CN116509763A - Pericarpium citri reticulatae compound massage essential oil composition and preparation method and application thereof - Google Patents
Pericarpium citri reticulatae compound massage essential oil composition and preparation method and application thereof Download PDFInfo
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- CN116509763A CN116509763A CN202310516530.0A CN202310516530A CN116509763A CN 116509763 A CN116509763 A CN 116509763A CN 202310516530 A CN202310516530 A CN 202310516530A CN 116509763 A CN116509763 A CN 116509763A
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/522—Antioxidants; Radical scavengers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Inorganic Chemistry (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a tangerine peel compound massage essential oil composition, a preparation method and application thereof, wherein the tangerine peel compound massage essential oil composition comprises 30-50 parts of plant essential oil; 50-80 parts of ester lubricant; 0.01-0.5 part of heat-rubbing agent, wherein the plant essential oil consists of the following components in percentage by mass: (0.8-1.5): (0.2-0.6): (0.2-0.6) orange peel oil, jojoba seed oil, olive fruit oil, and sweet almond oil. According to the tangerine peel compound massage essential oil composition, the plant essential oil such as the orange peel oil, the jojoba seed oil, the olive fruit oil and the sweet almond oil is matched with the ester lubricant and the heat rubbing agent, and the massage rubbing method is matched, so that the heat rubbing essential oil can be rubbed within the shortest time, and the greatest effect can be exerted.
Description
Technical Field
The invention relates to the technical field of tangerine peel essential oil, in particular to a tangerine peel compound massage essential oil composition and a preparation method and application thereof.
Background
Essential oils refer to the collective term for volatile fragrance-containing substances obtained by processing and extracting from spice plants or spice animals. In general, plant essential oils are volatile aromatic substances extracted from flowers, leaves, roots, seeds, fruits, bark, resins, wood cores and other parts of plants by steam distillation, cold pressing, fat absorption or solvent extraction. The plant essential oils are lipophilic and easily dissolved in grease because the molecular chains of the plant essential oils are generally short, which makes them very permeable to the skin and enter the body through the abundant capillaries under the subcutaneous fat, each plant essential oil has a chemical structure to determine its fragrance, color, fluidity and the way it works with the system, and each plant essential oil has a set of special functional characteristics.
Plant essential oils can be classified into single essential oils and compound essential oils according to their components. The single essential oil is an essential oil extracted from a single plant, and is usually named after the extracted plant name without any addition. For example, the tangerine peel essential oil is the main component of citrus essential oil, has mild stimulation effect on gastrointestinal tract, can promote secretion of digestive juice, remove intestinal qi stagnation, and has the effects of invigorating stomach and dispelling pathogenic wind; it also has expectorant and antiasthmatic effects; in addition, it has certain antioxidant and anti-inflammatory activities. The compound essential oil is formed by mixing more than two kinds of plant essential oil, so that the essential oil and the other essential oil are mutually coordinated, and the curative effect can be enhanced. For example, the combination of the tangerine peel essential oil and the lavender essential oil improves the absorption effect of the tangerine peel essential oil in the skin through the effect of the lavender essential oil.
The massage therapy is an external therapy of traditional Chinese medicine, plays a certain role in the health care rehabilitation therapy of human bodies in the medical industry, and is a popular and wide health care rehabilitation therapy method of human bodies in the world. Massage is to stimulate the body surface, strengthen the circulation of blood and lymph fluid, promote metabolism, strengthen the physiological functions of organs and tissues in the body, and achieve the therapeutic purposes of strengthening the body, caring skin and deferring aging. In the course of massage, essential oil is usually needed to be used to combine with the theory of meridians and collaterals of traditional Chinese medicine, and massage is used to stimulate body surface acupoints, so that the essential oil directly acts on specific acupoints and is absorbed through skin, thereby achieving the purposes of enhancing curative effect and promoting cure of diseases.
In the prior art, CN112353873a discloses a massage essential oil with mint fragrance, which comprises mint essential oil, tea oil, jasmine flower extract, magnolia flower extract, orange peel extract and glycerin, and the essential oil can quickly infiltrate into pores of a human body through the actions of various essential oils and the means of promoting qi and blood circulation of massage. The essential oil needs to be rubbed back and forth in hands or on skin, so that the essential oil can be promoted to better permeate into the skin after rubbing heat, and the essential oil and acupuncture points are massaged to the best effect, but the essential oil composition of the technology needs longer rubbing heat time, and the essential oil is easy to volatilize in the rubbing heat process, so that the essential oil remained on hands or on the skin is little, and the effect of the final essential oil is affected.
Disclosure of Invention
In order to overcome the defects in the prior art, one of the purposes of the invention is to provide a tangerine peel compound massage essential oil composition which solves the above traditional technical problems and can rub hot essential oil in the shortest time so as to exert the maximum effect.
