CN117243835A - Oil-control moisturizing composition and preparation method and application thereof - Google Patents
Oil-control moisturizing composition and preparation method and application thereof Download PDFInfo
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- CN117243835A CN117243835A CN202311387914.3A CN202311387914A CN117243835A CN 117243835 A CN117243835 A CN 117243835A CN 202311387914 A CN202311387914 A CN 202311387914A CN 117243835 A CN117243835 A CN 117243835A
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- 230000003020 moisturizing effect Effects 0.000 title claims abstract description 83
- 239000000203 mixture Substances 0.000 title claims abstract description 54
- 238000002360 preparation method Methods 0.000 title abstract description 8
- 235000019198 oils Nutrition 0.000 claims abstract description 55
- 239000002537 cosmetic Substances 0.000 claims abstract description 38
- DFPAKSUCGFBDDF-UHFFFAOYSA-N Nicotinamide Chemical compound NC(=O)C1=CC=CN=C1 DFPAKSUCGFBDDF-UHFFFAOYSA-N 0.000 claims abstract description 28
- 235000015112 vegetable and seed oil Nutrition 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229960003966 nicotinamide Drugs 0.000 claims abstract description 14
- 235000005152 nicotinamide Nutrition 0.000 claims abstract description 14
- 239000011570 nicotinamide Substances 0.000 claims abstract description 14
- 241000721098 Epilobium Species 0.000 claims abstract description 4
- 239000003921 oil Substances 0.000 claims description 52
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 24
- 239000002904 solvent Substances 0.000 claims description 20
- 238000003756 stirring Methods 0.000 claims description 16
- 238000001816 cooling Methods 0.000 claims description 15
- TXFPEBPIARQUIG-UHFFFAOYSA-N 4'-hydroxyacetophenone Chemical group CC(=O)C1=CC=C(O)C=C1 TXFPEBPIARQUIG-UHFFFAOYSA-N 0.000 claims description 14
- 239000002562 thickening agent Substances 0.000 claims description 14
- 239000002738 chelating agent Substances 0.000 claims description 12
- 230000001804 emulsifying effect Effects 0.000 claims description 12
- 239000003963 antioxidant agent Substances 0.000 claims description 10
- 230000003078 antioxidant effect Effects 0.000 claims description 8
- 125000003118 aryl group Chemical group 0.000 claims description 8
- 239000003906 humectant Substances 0.000 claims description 8
- 229940015975 1,2-hexanediol Drugs 0.000 claims description 7
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 7
- FHKSXSQHXQEMOK-UHFFFAOYSA-N hexane-1,2-diol Chemical compound CCCCC(O)CO FHKSXSQHXQEMOK-UHFFFAOYSA-N 0.000 claims description 7
- 241000124033 Salix Species 0.000 claims description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical group [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 5
- CCLARULDIPFTCP-BOYHRMMASA-N (2r,3r,4r,5s)-heptane-1,2,3,4,5,6-hexol Chemical compound CC(O)[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO CCLARULDIPFTCP-BOYHRMMASA-N 0.000 claims description 4
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 4
- BIVBRWYINDPWKA-VLQRKCJKSA-L Glycyrrhizinate dipotassium Chemical compound [K+].[K+].O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@H]1CC[C@]2(C)[C@H]3C(=O)C=C4[C@@H]5C[C@](C)(CC[C@@]5(CC[C@@]4(C)[C@]3(C)CC[C@H]2C1(C)C)C)C(O)=O)C([O-])=O)[C@@H]1O[C@H](C([O-])=O)[C@@H](O)[C@H](O)[C@H]1O BIVBRWYINDPWKA-VLQRKCJKSA-L 0.000 claims description 4
- 229920002385 Sodium hyaluronate Polymers 0.000 claims description 4
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 230000003750 conditioning effect Effects 0.000 claims description 4
- 229940101029 dipotassium glycyrrhizinate Drugs 0.000 claims description 4
- 238000007599 discharging Methods 0.000 claims description 4
- 239000004744 fabric Substances 0.000 claims description 4
- 238000001914 filtration Methods 0.000 claims description 4
- 239000003205 fragrance Substances 0.000 claims description 4
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 claims description 4
- 239000003002 pH adjusting agent Substances 0.000 claims description 4
- 229960005323 phenoxyethanol Drugs 0.000 claims description 4
- 229940010747 sodium hyaluronate Drugs 0.000 claims description 4
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims description 4
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims description 2
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical group [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims description 2
- 239000004909 Moisturizer Substances 0.000 claims description 2
- 239000004359 castor oil Substances 0.000 claims description 2
- 235000019438 castor oil Nutrition 0.000 claims description 2
