CN1171606C - Watermelon frost and its preparing method - Google Patents
Watermelon frost and its preparing method Download PDFInfo
- Publication number
- CN1171606C CN1171606C CNB011291443A CN01129144A CN1171606C CN 1171606 C CN1171606 C CN 1171606C CN B011291443 A CNB011291443 A CN B011291443A CN 01129144 A CN01129144 A CN 01129144A CN 1171606 C CN1171606 C CN 1171606C
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- watermelon
- citrullus vulgaris
- frost
- white shape
- preparation
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- Medicines Containing Plant Substances (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The present invention relates to novel watermelon frost which comprises effective ingredients of a watermelon, and menthol crystal, wherein the percent of the contents of the effective ingredients of a watermelon is larger than 0.01% and smaller than 3% of the total weight. The present invention also relates to a preparation method of the watermelon frost, which comprises the following steps: 1) the watermelon is squeezed to obtain juice; 2) peppermint oil is used for extraction; 3) a peppermint oil layer which is formed after the extraction process is finished is refrigerated to separate frost; 4) the frost is filtered to form the watermelon frost. Because the novel watermelon frost contains the effective ingredients of a watermelon, and the menthol crystal without sodium sulphate, the novel watermelon frost can not generate side effects on the human body, the original taste of watermelon is maintained, and the mouth feel is good. The novel watermelon frost is extracted by the peppermint oil to separate frost, and the peppermint oil which is used in the process of preparation is recycled; thus, waste water with inorganic salt can not generate to pollute environment.
Description
(1) technical field:
The present invention relates to a kind of Chinese medicine preparation, particularly a kind of white shape thing that from Citrullus vulgaris, extracts.
The invention still further relates to its preparation method.
(2) background technology:
All contain Natrii Sulfas in the existing watermelon crystal, and Natrii Sulfas proportion in watermelon crystal even reaches 99.5% greater than 95%; But too much take Natrii Sulfas and can produce harmful effect health.
Though existing watermelon crystal preparation method improves to some extent, but still the same Natrii Sulfas crystallization that adopts with traditional method, the waste water discharge back of containing Natrii Sulfas can pollute environment.
(3) summary of the invention:
The present invention discloses a kind of white shape thing that extracts that does not contain Natrii Sulfas and preparation method thereof from Citrullus vulgaris.
A kind of white shape thing that extracts from Citrullus vulgaris comprises the Citrullus vulgaris active ingredient, and different is: composition is Citrullus vulgaris active ingredient and Mentholum; Wherein the Citrullus vulgaris content of effective accounts for total weight percent for greater than 0.01%, less than 3%.
A kind of preparation method of the white shape thing that extracts from Citrullus vulgaris is:
1) Citrullus vulgaris is squeezed extracting juice;
2) extract with Oleum menthae;
3) the freezing crystallization of Herba Menthae oil reservoir after will extracting;
4) filter white shape extract.
Extraction temperature is a room temperature, and freezing crystallization temperature is 0 ℃～-20 ℃.
Filtrate filtered is watermelon oil.
The extracted residual water layer is distilled under normal pressure, collect distilled water and be Watermelon syrup.
The ratio of Oleum menthae and Pulp Citrulli juice and extraction times can be set as required during extraction, but general extraction temperature is a room temperature, and freezing crystallization temperature is 0 ℃～-20 ℃.
Owing to only contain Citrullus vulgaris active ingredient and Mentholum in this white shape extract, therefore, can not have side effects, and used Oleum menthae is recycled in the preparation process of this white shape extract human body, can not produce the contaminated wastewater environment that contains inorganic salt.
Because contained Citrullus vulgaris active ingredient is about 10 times of former watermelon crystal in this white shape extract, therefore, its usage is similar to former watermelon crystal, and consumption is that one of ten parts of former watermelon crystal get final product.
Identical with former watermelon crystal, this white shape extract also can be made spray, tablet or mouthful larynx treasured, watermelon frost toothpaste, xiguashuang chewing-gum, watermelon crystal collutory etc.Because this white shape extract itself contains the Herba Menthae composition and do not contain Natrii Sulfas, therefore, has kept the Citrullus vulgaris original flavor, mouthfeel is better.
