CN117084933A - Hair conditioning composition and shampoo containing same - Google Patents
Hair conditioning composition and shampoo containing same Download PDFInfo
- Publication number
- CN117084933A CN117084933A CN202311274333.9A CN202311274333A CN117084933A CN 117084933 A CN117084933 A CN 117084933A CN 202311274333 A CN202311274333 A CN 202311274333A CN 117084933 A CN117084933 A CN 117084933A
- Authority
- CN
- China
- Prior art keywords
- extract
- conditioning composition
- hair
- hydrolyzed
- protein
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
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Classifications
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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- A61K8/9728—Fungi, e.g. yeasts
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9755—Gymnosperms [Coniferophyta]
- A61K8/9761—Cupressaceae [Cypress family], e.g. juniper or cypress
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- A—HUMAN NECESSITIES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
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Abstract
The invention relates to the field of washing and caring, and particularly discloses a conditioning composition for hair and shampoo containing the composition. Wherein the conditioning composition for hair comprises the following components: hydrolyzed vegetable protein, amaranthus caudatus seed extract, black ganoderma extract, cordyceps extract, lophatherum gracile extract, octanoylglycine, humectant, preservative and solvent. The composition is applied to shampoo, so that the shampoo can simultaneously have the effects of controlling oil and moisturizing scalp.
Description
Technical Field
The invention relates to the field of washing and caring, in particular to a conditioning composition for hair and shampoo containing the same.
Background
Shampoo, also known as shampoo, is one of the most widely used hair products, and is one of the most commonly used hair cosmetics, and its main function is to clean hair and scalp. In recent years, the scalp problems of people are increasingly serious due to the factors of quickening the life rhythm, staying up, scalding and dyeing hair, irregular diet and the like, especially the scalp oil is discharged, and the scalp is easier to discharge because the number of sebaceous glands of the scalp is more than that of the facial skin, the oil secretion speed is faster than that of the facial skin and the hair is covered.
Therefore, the shampoo products on the market mainly aims at cleaning and controlling scalp grease, but the shampoo products have strong cleaning power, so that the scalp and hair are easy to be too dry and even split, and people usually use other nourishing products to condition. However, for people who love oil from the scalp, after the nourishing product is used, a large amount of grease is easily generated on the scalp, and even the scalp is easily stinked. Therefore, there is a need to develop a product with both oil control and nourishing effects.
Disclosure of Invention
In order to provide a hair product with oil control and moisturizing effects, the invention provides a hair conditioning composition and shampoo containing the same.
In a first aspect, the present invention provides a conditioning composition for hair, which adopts the following technical scheme:
a conditioning composition for hair comprising the following components: hydrolyzed vegetable protein, amaranthus caudatus seed extract, black ganoderma extract, cordyceps extract, lophatherum gracile extract, octanoylglycine, humectant, preservative and solvent.
The hydrolyzed vegetable protein is the product of vegetable protein after hydrolysis under the acid catalysis. The composition is mainly amino acid, can generate good compatibility with skin, is favorable for permeation of nutrient substances and forms a protective film on the surface of the skin.
The small molecular peptide contained in the amaranthus caudatus seed extract can permeate into hair fibers, so that friction force of hair is reduced, scalp injury is prevented, and fluffiness and glossiness are improved.
The ganoderma atrum extract contains a large amount of polysaccharide, polypeptide and the like, has obvious effects of delaying aging, can promote and regulate immune function, regulate metabolic balance and promote synthesis of nucleic acid and protein. The ganoderan has obvious SOD-like activity, and can obviously remove free radicals generated by organisms, thereby preventing the damage of the free radicals to the organisms, preventing peroxidation of lipid, protecting cells and delaying cell aging.
Adenosine contained in Cordyceps sinensis extract can strengthen hair root, reduce alopecia, and is rich in amino acids, and can provide nutrition for scalp, enhance activity of epidermal cells, promote cell metabolism, and protect glycine, arginine and isoleucine from radiation, and resist sunlight irradiation.
The Lophatherum gracile extract has excellent effects of resisting free radicals, oxidation, aging, bacteria and viruses, protecting hair follicle, and inhibiting scalp aging.
Octanoyl glycine can limit excessive secretion of grease by inhibiting 5 alpha reductase activity, so that an effective oil control effect is achieved, and in addition, the octanoyl glycine also has a good antibacterial effect and has a strong inhibition effect on staphylococcus aureus, propionibacterium acnes and the like.
The lophatherum gracile and the octanoylglycine are compounded, so that the inhibition of 5 alpha reductase activity is facilitated, the content of DHT in the scalp is reduced, the secretion of scalp grease is reduced, and in addition, the growth of staphylococcus aureus is inhibited, so that the secretion of scalp grease is reduced better.
The composition is beneficial to better nourish the scalp by compounding the hydrolyzed vegetable protein and the humectant, and the hydrolyzed vegetable protein provides various amino acids, so that the hydrolyzed vegetable protein is beneficial to forming a uniform film on the surface of the hair, protecting the cuticle, reducing the loss of protein and moisture, and ensuring that the composition has better moisturizing and moisturizing effects on the scalp.
