CN109966214A - A kind of preparation method of rose water extract essence and oral cavity composite cream containing the essence - Google Patents

A kind of preparation method of rose water extract essence and oral cavity composite cream containing the essence Download PDF

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CN109966214A
CN109966214A CN201910389782.5A CN201910389782A CN109966214A CN 109966214 A CN109966214 A CN 109966214A CN 201910389782 A CN201910389782 A CN 201910389782A CN 109966214 A CN109966214 A CN 109966214A
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rose
water extract
essence
oral cavity
oil
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不公告发明人
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DELBO (GUANGZHOU) Ltd
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DELBO (GUANGZHOU) Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P1/00Drugs for disorders of the alimentary tract or the digestive system
    • A61P1/02Stomatological preparations, e.g. drugs for caries, aphtae, periodontitis
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q11/00Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oral & Maxillofacial Surgery (AREA)
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  • Mycology (AREA)
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Abstract

The present invention relates to daily chemicals field, a kind of preparation method of rose water extract essence and the oral cavity composite cream containing the essence are concretely related to.The preparation method of rose water extract essence is to weigh dried rose, rose root, water, dipropylene glycol, and stirring homogeneous distills up to rose water extract, then plus rose perfume base to get rose water extract essence;Oral cavity composite cream will be obtained after rose water extract essence, oral cavity ointment raw material homogeneous.Oral cavity composite cream of the present invention, rose fragrance alcohol just, good in taste, and preventable disease, have promoting blood circulation, Thyme Extract, especially have preferable remission effect to canker sore.The essence oral cavity ointment of water extract containing rose being fabricated to, the rose fragrance strong, alcohol is positive can provide the mouthfeel of unique flavor for consumer, meet consumer personalization's demand.

Description

A kind of preparation method of rose water extract essence and oral cavity ointment group containing the essence Close object
Technical field
The present invention relates to daily chemicals field, the preparation method of specifically a kind of rose water extract essence and the mouth containing the essence Chamber composite cream.
Background technique
As the improvement of people's living standards, oral problem is increasingly valued by people, if there is oral problem, It sees a doctor to hospital, it is more late, miss best Waiting time.Therefore, how to pass through these simple sides of brushing teeth, gargle Formula prevents oral problem, it should be that cost is minimum, the highest solution of efficiency, allow gargle, the process of brushing teeth becomes kind Enjoy then be attract gargle, more efficient way of brushing teeth, it is great to oral cavity health effect.
Rose is bright-coloured, beautiful, this is also the reason of rose is always subjected to praise in history, ancient times doctor's rose water Neurasthenia is treated, treats tuberculosis with rose stacte, treats heart disease and nephrosis with rose-juice.Rose extract has anti- Bacterium anti-spasm, is sterilized, promotes the sexual maturity, purifying, is calm, mending body and other effects, and there are also strong and shrink the effect of capilary, counterparts for rose Transmucosal has splendid rejuvenation.Daily use chemicals industry, can with emphasis using rose extract anti-inflammation and sterilization, can anti-communicable disease, anti- Inflammation, anti-spasm promote cell metabolism and cytothesis function, such as can solve oral problem includes promoting blood circulation, convergence (spy It is not canker sore) etc..Rose water extract essence applied by daily use chemicals industry is more complicated, not only will be in daily chemical products formula Test, the screening of weight proportion, by prevention canker sore effect of rose water extract essence and daily chemical products itself effect knot It closes, more suitable therapeutic efficiency is obtained by weight proportion appropriate, also to study rose water extract essence and oral cavity ointment The compatibility of raw material is simultaneously confirmed by formula test, to guarantee that oral cavity composite cream is affected in storage process mesometamorphism Effect.
On the basis of ensuring the functions such as oral cavity ointment prevention canker sore, the impression gargled, brushed teeth how is improved, allows and gargles Mouth is brushed teeth as a kind of enjoyment, is allowed the office worker for being not easy to brush teeth in office that can use mode snout cavity health care of gargling, will is rose The core direction of scientific rersearch of rare water extract essence and oral cavity dentifrice composition.
