CN1411739A - Konjak glucomannan degradation product and ginkgo leaf extract health-care food and its preparation method - Google Patents
Konjak glucomannan degradation product and ginkgo leaf extract health-care food and its preparation method Download PDFInfo
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- CN1411739A CN1411739A CN01134074A CN01134074A CN1411739A CN 1411739 A CN1411739 A CN 1411739A CN 01134074 A CN01134074 A CN 01134074A CN 01134074 A CN01134074 A CN 01134074A CN 1411739 A CN1411739 A CN 1411739A
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Abstract
The production method of health-care food combined by using konjak glucomannan catabolite and ginkgo leaf extract mainly includes the steps of 1. preparing konjak glucomannan catabolite; and 2. preparing ginkgo leaf extract. Said health-care food has the functions of controlling blood sugar, preventing obesity, reducing angiocardiopathy incidence, improving digestive and excretory function and raising health level, etc.
Description
The present invention relates to a kind of food.Exactly be a kind of food that utilizes konjaku for raw material.
Contain Glucomannan in the konjak corm, do not have suitable digestive ferment it can be degraded in the gastric juice because of the people, after eating, do not digested and assimilated, but discharge by enteron aisle.Based on this, konjaku glucomannan is considered to a kind of dietary fiber of function admirable.It prevents constipation to improving function of intestinal canal, and effect is very remarkable
Oneself more and more causes people's attention to konjaku because of its unique health care, existing relevant patented technology relates to the application of konjaku as functional food, relevant technology is disclosed respectively as Chinese patent 97105090,98121819,98330956,98125046,99117437, konjaku mainly is to utilize Glucomannan as functional food, and the problem of its existence is to lack the Glucomannan in the konjaku is carried out deep processing.The sweet oligosaccharides in the edible poly-Portugal of existing document proof can improve profitable strain activity such as Bifidobacterium in the human body intestinal canal, Lactobacillus casei, lactobacillus acidophilus, suppresses the activity of pernicious bacterias such as clostridium botulinum, living rotten clostridium, salmonella.Early stage oligosaccharides multi-source is in the cell membrane or the microbial fermentation of yeast, its source is restricted, use also limited, have mannosan and Glucomannan in finding numerous plant carbohydrates since, people attempt to utilize poly-manna oligosacchride of natural plant gum production and the sweet oligosaccharides in poly-Portugal such as konjac glucomannan and guar gum, fenugreek gum, field Pu's glue.The method of the sweet oligosaccharides in the poly-Portugal of konjaku production has two classes: a class is with the chemical degradation Glucomannan, and its advantage is that technology is simple, and efficient is higher, and its shortcoming is that product quality control is difficult, is difficult to obtain stay-in-grade Glucomannan.Another kind of method is with the bio-enzyme degradation Glucomannan, and its advantage is that product quality control is convenient, and end product quality is good, but its production efficiency is low, and the industrial production cost is too high.
At the health food function is more single in the market, still rare complex function health food, the health food and the preparation method of compound ginkgo leaf extract in kanjak mannan oligosaccharides food who the invention provides that a kind of product quality control is convenient, production efficiency is high.
Concrete food formula and manufacture method are as follows:
Konjak glucomannan degradation product and ginkgo leaf extract health-care food is characterized in that: be made up of following substances
Konjak glucomannan degradation product 10～95%,
Ginkgo biloba p.e 0.5～50%,
Mannose 0～15%,
Edible refinement konjaku powder 0～15%,
Vitamin C 0.05～5%.