Through the compounding of the amaranthus caudatus seed extract, the ganoderma atrum extract and the cordyceps sinensis extract, the oil control and bacteriostasis effects of lophatherum gracile and octanoylglycine and the nourishing effects of hydrolyzed vegetable proteins and humectants are better balanced, so that the scalp is nourished, the water-oil balance is better realized, the hair conditioning composition can simultaneously have the effects of bacteriostasis and oil control and nourishing, the bacteriostasis and oil control and the nourishing effects are not easy to influence each other, the scalp is moist but not greasy, and the scalp is better kept in a balanced state.
Preferably, the conditioning composition for hair comprises the following components in percentage by mass:
26% -30% of hydrolyzed vegetable protein;
4-6% of amaranthus caudatus seed extract;
0.4-0.5% of ganoderma atrum extract;
0.5-0.7% of Cordyceps sinensis extract;
0.3-0.4% of lophatherum gracile extract;
0.4-0.8% of octanoylglycine;
4.5 to 7.5 percent of humectant;
a preservative; 0.6-1.2%;
the balance being solvent.
The substances with specific proportions are mutually synergistic and compounded, so that the scalp can be better nourished, the water-oil balance of the scalp can be better regulated and controlled, the hair regulating composition has the effects of inhibiting bacteria and controlling oil and nourishing, and the effects of inhibiting bacteria and controlling oil and nourishing are less likely to be affected.
Preferably, the plant protein comprises one or more of hydrolyzed wheat protein, hydrolyzed corn protein, and hydrolyzed soy protein.
Preferably, the plant protein is a compound of hydrolyzed wheat protein, hydrolyzed corn protein and hydrolyzed soybean protein, and the compound mass ratio of the hydrolyzed wheat protein, the hydrolyzed corn protein and the hydrolyzed soybean protein is as follows: (1-1.5): (1.5-2): (1.25-1.75).
The hydrolyzed wheat protein is low molecular weight protein extracted from soft wheat, forms a layer of glossy protective film on the surface of hair, nourishes dry and fragile hair, solves the problem of bifurcation of the tips of the hair, increases the hair volume, makes the hair at the top of the head fluffy, and regains elasticity and vitality.
The hydrolyzed zein is a protein extracted from corn, has the main functions of antistatic, softening and antioxidant in cosmetics and skin care products, can stabilize foam, can be quickly absorbed by skin, and is suitable for being used as a skin care raw material of cosmetics.
The hydrolyzed soybean protein is a protein extracted from soybean, has high-efficiency moisturizing effect, and can be used as humectant and skin conditioner. The hydrolyzed soy protein is favorable for inducing the skin to produce hyaluronic acid, and is an ideal natural moisturizing factor.
By adopting the compounding of three plant proteins, namely hydrolyzed wheat protein, hydrolyzed corn protein and hydrolyzed soybean protein, the method is favorable for providing more amino acids for the hydrolyzed plant proteins, providing various nutrients for scalp and hair and moistening the scalp better; meanwhile, the conditioning composition for the hair is beneficial to better protecting the stratum corneum, reducing the loss of protein and moisture and ensuring that the composition has better moisturizing and moisturizing effects on the scalp.
Preferably, the conditioning composition for hair further comprises the following components in percentage by mass:
0.2% -0.3% of acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer.
By adopting the technical scheme, the acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer is added to be beneficial to increasing the hydrophobicity of the hair surface, so that the hair is not easy to knot; meanwhile, the conditioning composition is beneficial to promoting the moisturizing state of hair and scalp and promoting the moisturizing effect of the conditioning composition for hair on hair.
In a second aspect, the invention provides a shampoo containing a conditioning composition for hair, which adopts the following technical scheme: a shampoo containing a conditioning composition for hair, comprising the following components in percentage by mass:
22-25% of a surfactant; 1-2% of pearling agent; 0.04 to 0.06 percent of stabilizer; 1 to 1.5 percent of bacteriostat; 0.1-0.2% of pH regulator; 1-2% of a thickening agent; 0.2-0.3% of anti-dandruff agent; 2.5-3% of softener; 0.5-0.7% of essence; 1.5-2.5% of a hair conditioning composition; the balance being water.
By adopting the technical scheme, the conditioning composition for hair is prepared into the shampoo, so that the shampoo has the effects of better controlling oil, supplementing water and balancing water and oil, is beneficial to people to clean hair, and can better regulate and control the balancing water and oil of scalp, thereby the shampoo achieves the effect of nourishing scalp; meanwhile, the shampoo can inhibit bacteria on scalp to achieve the effect of controlling oil, and the effects of inhibiting bacteria, controlling oil and nourishing in the shampoo are not easy to influence each other.
Preferably, the shampoo containing the conditioning composition for hair further comprises the following components: arborvitae twig extract, polygonum multiflorum extract and soapberry extract.
Preferably, the shampoo containing the hair conditioning composition further comprises the following components in percentage by mass:
0.008-0.012% of cacumen Platycladi extract; 0.008-0.012% of Polygonum multiflorum extract; the soapberry extract is 0.4-0.6%.
