water into a container, heating to 65 ℃, then adding a thickening agent, a surfactant, behenyl trimethyl ammonium methyl sulfate, PPG-26-butanol polyether-26, piroctone olamine salt, hexamidine di (hydroxyethyl sulfonic acid) salt, azelaic acid, laurocapram, a humectant, an emollient and a softener, stirring for 0.5 hour at a stirring speed of 100 revolutions per minute, and uniformly stirring;
step 2: cooling to 25deg.C, adding skin conditioner, herba Artemisiae Annuae extract, folium Pini extract, antiseptic, chelating agent, and pH regulator, stirring at 80 rpm for 0.6 hr, stirring uniformly, and sterilizing to obtain composition 5.
6. Shampoo composition 6
The preparation method comprises the following raw materials in percentage by mass: 0.28% azelaic acid, 0.15% piroctone olamine, 0.05% hexamidine bis (isethionic acid) salt, 1.8% sweet wormwood extract, 0.6% red pine leaf extract, 3.6% behenyl trimethyl ammonium methyl sulfate, 3% ppg-26-butanol polyether-26, 0.2% laurocapram, 6.5% skin conditioning agent, 7.5% surfactant, 8% humectant, 6.2% emollient, 1.2% thickener, 1.8% softener, 0.4% preservative, 0.5% chelating agent, 0.6% ph adjuster and balance water;
the mass ratio of the sweet wormwood extract to the red pine leaf extract is 3:1, a step of;
the mass ratio of the behenyl trimethyl ammonium methyl sulfate to the PPG-26-butanol polyether-26 is 1.2:1, a step of;
the skin conditioner comprises 0.8% fructus forsythiae extract, 0.7% radix et rhizoma Rhei extract, 1% Scutellariae radix extract, 1% Coptidis rhizoma extract, 1% rhizoma paridis extract, 1% caulis Lonicerae extract and 1% herba Taraxaci extract; the surfactant is 2% sodium lauroyl oat amino acid, 2% cocamidopropyl PG-dimethyl ammonium chloride phosphate and 3.5% cocamidopropyl betaine; the humectant is 3% glycerol, 1%1, 2-butanediol, 0.5% beta-dextran, 1%1, 2-propylene glycol, 1.5% betaine and 1% sorbitol; the emollient is 1.2% grape seed oil, 2% jojoba oil, 1% oleum Camelliae Japonicae and 2% oleum Armeniacae amarum; the thickener is 0.6% sodium chloride and 0.6% xanthan gum; the softener comprises 0.9% of polyquaternium-7 and 0.9% of polyquaternium-22; the preservative is 0.2% phenoxyethanol and 0.2% methyl benzoate; the chelating agent is EDTA-disodium; the pH regulator is citric acid;
the preparation method comprises the following steps:
step 1: adding water into a container, heating to 65 ℃, then adding a thickening agent, a surfactant, behenyl trimethyl ammonium methyl sulfate, PPG-26-butanol polyether-26, piroctone olamine salt, hexamidine di (hydroxyethyl sulfonic acid) salt, azelaic acid, laurocapram, a humectant, an emollient and a softener, stirring for 0.5 hour at a stirring speed of 100 revolutions per minute, and uniformly stirring;
step 2: cooling to 25deg.C, adding skin conditioner, herba Artemisiae Annuae extract, folium Pini extract, antiseptic, chelating agent, and pH regulator, stirring at 80 rpm for 0.6 hr, stirring uniformly, and sterilizing to obtain composition 6.