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims description 2
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 2
- 230000001333 moisturizer Effects 0.000 claims description 2
- 229920000058 polyacrylate Polymers 0.000 claims description 2
- -1 skin conditioners Substances 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 18
- 239000000084 colloidal system Substances 0.000 abstract description 4
- 210000003491 skin Anatomy 0.000 description 24
- 238000002156 mixing Methods 0.000 description 10
- 230000028327 secretion Effects 0.000 description 10
- 230000000052 comparative effect Effects 0.000 description 8
- 238000012360 testing method Methods 0.000 description 7
- 239000002994 raw material Substances 0.000 description 6
- 239000000463 material Substances 0.000 description 4
- 210000002374 sebum Anatomy 0.000 description 4
- 206010000496 acne Diseases 0.000 description 3
- 238000004090 dissolution Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000004519 grease Substances 0.000 description 3
- 230000002401 inhibitory effect Effects 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000011148 porous material Substances 0.000 description 3
- 208000020154 Acnes Diseases 0.000 description 2
- 108010066551 Cholestenone 5 alpha-Reductase Proteins 0.000 description 2
- 102000004127 Cytokines Human genes 0.000 description 2
- 108090000695 Cytokines Proteins 0.000 description 2
- 101710172711 Structural protein Proteins 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000009924 canning Methods 0.000 description 2
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 210000004207 dermis Anatomy 0.000 description 2
- 235000014113 dietary fatty acids Nutrition 0.000 description 2
- 229930195729 fatty acid Natural products 0.000 description 2
- 239000000194 fatty acid Substances 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 244000005700 microbiome Species 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- 238000004806 packaging method and process Methods 0.000 description 2
- 230000000770 proinflammatory effect Effects 0.000 description 2
- 210000001732 sebaceous gland Anatomy 0.000 description 2
- 238000013112 stability test Methods 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- DCXXMTOCNZCJGO-UHFFFAOYSA-N tristearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 2
- 208000002874 Acne Vulgaris Diseases 0.000 description 1
- 235000008302 Chamaenerion angustifolium Nutrition 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 241001299686 Salix triandra Species 0.000 description 1
- 206010047697 Volvulus Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 201000007647 intestinal volvulus Diseases 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to an oil-control moisturizing composition, and a preparation method and application thereof, and belongs to the technical field of cosmetics. The oil-control moisturizing composition comprises the following components: octanoylglycine, extract of Epilobium freundum, nicotinamide and white pool seed oil; the average grain diameter of the white pond flower seed oil is 100-150nm. According to the invention, the oil control effect of the oil control moisturizing composition on skin can be synergistically enhanced by selecting the specific components for matching. The white pool flower seed oil with the average grain diameter of 100-150nm is adopted, so that the moisturizing effect of the composition can be enhanced, and the water phase and the oil phase in the composition can be fully and uniformly mixed to form a colloid system capable of generating the Tyndall phenomenon.
Description
Technical Field
The invention relates to the technical field of daily chemical products, in particular to an oil-control moisturizing composition and a preparation method and application thereof.
Background
With the improvement of the living standard of people, more and more people begin to pay attention to the skin of the people; excessive secretion of skin oil can cause pores to be large, skin to be greasy and bright, and even cause a series of problems such as acnes and acnes, so that the skin oil control and moisture preservation are necessary.
Skin care products with oil control effect are various in the market, such as a cleaning product for cleaning and controlling oil, astringent containing high-concentration alcohol, and the like, and some skin care products adopt physical adsorbents to control grease secretion through adsorption; however, the oil control products on the market at present adopt water and oil layering, need to be uniformly shaken before use, have poor oil control effect and bring a plurality of inconveniences for users.