The second purpose of the invention is to provide a preparation method of the tangerine peel compound massage essential oil composition.
The invention further aims to provide a method for applying the tangerine peel compound massage essential oil composition to preparation of massage products.
One of the purposes of the invention is realized by adopting the following technical scheme:
the tangerine peel compound massage essential oil composition comprises the following components in parts by weight:
30-50 parts of plant essential oil; 50-80 parts of ester lubricant; 0.01-0.5 part of heat-rubbing agent, wherein the plant essential oil consists of the following components in percentage by mass: (0.8-1.5): (0.2-0.6): (0.2-0.6) orange peel oil, jojoba seed oil, olive fruit oil, and sweet almond oil.
The invention combines the effects of the ester lubricant and the heat rubbing agent with the plant essential oil such as the orange peel oil, the jojoba seed oil, the olive fruit oil and the sweet almond oil, and combines the manipulation of massage and rubbing to rub the essential oil in the shortest time, so that the essential oil can exert the maximum effect.
Wherein the oil is extracted from pericarpium Citri Tangerinae, and has antioxidant, antiinflammatory, antibacterial, and antiinflammatory effects. The volatile oil content in the tangerine peel is gradually reduced along with the higher year, the flavonoid substances are increased, and the active ingredients are more efficient, so that the tangerine peel is prepared from the tangerine peel for about 3 years to 6 years, and the tangerine peel oil is prepared by combining a wall breaking technology and a molecular film activation orientation technology and through the steps of wall breaking, separation, extraction and concentration. The combination of the wall breaking technology and the molecular film activation orientation technology can keep the activity of each anti-radiation traditional Chinese medicine extract to the maximum extent, improve the content and purity of the active ingredients, convert the substances of the macromolecular groups into the micromolecular groups, directly maximize the effective performance of the active ingredients, enhance the fat solubility of the active ingredients, easily penetrate through the fat film, quickly permeate into human bodies, and facilitate the absorption and utilization of each active ingredient by the human bodies. Wherein the orange peel oil comprises 30-55wt% of hesperidin, 20-40wt% of limonoid, 5-15wt% of gamma-terpinene and the balance of 2-methylamino-methyl benzoate.
Jojoba seed oil is rich in vitamin a, vitamin b, vitamin e, minerals such as calcium, magnesium and the like, has good permeability, can penetrate deep into the skin to soften the skin, has good permeability, so that the jojoba seed oil has permeability and high stability as long as gaps exist. The chemical molecular arrangement of jojoba seed oil is very similar to that of human cortex, is easily absorbed by skin classification, and is suitable for all skin types, especially dry and dark skin types and acne skin types. The skin care product has good air permeability and high temperature resistance, can highly lock water and supplement water, moisten skin, and also can lighten wrinkles and supplement nutrient substances required by the skin, so that the skin care product has very obvious beautifying effect.
Olive oil generally refers to olive pomace oil. The olive residue is obtained by subjecting the rest of olive fruit after all squeezing extraction processes to chemical dissolution treatment. The olive oil residue has the moisturizing effect, and the olive oil can protect eye skin, promote self-care effect of skin around eyes, and make the skin moist and tender.
Sweet almond oil is a relatively soft, lubricating and non-greasy base oil, and has the effects of nourishing, moisturizing, relieving and resisting allergy.
Preferably, the plant essential oil consists of the following components in mass ratio 1: (1-1.2): (0.4-0.6): (0.2-0.4) orange peel oil, jojoba seed oil, olive fruit oil, and sweet almond oil.
Preferably, the ester lubricant consists of the following components in mass ratio 1: (0.5-0.8) ethylhexyl palmitate, caprylic/capric triglyceride.
Among them, ethylhexyl palmitate is an excellent skin softener, has good chemical stability and thermal stability, and can make the skin soft and tender without greasy feeling, and has good permeability. Caprylic/capric triglyceride is a high purity oil and fat esterified from caprylic/capric and glycerol. It is an excellent moisturizing oil, has good spreadability, makes skin have a slippery but not greasy feel, and is easily absorbed by skin. Has good effect on the uniformity and fineness of cosmetics, and can lubricate and shiny skin.
Further preferably, the ester lubricant consists of the following components in mass ratio 1: (0.7-0.8) ethylhexyl palmitate, caprylic/capric triglyceride.
Preferably, the heat-scrubbing agent consists of the following components in mass ratio 1: (1.5-3) vanillyl butyl ether, PEG-40 hydrogenated castor oil.
