CN117447649A - 一种凝胶颗粒封堵剂体系及制备方法 - Google Patents
一种凝胶颗粒封堵剂体系及制备方法 Download PDFInfo
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- CN117447649A CN117447649A CN202311663537.1A CN202311663537A CN117447649A CN 117447649 A CN117447649 A CN 117447649A CN 202311663537 A CN202311663537 A CN 202311663537A CN 117447649 A CN117447649 A CN 117447649A
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- solution
- hydrophobic monomer
- monomer
- plugging agent
- initiator
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- 239000007863 gel particle Substances 0.000 title claims abstract description 65
- 238000002360 preparation method Methods 0.000 title abstract description 9
- 239000000178 monomer Substances 0.000 claims abstract description 85
- 230000002209 hydrophobic effect Effects 0.000 claims abstract description 72
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 64
- 239000003431 cross linking reagent Substances 0.000 claims abstract description 44
- 239000003999 initiator Substances 0.000 claims abstract description 40
- 239000002994 raw material Substances 0.000 claims abstract description 11
- 239000000243 solution Substances 0.000 claims description 117
- 238000003756 stirring Methods 0.000 claims description 47
- -1 cetyl dimethylallyl ammonium chloride Chemical compound 0.000 claims description 26
- KWYHDKDOAIKMQN-UHFFFAOYSA-N N,N,N',N'-tetramethylethylenediamine Chemical compound CN(C)CCN(C)C KWYHDKDOAIKMQN-UHFFFAOYSA-N 0.000 claims description 19
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims description 18
- 238000001035 drying Methods 0.000 claims description 17
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 14
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 14
- 238000000034 method Methods 0.000 claims description 14
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 11
- 239000002981 blocking agent Substances 0.000 claims description 10
- 239000002904 solvent Substances 0.000 claims description 8
- 239000000565 sealant Substances 0.000 claims description 7
- 239000011259 mixed solution Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 239000011435 rock Substances 0.000 abstract description 14
- 125000000524 functional group Chemical group 0.000 abstract description 12
- 239000000126 substance Substances 0.000 abstract description 11
- 230000003993 interaction Effects 0.000 abstract description 9
- 239000002245 particle Substances 0.000 abstract description 9
- 230000009471 action Effects 0.000 abstract description 8
- 241000237536 Mytilus edulis Species 0.000 abstract description 7
- 235000020638 mussel Nutrition 0.000 abstract description 7
- 239000002131 composite material Substances 0.000 abstract description 6
- 229910052739 hydrogen Inorganic materials 0.000 abstract description 6
- 239000001257 hydrogen Substances 0.000 abstract description 6
- 239000011664 nicotinic acid Substances 0.000 abstract description 6
- 125000001165 hydrophobic group Chemical group 0.000 abstract description 3
- 229920000642 polymer Polymers 0.000 abstract description 3
- 230000021615 conjugation Effects 0.000 abstract description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 37
- 239000008367 deionised water Substances 0.000 description 34
- 229910021641 deionized water Inorganic materials 0.000 description 34
- 239000000499 gel Substances 0.000 description 30
- 238000005303 weighing Methods 0.000 description 25
- 239000000463 material Substances 0.000 description 18
- 238000012360 testing method Methods 0.000 description 15
- 230000000052 comparative effect Effects 0.000 description 10
- 230000000694 effects Effects 0.000 description 9
- 239000012530 fluid Substances 0.000 description 8
- 238000005553 drilling Methods 0.000 description 7
- 238000005485 electric heating Methods 0.000 description 7
- 230000000977 initiatory effect Effects 0.000 description 7
- 230000008901 benefit Effects 0.000 description 5
- 238000004132 cross linking Methods 0.000 description 5
- 238000005411 Van der Waals force Methods 0.000 description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical group [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 4
- 238000011056 performance test Methods 0.000 description 4