Aiming at the defects of the oil control products, the development of an oil control moisturizing composition which has the advantages of moist texture, quick absorption, oil control and excellent moisturizing effect is the key point of the current research.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provide an oil control and moisturizing composition, a preparation method and application thereof, wherein the oil control and moisturizing composition has excellent oil control and moisturizing effects, and is moist in texture and can be quickly absorbed during use.
In order to achieve the above purpose, the technical scheme adopted by the invention is as follows:
in a first aspect, the present invention provides an oil control moisturizing composition comprising the following components: octanoylglycine, extract of Epilobium freundum, nicotinamide and white pool seed oil; the average grain diameter of the white pond flower seed oil is 100-150nm.
The octanoylglycine in the oil-control moisturizing composition is the main component of the dermis structural protein, can provide free carboxyl, keep the balance of the pH value of the skin, inhibit the growth of harmful microorganisms, regulate the microecology of the skin and regulate the secretion of skin grease; the extract of Epigallosis has effects of inhibiting 5 alpha-reductase, reducing proinflammatory cytokines, reducing skin oil secretion, and reducing blackhead; nicotinamide has the effects of specifically inhibiting the synthesis of fatty acid and triacylglycerol and reducing sebum secretion, and can reduce sebum secretion by removing an oil layer existing in a catheter connecting sebaceous glands and pores on the skin surface; according to the invention, the oil control effect of the oil control moisturizing composition on skin can be synergistically enhanced by selecting the specific components for matching.
The inventor discovers that the invention adopts the white pool flower seed oil with the average grain diameter of 100-150nm, not only can enhance the moisturizing effect of the composition, but also can fully and uniformly mix the water phase and the oil phase in the composition to form a colloid system which can generate the tyndall phenomenon.
As a preferred embodiment of the oil control and moisturizing composition of the present invention, the oil control and moisturizing composition comprises the following components in parts by weight: 0.1-0.8 part of octanoylglycine, 1-5 parts of French willow leaf extract, 1-5 parts of nicotinamide and 0.1-1 part of white pond flower seed oil; the inventor finds that when each component in the oil control moisturizing composition is in the range of the weight parts, the prepared oil control moisturizing product has good oil control and moisturizing effects and excellent stability.
As a more preferred embodiment of the oil control and moisturizing composition of the present invention, the oil control and moisturizing composition comprises the following components in parts by weight: 0.1-0.5 part of octanoylglycine, 2-5 parts of salix volvata extract, 1-3 parts of nicotinamide and 0.1-0.5 part of white pond flower seed oil; the inventor finds through experiments that when each component in the oil-control moisturizing composition is in the weight part range, the oil-control moisturizing composition has better oil-control effect, the oil phase and the water phase are mixed more uniformly, and the tyndall phenomenon is more obvious.
As a most preferred embodiment of the oil control and moisturizing composition of the present invention, the oil control and moisturizing composition comprises the following components in parts by weight: 0.4 part of octanoylglycine, 3 parts of a salix volvulus extract, 2 parts of nicotinamide and 0.3 part of white pond flower seed oil; the inventor found through experiments that the oil control effect of the oil control moisturizing composition can be best when each component in the oil control moisturizing composition is under the condition of the weight parts.
In a second aspect, the present invention provides an oil-control moisturizing cosmetic comprising an oil-control moisturizing composition as described in the first aspect.
As a preferred embodiment of the oil-control moisturizing cosmetic of the present invention, the oil-control moisturizing cosmetic further comprises the following components: moisturizers, antioxidants, pH modifiers, solvents, chelating agents, thickeners, skin conditioners, fragrances, and solubilizers.