The cacumen Platycladi extract is a pure natural plant extract product, can smooth scalp, enable nutrient components to be better absorbed by hair roots, stimulate and care hair stems, prevent falling off, promote normal growth of hair, and achieve the effects of preventing hair loss and hair growth.
The Polygoni Multiflori radix extract can effectively promote scalp blood circulation, nourish hair root, improve hair quality, and prevent alopecia and canities.
The soapberry extract has the main effects of resisting bacteria, resisting inflammation, removing acnes, cleaning and decontaminating.
The addition of the combination of the biota orientalis leaf extract, the polygonum multiflorum extract and the soapberry fruit extract in a specific proportion is beneficial to better promoting the effect of the conditioning composition for hair on inhibiting staphylococcus aureus, thereby being beneficial to better controlling the grease of scalp; meanwhile, the scalp care agent is beneficial to better supplementing nutrients needed by the scalp, nourishing the scalp, repairing the hair, maintaining the water-oil balance of the scalp and making the scalp and the hair healthier.
In summary, the invention has the following beneficial effects:
1. the compound of the lophatherum gracile and the octanoylglycine is beneficial to better reducing secretion of scalp grease, the compound of the hydrolyzed vegetable protein and the humectant is beneficial to better moistening scalp, and the compound of the amaranthus caudatus seed extract, the black ganoderma extract and the Cordyceps sinensis extract is beneficial to better balancing the oil control antibacterial effect of the lophatherum gracile and the octanoylglycine and the nourishing effect of the hydrolyzed vegetable protein and the humectant, so that the hair conditioning composition can simultaneously have the effects of bacteriostasis oil control and nourishing, and the bacteriostasis oil control and nourishing effects of the hair conditioning composition are not easy to influence each other.
2. By adopting the compounding of three plant proteins, namely hydrolyzed wheat protein, hydrolyzed corn protein and hydrolyzed soybean protein in a specific proportion, the method is favorable for providing more amino acids for the hydrolyzed plant proteins and better moistening the scalp.
3. The compound of the biota orientalis leaf extract, the polygonum multiflorum extract and the soapberry fruit extract in a specific proportion is added, so that the scalp grease can be better controlled; meanwhile, the scalp care agent is beneficial to better supplementing nutrients needed by the scalp, nourishing the scalp, repairing the hair, and maintaining the water-oil balance of the scalp.
Detailed Description
The present invention will be described in further detail with reference to examples.
In the examples below, each material was commercially available.
Sodium laureth sulfate was purchased from Oryza Glutinosa, inc. of Nanli.
Ammonium lauryl sulfate was purchased from aowei practice company, south lake.
Quaternary ammonium salt-10 was purchased from Dow (Zhang Jiang Kong) investment Limited.
Guar hydroxypropyl trimethylammonium chloride was purchased from Ashland LLC.
Sodium salicylate was purchased from lang Cheng Huaxue (china) limited.
Sodium cocoyl methyl taurate was purchased from Zhang Kong Greek chemical Co.
Cocamidopropyl betaine is available from Ganggao New Material Co., ltd.
Palm kernel oleyl amide DEA is available from WOODLAND FOOD INDUSTRIES PTE LTD.
Piroctone olamine salt was purchased from Shanghai atlanto Utility development Co.
7137 Silicone emulsions were purchased from Dow (Zhangjichong) investment Co.
1785 Silicone emulsions were purchased from Dow (Zhangjichong) investment Co.
Cocoamidomethyl MEA was purchased from the chemical industry limited of the king (Shanghai).
The fragrances were purchased from De Xin essence fragrances (Nantong) Inc.
Citric acid monohydrate was purchased from shandong english real stock.
Industrial salts were purchased from Jiangxi Jiujiu Di salt industry Limited liability company.
Trehalose was purchased from the company of biosciences, fuxi, hangzhou.
The cacumen Platycladi extract was purchased from Shanghai Hui Biotechnology Co., ltd.
The polygonum multiflorum extract was purchased from Guangzhou cosmetic biotechnology limited.
Soapberry fruit extract was purchased from guangdong cyanine extract biotechnology limited.
Dioscorea longa root extract was purchased from Nantong fragrance adding bioengineering Co.
Kelp extract was purchased from volley biotechnology limited, lanzhou.
The extract of Malva sylvestris was purchased from Anhui co-invasive Va Biotechnology Co.
Amaranthus caudatus seed extract was purchased from Sesambac chemical Co.
The black ganoderma extract was purchased from guangzhou Tianjia biotechnology limited.
Cordyceps sinensis extract was purchased from Baozhen Liuji Biotechnology Co., ltd.
Lophatherum gracile extract was purchased from Bao Ji Liu Pan rhyme Biotechnology Co.
Hydrolyzed wheat proteins were purchased from the biological sciences company, finest.
Hydrolyzed zein was purchased from Shaanxi Xinkang biotechnology Co.
Hydrolyzed soy protein was purchased from biotechnology limited in the state of shanxi, summer.
Example 1
The embodiment of the invention discloses a conditioning composition for hair, which comprises the following components in parts by mass:
300kg of hydrolyzed vegetable protein, 40kg of amaranthus caudatus seed extract, 4kg of ganoderma atrum extract, 5kg of cordyceps sinensis extract, 3kg of lophatherum gracile extract, 4kg of octanoylglycine, 4.5kg of humectant and 6kg of preservative; 633.5kg of solvent.