The preparation method of a kind of konjak glucomannan degradation product and ginkgo leaf extract health-care food is characterized in that:
The preparation of A, konjak glucomannan degradation product
(1), get konjaku powder 20～100 gram and place 80～1000 milliliters of aqueous solution that contain 5～85% organic solvents, with salt acid for adjusting pH value to 0～6.0, stirred 5～500 minutes intensification degree to 35～125 ℃;
(2), regulate pH value to 6.5～8.9 with phosphate, filter, add 200～800 ml distilled waters in the filter residue, adjust the temperature to 25～65 ℃, add 0.1～1.0 milliliter of Glucomannan restriction endonuclease, 20～2800 minutes reaction time to viscosity is reduced to 1000～8000 centipoises, is heated to 75～95 ℃, remove by filter insoluble matter with 100～300 mesh filter screens, spray-drying gets the pressed powder that main component is the grape manna oligosacchride;
The preparation of B, ginkgo biloba p.e
(1), gets dry ginkgo leaf 1000 grams, pulverize, 15～95 ℃ of temperature, in extractor, with 400～1000 milliliters of organic solvent extractings 15～600 minutes, 300～900 milliliters of solvents were removed in the extract decompression distillation, added 50～300 ml distilled waters, continue decompression distillation organic solvent content to the extract and remove by filter insoluble matter to less than 5%;
(2), with macropore phenolic resins as adsorbent, filtrate by 50～1000 gram adsorbents, is carried out desorption with 50～1000 milliliters of organic solvents to adsorbent.Obtain a kind of mixing material of lark;
(3), decompression distillation removes 20～800 milliliters of solvents, spray-drying gets the extract that main component is GINKGO BILOBA EXTRACT and ginkgolides mixture.
Organic solvent in the preparation of described konjak glucomannan degradation product or be methyl alcohol or for ethanol or be isopropyl alcohol.
Phosphate in the preparation of described konjak glucomannan degradation product or be sodium phosphate or for potassium phosphate or for sodium dihydrogen phosphate or for potassium dihydrogen or for sodium hydrogen phosphate or be dipotassium hydrogen phosphate.
Organic solvent in the preparation of described ginkgo biloba extract or be methyl alcohol or for ethanol or be acetone.
Glucomannan content height is big in the cultivated area of China in the stem tuber of konjaku, wide material sources; Contain GINKGO BILOBA EXTRACT and ginkgolides in the ginkgo leaf, it has the hemangiectasis effect modern medicine proof, therefore has the effect of protection cardiovascular and cerebrovascular; By compound ginkgo extract in the konjak portuguese gansu polyose confectionery, bring into play the health-care effect of konjaku glucomannan and GINKGO BILOBA EXTRACT, ginkgolides jointly.Developing this functional food can be that extremely long-pending effect is arranged to preventing hyperglycaemia, keeping healthy cardiovascular with functions of intestines and stomach.
The method that the present invention adopts chemistry to combine with bio-enzyme degradation with lower production cost, obtains konjaku glucomannan best in quality.According to this Ricipe for health care food characteristics, long-term edible, blood sugar rising, prevention of obesity, the generation of minimizing angiocardiopathy be can control, digestion and excretory function improved, improve body health level.
Below by embodiment the present invention is done to describe further.
Embodiment 1
Get 75 parts of konjak glucomannan degradation products, get 20 parts of ginkgo biloba p.es, 3 parts of mannoses, Catergen part.Through ground and mixed, form the homogeneous solid mixture.Solid mixture 0.5 gram packed into get final product in the edible capsule.
Embodiment 2
Get 82.45 parts of konjak glucomannan degradation products, 0.85 part of ginkgo biloba p.e, 6 parts of mannoses, 1.5 parts of citric acids, 9 parts of edible refinement konjaku powders, 0.2 part of vitamin C.Through ground and mixed, form the homogeneous solid mixture.Solid mixture 12 gram packed into get final product in the vacuum edible plastic bag.
Embodiment 3
One, gets 100 gram konjaku powders, place 650 milliliters of aqueous solution that contain ethanol 15%, regulate pH to 1.0 with hydrochloric acid, 120 ℃ of temperature, stirring reaction 60 minutes is to room temperature, remove by filter organic solvent, add water to solid content 10%, obtain the solution of viscosity at 20000 centipoises.
