CN1174924C - 氟化乳化剂的回收方法 - Google Patents

氟化乳化剂的回收方法 Download PDF

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Publication number
CN1174924C
CN1174924C CNB008154090A CN00815409A CN1174924C CN 1174924 C CN1174924 C CN 1174924C CN B008154090 A CNB008154090 A CN B008154090A CN 00815409 A CN00815409 A CN 00815409A CN 1174924 C CN1174924 C CN 1174924C
Authority
CN
China
Prior art keywords
fluorinated
acid
emulsifying agent
emulsifiers
molecular formula
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNB008154090A
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English (en)
Chinese (zh)
Other versions
CN1387498A (zh
Inventor
S・富尔
S·富尔
ざ特费热
K·欣策
G·洛尔
W·施韦尔特费热
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
3M Innovative Properties Co
Original Assignee
Dyneon GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dyneon GmbH filed Critical Dyneon GmbH
Publication of CN1387498A publication Critical patent/CN1387498A/zh
Application granted granted Critical
Publication of CN1174924C publication Critical patent/CN1174924C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J41/00Anion exchange; Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
    • B01J41/04Processes using organic exchangers
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/47Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00Nature of the contaminant
    • C02F2101/10Inorganic compounds
    • C02F2101/12Halogens or halogen-containing compounds
    • C02F2101/14Fluorine or fluorine-containing compounds
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/34Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32
    • C02F2103/36Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32 from the manufacture of organic compounds
    • C02F2103/38Polymers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treatment Of Water By Ion Exchange (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
CNB008154090A 1999-11-05 2000-10-28 氟化乳化剂的回收方法 Expired - Fee Related CN1174924C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19953285A DE19953285A1 (de) 1999-11-05 1999-11-05 Verfahren zur Rückgewinnung fluorierter Emulgatoren
DE19953285.0 1999-11-05

Publications (2)

Publication Number Publication Date
CN1387498A CN1387498A (zh) 2002-12-25
CN1174924C true CN1174924C (zh) 2004-11-10

Family

ID=7928031

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB008154090A Expired - Fee Related CN1174924C (zh) 1999-11-05 2000-10-28 氟化乳化剂的回收方法

Country Status (11)

Country Link
US (1) US6642415B1 (enExample)
EP (1) EP1240107B1 (enExample)
JP (1) JP2003512931A (enExample)
CN (1) CN1174924C (enExample)
AU (1) AU7924000A (enExample)
CA (1) CA2387781A1 (enExample)
DE (2) DE19953285A1 (enExample)
PL (1) PL354617A1 (enExample)
RU (1) RU2255807C2 (enExample)
WO (1) WO2001032563A1 (enExample)
ZA (1) ZA200203488B (enExample)