7. Shampoo composition 7
The preparation method comprises the following raw materials in percentage by mass: 0.28% azelaic acid, 0.15% piroctone olamine, 0.05% hexamidine bis (isethionic acid) salt, 1.4% sweet wormwood extract, 1% red pine leaf extract, 6.6% ppg-26-butanol polyether-26, 0.2% laurocapram, 6.5% skin conditioning agent, 7.5% surfactant, 8% humectant, 6.2% emollient, 1.2% thickener, 1.8% softener, 0.4% preservative, 0.5% chelating agent, 0.6% ph adjuster and balance water;
the mass ratio of the sweet wormwood extract to the red pine leaf extract is 1.4:1, a step of;
the skin conditioner comprises 0.8% fructus forsythiae extract, 0.7% radix et rhizoma Rhei extract, 1% Scutellariae radix extract, 1% Coptidis rhizoma extract, 1% rhizoma paridis extract, 1% caulis Lonicerae extract and 1% herba Taraxaci extract; the surfactant is 2% sodium lauroyl oat amino acid, 2% cocamidopropyl PG-dimethyl ammonium chloride phosphate and 3.5% cocamidopropyl betaine; the humectant is 3% glycerol, 1%1, 2-butanediol, 0.5% beta-dextran, 1%1, 2-propylene glycol, 1.5% betaine and 1% sorbitol; the emollient is 1.2% grape seed oil, 2% jojoba oil, 1% oleum Camelliae Japonicae and 2% oleum Armeniacae amarum; the thickener is 0.6% sodium chloride and 0.6% xanthan gum; the softener comprises 0.9% of polyquaternium-7 and 0.9% of polyquaternium-22; the preservative is 0.2% phenoxyethanol and 0.2% methyl benzoate; the chelating agent is EDTA-disodium; the pH regulator is citric acid;
the preparation method comprises the following steps:
step 1: adding water into a container, heating to 65 ℃, then adding a thickening agent, a surfactant, PPG-26-butanol polyether-26, piroctone olamine salt, hexamidine di (isethionate), azelaic acid, laurocapram, a humectant, an emollient and a softener, stirring for 0.5 hour at a stirring speed of 100 r/min, and uniformly stirring;
step 2: cooling to 25deg.C, adding skin conditioner, herba Artemisiae Annuae extract, folium Pini extract, antiseptic, chelating agent, and pH regulator, stirring at 80 rpm for 0.6 hr, stirring uniformly, and sterilizing to obtain composition 7.
8. Shampoo composition 8
The preparation method comprises the following raw materials in percentage by mass: 0.28% azelaic acid, 0.15% piroctone olamine, 0.05% hexamidine bis (isethionic acid) salt, 1.4% sweet wormwood extract, 1% red pine leaf extract, 6.6% behenyl trimethyl ammonium methyl sulfate, 0.2% laurocapram, 6.5% skin conditioning agent, 7.5% surfactant, 8% humectant, 6.2% emollient, 1.2% thickener, 1.8% softener, 0.4% preservative, 0.5% chelating agent, 0.6% ph adjuster and balance water;
the mass ratio of the sweet wormwood extract to the red pine leaf extract is 1.4:1, a step of;
the skin conditioner comprises 0.8% fructus forsythiae extract, 0.7% radix et rhizoma Rhei extract, 1% Scutellariae radix extract, 1% Coptidis rhizoma extract, 1% rhizoma paridis extract, 1% caulis Lonicerae extract and 1% herba Taraxaci extract; the surfactant is 2% sodium lauroyl oat amino acid, 2% cocamidopropyl PG-dimethyl ammonium chloride phosphate and 3.5% cocamidopropyl betaine; the humectant is 3% glycerol, 1%1, 2-butanediol, 0.5% beta-dextran, 1%1, 2-propylene glycol, 1.5% betaine and 1% sorbitol; the emollient is 1.2% grape seed oil, 2% jojoba oil, 1% oleum Camelliae Japonicae and 2% oleum Armeniacae amarum; the thickener is 0.6% sodium chloride and 0.6% xanthan gum; the softener comprises 0.9% of polyquaternium-7 and 0.9% of polyquaternium-22; the preservative is 0.2% phenoxyethanol and 0.2% methyl benzoate; the chelating agent is EDTA-disodium; the pH regulator is citric acid;
the preparation method comprises the following steps:
step 1: adding water into a container, heating to 65 ℃, then adding a thickening agent, a surfactant, behenyl trimethyl ammonium methyl sulfate, piroctone olamine salt, hexamidine di (isethionic acid) salt, azelaic acid, laurocapram, a humectant, an emollient and a softener, stirring for 0.5 hour at a stirring speed of 100 revolutions per minute, and uniformly stirring;
step 2: cooling to 25deg.C, adding skin conditioner, herba Artemisiae Annuae extract, folium Pini extract, antiseptic, chelating agent, and pH regulator, stirring at 80 rpm for 0.6 hr, stirring uniformly, and sterilizing to obtain composition 8.