Get above-mentioned solution 100 grams, regulate pH to 6.8 with potassium phosphate, add 0.5 gram vigor and be 450 'beta '-mannase,, slowly stirred 350 minutes 48 ℃ of temperature, reduce to about 5000 centipoises to viscosity, be heated to 85 ℃, utilize aperture 120 mesh filter screens to filter, remove the sediment reserved filtrate, spray-drying obtains powdery white solid 7.8 grams.
Two, get dry ginkgo leaf 500 grams, pulverize, 80 ℃ of temperature, in extractor with 400 milliliters of alcohol solvent extractings 480 minutes, 300 milliliters of solvents are removed in the extract decompression distillation, add 100 ml distilled waters, continue decompression distillation organic solvent content to the extract and remove by filter insoluble matter to less than 5%;
As adsorbent, filtrate by 78 gram adsorbents, is carried out desorption with 500 milliliters of alcohol solvents to adsorbent with macropore phenolic resins, obtain a kind of mixing material;
400 milliliters of solvents are removed in decompression distillation, and spray-drying gets the extract that main component is GINKGO BILOBA EXTRACT and ginkgolides mixture.
Embodiment 4
One, gets 100 gram konjaku powders, place 700 milliliters of aqueous solution that contain isopropyl alcohol 10%, regulate pH to 1.0 with hydrochloric acid, 110 ℃ of temperature, stirring reaction 70 minutes is to room temperature, remove by filter organic solvent, add water to solid content 12%, obtain the solution of viscosity at 25000 centipoises.
Get above-mentioned solution 100 grams, regulate pH to 6.8 with sodium hydrogen phosphate, add 0.5 gram vigor and be 450 'beta '-mannase, 48 ℃ of temperature slowly stirred 400 minutes, reduce to about 5000 centipoises to viscosity, be heated to 85 ℃, utilize aperture 120 mesh filter screens to filter, remove the sediment reserved filtrate, spray-drying obtains powdery white solid 8.3 grams.
Two, get dry ginkgo leaf 500 grams, pulverize, 70 ℃ of temperature, in extractor with 500 ml methanol solvent extractions 500 minutes, 400 milliliters of solvents are removed in the extract decompression distillation, add 100 ml distilled waters, continue decompression distillation organic solvent content to the extract and remove by filter insoluble matter to less than 5%;
As adsorbent, filtrate by 78 gram adsorbents, is carried out desorption with 500 milliliters of alcohol solvents to adsorbent with macropore phenolic resins, obtain a kind of mixing material;
400 milliliters of solvents are removed in decompression distillation, and spray-drying gets the extract that main component is GINKGO BILOBA EXTRACT and ginkgolides mixture.
Embodiment 5
One, gets 100 gram konjaku powders, place 650 milliliters of aqueous solution that contain ethanol 15%, regulate pH to 1.0 with hydrochloric acid, 120 ℃ of temperature, stirring reaction 60 minutes is to room temperature, remove by filter organic solvent, add water to solid content 10%, obtain the solution of viscosity at 22000 centipoises.
Get above-mentioned solution 100 grams, regulate pH to 6.8 with potassium dihydrogen phosphate and dipotassium hydrogen phosphate, add 0.5 gram vigor and be 450 'beta '-mannase,, slowly stirred 350 minutes 48 ℃ of temperature, reduce to about 5000 centipoises to viscosity, be heated to 85 ℃, utilize aperture 120 mesh filter screens to filter, remove the sediment reserved filtrate, spray-drying obtains powdery white solid 7.9 grams.
Two, get dry ginkgo leaf 500 grams, pulverize, 70 ℃ of temperature, in extractor with 480 ml methanol solvent extractions 480 minutes, 320 milliliters of solvents are removed in the extract decompression distillation, add 100 ml distilled waters, continue decompression distillation to the extract organic solvent content to removing by filter insoluble matter less than 5%;
As adsorbent, filtrate by 78 gram adsorbents, is carried out desorption with 500 ml methanol solvents to adsorbent with macropore phenolic resins, obtain a kind of mixing material;
400 milliliters of solvents are removed in decompression distillation, and spray-drying gets the extract that main component is GINKGO BILOBA EXTRACT and ginkgolides mixture.