- 238000011065 in-situ storage Methods 0.000 description 3
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 239000000853 adhesive Substances 0.000 description 2
- 230000001070 adhesive effect Effects 0.000 description 2
- 229920006037 cross link polymer Polymers 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000001125 extrusion Methods 0.000 description 2
- 230000006870 function Effects 0.000 description 2
- 230000035876 healing Effects 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- ZIUHHBKFKCYYJD-UHFFFAOYSA-N n,n'-methylenebisacrylamide Chemical compound C=CC(=O)NCNC(=O)C=C ZIUHHBKFKCYYJD-UHFFFAOYSA-N 0.000 description 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 230000008961 swelling Effects 0.000 description 2
- 230000002522 swelling effect Effects 0.000 description 2
- 235000009328 Amaranthus caudatus Nutrition 0.000 description 1
- 240000001592 Amaranthus caudatus Species 0.000 description 1
- 239000004971 Cross linker Substances 0.000 description 1
- 230000005526 G1 to G0 transition Effects 0.000 description 1
- 239000006087 Silane Coupling Agent Substances 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 150000001253 acrylic acids Chemical class 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 235000012735 amaranth Nutrition 0.000 description 1
- 239000004178 amaranth Substances 0.000 description 1
- 125000003368 amide group Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 239000011203 carbon fibre reinforced carbon Substances 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000010382 chemical cross-linking Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000004581 coalescence Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000010485 coping Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 229920006335 epoxy glue Polymers 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
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- 238000001000 micrograph Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
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- 239000003345 natural gas Substances 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 230000010355 oscillation Effects 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000003209 petroleum derivative Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
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- 238000011160 research Methods 0.000 description 1
- 230000002441 reversible effect Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000001612 separation test Methods 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/52—Amides or imides
- C08F220/54—Amides, e.g. N,N-dimethylacrylamide or N-isopropylacrylamide
- C08F220/56—Acrylamide; Methacrylamide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F226/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen
- C08F226/02—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen by a single or double bond to nitrogen
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
- C09K8/42—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells
- C09K8/426—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells for plugging
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
- C09K8/42—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells
- C09K8/44—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells containing organic binders only
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN202311663537.1A CN117447649B (zh) | 2023-12-06 | 2023-12-06 | 一种凝胶颗粒封堵剂及制备方法 |
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CN202311663537.1A CN117447649B (zh) | 2023-12-06 | 2023-12-06 | 一种凝胶颗粒封堵剂及制备方法 |
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CN117447649A true CN117447649A (zh) | 2024-01-26 |
CN117447649B CN117447649B (zh) | 2024-04-02 |
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Citations (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0161881A2 (en) * | 1984-05-07 | 1985-11-21 | MITSUI TOATSU CHEMICALS, Inc. | High molecular weight composite materialsfor releasing a water soluble organic compound |
EP0161882A2 (en) * | 1984-05-07 | 1985-11-21 | MITSUI TOATSU CHEMICALS, Inc. | Adsorption-desorption method for the separation of water soluble organic compounds from aqueous solution |