Summary of the invention
An object of the present invention is: provide a kind of fragrance alcohol just, the rose water extract of obvious effect, unique flavor it is fragrant Essence, natural extract mainly use dried rose, rose root.The second object of the present invention is to: provide a fragrance alcohol just, effect Significantly, the oral cavity composite cream of the essence of water extract containing rose of unique flavor.
In order to realize the purpose, the technical scheme adopted by the invention is as follows:
A kind of preparation method of rose water extract essence, includes the following steps:
1., weigh dried rose, rose root, water, dipropylene glycol be raw material for standby, dried rose, rose root are ground into Rose powder A;
2., rose powder A, water, dipropylene glycol be mixed in homogenizer, homogeneous under room temperature, normal pressure, ageing is at ageing liquid B;
3., by above-mentioned ageing liquid B move into distiller in, distill to obtain rose water extract C;
4., rose water extract C is uniformly mixed with rose perfume base D according to weight ratio 1:1 to get rose water extract Essence E.
Preferably, step 1. in dried rose: rose root: water: the weight ratio of dipropylene glycol be 1~6:21~26:31 ~39:11~16, and rose, rose root will be crushed before extraction, and benefit is that effect of extracting can be improved after crushing.
Preferably, step 2. in homogenizing time 1~6h, 36~72h of digestion time, using the side of homogeneous motor spindle homogeneous Mixture elder generation bottom homogeneous after the completion of homogeneous, is pumped into the middle part of homogenizer, fill-before-fire is returned by formula by homogenizer exterior line In homogenizer, a circulation is completed, the benefit of outer loop is that homogenisation cycle effect is more preferable, homogeneous is more thorough, improves extraction effect Fruit.
Preferably, 3. middle vapo(u)rizing temperature is 90~95 DEG C to step.
Preferably, 4. middle rose perfume base D includes menthol, spearmint oil, fennel oil, borneol, lemon oil, ginger to step Oil, mentha piperita oil, and the weight ratio of menthol, spearmint oil, fennel oil, borneol, lemon oil, oil of ginger, mentha piperita oil Example is 3~9:31~36:31~36:1~6:1~3:1~6:1~3:1~6.
A kind of oral cavity composite cream of the essence of water extract containing rose is prepared according to following weight ratio: rose water extracts Object essence 3~9%, oral cavity ointment raw material 91~97%, wherein the sum of percentage shared by rose water extract essence and oral cavity ointment It is 100%.
Preferably, oral cavity ointment raw material includes the raw material of following weight ratio: silica 1~29%, glycerol 17~70%, Xanthan gum 0.3~2%, SLS 1~2.5%, sodium phosphate 0.1~0.3%, saccharin sodium 0.1~0.3%, Mint Essence 0.5~ 1.5%, pure water 6.5~68.6%, the sum of oral cavity ointment raw material percentage are 100%.
A kind of preparation method of the oral cavity composite cream of the essence of water extract containing rose, by rose water extract essence and mouth Chamber cream raw material, it is homogeneous uniform, degassing, filling into toothpaste pipe or bottle, seal the oral cavity to get the essence of water extract containing rose Composite cream.
The beneficial effects of the present invention are:
1, prepare rose water extract essence, fragrance alcohol just, stabilizations, unique flavor, securely and reliably, rose water extract It is to be extracted by the similar principle that mixes of dipropylene glycol by mixing homogenizing process, bottom confrontation effect of extracting influences higher It imitates, more completely, and forms essence.
2, the oral cavity composite cream of the essence of water extract containing rose prepared, unique in taste, obvious effect, emphasis is embodied in Prevent canker sore, mouthfeel aroma of pure after gargling, brushing teeth and it is dense, other than daily brush teeth, at the same also be suitble to inconvenience Oral health is carried out in the case where brushing teeth to be used, and provides option for personalized consumption.Because main component is dried rose, rose Root has natural unique rose local flavor, without side-effects.