In this example, the hydrolyzed vegetable protein is formed by mixing hydrolyzed wheat protein, hydrolyzed corn protein, and hydrolyzed soybean protein in a mass ratio of 1:1.5:1.25, and the solvent is water.
The humectant can be any humectant conventional in the art, in this embodiment, butanediol and glycerol are specifically selected, and the mass ratio of butanediol to glycerol is 5:3.
The preservative can be any preservative conventional in the art, in this embodiment, phenoxyethanol, sodium benzoate and p-hydroxyacetophenone are specifically selected, and the mass ratio of phenoxyethanol, sodium benzoate and p-hydroxyacetophenone is 5:4:0.3.
The embodiment of the invention also discloses a preparation method of the conditioning composition for hair, which comprises the following steps:
step 1: cleaning and sterilizing equipment for production, accurately weighing the substances with the above quality, adding hydrolyzed wheat protein, hydrolyzed corn protein, hydrolyzed soybean protein, amaranthus caudatus seed extract, ganoderma atrum extract, cordyceps extract, lophatherum gracile extract, octanoylglycine, butanediol, glycerol phenoxyethanol, sodium benzoate, p-hydroxyacetophenone and water into a main pot of an emulsifying machine, controlling the temperature at 25 ℃, and stirring at 150r/min for 30 minutes.
Step 2: filtering, and taking out filtrate to obtain the hair conditioning composition.
Example 2
The difference from example 1 is that:
the dosage of each component is different, and the specific steps are as follows:
260kg of hydrolyzed vegetable protein; 50kg of amaranthus caudatus seed extract; 4.5kg of ganoderma atrum extract; 6kg of Cordyceps sinensis extract; 3.5kg of lophatherum gracile extract; 6kg of octanoylglycine; 60kg of humectant; 12kg of preservative; 569kg of solvent.
Example 3
The difference from example 1 is that:
the dosage of each component is different, and the specific steps are as follows:
280kg of hydrolyzed vegetable protein; 60kg of amaranthus caudatus seed extract; 5kg of ganoderma atrum extract; 7kg of Cordyceps sinensis extract; 4kg of lophatherum gracile extract; 8kg of octanoylglycine; 75kg of humectant; 8kg of preservative; 573kg of solvent.
Example 4
The difference from example 3 is that: in this example, the hydrolyzed vegetable protein is formed by mixing hydrolyzed wheat protein, hydrolyzed corn protein, and hydrolyzed soy protein in a mass ratio of 1.5:2:1.75.
Example 5
The difference from example 3 is that: in this example, the hydrolyzed vegetable protein is formed by mixing hydrolyzed wheat protein, hydrolyzed corn protein, and hydrolyzed soy protein in a mass ratio of 1.25:1.75:1.5.
Example 6
The difference from example 3 is that: in this example, the hydrolyzed vegetable protein is formed by mixing hydrolyzed wheat protein, hydrolyzed corn protein, and hydrolyzed soy protein in a mass ratio of 0.5:1:1.
Example 7
The difference from example 3 is that: in this example, the hydrolyzed vegetable protein is formed by mixing hydrolyzed wheat protein, hydrolyzed corn protein, and hydrolyzed soy protein in a mass ratio of 2:2.5:2.
Example 8
The difference from example 5 is that:
the hair conditioning composition further comprises the following components in mass:
2kg of acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer and the addition amount of the solvent was adjusted to 631.5g.
In addition, the conditioning composition for hair is prepared by adding acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer together with hydrolyzed wheat protein, hydrolyzed corn protein, hydrolyzed soybean protein, etc. in step 1.
Example 9
The difference from example 8 is that:
the hair conditioning composition further comprises the following components in mass:
3kg of acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, and the addition amount of the solvent was adjusted to 630.5g.
Comparative example 1
The difference from example 1 is that: the amaranthus caudatus seed extract, ganoderma atrum extract, cordyceps extract, lophatherum gracile extract and octanoylglycine are replaced by equal amount of water.
Comparative example 2
The difference from example 1 is that: the water is used to replace hydrolyzed vegetable protein, amaranthus caudatus seed extract, ganoderma atrum extract, cordyceps sinensis extract and humectant.
Comparative example 3
The difference from example 1 is that: the amaranthus caudatus seed extract, the ganoderma atrum extract and the Cordyceps sinensis extract are replaced by the same amount of water.
Comparative example 4
The difference from example 1 is that: the amaranthus caudatus seed extract is replaced by an equivalent amount of the dioscorea longifolia root extract.
Comparative example 5
The difference from example 1 is that: the same amount of herba Zosterae Marinae extract is used to replace Ganoderma atrum extract.
Comparative example 6
The difference from example 1 is that: the Cordyceps extract is replaced by equal amount of Malva sylvestris extract.
Application example 1
The application example of the invention discloses shampoo containing a conditioning composition for hair, which comprises the following components in parts by mass:
250kg of surfactant; 10kg of pearling agent; 0.4kg of stabilizer; 10kg of bacteriostat; 1kg of pH regulator; 10kg of thickening agent; 2kg of anti-dandruff agent; 25kg of softener; 5kg of essence; 15kg of a hair conditioning composition; 671.6kg of water.