US6417249B1 (en) * | 1997-10-31 | 2002-07-09 | Hewlett-Packard Company | Ink-jet printing ink compositions having superior smear-fastness |
JP2008133396A (ja) * | 2006-11-29 | 2008-06-12 | Sumitomo Seika Chem Co Ltd | 吸水性樹脂の製造方法 |
WO2011141526A1 (de) * | 2010-05-11 | 2011-11-17 | Geohumus International Research & Development Gmbh | Bioabbaubares wasserquellbares hybridmaterial |
WO2015018203A1 (zh) * | 2013-08-09 | 2015-02-12 | 西南石油大学 | 堵漏剂及其制备方法 |
CN104448125A (zh) * | 2013-09-24 | 2015-03-25 | 中国石油化工股份有限公司 | 两性疏水缔合聚合物及其制备方法 |
CN108084296A (zh) * | 2016-11-21 | 2018-05-29 | 中国石油化工股份有限公司 | 具有引发聚合反应功能的组合物及制备丙烯酰胺共聚物的方法 |
CN108822672A (zh) * | 2018-07-06 | 2018-11-16 | 天津市建筑材料科学研究院有限公司 | 一种抗油污喷剂 |
WO2019036378A1 (en) * | 2017-08-18 | 2019-02-21 | The Regents Of The University Of California | SUPRAMOLECULAR MEDICAL ADHESIVES BIO-INSPIRED |
US20200407622A1 (en) * | 2016-06-02 | 2020-12-31 | The Curators Of The University Of Missouri | Fiber assisted re-crosslinkable polymer gel and preformed particle gels for fluid loss and conformance control |
US20210087453A1 (en) * | 2020-08-04 | 2021-03-25 | China University Of Petroleum | High-Temperature Resistant, High-Strength, and Thixotropic Gel Plugging Agent and Its Preparation Method and Application |
-
2023
- 2023-12-06 CN CN202311663537.1A patent/CN117447649B/zh active Active
Patent Citations (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0161881A2 (en) * | 1984-05-07 | 1985-11-21 | MITSUI TOATSU CHEMICALS, Inc. | High molecular weight composite materialsfor releasing a water soluble organic compound |
EP0161882A2 (en) * | 1984-05-07 | 1985-11-21 | MITSUI TOATSU CHEMICALS, Inc. | Adsorption-desorption method for the separation of water soluble organic compounds from aqueous solution |
US6417249B1 (en) * | 1997-10-31 | 2002-07-09 | Hewlett-Packard Company | Ink-jet printing ink compositions having superior smear-fastness |
JP2008133396A (ja) * | 2006-11-29 | 2008-06-12 | Sumitomo Seika Chem Co Ltd | 吸水性樹脂の製造方法 |
WO2011141526A1 (de) * | 2010-05-11 | 2011-11-17 | Geohumus International Research & Development Gmbh | Bioabbaubares wasserquellbares hybridmaterial |
WO2015018203A1 (zh) * | 2013-08-09 | 2015-02-12 | 西南石油大学 | 堵漏剂及其制备方法 |
CN104448125A (zh) * | 2013-09-24 | 2015-03-25 | 中国石油化工股份有限公司 | 两性疏水缔合聚合物及其制备方法 |
US20200407622A1 (en) * | 2016-06-02 | 2020-12-31 | The Curators Of The University Of Missouri | Fiber assisted re-crosslinkable polymer gel and preformed particle gels for fluid loss and conformance control |
CN108084296A (zh) * | 2016-11-21 | 2018-05-29 | 中国石油化工股份有限公司 | 具有引发聚合反应功能的组合物及制备丙烯酰胺共聚物的方法 |
WO2019036378A1 (en) * | 2017-08-18 | 2019-02-21 | The Regents Of The University Of California | SUPRAMOLECULAR MEDICAL ADHESIVES BIO-INSPIRED |
CN108822672A (zh) * | 2018-07-06 | 2018-11-16 | 天津市建筑材料科学研究院有限公司 | 一种抗油污喷剂 |
US20210087453A1 (en) * | 2020-08-04 | 2021-03-25 | China University Of Petroleum | High-Temperature Resistant, High-Strength, and Thixotropic Gel Plugging Agent and Its Preparation Method and Application |
Non-Patent Citations (4)
Title |
---|
SUN, DL: "Heat-Resistant Hydrogel for Temporary Plugging in High-Temperature and High-Pressure Fractured Reservoirs", ACS APPLIED POLYMER MATERIALS, vol. 5, no. 10, 7 September 2023 (2023-09-07), pages 7746 - 7754 * |
TSUEY NING SOON: "Prospects of antiviral drugs derived from natural products", CURRENT TRADITIONAL MEDICINE, vol. 7, no. 5, 22 January 2021 (2021-01-22), pages 1 - 7 * |
姚春所;林茂;杨庆云;: "氧化偶联反应和酸催化反应制备活性买麻藤醇二聚体衍生物", 有机化学, no. 02, 15 February 2013 (2013-02-15), pages 122 - 128 * |
杨洋: "可酸溶固化堵漏材料的封堵及储层保护性能", 油田化学, vol. 37, no. 4, 25 December 2020 (2020-12-25), pages 581 - 583 * |
Also Published As
Publication number | Publication date |
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CN117447649B (zh) | 2024-04-02 |
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Inventor after: Ye Shuangxiang Inventor after: Yang Yang Inventor after: Wu Zhiming Inventor after: Liu Yiheng Inventor after: Zhong Ying Inventor after: Zhang Hao Inventor before: Yang Yang Inventor before: Ye Shuangxiang Inventor before: Wu Zhiming Inventor before: Liu Yiheng Inventor before: Zhong Ying Inventor before: Zhang Hao |
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