3, the manufacture craft of rose water extract essence and oral cavity composite cream is simple, and lotion dosage form is from flowable liquid It to not flowable lotion, can produce, be suitble to industrialized production.
4, oral cavity composite cream of the invention can be applied to half flow model liquid tooth paste, also there is the common tooth of not flow-type ones Cream, also between the oral cavity ointment between both for configuration.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of homogenizer in the present invention.
Specific embodiment
The present invention is further illustrated with reference to embodiments, it should be noted that various raw materials are commercially available food Grade, or obtained according to prior art preparation, rose, rose Root Resource are sufficient, reliable.
Embodiment 1
1, a kind of preparation method of rose water extract essence, includes the following steps:
1., weigh dried rose 1kg, rose root 26kg, water 31kg, dipropylene glycol 16kg be raw material for standby, by dry rose Flower, rose root are ground into rose powder A;
2., rose powder A, water, dipropylene glycol be mixed in homogenizer, homogeneous 1h under room temperature, normal pressure, be aged after 72h at It is aged liquid B;Wherein homogeneous head 2 is mounted on 1 bottom of homogenizer, and the outlet of homogeneous head 2 returns to 1 middle part of homogenizer by extension tube attached, mixes The flow direction for closing object is: being pumped in the middle part of homogenizer from bottom by extension tube attached 3 by homogeneous head 2, fill-before-fire returns homogenizer 1 It is interior, complete a circulation, it is ensured that mixture 100% passes through the shearing homogeneous of homogeneous head, and homogeneous head has the function of homogeneous and pumping Energy;Outer loop working principle is as shown in Figure 1.
3., by above-mentioned ageing liquid B move into distiller in, at 95 DEG C distill 1h obtain rose water extract C;
4., rose water extract C is uniformly mixed with rose perfume base D according to weight ratio 1:1 to get rose water extract Essence E.
Step 4. in, rose perfume base D includes the raw material of following weight: menthol 36kg, spearmint oil 36kg, fennel oil 1kg, borneol 1kg, lemon oil 6kg, oil of ginger 3kg, mentha piperita oil 6kg.
2, a kind of preparation method of the oral cavity composite cream of the essence of water extract containing rose
1., composition and ratio (in terms of 100g) weigh following raw material: rose water extract essence 3g, oral cavity ointment raw material 97g, Middle oral cavity ointment raw material composition and ratio are as follows: silica 1 g, glycerol 70g, xanthan gum 0.3g, SLS 1g, sodium phosphate 0.1g, saccharin sodium 0.1g, Mint Essence 0.5g, pure water 24g.
2., according to ordinary toothpaste production technology rose water extract essence and oral cavity ointment raw material are subjected to homogeneous, homogeneous is extremely Uniformly, it deaerates, then filling into mouthwash bottle, seals the oral cavity composite cream to get the essence of water extract containing rose.
The oral cavity ointment of the present embodiment is liquor that is flowable, having certain viscosity.
Embodiment 2
1, a kind of preparation method of rose water extract essence, includes the following steps:
1., weigh dried rose 2kg, rose root 25kg, water 32kg, dipropylene glycol 15kg be raw material for standby, by dry rose Flower, rose root are ground into rose powder A;
2., rose powder A, water, dipropylene glycol be mixed in homogenizer, homogeneous 2h under room temperature, normal pressure, be aged after 60h at It is aged liquid B;Wherein homogeneous head 2 is mounted on 1 bottom of homogenizer, and the outlet of homogeneous head 2 returns to 1 middle part of homogenizer by extension tube attached, mixes The flow direction for closing object is: being pumped in the middle part of homogenizer from bottom by extension tube attached 3 by homogeneous head 2, fill-before-fire returns homogenizer 1 It is interior, complete a circulation, it is ensured that mixture 100% passes through the shearing homogeneous of homogeneous head, and homogeneous head has the function of homogeneous and pumping Energy;Outer loop working principle is as shown in Figure 1.