9. Shampoo composition 9
The preparation method comprises the following raw materials in percentage by mass: 0.28% azelaic acid, 0.15% piroctone olamine, 0.05% hexamidine bis (isethionic acid) salt, 1.4% sweet wormwood extract, 1% red pine leaf extract, 2% behenyl trimethyl ammonium methyl sulfate, 4.6% ppg-26-butanol polyether-26, 0.2% laurocapram, 6.5% skin conditioning agent, 7.5% surfactant, 8% humectant, 6.2% emollient, 1.2% thickener, 1.8% softener, 0.4% preservative, 0.5% chelating agent, 0.6% ph adjuster and balance water;
the mass ratio of the sweet wormwood extract to the red pine leaf extract is 1.4:1, a step of;
the mass ratio of the behenyl trimethyl ammonium methyl sulfate to the PPG-26-butanol polyether-26 is 0.43:1, a step of;
the skin conditioner comprises 0.8% fructus forsythiae extract, 0.7% radix et rhizoma Rhei extract, 1% Scutellariae radix extract, 1% Coptidis rhizoma extract, 1% rhizoma paridis extract, 1% caulis Lonicerae extract and 1% herba Taraxaci extract; the surfactant is 2% sodium lauroyl oat amino acid, 2% cocamidopropyl PG-dimethyl ammonium chloride phosphate and 3.5% cocamidopropyl betaine; the humectant is 3% glycerol, 1%1, 2-butanediol, 0.5% beta-dextran, 1%1, 2-propylene glycol, 1.5% betaine and 1% sorbitol; the emollient is 1.2% grape seed oil, 2% jojoba oil, 1% oleum Camelliae Japonicae and 2% oleum Armeniacae amarum; the thickener is 0.6% sodium chloride and 0.6% xanthan gum; the softener comprises 0.9% of polyquaternium-7 and 0.9% of polyquaternium-22; the preservative is 0.2% phenoxyethanol and 0.2% methyl benzoate; the chelating agent is EDTA-disodium; the pH regulator is citric acid;
the preparation method comprises the following steps:
step 1: adding water into a container, heating to 65 ℃, then adding a thickening agent, a surfactant, behenyl trimethyl ammonium methyl sulfate, PPG-26-butanol polyether-26, piroctone olamine salt, hexamidine di (hydroxyethyl sulfonic acid) salt, azelaic acid, laurocapram, a humectant, an emollient and a softener, stirring for 0.5 hour at a stirring speed of 100 revolutions per minute, and uniformly stirring;
step 2: cooling to 25deg.C, adding skin conditioner, herba Artemisiae Annuae extract, folium Pini extract, antiseptic, chelating agent, and pH regulator, stirring at 80 rpm for 0.6 hr, stirring uniformly, and sterilizing to obtain composition 9.
10. Shampoo composition 10
The preparation method comprises the following raw materials in percentage by mass: 0.28% azelaic acid, 0.15% piroctone olamine, 0.05% hexamidine bis (isethionic acid) salt, 1.4% sweet wormwood extract, 1% red pine leaf extract, 4.4% behenyl trimethyl ammonium methyl sulfate, 2.2% ppg-26-butanol polyether-26, 0.2% laurocapram, 6.5% skin conditioning agent, 7.5% surfactant, 8% humectant, 6.2% emollient, 1.2% thickener, 1.8% softener, 0.4% preservative, 0.5% chelating agent, 0.6% ph adjuster and balance water;
the mass ratio of the sweet wormwood extract to the red pine leaf extract is 1.4:1, a step of;
the mass ratio of the behenyl trimethyl ammonium methyl sulfate to the PPG-26-butanol polyether-26 is 2:1, a step of;
the skin conditioner comprises 0.8% fructus forsythiae extract, 0.7% radix et rhizoma Rhei extract, 1% Scutellariae radix extract, 1% Coptidis rhizoma extract, 1% rhizoma paridis extract, 1% caulis Lonicerae extract and 1% herba Taraxaci extract; the surfactant is 2% sodium lauroyl oat amino acid, 2% cocamidopropyl PG-dimethyl ammonium chloride phosphate and 3.5% cocamidopropyl betaine; the humectant is 3% glycerol, 1%1, 2-butanediol, 0.5% beta-dextran, 1%1, 2-propylene glycol, 1.5% betaine and 1% sorbitol; the emollient is 1.2% grape seed oil, 2% jojoba oil, 1% oleum Camelliae Japonicae and 2% oleum Armeniacae amarum; the thickener is 0.6% sodium chloride and 0.6% xanthan gum; the softener comprises 0.9% of polyquaternium-7 and 0.9% of polyquaternium-22; the preservative is 0.2% phenoxyethanol and 0.2% methyl benzoate; the chelating agent is EDTA-disodium; the pH regulator is citric acid;
the preparation method comprises the following steps:
step 1: adding water into a container, heating to 65 ℃, then adding a thickening agent, a surfactant, behenyl trimethyl ammonium methyl sulfate, PPG-26-butanol polyether-26, piroctone olamine salt, hexamidine di (hydroxyethyl sulfonic acid) salt, azelaic acid, laurocapram, a humectant, an emollient and a softener, stirring for 0.5 hour at a stirring speed of 100 revolutions per minute, and uniformly stirring;
step 2: cooling to 25deg.C, adding skin conditioner, herba Artemisiae Annuae extract, folium Pini extract, antiseptic, chelating agent, and pH regulator, stirring at 80 rpm for 0.6 hr, stirring uniformly, and sterilizing to obtain composition 10.