In this example, a hair conditioning composition was prepared as in example 1.
The surfactant may be any surfactant conventionally used in the art, in this embodiment, sodium laureth sulfate, ammonium laureth sulfate, sodium laurylsulfate, sodium cocoyl methyl taurate, cocamidopropyl betaine, and palm kernel oleyl amide DEA are specifically selected, and the mass ratio of sodium laureth sulfate, ammonium laurylsulfate, sodium cocoyl methyl taurate, cocamidopropyl betaine, and palm kernel oleyl amide DEA is 16:1.5:0.5:0.5:4:1.
The pearling agent may be any pearling agent conventional in the art, and in this embodiment, specifically, pearling flakes DM125H are selected.
The stabilizer may be any stabilizer conventional in the art, and in this embodiment, zinc chloride is specifically selected.
The bacteriostat can be any bacteriostat conventional in the art, in this embodiment, sodium salicylate, phenoxyethanol and sodium benzoate are specifically selected, and the mass ratio of the sodium salicylate, the phenoxyethanol and the sodium benzoate is 5:12:9.
The pH regulator may be any pH regulator conventional in the art, and in this embodiment, citric acid monohydrate is specifically selected.
The thickener may be any thickener conventional in the art, in this embodiment, cocamidomethyl MEA and industrial salt are specifically selected, and the mass ratio of cocamidomethyl MEA to industrial salt is 1:2.
The antidandruff agent may be any antidandruff agent conventional in the art, in this example piroctone olamine salt.
The softener can be any softener conventional in the art, in this embodiment, the softener is specifically selected from polyquaternium-10, guar hydroxypropyltrimonium chloride, 7137 emulsified silicone oil and 1785 emulsified silicone oil, and the mass ratio of polyquaternium-10, guar hydroxypropyltrimonium chloride, 7137 emulsified silicone oil and 1785 emulsified silicone oil is 0.6:3:8:15.
The embodiment of the invention also discloses a preparation method of the shampoo containing the conditioning composition for hair, which comprises the following steps:
and step 1, adding deionized water, sodium laureth sulfate, ammonium laureth sulfate, sodium laureth sulfate, pearly luster pieces DM125H, zinc chloride and sodium cocoyl methyl taurate into an emulsifying pot, stirring at the rotating speed of 150r/min, heating to 85 ℃, stirring and homogenizing for 3 minutes, and dissolving uniformly.
And 2, after the solution is uniformly dissolved, adding the polyquaternium-10 and guar hydroxypropyl trimethyl ammonium chloride, stirring and homogenizing for 3 minutes, uniformly dissolving, and preserving heat for 20 minutes.
And 3, adding sodium salicylate, cocamidopropyl betaine, palm kernel oleyl amide DEA and cocamidomethyl MEA when the mixture starts to stand and naturally cool, and uniformly stirring.
And 4, when the temperature is reduced to 60 ℃, adding piroctone olamine salt, stirring at the rotating speed of 150r/min, and uniformly stirring.
And 5, when the temperature is reduced below 45 ℃, 7137 emulsified silicone oil, 1785 emulsified silicone oil, essence, citric acid monohydrate, industrial salt, phenoxyethanol, sodium benzoate, trehalose and a hair conditioning composition are added, stirring is carried out at the rotating speed of 150r/min, and the mixture is cooled to normal temperature and discharged to obtain the shampoo containing the hair conditioning composition.
Application example 2
The difference from application example 1 is that:
the dosage of each component is different, and the specific steps are as follows:
220kg of a surfactant; 20kg of pearling agent; 0.6kg of stabilizer; 15kg of bacteriostat; pH regulator 2kg; 20kg of a thickening agent; 3kg of anti-dandruff agent; 30kg of softener; 7kg of essence; 25kg of a hair conditioning composition; 657.4kg of water.
Application example 3
The difference from application example 1 is that:
the dosage of each component is different, and the specific steps are as follows:
235kg of surfactant; 15kg of pearling agent; 0.5kg of stabilizer; 13kg of bacteriostat; 1.3kg of pH regulator; 15kg of a thickening agent; 2.5kg of anti-dandruff agent; 26.6kg of softener; 6kg of essence; 20kg of a hair conditioning composition; 665.1kg of water.
Application example 4
The difference from application example 3 is that:
a shampoo comprising a conditioning composition for hair, further comprising the following components by mass:
0.08kg of cacumen Platycladi extract; 0.08kg of polygonum multiflorum extract; 4kg of soapberry fruit extract; 660.94kg of water
In addition, in step 5 of preparing shampoo containing hair conditioning composition, folium Platycladi extract, polygoni Multiflori radix extract, and fructus Sapindi Mukouossi extract are added together with 7137 emulsified silicone oil, 1785 emulsified silicone oil, essence, etc.
Application example 5
The difference from application example 4 is that:
the dosage of each component is different, and the specific steps are as follows:
0.12kg of cacumen Platycladi extract; 0.12kg of polygonum multiflorum extract; 6kg of soapberry fruit extract; 658.86kg of water.
