CN109674713A - A kind of preparation method of essence that alleviating canker sore and composition for oral cavity containing the essence - Google Patents
A kind of preparation method of essence that alleviating canker sore and composition for oral cavity containing the essence Download PDFInfo
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- CN109674713A CN109674713A CN201910158862.XA CN201910158862A CN109674713A CN 109674713 A CN109674713 A CN 109674713A CN 201910158862 A CN201910158862 A CN 201910158862A CN 109674713 A CN109674713 A CN 109674713A
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- essence
- canker sore
- oral cavity
- dry
- alleviating
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/02—Stomatological preparations, e.g. drugs for caries, aphtae, periodontitis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
Abstract
The present invention relates to daily chemicals fields, concretely relate to a kind of preparation method of the essence of alleviation canker sore and the composition for oral cavity containing the essence.The preparation method for alleviating the essence of canker sore is to weigh dry watermelon seeds, dry watermelon peel, dry cucumber, pomelo peel oil, propylene glycol, mentha piperita oil, hyacinth oil, and homogeneous, squeeze and filter is to get the essence for alleviating canker sore；Composition for oral cavity will be obtained after the essence for alleviating canker sore, oral cavity ointment raw material homogeneous.Composition for oral cavity of the present invention, miscellaneous fruity gas alcohol just, it is good in taste, and preventable disease, the effects of prevention canker sore, anti-dry can be played, wherein the effect of prevention canker sore has good remission effect to the canker sore for lacking vitamins, inflammation class, it is without side-effects, the mouthfeel of unique flavor is provided for consumer, meets consumer personalization's demand.
Description
Technical field
The present invention relates to daily chemicals fields, concretely relate to a kind of preparation method of essence for alleviating canker sore, with
And the composition for oral cavity containing the essence for alleviating canker sore (has half flow model liquid tooth paste, also there is the common of not flow-type ones
Toothpaste, also between the oral cavity ointment between both for configuration).
Background technique
In developed country, its people pay much attention to oral problem, but in China, oral problem fails to obtain its people always
Attention, usually there is oral problem, just see a doctor to hospital, it is typically late, miss best Waiting time.
Therefore, how by brushing teeth, gargling these simple modes to prevent oral problem, it should be that cost is minimum, efficiency is highest
Solution, allow gargle, the process of brushing teeth become kind enjoy then be attract gargle, more efficient way of brushing teeth, oral cavity is protected
It is good for significant.
Watermelon can be rated as " king in midsummer ", clearly quench one's thirst, taste sugariness succulence, be midsummer good fruit, watermelon except not fatty and
Outside cholesterol, containing substances such as a large amount of glucose, malic acid, fructose, Argine Monohydrochloride, tomatin and vitamin Cs abundant, it is
One kind is rich in very high nutrition, pure, edible safety food.The fatty oil of dry watermelon seeds, protein, vitamin B2, starch, penta
Glycan, propionic acid, urea, sucrose etc., dry watermelon peel are rich in injection Vitamin B_6." this is through meeting source ", which records watermelon, can draw the heat of pericardium, from
Small intestine, bladder drop, function clearing heat and promoting fluid, relieving restlessness of quenching one's thirst." occupying diet spectrum with breath " is recorded raw sore in lip and is ground with dry watermelon peel burning
It is held in the mouth or the eyes, stomatitis is dried with dry watermelon peel, stir-bake to brown, and it is on the rocks a little with grinding, affected part is applied with honey tune.
Dry cucumber is sweet in flavor, sweet tea, cool in nature, bitter, nontoxic, enters spleen, stomach, large intestine；With except heat, sharp water diuresis is clearing heat and detoxicating
Effect；Cure mainly polydipsia, abscess of throat, acute conjunctivitis, burning hot wound.There are also effect of weight reducing.Dry cucumber is applied just very extensively from ancient times civil,
It is food sources and Chinese medicine source.Fruit is used for epidemic conjunctivitis in Yi nationality's medicine, red eye, swell pain, tonsillitis larynx is swollen, and dispute is rotten
It is rotten, the hot polydipsia of the heart, skin allergy.In anaesthetic, fruit, melon seedling, melon skin, radical cure convulsion, hypertension, oedema, hot dysentery, pharynx
Larynx swelling and pain, injury of tendon and muscle fracture.