Embodiment 6
One, gets 100 gram konjaku powders, place 650 milliliters of aqueous solution that contain methyl alcohol 17%, regulate pH to 1.0 with hydrochloric acid, 110 ℃ of temperature, stirring reaction 80 minutes is to room temperature, remove by filter organic solvent, add water to solid content 10%, obtain the solution of viscosity at 19000 centipoises.
Get above-mentioned solution 100 grams, regulate pH to 6.8 with sodium hydrogen phosphate and sodium dihydrogen phosphate, add 0.5 gram vigor and be 450 'beta '-mannase,, slowly stirred 350 minutes 48 ℃ of temperature, reduce to about 5000 centipoises to viscosity, be heated to 85 ℃, utilize aperture 120 mesh filter screens to filter, remove the sediment reserved filtrate, spray-drying obtains powdery white solid 7.9 grams.
Two, get dry ginkgo leaf 500 grams, pulverize, 85 ℃ of temperature, in extractor with 500 milliliters of alcohol solvent extractings 450 minutes, 400 milliliters of solvents are removed in the extract decompression distillation, add 100 ml distilled waters, continue decompression distillation to the extract organic solvent content to removing by filter insoluble matter less than 5%;
As adsorbent, filtrate by 78 gram adsorbents, is carried out desorption with 500 milliliters of alcohol solvents to adsorbent with macropore phenolic resins, obtain a kind of mixing material;
400 milliliters of solvents are removed in decompression distillation, and spray-drying gets the extract that main component is GINKGO BILOBA EXTRACT and ginkgolides mixture.
Embodiment 7
One, gets 100 gram konjaku powders, place 600 milliliters of aqueous solution that contain ethanol 16%, regulate pH to 1.0 with hydrochloric acid, 110 ℃ of temperature, stirring reaction 80 minutes is to room temperature, remove by filter organic solvent, add water to solid content 12%, obtain the solution of viscosity at 21000 centipoises.
Get above-mentioned solution 100 grams, regulate pH to 6.8 with sodium phosphate, add 0.5 gram vigor and be 450 'beta '-mannase, 48 ℃ of temperature slowly stirred 400 minutes, reduce to about 5000 centipoises to viscosity, be heated to 85 ℃, utilize aperture 120 mesh filter screens to filter, remove the sediment reserved filtrate, spray-drying obtains powdery white solid 8.6 grams.
Two, get dry ginkgo leaf 500 grams, pulverize, 70 ℃ of temperature, with 300 milliliters of acetone and 100 ml water extractings 450 minutes, 300 milliliters of solvents were removed in the extract decompression distillation, extremely less than 5%, remove by filter insoluble matter until organic solvent content in extractor;
As adsorbent, filtrate by 78 gram adsorbents, is carried out desorption with 500 milliliters of isopropanol solvents to adsorbent with macropore phenolic resins, obtain a kind of mixing material;
400 milliliters of solvents are removed in decompression distillation, and spray-drying gets the extract that main component is GINKGO BILOBA EXTRACT and ginkgolides mixture.
Embodiment 8
One, gets 100 gram konjaku powders, place 700 milliliters of aqueous solution that contain isopropyl alcohol 12%, regulate pH to 1.0 with hydrochloric acid, 120 ℃ of temperature, stirring reaction 55 minutes is to room temperature, remove by filter organic solvent, add water to solid content 12%, obtain the solution of viscosity at 18000 centipoises.
Get above-mentioned solution 100 grams, regulate pH to 6.8 with sodium hydrogen phosphate, add 0.5 gram vigor and be 450 'beta '-mannase,, slowly stirred 360 minutes 48 ℃ of temperature, reduce to about 5000 centipoises to viscosity, be heated to 85 ℃, utilize aperture 120 mesh filter screens to filter, remove the sediment reserved filtrate, spray-drying obtains powdery white solid 8.2 grams.