As a more preferable embodiment of the oil-control moisturizing cosmetic composition of the present invention, the oil-control moisturizing cosmetic composition comprises the following components in parts by weight: 4.22 to 14.7 parts of humectant, 0.2 to 0.5 part of antioxidant, 0.01 to 0.06 part of pH regulator, 0.55 to 13 parts of solvent, 0 to 0.05 part of chelating agent, 0.05 to 0.5 part of thickener, 0.06 to 2.9 parts of skin conditioning agent, 0.0002 to 0.03 part of aromatic and 0.001 to 0.015 part of solubilizer.
As the most preferable implementation mode of the oil-control moisturizing cosmetic, the oil-control moisturizing cosmetic comprises the following components in parts by weight: 5.33-9.55 parts of humectant, 0.3-0.5 part of antioxidant, 0.02-0.06 part of pH regulator, 3-9 parts of solvent, 0.01-0.03 part of chelating agent, 0.1-0.4 part of thickener, 0.62-2.6 parts of skin conditioner, 0.001-0.03 part of aromatic and 0.005-0.015 part of solubilizer.
As the most preferable implementation mode of the oil-control moisturizing cosmetic, the oil-control moisturizing cosmetic comprises the following components in parts by weight: 7.05 parts of humectant, 0.5 part of antioxidant, 0.04 part of pH regulator, 8 parts of solvent, 0.02 part of chelating agent, 0.3 part of thickener, 1.45 parts of skin conditioning agent, 0.003 part of aromatic and 0.015 part of solubilizer.
Experiments show that when the components in the oil-control moisturizing cosmetic are in specific weight parts, the oil-control moisturizing cosmetic has better oil-control effect, and particularly under the most preferred conditions, the oil-control moisturizing performance can be optimized.
As a preferred embodiment of the oil-control moisturizing cosmetic of the present invention, at least one of the following is adopted:
(1) The humectant comprises sodium hyaluronate, glycerol, butanediol, 1, 2-hexanediol, methyl glucitol polyether-20, PEG/PPG/polytetramethylene glycol-8/5/3 glycerol;
(2) The antioxidant is p-hydroxyacetophenone;
(3) The pH regulator is sodium hydroxide;
(4) The solvent is water;
(5) The chelating agent is disodium EDTA;
(6) The thickener is polyacrylate crosslinked polymer-6;
(7) The skin conditioner comprises biological sugar gum-1, phenoxyethanol and dipotassium glycyrrhizinate;
(8) The aromatic is essence;
(9) The solubilizer is PEG-40 hydrogenated castor oil.
As a more preferable embodiment of the oil-control moisturizing cosmetic, the oil-control moisturizing cosmetic comprises an A-G phase; wherein, phase A includes: water, chelating agent, thickener, sodium hyaluronate and glycerol; the phase B comprises: butanediol, 1, 2-hexanediol and p-hydroxyacetophenone; the phase C comprises: water, pH adjuster, octanoylglycine; phase D comprises: biological sugar gum-1, phenoxyethanol, methyl glucitol polyether-20 and PEG/PPG/polytetramethylene glycol-8/5/3 glycerol; phase E comprises water, nicotinamide and dipotassium glycyrrhizinate; phase F includes fragrance and thickener; phase G included pooled seed oil.
In a third aspect, the present invention provides a method for preparing the oil-control moisturizing cosmetic, which comprises the following steps:
s1, putting the phase A into an emulsifying pot, homogenizing for 2-3min, stirring and heating to 80-85 ℃, preserving heat and stirring for 10-20min until the phase A is completely dissolved, and cooling to 45-50 ℃;
s2, sequentially adding a phase B and a phase C into the emulsifying pot in the step S1, uniformly stirring, and cooling to 40-45 ℃;
and S3, sequentially adding a D phase, an E phase, an F phase and a G phase into the emulsifying pot in the step S2, uniformly stirring, cooling to below 40 ℃, and filtering and discharging by using 200-mesh filter cloth to obtain the oil-control moisturizing cosmetic.
As a preferred embodiment of the method for producing an oil-controlling and moisturizing cosmetic of the present invention, each phase needs to be pretreated, i.e., each raw material is mixed and dissolved, before step S1.