The miscellaneous fruity essence of watermelon water obtained by daily use chemicals application aspect, dry watermelon seeds, dry watermelon peel, dry cucumber compounding is not only
It is for being widely used on fragrance, actually effect is also one of the central factor applied, and such as prevents canker sore, anti-dry
Deng.Watermelon water extract applied by daily use chemicals industry is more complicated, not only will daily chemical products formulation weight match test, sieve
Choosing, by the prevention canker sore of watermelon water extract, anti-dry effect in conjunction with daily chemical products itself effect, by appropriate heavy
Amount proportion will also study the compatibility of the essence and oral cavity ointment raw material of alleviating canker sore simultaneously to obtain more suitable therapeutic efficiency
Confirmed by formula test, to guarantee that composition for oral cavity affects effect in storage process mesometamorphism.
On the basis of ensuring oral cavity ointment prevention canker sore, the functions such as anti-dry, how by the impression gargled, brushed teeth,
Feel to be increased to more excellent level, allow and gargle, brush teeth as a kind of enjoyment, also becomes the working for being not easy to brush teeth in office
Race can use mode snout cavity health care of gargling, and will be the core scientific research side for alleviating the essence and oral cavity dentifrice composition of canker sore
To.
Summary of the invention
An object of the present invention is: provide a kind of fragrance alcohol just, the alleviation canker sore of obvious effect, unique flavor
Essence and composition for oral cavity, natural extract mainly use dry watermelon seeds, dry watermelon peel, dry cucumber, pomelo peel oil.
In order to realize the purpose, the technical scheme adopted by the invention is as follows:
A kind of preparation method of essence that alleviating canker sore, includes the following steps:
1., weigh dry watermelon seeds, dry watermelon peel, dry cucumber, pomelo peel oil, propylene glycol, mentha piperita oil, hyacinth oil and be
Raw material for standby；
2., dry watermelon seeds, dry watermelon peel, dry cucumber mixed with mentha piperita oil, homogeneous in sealed states, ageing；
3., pomelo peel oil, propylene glycol, hyacinth oil be added in step product 2., homogeneous in sealed states；
4., keep sealing state, stand, then squeeze and filter up to alleviate canker sore essence.
Preferably, the step 1. in raw material weight ratio be dry watermelon seeds: dry watermelon peel: dry cucumber: pomelo peel oil:
Propylene glycol: mentha piperita oil: hyacinth oil=1~6:11~16:2~9:1~11:1~9:21~39:0.1~0.6.
Preferably, 2. middle homogenizing temperature is room temperature to the step, and homogenizing time is 1~6h；Aging Temperature is room temperature, ageing
36~72h of time.
Preferably, the step 3. in 55~85 DEG C of temperature condition and 1~6h of homogenizing time.
The second object of the present invention is to: provide a fragrance alcohol just, obvious effect, unique flavor containing alleviate oral cavity burst
The essence composition for oral cavity of ulcer can provide more personnalité selection (from flowable liquid paste to can not to consumer
The paste of flowing is configurable).
In order to realize the purpose, the technical scheme adopted by the invention is as follows:
A kind of composition for oral cavity containing the essence for alleviating canker sore, is prepared according to following weight ratio: alleviating mouth
Essence 3~9%, the oral cavity ointment raw material 91~97% of chamber ulcer, wherein alleviate shared by the essence and oral cavity ointment raw material of canker sore
The sum of percentage be 100%.