(4) specific embodiment:
Implement when of the present invention concrete, the Oleum menthae that can add 0.3～5 times in pressing good Pulp Citrulli juice extracts repeatedly, gets the freezing crystallization of Herba Menthae oil reservoir after the extraction, and cryogenic temperature is generally 0 ℃～-20 ℃; Filter the Herba Menthae oil reservoir then white shape extract.In this white shape extract, the Citrullus vulgaris content of effective can reach 0.01～3 percent.In extraction process, Pulp Citrulli juice with after Oleum menthae fully mixes, was generally placed under the room temperature 10～48 hours, concrete time Yin Wendu is different and change, and treats to get final product behind oil and the water stratification.In the crystallization process, oil reservoir should place the following crystallization of 0 degree, and crystallization time Yin Wendu is different and different.
Embodiment 1:
1, get 100 kilograms of Citrullus vulgariss, the squeezing extracting juice gets 50 kilograms of Pulp Citrulli juice;
2, in Pulp Citrulli juice, add 25 kilograms of Oleum menthae, stir;
3, under 27 ℃, left standstill 24 hours, obtain oil reservoir A and water layer B;
4, separate oil reservoir A and water layer B, and collect respectively;
5, water layer B was distilled 20 minutes under normal pressure, get Watermelon syrup;
6, oil reservoir A is placed 0 ℃ of 30 hours freezing crystallization; Get white shape extract after the filtration.
The Citrullus vulgaris effective ingredient is 0.02% in this white shape extract.
7, filtrate filtered is watermelon oil.
8, this white shape extract is made according to a conventional method spray, tablet or mouthful larynx treasured, watermelon frost toothpaste, xiguashuang chewing-gum, watermelon crystal collutory etc.
Embodiment 2:
1,100 kilograms of Citrullus vulgariss, the squeezing extracting juice gets 40 kilograms of Pulp Citrulli juice;
2, add 70 kilograms of Oleum menthae in the Pulp Citrulli juice, stir;
3,25 ℃ left standstill 12 hours, obtained oil reservoir A and water layer B;
4, separate oil reservoir A and water layer B, and collect respectively;
5, water layer B was distilled 30 minutes under normal pressure, get Watermelon syrup;
6, oil reservoir A is placed-5 ℃ of 24 hours freezing crystallization; Get white shape extract after the filtration.
The Citrullus vulgaris effective ingredient is 1% in this white shape extract.
7, the filtrate after the filter is watermelon oil.
8, this white shape extract is made spray, tablet or mouthful larynx treasured, watermelon frost toothpaste, xiguashuang chewing-gum, watermelon crystal collutory etc. according to a conventional method.
Embodiment 3:
1, get 100 kilograms of Citrullus vulgariss, the squeezing extracting juice gets 60 kilograms of Pulp Citrulli juice;
2, in Pulp Citrulli juice, add the 120 kg Oleum menthae, stir;
3, left standstill 20 hours at 30 ℃, obtain oil reservoir A and water layer B;
4, separate oil reservoir A and water layer B, and collect respectively;
5, water layer B is added 100 kilograms of Oleum menthae again, stir;
6, left standstill 20 hours at 30 ℃, obtain oil reservoir A1 and water layer B1;
7, separate oil reservoir A1 and water layer B1, and collect respectively;
8, water layer B1 was distilled 15 minutes under normal pressure, get Watermelon syrup;
Oil reservoir A and A1 merging are placed-15 ℃ of 12 hours freezing crystallization; Get white shape extract after the filtration.The Citrullus vulgaris effective ingredient is 2% in this white shape extract.
9, filtrate filtered is watermelon oil.
10, this white shape extract is made spray, tablet or mouthful larynx treasured, watermelon frost toothpaste, xiguashuang chewing-gum, watermelon crystal collutory etc. according to a conventional method.