As a more preferable embodiment of the preparation method of the oil-control moisturizing cosmetic of the present invention, the pretreatment process of the B phase is: mixing and heating butanediol and p-hydroxyacetophenone to 60-65 ℃, cooling to about 45 ℃ after complete dissolution, adding 1,2 hexanediol, and uniformly mixing to complete pretreatment.
Compared with the prior art, the invention has the beneficial effects that:
(1) The octanoylglycine in the oil-control moisturizing composition is the main component of the dermis structural protein, can provide free carboxyl, keep the balance of the pH value of the skin, inhibit the growth of harmful microorganisms, regulate the microecology of the skin and regulate the secretion of skin grease;
(2) The oil-control moisturizing composition has the advantages that the Fuleys willow leaf extract in the oil-control moisturizing composition can inhibit 5 alpha-reductase, reduce pro-inflammatory cytokines, reduce oil secretion of skin and reduce comedones;
(3) The nicotinamide in the oil-control moisturizing composition has the effects of specifically inhibiting the synthesis of fatty acid and triacylglycerol and reducing sebum secretion, and can remove an oil layer in a catheter connecting sebaceous glands and skin surface pores, so that the effect of reducing sebum secretion is achieved;
(4) According to the invention, the oil control effect of the oil control moisturizing composition on skin can be synergistically enhanced by selecting the specific components for matching;
(5) The white pool flower seed oil with the average grain diameter of 100-150nm not only can enhance the moisturizing effect of the composition, but also can fully and uniformly mix the water phase and the oil phase in the composition to form a colloid system capable of generating the Tyndall phenomenon.
Drawings
Fig. 1 is a graph showing the effect of light paths of different parts by weight of white pool flower seed oil in the acne-removing and oil-controlling cosmetic.
Detailed Description
For a better description of the objects, technical solutions and advantages of the present invention, the present invention will be further described with reference to the following specific examples.
The reagents, methods and apparatus employed in the present invention are those conventional in the art unless otherwise indicated.
When the weight parts of the components involved in the examples and comparative examples were changed, the amount of the empty or insufficient water generated by the change was maintained at 100 parts.
The information of part of raw materials of the invention is as follows:
examples 1 to 6
The formulas of the oil-control moisturizing cosmetics disclosed by the embodiments 1-6 are shown in the table 1, and the preparation method comprises the following steps:
pretreatment:
1. taking a clean external container, mixing and heating the B-phase butanediol and the p-hydroxyacetophenone to 60-65 ℃, cooling to about 45 ℃ after complete dissolution, and adding 1, 2-hexanediol to uniformly mix for later use;
2. taking a clean external container, and pre-mixing and dissolving the phase C for use;
3. taking a clean external container, and pre-mixing and dissolving the E phase for use;
4. taking a clean external container, and pre-mixing and dissolving the phase F for use.
S1, putting the phase A raw material into an emulsifying pot, homogenizing for 2-3min, stirring and heating to 80-85 ℃, preserving heat and stirring for 10-20min until the phase A raw material is completely dissolved, and cooling to 45-50 ℃;
s2, sequentially adding a phase B and a phase C into the emulsifying pot in the step S1, uniformly stirring, and cooling to 40-45 ℃;
and S3, sequentially adding a D phase, an E phase, an F phase and a G phase into the emulsifying pot in the step S2, uniformly stirring, cooling to below 40 ℃, filtering and discharging by using 200-mesh filter cloth, sending the materials to be inspected, and after the materials are inspected to be qualified, canning, packaging, inspecting a finished product and delivering the products to obtain the oil-control moisturizing cosmetic.
In examples 1 to 6, the average particle diameter of the white pool seed oil was 100 to 150nm.
TABLE 1
Comparative examples 1 to 7
The formulas of the oil-control moisturizing cosmetics according to comparative examples 1 to 7 are shown in table 2, and the preparation method comprises the following steps:
pretreatment:
1. taking a clean external container, mixing and heating the B-phase butanediol and the p-hydroxyacetophenone to 60-65 ℃, cooling to about 45 ℃ after complete dissolution, and adding 1, 2-hexanediol to uniformly mix for later use;
2. taking a clean external container, and pre-mixing and dissolving the phase C for use;
3. taking a clean external container, and pre-mixing and dissolving the E phase for use;
4. taking a clean external container, and pre-mixing and dissolving the phase F for use.