Application example 6
The difference from application example 4 is that:
the dosage of each component is different, and the specific steps are as follows:
0.1kg of cacumen Platycladi extract; 0.1kg of polygonum multiflorum extract; 5kg of soapberry fruit extract; 659.9kg of water.
Application example 7
The difference from application example 6 is that: the hair conditioning composition was the hair conditioning composition prepared in example 2.
Application example 8
The difference from application example 6 is that: the hair conditioning composition was the hair conditioning composition prepared in example 3.
Application example 9
The difference from application example 6 is that: the hair conditioning composition was the hair conditioning composition prepared in example 4.
Application example 10
The difference from application example 6 is that: the hair conditioning composition was the hair conditioning composition prepared in example 5.
Application example 11
The difference from application example 6 is that: the hair conditioning composition was the hair conditioning composition prepared in example 6.
Application example 12
The difference from application example 6 is that: the hair conditioning composition was the hair conditioning composition prepared in example 7.
Application example 13
The difference from application example 6 is that: the hair conditioning composition was the hair conditioning composition prepared in example 8.
Application example 14
The difference from application example 6 is that: the hair conditioning composition was the hair conditioning composition prepared in example 9.
Comparative application example 1
The difference from application example 1 is that: the hair conditioning composition was the hair conditioning composition prepared in comparative example 1.
Comparative application example 2
The difference from application example 1 is that: the hair conditioning composition was the hair conditioning composition prepared in comparative example 2.
Comparative application example 3
The difference from application example 1 is that: the hair conditioning composition was the hair conditioning composition prepared in comparative example 3.
Comparative application example 4
The difference from application example 1 is that: the hair conditioning composition was the hair conditioning composition prepared in comparative example 4.
Comparative application example 5
The difference from application example 1 is that: the hair conditioning composition was the hair conditioning composition prepared in comparative example 5.
Comparative application example 6
The difference from application example 1 is that: the hair conditioning composition was the hair conditioning composition prepared in comparative example 6.
Experiment 1
The bacteriostasis of the shampoo containing the conditioning composition for hair prepared by the application example and the comparative application example is detected by adopting an oxford cup method bacteriostasis experiment, and the method is as follows:
sterilizing the nutrient broth at 120deg.C under high pressure for 25 min, and adding the nutrient broth with a content of about 10 6 cfu/ml of staphylococcus aureus was inoculated in the nutrient broth medium to form a culture broth. Then placing the nutrient agar culture medium at the high temperature and the high pressure of 120 ℃ for sterilization for 25 minutes, pouring the nutrient agar culture medium into a flat plate, pouring about 20ml of agar culture medium into each flat plate, sucking 1ml of culture solution after the agar culture medium is solidified, dripping the culture solution into the surface of the flat plate, uniformly coating the culture solution by using a coater, uniformly dividing each flat plate into four areas, vertically and uniformly placing an oxford cup in each area, and lightly pressing the oxford cup to ensure that the oxford cup is contacted with the culture medium without gaps. Taking one part of shampoo and one part of commercially available shampoo prepared in application examples 1-14 and comparative application examples 1-6, respectively dripping 200 mu L of shampoo into each oxford cup, wherein one plate is not dripped, and using the same as a blank control group; then the plate is placed in a laboratory with the temperature of 37 ℃ for culture for 16 hours, then the diameter of each inhibition zone is measured, the average value is taken from the experimental result, and the diameter of the inhibition zone is calculated<10mm indicates no bacteriostasis, and the diameter of the bacteriostasis zone>Diameter of inhibition zone of 10mm<15mm is moderate antibacterial, and the diameter of the antibacterial circle>15mm is highly bacteriostatic, and the experimental results are averaged.
Staphylococcus aureus was purchased from the institute of microorganisms, cantonese province.
Nutrient agar medium was purchased from south Beijing , technology Co.
Nutrient broth medium was purchased from Guangdong Crypton microbiological technologies Co.
The test data of the above experiment are shown in Table 1.
Experiment 2
200 female volunteers with similar hair lengths and similar hair quality and easy hair adhesion into a strip are randomly selected, the age range is 25-40 years, the volunteers are randomly divided into 20 groups of 10 people, each group of volunteers washes hair every three days and respectively and correspondingly uses the shampoo prepared by the application example and the comparative application example and the commercial shampoo, the volunteers are adhered to the hair for 30 days, and the volunteers are tested as follows:
on the 29 th day of the experiment, the volunteer shaves 1 block of 1.5cm×1.5cm specific area on the top of the head, on the 30 th day of the experiment and before the shampoo is used, the volunteer sits still in a laboratory with the temperature of 26 ℃ and the relative humidity of 50±5% for 30min, then the inspector detects the scalp of the specific area of the volunteer by using a grease meter SM815 and calculates the average value of the detection value of each group of volunteers to obtain the scalp grease content before the shampoo is used, then the inspector washes the hair uniformly for the volunteers, the hair is naturally dried after the hair is dried, the inspector detects the scalp of the specific area of the volunteer by using a grease meter SM815 and calculates the average value of the detection value of each group of the volunteers to obtain the scalp grease content after the shampoo is used, and the average value of the detection values of each volunteer is calculated after the shampoo is used for 4h and 8 h.