3., by above-mentioned ageing liquid B move into distiller in, at 94 DEG C distill 2h obtain rose water extract C;
4., rose water extract C is uniformly mixed with rose perfume base D according to weight ratio 1:1 to get rose water extract Essence E.
Step 4. in, rose perfume base D includes the raw material of following weight: menthol 35kg, spearmint oil 35kg, fennel oil 2kg, borneol 2kg, lemon oil 5kg, oil of ginger 2kg, mentha piperita oil 5kg.
2, the preparation of the oral cavity composite cream of the essence of water extract containing rose
1., following raw material: rose water extract essence 5g, oral cavity ointment raw material 95g is weighed by composition and ratio (in terms of 100g), Wherein oral cavity ointment raw material composition and ratio are as follows: silica 5g, glycerol 17g, xanthan gum 2g, SLS 1.5g, sodium phosphate 0.15g, sugar Smart sodium 0.15g, Mint Essence 0.6g, pure water 68.6g.
2., according to ordinary toothpaste production technology carry out homogeneous, extremely by rose water extract essence and oral cavity ointment raw material homogeneous Uniformly, it deaerates, then filling into mouthwash bottle, seals the oral cavity composite cream to get the essence of water extract containing rose.
The oral cavity ointment of the present embodiment is flowable, relatively more viscous liquor.
Embodiment 3
1, a kind of preparation preparation method of rose water extract essence, includes the following steps:
1., weigh dried rose 3kg, rose root 24kg, water 33kg, dipropylene glycol 14kg be raw material for standby, by dry rose Flower, rose root are ground into rose powder A;
2., rose powder A, water, dipropylene glycol be mixed in homogenizer, homogeneous 3h under room temperature, normal pressure, be aged after 55h at It is aged liquid B;Wherein homogeneous head 2 is mounted on 1 bottom of homogenizer, and the outlet of homogeneous head 2 returns to 1 middle part of homogenizer by extension tube attached, mixes The flow direction for closing object is: being pumped in the middle part of homogenizer from bottom by extension tube attached 3 by homogeneous head 2, fill-before-fire returns homogenizer 1 It is interior, complete a circulation, it is ensured that mixture 100% passes through the shearing homogeneous of homogeneous head, and homogeneous head has the function of homogeneous and pumping Energy;Outer loop working principle is as shown in Figure 1.
3., by above-mentioned ageing liquid B move into distiller in, at 93 DEG C distill 3h obtain rose water extract C;
4., rose water extract C is uniformly mixed with rose perfume base D according to weight ratio 1:1 to get rose water extract Essence E.
Step 4. in, rose perfume base D includes the raw material of following weight: menthol 34kg, spearmint oil 34kg, fennel oil 3kg, borneol 3kg, lemon oil 4kg, oil of ginger 3kg, mentha piperita oil 4kg.
2, a kind of preparation method of the oral cavity composite cream of the essence of water extract containing rose, includes the following steps:
1., by composition and ratio (in terms of 100g) weigh the following raw material: rose water extract essence 6g, oral cavity ointment raw material 94g, Wherein oral cavity ointment raw material composition and ratio are as follows: silica 9g, glycerol 40g, xanthan gum 1.5g, SLS 1.6g, sodium phosphate 0.2g, sugar Smart sodium 0.2g, Mint Essence 0.7g, pure water 40.8g.
2., according to ordinary toothpaste production technology carry out homogeneous, extremely by rose water extract essence and oral cavity ointment raw material homogeneous Uniformly, it deaerates, then filling into mouthwash bottle, seals the oral cavity composite cream to get the essence of water extract containing rose.
The oral cavity ointment of the present embodiment is half mobility paste.