Wherein, the vanillyl butyl ether is an oil-soluble thermosensitive agent, and can generate rapid and durable pyrogen to local skin, including promoting skin microcirculation, promoting subcutaneous fat metabolism, promoting capillary circulation, etc. The vanillyl butyl ether has several times higher thermal sensation than that of common capsicum extract, has low irritation, can last for several hours, and can generate strong thermal sensation at extremely low dosage. Meanwhile, vanillyl butyl ether is a stable and safe ingredient with a pleasant vanilla taste.
The PEG-40 hydrogenated castor oil contains two parts of hydrophilic groups and hydrophobic groups, and the HLB value of the PEG-40 hydrogenated castor oil is between 14 and 16, and the PEG-40 hydrogenated castor oil is used for wrapping the vanillyl butyl ether so as to reduce the thermal sensation of the vanillyl butyl ether and ensure that the thermal effect of the vanillyl butyl ether is longer in duration.
Preferably, the heat-scrubbing agent consists of the following components in mass ratio 1: (2-3) vanillyl butyl ether, PEG-40 hydrogenated castor oil.
Preferably, the tangerine peel compound massage essential oil composition further comprises the following components in parts by weight: 0.01-0.1 part of heat-rubbing auxiliary agent and heat-rubbing auxiliary agentThe auxiliary agent is nano SiO 2 And (3) particles.
By adding nano SiO 2 Particles, which can rub, improve the rubbing effect, and simultaneously due to nano SiO 2 The particle is 10-30nm, the dosage is small, and other adverse effects on the body are avoided.
The second purpose of the invention is realized by adopting the following technical scheme:
a preparation method of a tangerine peel compound massage essential oil composition comprises the following preparation steps:
s1: uniformly mixing the tangerine peel oil, jojoba seed oil, olive fruit oil and sweet almond oil to obtain plant essential oil;
s2: mixing the components of the ester lubricant uniformly, adding plant essential oil, homogenizing for 10-30min, and dripping a heat-rubbing agent in the process of continuously stirring, and adding within 1-3 min.
Preferably, in step S2, the heat scavenger is prepared by first dripping vanillyl butyl ether into PEG-40 hydrogenated castor oil during stirring to form a wrapper.
The third purpose of the invention is realized by adopting the following technical scheme:
an application of the tangerine peel compound massage essential oil composition in preparing massage products.
Compared with the prior art, the invention has the beneficial effects that:
according to the tangerine peel compound massage essential oil composition, the plant essential oil such as the orange peel oil, the jojoba seed oil, the olive fruit oil and the sweet almond oil is matched with the ester lubricant and the heat rubbing agent, and the massage rubbing method is matched, so that the heat rubbing essential oil can be rubbed within the shortest time, and the greatest effect can be exerted.
Detailed Description
The present invention will be further described with reference to the following specific embodiments, and it should be noted that, on the premise of no conflict, new embodiments may be formed by any combination of the embodiments or technical features described below. In the following examples, raw materials are all outsourced, if not illustrated, wherein the orange peel oil is obtained by combining a wall breaking technology and a molecular film activation orientation technology, and the orange peel oil is prepared from 50wt% of hesperidin, 40wt% of limonoid, 8wt% of gamma-terpinene and 2wt% of 2-methylamino-methyl benzoate.
Example 1
The tangerine peel compound massage essential oil composition comprises the following components in parts by weight:
30 parts of plant essential oil; 60 parts of ester lubricant; 0.1 part of a heat-rubbing agent, wherein the plant essential oil consists of the following components in percentage by mass: 1:0.3:0.5 of orange peel oil, jojoba seed oil, olive fruit oil and sweet almond oil.
The ester lubricant comprises the following components in percentage by mass: 0.6 of ethylhexyl palmitate, caprylic/capric triglyceride.
The heat-rubbing agent comprises the following components in percentage by mass: 1.5, vanillyl butyl ether, PEG-40 hydrogenated castor oil.
The preparation method comprises the following preparation steps:
s1: uniformly mixing the tangerine peel oil, jojoba seed oil, olive fruit oil and sweet almond oil to obtain plant essential oil;
s2: firstly, dripping vanillyl butyl ether into PEG-40 hydrogenated castor oil in the stirring process to form a wrapper;
s3: mixing the components of the ester lubricant uniformly, adding the plant essential oil, homogenizing for 20min, and dripping the heat-rubbing agent in the process of continuously stirring, and finishing the adding within 1 min.
Example 2
The tangerine peel compound massage essential oil composition comprises the following components in parts by weight:
40 parts of plant essential oil; 60 parts of ester lubricant; 0.2 part of a heat-rubbing agent, wherein the plant essential oil consists of the following components in percentage by mass: 1.1:0.4:0.5 of orange peel oil, jojoba seed oil, olive fruit oil and sweet almond oil.