The larger the data detected, the more greasy the scalp is indicated.
The test data from the above experiments are detailed in Table 2.
Experiment 3
After the volunteer of experiment 2 finally used the shampoo containing the conditioning composition for hair for 30 days, the volunteer's experience of the degree of dryness of the scalp was recorded after the last use of the shampoo, and the degree of greasiness of the hair was observed and recorded after 3 days of the last use of the shampoo.
The test data from the above experiments are detailed in Table 3.
TABLE 1
Group of | Diameter of inhibition zone (mm) |
Blank control group | 2.4 |
Commercial shampoo | 12.2 |
Example 1 | 16.3 |
Example 2 | 16.4 |
Example 3 | 16.6 |
Example 4 | 16.0 |
Example 5 | 16.2 |
Example 6 | 14.1 |
Example 7 | 14.2 |
Example 8 | 15.8 |
Example 9 | 15.9 |
ComparisonExample 1 | 5.5 |
Comparative example 2 | 18.4 |
Comparative example 3 | 12.5 |
Comparative example 4 | 10.7 |
Comparative example 5 | 10.1 |
Comparative example 6 | 10.6 |
Table 2:
table 3:
according to the comparison of the data of the example 1 and the comparative examples 1 to 6 in the table 1, the comparison of the data of the application example 6 and the comparative examples 1 to 6 in the table 2 and the comparison of the data of the application example 6 and the comparative examples 1 to 6 in the table 3, only the hydrolyzed vegetable protein and the humectant are added to the hair conditioning composition of the comparative example 1, only the lophatherum gracile extract and the caprylylglycine are added to the hair conditioning composition of the comparative example 2, only the hydrolyzed vegetable protein, the humectant, the lophatherum gracile extract and the caprylylglycine are added to the hair conditioning composition of the comparative example 3, and the comparison of the data shows that the hair conditioning composition of the comparative examples 4 to 6 replaces one of the three of the amaranthus caudatus seed extract, the black glossy ganoderma extract and the black glossy ganoderma extract, and only the compounding of the hydrolyzed vegetable protein, the amaranthus caudatus seed extract, the caprylylglycium gracile extract and the caprylylglycine and the humectant is beneficial to the hair conditioning composition to simultaneously have the effects of antibacterial oil control and the antibacterial effect, so that the antibacterial oil control effect and the nutritional effect of the hair conditioning composition are not easy to influence each other.
According to the comparison of the data of application examples 8 and 6-7 in Table 2, application examples 6-8 change the mass percentage of hydrolyzed vegetable protein, amaranth extract, black ganoderma lucidum extract, cordyceps extract, lophatherum gracile extract, caprylylglycine, humectant, preservative and solvent in the composition, and the effects of controlling oil and supplementing water are optimal by comparison, according to the data, the synergistic compounding of hydrolyzed vegetable protein, amaranth extract, black ganoderma lucidum extract, cordyceps sinensis extract, lophatherum gracile extract, caprylylglycine, humectant, preservative and solvent in a specific proportion is beneficial to better controlling oil and moisturizing scalp, and is beneficial to better keeping water-oil balance of scalp, so that the hair conditioning composition can simultaneously have the effects of controlling oil by bacteriostasis and nourishing, and the effects of controlling oil by bacteriostasis and nourishing by the hair conditioning composition are not easy to influence each other.
According to the data comparison of application examples 10, 8-9 and 11-12 in Table 2, the mass ratio of hydrolyzed wheat protein, hydrolyzed corn protein and hydrolyzed soybean protein in hydrolyzed vegetable protein is changed in application examples 8-12, and the data comparison shows that the water-oil balance of the scalp can be better regulated on the premise of ensuring better deep nourishing of the scalp only by adopting the compounding of hydrolyzed wheat protein, hydrolyzed corn protein and hydrolyzed soybean protein in specific proportions, so that the scalp is not easy to be greasy due to overnutrition.
According to the data comparison of application example 12 and application examples 13 to 14 in Table 2, by adding acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer of different quality to application example 12, it is advantageous to maintain the state of scalp moisturization and promote the moisturizing effect of the conditioning composition for hair on scalp.
According to the data of application example 6 and comparative application examples 4-6 in Table 2, the comparative application example only replaces one of amaranthus caudatus seed extract, ganoderma atrum extract and Cordyceps sinensis extract, the scalp grease content of the comparative application example is higher, and the scalp moisture is less, and according to the data, only by adopting the synergistic compounding of amaranthus caudatus seed extract, ganoderma atrum extract and Cordyceps sinensis extract in specific proportions, the water-oil balance of the scalp can be better maintained, any substance is absent, and the effect of maintaining the water-oil balance of the scalp is difficult to play.
As can be seen from the comparison of the data of application example 3 and application examples 4-6 in Table 2, application examples 4-6 are characterized in that the specific proportions of the biota orientalis extract, the polygonum multiflorum extract and the soapberry extract are added into application example 3, and the scalp is better nourished by compounding the specific proportions of the biota orientalis extract, the polygonum multiflorum extract and the soapberry extract, so that the nourished effect of the conditioner is better, and the condition that the scalp is dried due to the too strong cleaning force after use is more difficult to occur.