Embodiment 4
1, a kind of preparation method of rose water extract essence, includes the following steps:
1., weigh dried rose 4kg, rose root 23kg, water 35kg, dipropylene glycol 13kg be raw material for standby, by dry rose Flower, rose root are ground into rose powder A;
2., rose powder A, water, dipropylene glycol be mixed in homogenizer, homogeneous 4h under room temperature, normal pressure, be aged after 50h at It is aged liquid B;Wherein homogeneous head 2 is mounted on 1 bottom of homogenizer, and the outlet of homogeneous head 2 returns to 1 middle part of homogenizer by extension tube attached, mixes The flow direction for closing object is: being pumped in the middle part of homogenizer from bottom by extension tube attached 3 by homogeneous head 2, fill-before-fire returns homogenizer 1 It is interior, complete a circulation, it is ensured that mixture 100% passes through the shearing homogeneous of homogeneous head, and homogeneous head has the function of homogeneous and pumping Energy;Outer loop working principle is as shown in Figure 1.
3., by above-mentioned ageing liquid B move into distiller in, at 92 DEG C distill 4h obtain rose water extract C;
4., rose water extract C is uniformly mixed with rose perfume base D according to weight ratio 1:1 to get rose water extract Essence E.
Step 4. in, rose perfume base D includes the raw material of following weight: menthol 33kg, spearmint oil 33kg, fennel oil 4kg, borneol 1kg, lemon oil 3kg, oil of ginger 1kg, mentha piperita oil 3kg.
2, a kind of preparation method of the oral cavity composite cream of the essence of water extract containing rose, includes the following steps:
1., by composition and ratio (in terms of 100g) weigh the following raw material: rose water extract essence 7g, oral cavity ointment raw material 93g, Wherein oral cavity ointment raw material composition and ratio are as follows: silica 1 2g, glycerol 55g, xanthan gum 1.4g, SLS 2g, sodium phosphate 0.25g, sugar Smart sodium 0.25g, Mint Essence 0.9g, pure water 21.2g.
2., according to ordinary toothpaste production technology carry out homogeneous, extremely by rose water extract essence and oral cavity ointment raw material homogeneous Uniformly, it deaerates, then filling into toothpaste pipe, seals the oral cavity composite cream to get the essence of water extract containing rose.
The oral cavity ointment of the present embodiment is illiquidity paste.
Embodiment 5
1, a kind of preparation method of rose water extract essence, includes the following steps:
1., weigh dried rose 5kg, rose root 22kg, water 37kg, dipropylene glycol 12kg be raw material for standby, by dry rose Flower, rose root are ground into rose powder A;
2., rose powder A, water, dipropylene glycol be mixed in homogenizer, homogeneous 5h under room temperature, normal pressure, be aged after 40h at It is aged liquid B;Wherein homogeneous head 2 is mounted on 1 bottom of homogenizer, and the outlet of homogeneous head 2 returns to 1 middle part of homogenizer by extension tube attached, mixes The flow direction for closing object is: being pumped in the middle part of homogenizer from bottom by extension tube attached 3 by homogeneous head 2, fill-before-fire returns homogenizer 1 It is interior, complete a circulation, it is ensured that mixture 100% passes through the shearing homogeneous of homogeneous head, and homogeneous head has the function of homogeneous and pumping Energy;Outer loop working principle is as shown in Figure 1.
3., by above-mentioned ageing liquid B move into distiller in, at 91 DEG C distill 5h obtain rose water extract C;
4., rose water extract C is uniformly mixed with rose perfume base D according to weight ratio 1:1 to get rose water extract Essence E.
Step 4. in, rose perfume base D includes the raw material of following weight: menthol 32kg, spearmint oil 32kg, fennel oil 5kg, borneol 2kg, lemon oil 2kg, oil of ginger 2kg, mentha piperita oil 2kg.
2, a kind of preparation method of the oral cavity composite cream of the essence of water extract containing rose, includes the following steps:
1., by composition and ratio (in terms of 100g) weigh the following raw material: rose water extract essence 8g, oral cavity ointment raw material 92g, Wherein oral cavity ointment raw material composition and ratio are as follows: silica 1 5g, glycerol 60g, xanthan gum 1.2g, SLS 2.2g, sodium phosphate 0.3g, Saccharin sodium 0.3g, Mint Essence 1g, pure water 12g.