Preferably, oral cavity ointment raw material includes the raw material of following weight ratio: silica 1~29%, glycerol 17~70%,
Xanthan gum 0.3~2%, SLS 1~2.5%, sodium phosphate 0.1~0.3%, saccharin sodium 0.1~0.3%, Mint Essence 0.5~
1.5%, pure water 12.7~38.4%.
A kind of preparation method of the composition for oral cavity containing the essence for alleviating canker sore, will alleviate the perfume (or spice) of canker sore
Essence and oral cavity ointment raw material, homogeneous uniform, dechlorination, the filling oral cavity for containing the essence for alleviating canker sore into toothpaste pipe
Use composition.
The beneficial effects of the present invention are:
1, the essence of the alleviations canker sore prepared, miscellaneous fruity gas alcohol just, it is stabilizations, unique flavor, safe and reliable, it is naturally western
Melon water extract is to be extracted by the similar principle that mixes of mentha piperita oil by mixing homogenizing process, and form essence.
2, the composition for oral cavity containing the essence for alleviating canker sore of preparation, unique in taste, obvious effect, emphasis body
Now prevention canker sore, anti-dry, mouthfeel aroma of pure after gargling, brushing teeth and it is dense, other than daily brush teeth, while
It is suitable be inconvenient in the case where brushing teeth carry out oral health be used, provide option for personalized consumption.Because main component is natural
Dry watermelon seeds, dry watermelon peel, dry cucumber have the natural miscellaneous fruit flavor of uniqueness, without side-effects.
3, the manufacture craft of the essence and composition for oral cavity of alleviating canker sore is simple, and lotion dosage form is from flowable liquid
Body can be produced to not flowable lotion, be suitble to industrialized production.
Specific embodiment
The present invention is further illustrated with reference to embodiments, it should be noted that various raw materials are commercially available food
Grade, or obtained according to prior art preparation, dry watermelon seeds, dry watermelon peel, dry cucumber resource are sufficient, reliable.
Embodiment 1
1, alleviate the preparation of the essence of canker sore
1., weigh dry watermelon seeds 1kg, dry watermelon peel 16kg, dry cucumber 2kg, pomelo peel oil 1kg, propylene glycol 1kg,
Mentha piperita oil 39kg, hyacinth oil 0.1kg are raw material for standby；
2., dry watermelon seeds, dry watermelon peel, dry cucumber and mentha piperita oil be mixed in homogenizer, room temperature seals homogeneous
1h, then room temperature sealing ageing 72h；
3., pomelo peel oil, propylene glycol, hyacinth oil be added in step product 2., seal homogeneous at 55 DEG C of temperature
Time 6h；
4., keep sealing state, stand, then carry out squeeze and filter and obtain fresh ginger extract essence.
2, the preparation of the composition for oral cavity containing the essence for alleviating canker sore
1., weigh composition and ratio be (in terms of 100g): alleviate essence 3g, the oral cavity ointment raw material 97g (titanium dioxide of canker sore
Silicon 1g, glycerol 70g, xanthan gum 0.3g, SLS 1g, sodium phosphate 0.1g, saccharin sodium 0.1g, Mint Essence 0.5g, pure water 24g).
2., according to ordinary toothpaste production technology carry out homogeneous, the essence and oral cavity ointment raw material homogeneous of canker sore will be alleviated
(implement to uniform, degassing, then the filling composition for oral cavity into mouthwash bottle to get the essence containing alleviation canker sore
Example 1 is liquor that is flowable, having certain viscosity).
Embodiment 2
1, alleviate the preparation of the essence of canker sore
1., weigh dry watermelon seeds 2kg, dry watermelon peel 15kg, dry cucumber 3kg, pomelo peel oil 2kg, propylene glycol 2kg,
Mentha piperita oil 37kg, hyacinth oil 0.2kg are raw material for standby；
2., dry watermelon seeds, dry watermelon peel, dry cucumber and mentha piperita oil be mixed in homogenizer, room temperature seals homogeneous
2h, then room temperature sealing ageing 70h；
3., pomelo peel oil, propylene glycol, hyacinth oil be added in step product 2., seal homogeneous under temperature 60 C
Time 5h；
4., keep sealing state, stand, then carry out squeeze and filter and obtain fresh ginger extract essence.