2. Performance testing
The mass ratio of the sweet wormwood extract to the red pine leaf extract is (1-2): 1.
the mass ratio of the behenyl trimethyl ammonium methyl sulfate to the PPG-26-butanol polyether-26 is (0.8-1.5): 1.
1. scalp acne-removing effect test
Oily scalp, scalp easy to get oil, easy to get acne or folliculitis, and scalp with acne aged 20-35 male volunteers were randomly divided into 10 groups of 40 people. Volunteers did not use scalp products of similar efficacy two weeks before testing with the shampoo compositions 1-10 described above, and did not hair had been dyed, permed, bleached, straightened, etc. for one month. Volunteers in the test group used the above shampoo composition to wash their hair once every 2 days, with a duration of 5 times; the scalp was photographed before and after 5 consecutive uses of the shampoo composition, and the scalp acne improvement of each group of volunteers before and after the shampoo composition was evaluated by the same dermatologist. The evaluation criteria were: invalidation: the improvement of the skin damage of the patient is not obvious or the skin damage is aggravated; the method is effective: patient skin lesions are improved, but clear lesions are still visible; and (3) healing: the skin lesions of the patients completely resolved. The evaluation effect is shown in Table 1.
Table 1: scalp acne-removing effect test
As shown in the test results of the scalp acne-removing effect in Table 1, the shampoo composition provided by the invention has the advantages that the acne-removing cure rate reaches 40% and the effective rate reaches 95% after being used for 5 times, and the shampoo composition prepared by the invention has the high-efficiency acne-removing effect and gives the user excellent experience.
From the test results of the compositions 1 and 3-6, the amounts of the extract of the red pine leaves and the extract of the sweet wormwood herb in the compositions 3 and 4 are the same as the total amount of the extract of the sweet wormwood herb and the extract of the red pine leaves in the composition 1, but the test results show that the effect of the composition 1 is better, which shows that the combination of the extract of the sweet wormwood herb and the extract of the red pine leaves in the shampoo composition system of the invention can obviously increase the acne removing effect of the composition, and the two compositions show synergistic effect of mutual promotion on the acne removing effect of the composition. And when the dosage ratio of the two is (1-2): when the content is within the range of 1, the obtained shampoo composition has better acne removing effect.
From the test results of the compositions 1 and 7-10, the combination of the behenyl trimethyl ammonium methyl sulfate and the PPG-26-butanol polyether-26 in the shampoo composition can mutually promote so that the acne-removing active ingredients can be effectively delivered and exert an effect on the scalp, and the acne-removing effect of the composition is more excellent. And the mass ratio of the two is (0.8-1.5): 1, the acne-removing effect of the shampoo composition is more remarkable.
2. Test for controlling scalp grease secretion effect
Several male volunteers recruiting 35-50 years old oily scalp were randomized into 5 groups of 4 each; shampoo compositions 1 and 7-10 described above were used. The shampoo composition is used for cleaning hair every three days, and is continuously used for 20 times. Sebum levels of scalp surfaces of scalp 3cm x 3cm areas of the scalp top area of 10 times and 20 times before application of the shampoo composition were measured using a sebum tester sebumersm 815, and sebum reduction rates T10 and T20 of scalp surfaces of 10 times and 20 were converted. The results are shown in Table 2.
Table 2: test for controlling scalp grease secretion effect
As shown in the test results of the scalp grease secretion control effect shown in Table 2, the scalp grease reduction rate of the shampoo composition of the invention reaches 42.5% when the shampoo composition is used for 10 times continuously, and reaches 59.2% when the shampoo composition is used for 20 times continuously, the shampoo composition of the invention can effectively inhibit scalp grease secretion, and gives fresh and comfortable experience to the scalp.
From the test results of compositions 1 and 7-10, it is clear that the combination of behenyl trimethylammonium methyl sulfate and PPG-26-butanol polyether-26 in the shampoo composition of the invention can mutually promote the effective delivery of the oil control active ingredient and exert the effect on the scalp, so that the composition has better effect of controlling the secretion of scalp grease. The mass ratio of the behenyl trimethyl ammonium methyl sulfate to the PPG-26-butanol polyether-26 in the composition of the invention reaches (0.8-1.5): within the range of 1, the shampoo composition has the best effect of controlling scalp grease secretion.