Two, get dry ginkgo leaf 500 grams, pulverize, 65 ℃ of temperature, in extractor with 500 ml methanol solvent extractions 480 minutes, 400 milliliters of solvents are removed in the extract decompression distillation, add 100 ml distilled waters, continue decompression distillation to the extract organic solvent content to removing by filter insoluble matter less than 5%;
As adsorbent, filtrate by 78 gram adsorbents, is carried out desorption with 500 ml methanol solvents to adsorbent with macropore phenolic resins, obtain a kind of mixing material;
400 milliliters of solvents are removed in decompression distillation, and spray-drying gets the extract that main component is GINKGO BILOBA EXTRACT and ginkgolides mixture.
Embodiment 9
Get dry ginkgo leaf 500 grams, pulverize, 70 ℃ of temperature, in extractor with 500 ml methanol solvent extractions 500 minutes, 400 milliliters of solvents are removed in the extract decompression distillation, add 100 ml distilled waters, continue decompression distillation organic solvent content to the extract and remove by filter insoluble matter to less than 5%;
As adsorbent, filtrate by 78 gram adsorbents, is carried out desorption with 500 milliliters of acetone solvents to adsorbent with macropore phenolic resins, obtain a kind of mixing material;
400 milliliters of solvents are removed in decompression distillation, and spray-drying gets the extract that main component is GINKGO BILOBA EXTRACT and ginkgolides mixture.
Male and female rat test: oral administration solid mix powder 200mg.kg
-1.d
-1And 400mg.kg
-1.d
-1Irritated stomach 7 days, with the cornstarch is control group, measures rat stool weight and Bifidobacterium vigor, finds that there are notable difference in filling stomach group and control group, irritating stomach group stool weight is respectively 108% and 123%, and the Bifidobacterium vigor is respectively 126% and 135% of control group.
Through the human body mouthfeel is tested: find that mouthfeel is little sweet in oral powder dissolution 100 ml waters of 15 grams, little acid, slightly bitter, liquid has certain denseness, feels very good, and is edible very convenient.
Claims (5)
1, konjak glucomannan degradation product and ginkgo leaf extract health-care food is characterized in that: be made up of following substances
Konjak glucomannan degradation product 10～95%,
Ginkgo biloba p.e 0.5～50%,
Mannose 0～15%,
Edible refinement konjaku powder 0～15%,
Vitamin C 0.05～5%.
2, the preparation method of a kind of konjak glucomannan degradation product according to claim 1 and ginkgo leaf extract health-care food is characterized in that:
The preparation of A, konjak glucomannan degradation product
(1), get konjaku powder 20～100 gram and place 80～1000 milliliters of aqueous solution that contain 5～85% organic solvents, with salt acid for adjusting pH value to 0～6.0, stirred 5～500 minutes intensification degree to 35～125 ℃;
(2), regulate pH value to 6.5～8.9 with phosphate, filter, add 200～800 ml distilled waters in the filter residue, adjust the temperature to 25～65 ℃, add 0.1～1.0 milliliter of Glucomannan restriction endonuclease, reduced to 1000～8000 centipoises to viscosity in reaction time 20～2g00 minute, be heated to 75～95 ℃, remove by filter insoluble matter with 100～300 mesh filter screens, spray-drying gets the pressed powder that main component is the grape manna oligosacchride;
The preparation of B, ginkgo biloba p.e
(1), gets dry ginkgo leaf 20～1000 grams, pulverize, 15～95 ℃ of temperature, in extractor, with 400～1000 milliliters of organic solvent extractings 15～600 minutes, 300～900 milliliters of solvents were removed in the extract decompression distillation, added 50～300 ml distilled waters, continue decompression distillation organic solvent content to the extract and remove by filter insoluble matter to less than 5%;
(2), with macropore phenolic resins as adsorbent, filtrate by 50～1000 gram adsorbents, is carried out desorption with 50～1000 milliliters of organic solvents to adsorbent.Obtain a kind of mixing material of lark;
(3), decompression distillation removes 20～800 milliliters of solvents, spray-drying gets the extract that main component is GINKGO BILOBA EXTRACT and ginkgolides mixture.