2, the preparation of the composition for oral cavity containing the essence for alleviating canker sore
1., weigh composition and ratio be (in terms of 100g): alleviate essence 5g, the oral cavity ointment raw material 95g (titanium dioxide of canker sore
Silicon 5g, glycerol 60g, xanthan gum 0.5g, SLS 1.2g, sodium phosphate 0.11g, saccharin sodium 0.12g, Mint Essence 0.7g, pure water
27.37g)。
2., according to ordinary toothpaste production technology carry out homogeneous, the essence and oral cavity ointment raw material homogeneous of canker sore will be alleviated
(implement to uniform, degassing, then the filling composition for oral cavity into mouthwash bottle to get the essence containing alleviation canker sore
Example 2 is flowable, relatively more viscous liquor).
Embodiment 3
1, alleviate the preparation of the essence of canker sore
1., weigh dry watermelon seeds 3kg, dry watermelon peel 14kg, dry cucumber 5kg, pomelo peel oil 3kg, propylene glycol 3kg,
Mentha piperita oil 35kg, hyacinth oil 0.3kg are raw material for standby；
2., dry watermelon seeds, dry watermelon peel, dry cucumber and mentha piperita oil be mixed in homogenizer, room temperature seals homogeneous
3h, then room temperature sealing ageing 60h；
3., pomelo peel oil, propylene glycol, hyacinth oil be added in step product 2., seal homogeneous at 65 DEG C of temperature
Time 4h；
4., keep sealing state, stand, then carry out squeeze and filter and obtain fresh ginger extract essence.
2, the preparation of the composition for oral cavity containing the essence for alleviating canker sore
1., weigh composition and ratio be (in terms of 100g): alleviate essence 6g, the oral cavity ointment raw material 94g (titanium dioxide of canker sore
Silicon 7g, glycerol 50g, xanthan gum 0.9g, SLS 1.5g, sodium phosphate 0.15g, saccharin sodium 0.15g, Mint Essence 0.9g, pure water
33.4g)。
2., according to ordinary toothpaste production technology carry out homogeneous, the essence and oral cavity ointment raw material homogeneous of canker sore will be alleviated
To uniform, degassing, then the filling composition for oral cavity (embodiment 3 for containing the essence for alleviating canker sore into toothpaste pipe
For half mobility paste).
Embodiment 4
1, alleviate the preparation of the essence of canker sore
1., weigh dry watermelon seeds 4kg, dry watermelon peel 13kg, dry cucumber 6kg, pomelo peel oil 5kg, propylene glycol 5kg,
Mentha piperita oil 33kg, hyacinth oil 0.4kg are raw material for standby；
2., dry watermelon seeds, dry watermelon peel, dry cucumber and mentha piperita oil be mixed in homogenizer, room temperature seals homogeneous
4h, then room temperature sealing ageing 55h；
3., pomelo peel oil, propylene glycol, hyacinth oil be added in step product 2., seal homogeneous under temperature 70 C
Time 3h；
4., keep sealing state, stand, then carry out squeeze and filter and obtain fresh ginger extract essence.
2, the preparation of the composition for oral cavity containing the essence for alleviating canker sore
1., weigh composition and ratio be (in terms of 100g): alleviate essence 7g, the oral cavity ointment raw material 93g (titanium dioxide of canker sore
Silicon 15g, glycerol 55g, xanthan gum 1.2g, SLS 1.9g, sodium phosphate 0.2g, saccharin sodium 0.2g, Mint Essence 1.2g, pure water
18.3g)。
2., according to ordinary toothpaste production technology carry out homogeneous, the essence and oral cavity ointment raw material homogeneous of canker sore will be alleviated
To uniform, degassing, then the filling composition for oral cavity (embodiment 4 for containing the essence for alleviating canker sore into toothpaste pipe
For illiquidity paste).