2., according to ordinary toothpaste production technology carry out homogeneous, extremely by rose water extract essence and oral cavity ointment raw material homogeneous Uniformly, it deaerates, then filling into toothpaste pipe, seals the oral cavity composite cream to get the essence of water extract containing rose.
The oral cavity ointment of embodiment 5 is illiquidity paste.
Embodiment 6
1, a kind of preparation method of rose water extract essence, includes the following steps:
1., weigh dried rose 6kg, rose root 21kg, water 39kg, dipropylene glycol 11kg be raw material for standby, by dry rose Flower, rose root are ground into rose powder A;
2., rose powder A, water, dipropylene glycol be mixed in homogenizer, homogeneous 6h under room temperature, normal pressure, be aged after 36h at It is aged liquid B;Wherein homogeneous head 2 is mounted on 1 bottom of homogenizer, and the outlet of homogeneous head 2 returns to 1 middle part of homogenizer by extension tube attached, mixes The flow direction for closing object is: being pumped in the middle part of homogenizer from bottom by extension tube attached 3 by homogeneous head 2, fill-before-fire returns homogenizer 1 It is interior, complete a circulation, it is ensured that mixture 100% passes through the shearing homogeneous of homogeneous head, and homogeneous head has the function of homogeneous and pumping Energy;Outer loop working principle is as shown in Figure 1.
3., by above-mentioned ageing liquid B move into distiller in, at 90 DEG C distill 6h obtain rose water extract C;
4., rose water extract C is uniformly mixed with rose perfume base D according to weight ratio 1:1 to get rose water extract Essence E.
Step 4. in, rose perfume base D includes the raw material of following weight: menthol 31kg, spearmint oil 31kg, fennel oil 6kg, borneol 3kg, lemon oil 1kg, oil of ginger 3kg, mentha piperita oil 1kg
2, a kind of preparation method of the oral cavity composite cream of the essence of water extract containing rose, includes the following steps:
1., by composition and ratio (in terms of 100g) weigh the following raw material: rose water extract essence 9g, oral cavity ointment raw material 91g, Wherein oral cavity ointment raw material composition and ratio are as follows: silica 29g, glycerol 50g, xanthan gum 1g, SLS 2.5g, sodium phosphate 0.25g, sugar Smart sodium 0.25g, Mint Essence 1.5g, pure water 6.5g.
2., according to ordinary toothpaste production technology carry out homogeneous, extremely by rose water extract essence and oral cavity ointment raw material homogeneous Uniformly, it deaerates, then filling into toothpaste pipe, seals the oral cavity composite cream to get the essence of water extract containing rose.
The oral cavity ointment of embodiment 6 is illiquidity paste.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims Variation is included within the present invention.Any reference signs in the claims should not be construed as limiting the involved claims.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art The other embodiments being understood that.

Claims (7)

1. a kind of preparation method of rose water extract essence, which comprises the steps of:
1., weigh dried rose, rose root, water, dipropylene glycol be raw material for standby, dried rose, rose root are ground into rose Powder A;
2., rose powder A, water, dipropylene glycol be mixed in homogenizer, homogeneous under room temperature, normal pressure, ageing is at ageing liquid B;
3., by above-mentioned ageing liquid B move into distiller in, distill to obtain rose water extract C;
4., rose water extract C is uniformly mixed with rose perfume base D according to weight ratio 1:1 to get rose water extract essence E。
2. the preparation method of rose water extract essence according to claim 1, which is characterized in that step 1. in dry rose Flower: rose root: water: the weight ratio of dipropylene glycol is 1~6:21~26:31~39:11~16, and rose, rose root It to be crushed before extraction, benefit is that effect of extracting can be improved after crushing.
3. the preparation method of rose water extract essence according to claim 1, which is characterized in that step 2. in homogeneous when Between 1~6h, 36~72h of digestion time, by the way of homogeneous motor spindle homogeneous, by mixture elder generation bottom homogeneous, homogeneous is completed Afterwards, it is pumped into the middle part of homogenizer by homogenizer exterior line, fill-before-fire is returned in homogenizer, and a circulation is completed.