S1, putting the phase A raw material into an emulsifying pot, homogenizing for 2-3min, stirring and heating to 80-85 ℃, preserving heat and stirring for 10-20min until the phase A raw material is completely dissolved, and cooling to 45-50 ℃;
s2, sequentially adding a phase B and a phase C into the emulsifying pot in the step S1, uniformly stirring, and cooling to 40-45 ℃;
and S3, sequentially adding a D phase, an E phase, an F phase and a G phase into the emulsifying pot in the step S2, uniformly stirring, cooling to below 40 ℃, filtering and discharging by using 200-mesh filter cloth, sending the materials to be inspected, and after the materials are inspected to be qualified, canning, packaging, inspecting a finished product and delivering the products to obtain the oil-control moisturizing cosmetic.
TABLE 2
Comparative example 8
This comparative example differs from example 4 only in that: the average particle size of the white pool seed oil was 50nm, the remainder being the same as in example 4.
Comparative example 9
This comparative example differs from example 4 only in that: the average particle size of the white pool seed oil was 200nm, the remainder being identical to example 4.
Test examples
1. Stability test
The oil-controlling moisturizing cosmetics described in examples 1 to 6 and comparative examples 1 to 7 were subjected to stability test, and the test results are shown in table 3 below.
TABLE 3 Table 3
As can be seen from Table 3, the oil-control moisturizing cosmetic provided by the invention has good stability, neutral pH and no irritation to skin.
2. Oil control effect and optical path testing
The testing method comprises the following steps:
1. optical path testing: the laser pen emits red light beam to irradiate the product, and whether clear light passage can be displayed in the product is observed in the direction perpendicular to the light beam;
2. and (3) testing an oil control effect: 130 volunteers were summoned, and the age was between 20 and 50, twice daily, and after one week of continuous use, the oil control effect was scored, with higher scores being the best.
The test results are shown in table 4 below.
TABLE 4 Table 4
As shown in table 4, the octanoylglycine, the flecheuch willow leaf extract and the nicotinamide in the oil control moisturizing composition are reasonably matched and synergistically increased, so that the oil control effect of the cosmetic is remarkably improved; the oil control effect is greatly reduced in the absence of either component.
The invention adopts the white pool flower seed oil with the average grain diameter of 100-150nm, which not only can enhance the moisturizing effect of the composition, but also can fully and uniformly mix the water phase and the oil phase in the composition to form a colloid system capable of generating the Tyndall phenomenon.
Finally, it should be noted that the above embodiments are only for illustrating the technical solution of the present invention and not for limiting the scope of the present invention, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that the technical solution of the present invention may be modified or substituted equally without departing from the spirit and scope of the technical solution of the present invention.
Claims (10)
1. An oil control moisturizing composition, characterized in that the oil control moisturizing composition comprises the following components: octanoylglycine, extract of Epilobium freundum, nicotinamide and white pool seed oil; the average grain diameter of the white pond flower seed oil is 100-150nm.
2. The oil control and moisturizing composition of claim 1, wherein the oil control and moisturizing composition comprises the following components in parts by weight: 0.1-0.8 part of octanoylglycine, 1-5 parts of extract of Epilobium freundum, 1-5 parts of nicotinamide and 0.1-1 part of white pond flower seed oil.
3. The oil control and moisturizing composition of claim 1, wherein the oil control and moisturizing composition comprises the following components in parts by weight: 0.1-0.5 part of octanoylglycine, 2-5 parts of salix volvata extract, 1-3 parts of nicotinamide and 0.1-0.5 part of white pond flower seed oil.
4. The oil control and moisturizing composition of claim 1, wherein the oil control and moisturizing composition comprises the following components in parts by weight: 0.4 part of octanoylglycine, 3 parts of salix volvata extract, 2 parts of nicotinamide and 0.3 part of white pond flower seed oil.
5. An oil-controlling moisturizing cosmetic characterized in that it comprises the oil-controlling moisturizing composition according to any one of claims 1 to 4.