Embodiment 4:
1, get 100 kilograms of Citrullus vulgariss, the squeezing extracting juice gets 60 kilograms of Pulp Citrulli juice;
2, in Pulp Citrulli juice, add 100 kilograms of Oleum menthae, stir;
3, left standstill 10 hours at 35 ℃, obtain oil reservoir A and water layer B;
4, separate oil reservoir A and water layer B, and collect respectively;
5, water layer B is added 100 kilograms of Oleum menthae again, stir;
6, left standstill 10 hours at 35 ℃, obtain oil reservoir A1 and water layer B1;
7, separate oil reservoir A1 and water layer B1, and collect respectively;
8, water layer B1 is added 100 kilograms of Oleum menthae again, stir;
9, left standstill 10 hours at 35 ℃, obtain oil reservoir A2 and water layer B2;
10, separate oil reservoir A2 and water layer B2, and collect respectively;
11, water layer B2 was distilled 15 minutes under normal pressure, get Watermelon syrup;
Oil reservoir A, A1 and A2 merging are placed-20 ℃ of 12 hours freezing crystallization; Get white shape extract after the filtration.The Citrullus vulgaris effective ingredient is 3% in this white shape extract.
12, get filtrate after the filtration and be watermelon oil.
13, this white shape extract is made spray, tablet or mouthful larynx treasured, watermelon frost toothpaste, xiguashuang chewing-gum, watermelon crystal collutory etc. according to a conventional method.
Claims (5)
1, a kind of white shape thing that extracts from Citrullus vulgaris comprises the Citrullus vulgaris active ingredient, and it is characterized in that: composition is Citrullus vulgaris active ingredient and Mentholum; Wherein the Citrullus vulgaris content of effective accounts for total weight percent for greater than 0.01%, less than 3%.
2, a kind of preparation method of the white shape thing that extracts from Citrullus vulgaris is characterized in that:
1) Citrullus vulgaris is squeezed extracting juice;
5) extract with Oleum menthae;
6) the freezing crystallization of Herba Menthae oil reservoir after will extracting;
7) filter white shape extract.
3, the preparation method of the white shape thing that extracts from Citrullus vulgaris according to claim 3 is characterized in that: extraction temperature is a room temperature, and freezing crystallization temperature is 0 ℃～-20 ℃.
4, according to the preparation method of claim 3 or the 4 described white shape things that extract from Citrullus vulgaris, it is characterized in that: filtrate filtered is watermelon oil.
5, according to the preparation method of claim 3 or the 4 described white shape things that from Citrullus vulgaris, extract, it is characterized in that: the extracted residual water layer is distilled under normal pressure, collect distilled water and be Watermelon syrup.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB011291443A CN1171606C (en) | 2001-12-01 | 2001-12-01 | Watermelon frost and its preparing method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB011291443A CN1171606C (en) | 2001-12-01 | 2001-12-01 | Watermelon frost and its preparing method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1364611A CN1364611A (en) | 2002-08-21 |
| CN1171606C true CN1171606C (en) | 2004-10-20 |
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ID=4668937
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB011291443A Expired - Fee Related CN1171606C (en) | 2001-12-01 | 2001-12-01 | Watermelon frost and its preparing method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1171606C (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105998141A (en) * | 2016-05-10 | 2016-10-12 | 王秋红 | Pure-fermenting method for preparing mirabilitum praeparatum and application thereof |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101416997B (en) * | 2007-10-26 | 2011-09-14 | 邹准 | Preparation technique of bitter melon powder and cucumber powder |
| CN101352476B (en) * | 2008-07-28 | 2011-02-16 | 莱芜钢铁集团有限公司医院 | Method for processing watermelon frost |
| CN103271267A (en) * | 2013-06-09 | 2013-09-04 | 湖南飙歌生物技术有限公司 | Citrulli degelatinatum and xylitol mixture and preparation method and application thereof |
| CN109674713A (en) * | 2019-03-04 | 2019-04-26 | 德利宝(广州)香料有限公司 | A kind of preparation method of essence that alleviating canker sore and composition for oral cavity containing the essence |
-
2001
- 2001-12-01 CN CNB011291443A patent/CN1171606C/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105998141A (en) * | 2016-05-10 | 2016-10-12 | 王秋红 | Pure-fermenting method for preparing mirabilitum praeparatum and application thereof |
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| Publication number | Publication date |
|---|---|
| CN1364611A (en) | 2002-08-21 |
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| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20041020 Termination date: 20100104 |