Various modifications and variations of the present invention may occur to those skilled in the art, and it is intended that the present invention also include such modifications and variations as fall within the scope of the appended claims and their equivalents.
Claims (10)
1. An acne-removing shampoo composition containing sweet wormwood herb extract is characterized by comprising the following components in percentage by mass: 0.01-1.5% azelaic acid, 0.05-0.9% piroctone olamine, 0.01-0.09% hexamidine bis (isethionic acid) salt, 0.1-3% sweet wormwood extract, 0.1-2.5% red pine leaf extract, 0.2-4% behenyl trimethylammonium methyl sulfate, 0.2-3.5% PPG-26-butanol polyether-26, 0.01-0.7% laurocapram, 1-8% skin conditioning agent, 0.5-9% surfactant, 3-10% humectant, 3-12% emollient, 0.1-3% thickener, 0.1-2% softener, 0.05-0.5% preservative, 0.01-1% chelating agent, 0.01-2% pH regulator and 30-80% water.
2. The composition of claim 1, wherein: the skin conditioner comprises at least one of fructus forsythiae extract, radix et rhizoma Rhei extract, scutellariae radix extract, coptidis rhizoma extract, rhizoma paridis extract, caulis Lonicerae extract, and herba Taraxaci extract.
3. The composition of claim 1, wherein: the surfactant comprises at least one of sodium lauroyl oat amino acid, cocamidopropyl PG-dimethyl ammonium chloride phosphate and cocamidopropyl betaine.
4. The composition of claim 1, wherein: the humectant comprises at least one of glycerol, 1, 2-butanediol, beta-glucan, 1, 2-propylene glycol, betaine and sorbitol.
5. The composition of claim 1, wherein: the emollient comprises at least one of grape seed oil, jojoba oil, polydimethylsiloxane, camellia oil, sweet almond oil, caprylic/capric glyceride.
6. The composition of claim 1, wherein: the thickener comprises at least one of sodium chloride, xanthan gum, carrageenan, polyacrylate, alginate, cellulose and derivatives thereof.
7. The composition of claim 1, wherein: the mass ratio of the sweet wormwood extract to the red pine leaf extract is (1-2): 1.
8. the composition of claim 1, wherein: the mass ratio of the behenyl trimethyl ammonium methyl sulfate to the PPG-26-butanol polyether-26 is (0.8-1.5): 1.
9. a process for the preparation of a composition as claimed in any one of claims 1 to 8, wherein: comprises the step of mixing the raw materials.
10. Use of a composition according to any one of claims 1 to 8 for the preparation of a hair cosmetic.
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| KR20170092817A (en) * | 2016-02-04 | 2017-08-14 | 주식회사 헤어레시피 | Composition for hair care treatment and preparing method thereof |
| CN111298124A (en) * | 2020-03-30 | 2020-06-19 | 黄泳华 | Anti-acne composition containing antibiotics and vegetable oil |
| KR102130260B1 (en) * | 2020-01-07 | 2020-07-23 | 주식회사 폴메디 | Cosmetic composition containing natural minerals having skin care activity |
| EP3708148A1 (en) * | 2014-04-03 | 2020-09-16 | Pola Chemical Industries Inc. | Melanogenesis inhibitor comprising d-pantothenyl alcohol, and skin-whitening cosmetic containing same melanogenesis inhibitor |
| CN116509774A (en) * | 2023-06-28 | 2023-08-01 | 云南群优生物科技有限公司 | Anti-dandruff shampoo preparation containing sweet wormwood herb extract and preparation method thereof |
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Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102014940A (en) * | 2008-05-02 | 2011-04-13 | 株式会社太平洋 | Medicinal plants extract using processing of herbal medicine and composition of skin external application comprising the same |
| EP3708148A1 (en) * | 2014-04-03 | 2020-09-16 | Pola Chemical Industries Inc. | Melanogenesis inhibitor comprising d-pantothenyl alcohol, and skin-whitening cosmetic containing same melanogenesis inhibitor |
| KR20170092817A (en) * | 2016-02-04 | 2017-08-14 | 주식회사 헤어레시피 | Composition for hair care treatment and preparing method thereof |
| KR102130260B1 (en) * | 2020-01-07 | 2020-07-23 | 주식회사 폴메디 | Cosmetic composition containing natural minerals having skin care activity |
| CN111298124A (en) * | 2020-03-30 | 2020-06-19 | 黄泳华 | Anti-acne composition containing antibiotics and vegetable oil |
| CN116509774A (en) * | 2023-06-28 | 2023-08-01 | 云南群优生物科技有限公司 | Anti-dandruff shampoo preparation containing sweet wormwood herb extract and preparation method thereof |
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