6. The oil-control moisturizing cosmetic of claim 5, further comprising the following components: moisturizers, antioxidants, pH modifiers, solvents, chelating agents, thickeners, skin conditioners, fragrances, and solubilizers.
7. The oil-control moisturizing cosmetic as recited in claim 6, wherein the oil-control moisturizing cosmetic comprises the following components in parts by weight: 4.22 to 14.7 parts of humectant, 0.2 to 0.5 part of antioxidant, 0.01 to 0.06 part of pH regulator, 0.55 to 13 parts of solvent, 0 to 0.05 part of chelating agent, 0.05 to 0.5 part of thickener, 0.06 to 2.9 parts of skin conditioning agent, 0.0002 to 0.03 part of aromatic and 0.001 to 0.015 part of solubilizer;
preferably, the oil-control moisturizing cosmetic comprises the following components in parts by weight: 5.33-9.55 parts of humectant, 0.3-0.5 part of antioxidant, 0.02-0.06 part of pH regulator, 3-9 parts of solvent, 0.01-0.03 part of chelating agent, 0.1-0.4 part of thickener, 0.62-2.6 parts of skin conditioner, 0.001-0.03 part of aromatic and 0.005-0.015 part of solubilizer.
More preferably, the oil-control moisturizing cosmetic comprises the following components in parts by weight: 7.05 parts of humectant, 0.5 part of antioxidant, 0.04 part of pH regulator, 8 parts of solvent, 0.02 part of chelating agent, 0.3 part of thickener, 1.45 parts of skin conditioning agent, 0.003 part of aromatic and 0.015 part of solubilizer.
8. The oil-control moisturizing cosmetic according to claim 6 or 7, wherein at least one of the following is used:
(1) The humectant comprises sodium hyaluronate, glycerol, butanediol, 1, 2-hexanediol, methyl glucitol polyether-20, PEG/PPG/polytetramethylene glycol-8/5/3 glycerol;
(2) The antioxidant is p-hydroxyacetophenone;
(3) The pH regulator is sodium hydroxide;
(4) The solvent is water;
(5) The chelating agent is disodium EDTA;
(6) The thickener is polyacrylate crosslinked polymer-6;
(7) The skin conditioner comprises biological sugar gum-1, phenoxyethanol and dipotassium glycyrrhizinate;
(8) The aromatic is essence;
(9) The solubilizer is PEG-40 hydrogenated castor oil.
9. The oil-control moisturizing cosmetic of claim 8, wherein the oil-control moisturizing cosmetic comprises an a-G phase; wherein, phase A includes: water, chelating agent, thickener, sodium hyaluronate and glycerol; the phase B comprises: butanediol, 1, 2-hexanediol and p-hydroxyacetophenone; the phase C comprises: water, pH adjuster, octanoylglycine; phase D comprises: biological sugar gum-1, phenoxyethanol, methyl glucitol polyether-20 and PEG/PPG/polytetramethylene glycol-8/5/3 glycerol; phase E comprises water, nicotinamide and dipotassium glycyrrhizinate; phase F includes fragrance and thickener; phase G included pooled seed oil.
10. A method for preparing an oil-controlling moisturizing cosmetic according to any one of claims 5 to 9, wherein said method comprises the steps of:
s1, putting the phase A into an emulsifying pot, homogenizing for 2-3min, stirring and heating to 80-85 ℃, preserving heat and stirring for 10-20min until the phase A is completely dissolved, and cooling to 45-50 ℃;
s2, sequentially adding a phase B and a phase C into the emulsifying pot in the step S1, uniformly stirring, and cooling to 40-45 ℃;
and S3, sequentially adding a D phase, an E phase, an F phase and a G phase into the emulsifying pot in the step S2, uniformly stirring, cooling to below 40 ℃, and filtering and discharging by using 200-mesh filter cloth to obtain the oil-control moisturizing cosmetic.
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| CN105342884A (en) * | 2015-11-05 | 2016-02-24 | 杭州堡资达生物科技有限公司 | BB cream having whitening, moisturizing and makeup-dizziness preventing functions |
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