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* Cited by examiner, † Cited by third party
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JP2002059160A (ja) * 2000-08-11 2002-02-26 Daikin Ind Ltd 含フッ素陰イオン系界面活性剤の分離方法
US7279522B2 (en) 2001-09-05 2007-10-09 3M Innovative Properties Company Fluoropolymer dispersions containing no or little low molecular weight fluorinated surfactant
JP2003220393A (ja) * 2001-11-22 2003-08-05 Asahi Glass Co Ltd 含フッ素乳化剤の吸着・回収方法
EP1364972B1 (en) * 2002-05-22 2006-08-30 3M Innovative Properties Company Process for reducing the amount of fluorinated surfactant in aqueous fluoropolymer dispersions
DE60301322T2 (de) * 2003-02-28 2006-06-08 3M Innovative Properties Co., St. Paul Fluoropolymerdispersion enthaltend kein oder wenig fluorhaltiges Netzmittel mit niedrigem Molekulargewicht
WO2005065800A1 (en) * 2003-12-30 2005-07-21 Daikin Industries, Ltd. Process for separating fluorine-containing surfactant
US20060014887A1 (en) * 2004-07-19 2006-01-19 3M Innovative Properties Company Method of hydrolyzing a dispersion of ionic fluoropolymer
US7304101B2 (en) * 2004-07-19 2007-12-04 3M Innovative Properties Company Method of purifying a dispersion of ionic fluoropolymer
US7666927B2 (en) * 2004-12-22 2010-02-23 E.I. Du Pont De Nemours And Company Removing fluorosurfactant from aqueous fluoropolymer dispersions using anion exchange polymer with functional groups resistant to degradation to trialkylamines
EP1700869A1 (en) * 2005-03-11 2006-09-13 3M Innovative Properties Company Recovery of fluorinated surfactants from a basic anion exchange resin having quaternary ammonium groups
US7671112B2 (en) 2005-07-15 2010-03-02 3M Innovative Properties Company Method of making fluoropolymer dispersion
US20080015304A1 (en) 2006-07-13 2008-01-17 Klaus Hintzer Aqueous emulsion polymerization process for producing fluoropolymers
GB0525978D0 (en) 2005-12-21 2006-02-01 3M Innovative Properties Co Fluorinated Surfactants For Making Fluoropolymers
GB0514398D0 (en) 2005-07-15 2005-08-17 3M Innovative Properties Co Aqueous emulsion polymerization of fluorinated monomers using a fluorinated surfactant
GB0523853D0 (en) 2005-11-24 2006-01-04 3M Innovative Properties Co Fluorinated surfactants for use in making a fluoropolymer
CN101282788B (zh) 2005-10-14 2011-04-06 旭硝子株式会社 碱性阴离子交换树脂的再生方法
US7728087B2 (en) 2005-12-23 2010-06-01 3M Innovative Properties Company Fluoropolymer dispersion and method for making the same
US7754795B2 (en) 2006-05-25 2010-07-13 3M Innovative Properties Company Coating composition
US7666928B2 (en) * 2006-05-31 2010-02-23 E.I. Du Pont De Nemours And Company Staged addition of non-fluorinated anionic surfactant to reduced fluorosurfactant fluoropolymer dispersion
US8119750B2 (en) 2006-07-13 2012-02-21 3M Innovative Properties Company Explosion taming surfactants for the production of perfluoropolymers
KR101500018B1 (ko) * 2007-02-16 2015-03-06 쓰리엠 이노베이티브 프로퍼티즈 캄파니 물로부터 불소화합물계 물질을 제거하는 시스템 및 방법
US20080264864A1 (en) * 2007-04-27 2008-10-30 3M Innovative Properties Company PROCESS FOR REMOVING FLUORINATED EMULSIFIER FROM FLUOROPOLMER DISPERSIONS USING AN ANION-EXCHANGE RESIN AND A pH-DEPENDENT SURFACTANT AND FLUOROPOLYMER DISPERSIONS CONTAINING A pH-DEPENDENT SURFACTANT
JP5492084B2 (ja) * 2008-08-12 2014-05-14 和光純薬工業株式会社 前処理カラムの充填剤用ポリマー
JP5256002B2 (ja) * 2008-11-25 2013-08-07 オルガノ株式会社 フォトレジスト現像排水の排水処理システム
CN102740974A (zh) 2010-02-03 2012-10-17 旭硝子株式会社 阴离子性含氟乳化剂的回收方法
JP2013519517A (ja) * 2010-02-18 2013-05-30 ランクセス・ドイチュランド・ゲーエムベーハー フッ素化酸またはそれらの塩を含む廃水の処理
EP2431334A1 (de) 2010-09-16 2012-03-21 LANXESS Deutschland GmbH Behandlung von Abwässern aus der Galvanikindustrie
WO2015053235A1 (ja) * 2013-10-10 2015-04-16 旭硝子株式会社 含フッ素乳化剤の回収方法
DE102014100694A1 (de) 2014-01-22 2015-07-23 Friedrich-Alexander-Universität Erlangen-Nürnberg Verfahren und Vorrichtung zur Abtrennung von fluorierten Kohlenwasserstoffen aus einer wässrigen Phase
CN106232231B (zh) * 2014-04-18 2020-11-20 3M创新有限公司 支链氟化乳化剂的回收
JP6123864B2 (ja) * 2015-10-19 2017-05-10 ダイキン工業株式会社 炭素数2〜7の含フッ素有機酸および不純物を含む組成物の処理方法
WO2017151935A1 (en) 2016-03-04 2017-09-08 3M Innovative Properties Company Method for removing perfluorinated alkanoic acids
CN113667247A (zh) 2017-03-31 2021-11-19 大金工业株式会社 包含含氟聚合物的组合物及其成型体
US12378138B2 (en) 2019-06-19 2025-08-05 The Johns Hopkins University Contaminant-sequestering coatings and methods of using the same
US11452987B2 (en) 2019-06-19 2022-09-27 The Johns Hopkins University Contaminate sequestering coatings and methods of using the same
US12240767B2 (en) 2019-06-28 2025-03-04 Katholieke Universiteit Leuven Adsorptive removal of perfluorinated or partially fluorinated surfactants
EP3945075A1 (en) 2020-07-30 2022-02-02 3M Innovative Properties Company Process for removal of fluoroorganic compounds from emulsions
EP3945099A1 (en) 2020-07-30 2022-02-02 3M Innovative Properties Company Process for removal of fluoroorganic compounds from aqueous media
EP3945074A1 (en) 2020-07-30 2022-02-02 3M Innovative Properties Company Process to reduce the concentration of fluoroorganic acidic compound in aqueous dispersions
US12410071B1 (en) 2020-10-19 2025-09-09 Wm Intellectual Property Holdings, L.L.C. System and method for removal of PFAS and other emerging contaminant micro-constituents from landfill leachate and other impacted liquids
EP4219412A1 (en) 2022-01-27 2023-08-02 3M Innovative Properties Company Closed-loop technologies for purifying fluorine containing water streams