As can be seen from the comparison of the data of application examples 1 to 3 in table 2, application examples 1 to 3 are shampoos prepared by using surfactants, pearlizing agents, stabilizers, bacteriostats, pH adjusters, thickeners, anti-dandruff agents, softeners, fragrances, hair conditioning compositions and water in different proportions, and the shampoo can better exert the effect of maintaining the scalp oil balance of the shampoo by preparing the materials in specific proportions.
The present embodiment is only for explanation of the present invention and is not to be construed as limiting the present invention, and modifications to the present embodiment, which may not creatively contribute to the present invention as required by those skilled in the art after reading the present specification, are all protected by patent laws within the scope of claims of the present invention.
Claims (8)
1. A conditioning composition for hair characterized in that: the composition comprises the following components: hydrolyzed vegetable protein, amaranthus caudatus seed extract, black ganoderma extract, cordyceps extract, lophatherum gracile extract, octanoylglycine, humectant, preservative and solvent.
2. A hair conditioning composition according to claim 1, characterized in that: the conditioning composition for the hair comprises the following components in percentage by mass:
26% -30% of hydrolyzed vegetable protein;
4-6% of amaranthus caudatus seed extract;
0.4-0.5% of ganoderma atrum extract;
0.5-0.7% of Cordyceps sinensis extract;
0.3-0.4% of lophatherum gracile extract;
0.4-0.8% of octanoylglycine;
4.5 to 7.5 percent of humectant;
a preservative; 0.6-1.2%;
the balance being solvent.
3. A hair conditioning composition according to any of claims 1-2 characterized in that: the plant protein comprises one or more of hydrolyzed wheat protein, hydrolyzed corn protein and hydrolyzed soybean protein.
4. A hair conditioning composition according to claim 3, characterized in that: the plant protein is the compound of hydrolyzed wheat protein, hydrolyzed corn protein and hydrolyzed soybean protein, and the compound mass ratio of the hydrolyzed wheat protein, the hydrolyzed corn protein and the hydrolyzed soybean protein is as follows: (1-1.5): (1.5-2): (1.25-1.75).
5. A hair conditioning composition according to any of claims 1-2 characterized in that: the hair conditioning composition further comprises the following components in percentage by mass:
0.2% -0.3% of acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer.
6. A shampoo comprising a hair conditioning composition according to any one of claims 1 to 5, characterized in that: comprises the following components in percentage by mass:
22-25% of a surfactant; 1-2% of pearling agent; 0.04 to 0.06 percent of stabilizer; 1 to 1.5 percent of bacteriostat; 0.1-0.2% of pH regulator; 1-2% of a thickening agent; 0.2-0.3% of anti-dandruff agent; 2.5-3% of softener; 0.5-0.7% of essence; 1.5-2.5% of a hair conditioning composition; the balance being water.
7. A hair conditioning composition according to claim 6, characterized in that: the shampoo containing the conditioning composition for hair further comprises the following components: arborvitae twig extract, polygonum multiflorum extract and soapberry extract.
8. A hair conditioning composition according to claim 7 characterized in that: the shampoo containing the hair conditioning composition further comprises the following components in percentage by mass:
0.008-0.012% of cacumen Platycladi extract; 0.008-0.012% of Polygonum multiflorum extract; the soapberry extract is 0.4-0.6%.
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CN107922956A (en) * | 2015-12-04 | 2018-04-17 | 丸自然美健有限公司 | Glycerine derived from staphylococcus epidermis produces accelerating agent, the antimicrobial peptide derived from skin epidermis keratinocyte produces accelerating agent and their applications in skin sparing external preparation |
CN108815084A (en) * | 2018-08-24 | 2018-11-16 | 国珍健康科技(北京)有限公司 | A kind of dandruff control shampoo containing and preparation method thereof containing Herba Lophatheri extract |
CN112494418A (en) * | 2020-12-08 | 2021-03-16 | 任世元 | Traditional Chinese medicine fermented shampoo and preparation method thereof |
CN115252649A (en) * | 2022-09-28 | 2022-11-01 | 广州集妍化妆品科技有限公司 | Application of thermophilic bacteria fermentation product in preventing alopecia and/or growing hair, composition and preparation thereof |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN107922956A (en) * | 2015-12-04 | 2018-04-17 | 丸自然美健有限公司 | Glycerine derived from staphylococcus epidermis produces accelerating agent, the antimicrobial peptide derived from skin epidermis keratinocyte produces accelerating agent and their applications in skin sparing external preparation |
CN108815084A (en) * | 2018-08-24 | 2018-11-16 | 国珍健康科技(北京)有限公司 | A kind of dandruff control shampoo containing and preparation method thereof containing Herba Lophatheri extract |
CN112494418A (en) * | 2020-12-08 | 2021-03-16 | 任世元 | Traditional Chinese medicine fermented shampoo and preparation method thereof |
CN115252649A (en) * | 2022-09-28 | 2022-11-01 | 广州集妍化妆品科技有限公司 | Application of thermophilic bacteria fermentation product in preventing alopecia and/or growing hair, composition and preparation thereof |
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