4. the preparation method of rose water extract essence according to claim 1, which is characterized in that 3. middle distillation is warm for step Degree is 90~95 DEG C.
5. the preparation method of rose water extract essence according to claim 1, which is characterized in that step 4. in rose fragrant Base D includes menthol, spearmint oil, fennel oil, borneol, lemon oil, oil of ginger, mentha piperita oil, and menthol, spearmint Oil, fennel oil, borneol, lemon oil, oil of ginger, mentha piperita oil weight ratio be menthol: spearmint oil: fennel oil: ice Piece: lemon oil: oil of ginger: mentha piperita oil=3~9:31~36:31~36:1~6:1~3:1~6:1~3:1~6.
6. a kind of oral cavity composite cream of the essence of water extract containing rose, which is characterized in that prepared according to following weight ratio: rose Rare water extract essence 3~9%, oral cavity ointment raw material 91~97%, wherein hundred shared by rose water extract essence and oral cavity ointment The sum of score is 100%.
7. the oral cavity composite cream of the essence of water extract containing rose according to claim 6, which is characterized in that oral cavity ointment is former Material includes the raw material of following weight ratio: silica 1~29%, glycerol 17~70%, xanthan gum 0.3~2%, SLS1~ 2.5%, sodium phosphate 0.1~0.3%, saccharin sodium 0.1~0.3%, Mint Essence 0.5~1.5%, pure water 6.5~68.6%, The sum of oral cavity ointment raw material percentage is 100%.
CN201910389782.5A 2019-05-10 2019-05-10 A kind of preparation method of rose water extract essence and oral cavity composite cream containing the essence Pending CN109966214A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110755337A (en) * 2019-12-11 2020-02-07 苏州清馨健康科技有限公司 Anti-allergy repairing toothpaste
CN111557889A (en) * 2020-05-26 2020-08-21 济南玖玫玫瑰制品有限公司 Rose anthocyanin mouthwash and preparation method thereof
CN114983885A (en) * 2022-05-17 2022-09-02 广州医家仁生物科技有限责任公司 Rose toothpaste and preparation method thereof

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CN101831354A (en) * 2010-04-22 2010-09-15 云南玫瑰庄园酒业有限责任公司 Method for extracting fresh rose extract
CN105542964A (en) * 2016-01-22 2016-05-04 两面针(江苏)实业有限公司 Rose compounded jasmine extract essence and preparation method thereof and toothpaste containing essence
CN109576054A (en) * 2017-09-28 2019-04-05 王少平 A kind of extracting method of Rosa Damascana
CN109833247A (en) * 2017-11-28 2019-06-04 沈阳华企力拓企业服务有限公司 A kind of preparation method of mothproof toothpaste

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CN101760303A (en) * 2008-11-24 2010-06-30 王晓明 Rose essence used for shampoo
CN101831354A (en) * 2010-04-22 2010-09-15 云南玫瑰庄园酒业有限责任公司 Method for extracting fresh rose extract
CN105542964A (en) * 2016-01-22 2016-05-04 两面针(江苏)实业有限公司 Rose compounded jasmine extract essence and preparation method thereof and toothpaste containing essence
CN109576054A (en) * 2017-09-28 2019-04-05 王少平 A kind of extracting method of Rosa Damascana
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Publication number Priority date Publication date Assignee Title
CN110755337A (en) * 2019-12-11 2020-02-07 苏州清馨健康科技有限公司 Anti-allergy repairing toothpaste
CN111557889A (en) * 2020-05-26 2020-08-21 济南玖玫玫瑰制品有限公司 Rose anthocyanin mouthwash and preparation method thereof
CN114983885A (en) * 2022-05-17 2022-09-02 广州医家仁生物科技有限责任公司 Rose toothpaste and preparation method thereof

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Application publication date: 20190705