Embodiment 5
1, alleviate the preparation of the essence of canker sore
1., weigh dry watermelon seeds 5kg, dry watermelon peel 12kg, dry cucumber 7kg, pomelo peel oil 7kg, propylene glycol 7kg,
Mentha piperita oil 27kg, hyacinth oil 0.5kg are raw material for standby；
2., dry watermelon seeds, dry watermelon peel, dry cucumber and mentha piperita oil be mixed in homogenizer, room temperature seals homogeneous
Time 5h, then room temperature sealing ageing 50h；
3., pomelo peel oil, propylene glycol, hyacinth oil be added in step product 2., seal homogeneous at 75 DEG C of temperature
Time 2h；
4., keep sealing state, stand, then carry out squeeze and filter and obtain fresh ginger extract essence.
2, the preparation of the composition for oral cavity containing the essence for alleviating canker sore
1., weigh composition and ratio be (in terms of 100g): alleviate essence 8g, the oral cavity ointment raw material 92g (titanium dioxide of canker sore
Silicon 17g, glycerol 57g, xanthan gum 1.5g, SLS 2g, sodium phosphate 0.25g, saccharin sodium 0.25g, Mint Essence 1.3g, pure water
12.7g)。
2., according to ordinary toothpaste production technology carry out homogeneous, the essence and oral cavity ointment raw material homogeneous of canker sore will be alleviated
To uniform, degassing, then the filling composition for oral cavity (embodiment 5 for containing the essence for alleviating canker sore into toothpaste pipe
For illiquidity paste).
Embodiment 6
1, alleviate the preparation of the essence of canker sore
1., weigh dry watermelon seeds 6kg, dry watermelon peel 11kg, dry cucumber 9kg, pomelo peel oil 11kg, propylene glycol
11kg, mentha piperita oil 21kg, hyacinth oil 0.6kg are raw material for standby；
2., dry watermelon seeds, dry watermelon peel, dry cucumber and mentha piperita oil be mixed in homogenizer, room temperature seals homogeneous
6h, then room temperature sealing ageing 36h；
3., pomelo peel oil, propylene glycol, hyacinth oil be added in step product 2., seal homogeneous at 85 DEG C of temperature
Time 1h；
4., keep sealing state, stand, then carry out squeeze and filter and obtain fresh ginger extract essence.
2, the preparation of the composition for oral cavity containing the essence for alleviating canker sore
1., weigh composition and ratio be (in terms of 100g): alleviate essence 9g, the oral cavity ointment raw material 91g (titanium dioxide of canker sore
Silicon 29g, glycerol 17g, xanthan gum 2g, SLS 2.5g, sodium phosphate 0.3g, saccharin sodium 0.3g, Mint Essence 1.5g, pure water
38.4g)。
2., according to ordinary toothpaste production technology carry out homogeneous, the essence and oral cavity ointment raw material homogeneous of canker sore will be alleviated
To uniform, degassing, then the filling composition for oral cavity (embodiment 6 for containing the essence for alleviating canker sore into toothpaste pipe
For illiquidity paste).
Comparative example 1
Difference with embodiment 1 is only that, does not add the essence for alleviating canker sore when preparing composition for oral cavity, other
Component and content are (being supplied less than 100g with pure water) same as Example 1.
Clinical trial result
Test method: choosing, there is 90 people of canker sore symptom subject to test, each half of men and women, the age from 30~
60 years old, average age general 45 years old.2 groups are randomly divided into, experimental group (is added with using composition for oral cavity prepared by embodiment 1
Alleviate the essence of canker sore, 1 dosage form of embodiment is water aqua type of gargling), control group is used using oral cavity prepared by comparative example 1
The composition essence of canker sore (be not added with alleviate), every morning, noon are brushed teeth with ordinary toothpaste at night and then with survey
Sample gargles 2 minutes, spues, and rinses oral cavity well.