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3882153A (en) 1969-09-12 1975-05-06 Kureha Chemical Ind Co Ltd Method for recovering fluorinated carboxylic acid
DE2903981A1 (de) 1979-02-02 1980-08-07 Hoechst Ag Rueckgewinnung fluorierter emulgatorsaeuren aus basischen anionenaustauschern
JPS632656A (ja) * 1986-06-23 1988-01-07 Furukawa Electric Co Ltd:The ウエハ研磨方法及びそれに用いるウエハ研磨基板
DE4318258A1 (de) * 1993-06-02 1994-12-08 Hoechst Ag Verfahren zur Rückgewinnung von fluorierten Carbonsäuren
DE19824615A1 (de) 1998-06-02 1999-12-09 Dyneon Gmbh Verfahren zur Rückgewinnung von fluorierten Alkansäuren aus Abwässern
DE19824614A1 (de) 1998-06-02 1999-12-09 Dyneon Gmbh Verfahren zur Rückgewinnung von fluorierten Alkansäuren aus Abwässern
DE19932771A1 (de) 1999-07-14 2001-01-18 Dyneon Gmbh Verfahren zur Eluierung fluorierter Emulgatoren

Also Published As

Publication number Publication date
JP2003512931A (ja) 2003-04-08
PL354617A1 (en) 2004-02-09
AU7924000A (en) 2001-05-14
DE19953285A1 (de) 2001-05-10
DE50002876D1 (de) 2003-08-14
EP1240107A1 (de) 2002-09-18
CN1387498A (zh) 2002-12-25
WO2001032563A1 (de) 2001-05-10
RU2255807C2 (ru) 2005-07-10
EP1240107B1 (de) 2003-07-09
US6642415B1 (en) 2003-11-04
ZA200203488B (en) 2003-08-04
CA2387781A1 (en) 2001-05-10

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C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20171030

Address after: American Minnesota

Patentee after: 3M Innovative Properties Company

Address before: The German Bogeke group

Patentee before: Dyneon GmbH & Co. KG

CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20041110

Termination date: 20191028