3, the preparation method of a kind of konjak glucomannan degradation product according to claim 2 and ginkgo leaf extract health-care food is characterized in that: the organic solvent in the preparation of described konjak glucomannan degradation product or for methyl alcohol or for ethanol or be isopropyl alcohol.
4, the preparation method of a kind of konjak glucomannan degradation product according to claim 2 and ginkgo leaf extract health-care food is characterized in that: the phosphate in the preparation of described konjak glucomannan degradation product or for sodium phosphate or for potassium phosphate or for sodium dihydrogen phosphate or for potassium dihydrogen phosphate or for sodium hydrogen phosphate or be dipotassium hydrogen phosphate.
5, the preparation method of a kind of konjak glucomannan degradation product according to claim 2 and ginkgo leaf extract health-care food is characterized in that: the organic solvent in the preparation of described ginkgo biloba extract or for methyl alcohol or for ethanol or be acetone.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB011340746A CN1287682C (en) | 2001-10-19 | 2001-10-19 | Konjak glucomannan degradation product and ginkgo leaf extract health-care food and its preparation method |
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| Application Number | Priority Date | Filing Date | Title |
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| CNB011340746A CN1287682C (en) | 2001-10-19 | 2001-10-19 | Konjak glucomannan degradation product and ginkgo leaf extract health-care food and its preparation method |
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| CN1411739A true CN1411739A (en) | 2003-04-23 |
| CN1287682C CN1287682C (en) | 2006-12-06 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1296082C (en) * | 2004-12-09 | 2007-01-24 | 王宝民 | Medication and health food in use for lowering blood sugar, improving function of intestinal tract and reducing platelet aggergation |
| CN100413425C (en) * | 2005-01-07 | 2008-08-27 | 周宓 | Diet fiber composition with blood lipid-reducing blood sugar-decreasing functions and its production method |
| CN102178873A (en) * | 2011-04-23 | 2011-09-14 | 王效山 | Chinese medicine weight-losing preparation comprising external preparation and internal preparation and preparation method thereof |
| CN109266272A (en) * | 2018-08-06 | 2019-01-25 | 岳西县明杰电子有限公司 | A kind of preparation method of the dedicated adhesive of transformer |
| CN113598358A (en) * | 2021-06-28 | 2021-11-05 | 长沙汉爵快乐养老服务有限公司 | Dietary therapy meal assisting in reducing blood fat and preparation method thereof |
-
2001
- 2001-10-19 CN CNB011340746A patent/CN1287682C/en not_active Expired - Fee Related
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1296082C (en) * | 2004-12-09 | 2007-01-24 | 王宝民 | Medication and health food in use for lowering blood sugar, improving function of intestinal tract and reducing platelet aggergation |
| CN100413425C (en) * | 2005-01-07 | 2008-08-27 | 周宓 | Diet fiber composition with blood lipid-reducing blood sugar-decreasing functions and its production method |
| CN102178873A (en) * | 2011-04-23 | 2011-09-14 | 王效山 | Chinese medicine weight-losing preparation comprising external preparation and internal preparation and preparation method thereof |
| CN102178873B (en) * | 2011-04-23 | 2012-11-28 | 王效山 | Chinese medicine weight-losing preparation comprising external preparation and internal preparation and preparation method thereof |
| CN109266272A (en) * | 2018-08-06 | 2019-01-25 | 岳西县明杰电子有限公司 | A kind of preparation method of the dedicated adhesive of transformer |
| CN113598358A (en) * | 2021-06-28 | 2021-11-05 | 长沙汉爵快乐养老服务有限公司 | Dietary therapy meal assisting in reducing blood fat and preparation method thereof |
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| CN1287682C (en) | 2006-12-06 |
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