It gargles before test, first unifies the canker sore symptom for examining and recording subject.
After gargling test the 14th day, then the unified canker sore symptom variation examined and record subject.
Criterion: after test of brushing teeth, it is effectively, conversely, nothing that subject oral cavity ulcer symptoms, which are effectively relieved or eliminate,
Variation or canker sore add severe one to be accordingly to be regarded as in vain.
It is examined after subject brushed teeth using 14 days, as a result as follows:
In terms of the inspection result of subject, the composition for oral cavity containing the essence for alleviating canker sore of the invention is right
In alleviate canker sore symptom effective percentage be 95.6%, hence it is evident that better than the statistical data 8.9% of control group.Therefore, of the invention
The composition for oral cavity containing the essence for alleviating canker sore, there is preferable alleviate and treatment is imitated for canker sore symptom
Fruit.
Above content is only to present inventive concept example and explanation, affiliated those skilled in the art couple
Described specific embodiment does various modifications or additions or is substituted in a similar manner, without departing from invention
Conceive or beyond the scope defined by this claim, is within the scope of protection of the invention.
Claims (8)
1. a kind of preparation method for the essence for alleviating canker sore, characterized by the following steps:
1., weigh dry watermelon seeds, dry watermelon peel, dry cucumber, pomelo peel oil, propylene glycol, mentha piperita oil, hyacinth oil be raw material
It is spare；
2., dry watermelon seeds, dry watermelon peel, dry cucumber mixed with mentha piperita oil, homogeneous in sealed states, ageing；
3., pomelo peel oil, propylene glycol, hyacinth oil be added in step product 2., homogeneous in sealed states；
4., keep sealing state, stand, then squeeze and filter up to alleviate canker sore essence.
2. a kind of preparation method of essence for alleviating canker sore according to claim 1, it is characterised in that: the step
1. the weight ratio of middle raw material is dry watermelon seeds: dry watermelon peel: dry cucumber: pomelo peel oil: propylene glycol: mentha piperita oil: wind
Seed oil=1~6:11~16:2~9:1~11:1~9:21~39:0.1~0.6.
3. a kind of preparation method of essence for alleviating canker sore according to claim 1, it is characterised in that: the step
2. middle homogenizing temperature is room temperature, homogenizing time is 1~6h；Aging Temperature is room temperature, 36~72h of digestion time.
4. a kind of preparation method of essence for alleviating canker sore according to claim 1, it is characterised in that: the step
3. the condition of middle homogeneous are as follows: homogenizing temperature is 55~85 DEG C, and homogenizing time is 1~6h.
5. a kind of essence of the alleviation canker sore of the preparation of the preparation method as described in any one of Claims 1 to 4.
6. a kind of composition for oral cavity containing the essence for alleviating canker sore, it is characterised in that: match according to following weight ratio
System: alleviate essence 3~9%, the oral cavity ointment raw material 91~97% of canker sore, wherein alleviate essence and the oral cavity of canker sore
The sum of percentage shared by cream is 100%.
7. a kind of composition for oral cavity containing the essence for alleviating canker sore according to claim 6, it is characterised in that:
Oral cavity ointment raw material includes the raw material of following weight ratio: silica 1~29%, glycerol 17~70%, xanthan gum 0.3~2%,
SLS 1~2.5%, sodium phosphate 0.1~0.3%, saccharin sodium 0.1~0.3%, Mint Essence 0.5~1.5%, pure water 12.7
~38.4%, the sum of raw material of toothpaste percentage is 100%.
8. a kind of preparation method of the composition for oral cavity containing the essence for alleviating canker sore, it is characterised in that: mouth will be alleviated
The essence and oral cavity ointment raw material of chamber ulcer, homogeneous uniform, degassing, it is filling into toothpaste pipe to get containing alleviating canker sore
The composition for oral cavity of essence.
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Application publication date: 20190426 |
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| RJ01 | Rejection of invention patent application after publication |