The ester lubricant comprises the following components in percentage by mass: 0.6 of ethylhexyl palmitate, caprylic/capric triglyceride.
The heat-rubbing agent comprises the following components in percentage by mass: 1.5, vanillyl butyl ether, PEG-40 hydrogenated castor oil.
The preparation method comprises the following preparation steps:
s1: uniformly mixing the tangerine peel oil, jojoba seed oil, olive fruit oil and sweet almond oil to obtain plant essential oil;
s2: firstly, dripping vanillyl butyl ether into PEG-40 hydrogenated castor oil in the stirring process to form a wrapper;
s3: mixing the components of the ester lubricant uniformly, adding the plant essential oil, homogenizing for 20min, and dripping the heat-rubbing agent in the process of continuously stirring, and finishing the adding within 1 min.
Example 3
The tangerine peel compound massage essential oil composition comprises the following components in parts by weight:
50 parts of plant essential oil; 80 parts of an ester lubricant; 0.3 part of a heat-rubbing agent, wherein the plant essential oil consists of the following components in percentage by mass: 1.1:0.4:0.5 of orange peel oil, jojoba seed oil, olive fruit oil and sweet almond oil.
The ester lubricant comprises the following components in percentage by mass: 0.8 ethylhexyl palmitate, caprylic/capric triglyceride.
The heat-rubbing agent comprises the following components in percentage by mass: 3, vanillyl butyl ether and PEG-40 hydrogenated castor oil.
The preparation method comprises the following preparation steps:
s1: uniformly mixing the tangerine peel oil, jojoba seed oil, olive fruit oil and sweet almond oil to obtain plant essential oil;
s2: firstly, dripping vanillyl butyl ether into PEG-40 hydrogenated castor oil in the stirring process to form a wrapper;
s3: mixing the components of the ester lubricant uniformly, adding the plant essential oil, homogenizing for 30min, and dripping the heat-rubbing agent in the process of continuously stirring, and finishing the adding within 2 min.
Example 4
The tangerine peel compound massage essential oil composition comprises the following components in parts by weight:
30 parts of plant essential oil; 70 parts of ester lubricant; 0.2 part of a heat-rubbing agent, wherein the plant essential oil consists of the following components in percentage by mass: 1:0.5:0.5 of orange peel oil, jojoba seed oil, olive fruit oil and sweet almond oil.
The ester lubricant comprises the following components in percentage by mass: 3, caprylic/capric triglyceride.
The heat-rubbing agent comprises the following components in percentage by mass: 2, vanillyl butyl ether, PEG-40 hydrogenated castor oil.
The preparation method comprises the following preparation steps:
s1: uniformly mixing the tangerine peel oil, jojoba seed oil, olive fruit oil and sweet almond oil to obtain plant essential oil;
s2: firstly, dripping vanillyl butyl ether into PEG-40 hydrogenated castor oil in the stirring process to form a wrapper;
s3: mixing the components of the ester lubricant uniformly, adding the plant essential oil, homogenizing for 20min, and dripping the heat-rubbing agent in the process of continuously stirring, and finishing the adding within 1 min.
Example 5
The tangerine peel compound massage essential oil composition comprises the following components in parts by weight:
30 parts of plant essential oil; 70 parts of ester lubricant; 0.2 part of heat-rubbing agent and nano SiO 2 0.05 parts of particles; wherein, the plant essential oil consists of the following components in percentage by mass: 1:0.5:0.5 of orange peel oil, jojoba seed oil, olive fruit oil and sweet almond oil.
The ester lubricant comprises the following components in percentage by mass: 3, caprylic/capric triglyceride.
The heat-rubbing agent comprises the following components in percentage by mass: 2, vanillyl butyl ether, PEG-40 hydrogenated castor oil.
The preparation method comprises the following preparation steps:
s1: uniformly mixing the tangerine peel oil, jojoba seed oil, olive fruit oil and sweet almond oil to obtain plant essential oil;
s2: firstly, dripping vanillyl butyl ether into PEG-40 hydrogenated castor oil in the stirring process to form a wrapper;
s3: mixing the components of the ester lubricant uniformly, adding plant essential oil, homogenizing for 20min, and adding nano SiO 2 And (3) uniformly stirring the particles, then dripping a heat-rubbing agent in the process of continuously stirring, and finishing the adding within 2 minutes.
Comparative example 1
The tangerine peel essential oil composition comprises the following components in parts by weight:
1 part of tangerine peel oil, 1 part of jojoba seed oil, 0.3 part of olive fruit oil and 0.5 part of sweet almond oil.
Performance testing
(1) Thermal performance testing
The compositions of comparative example 1 and examples 1-5 were subjected to thermal performance testing.
Test object: 60 women with healthy skin were selected and equally divided into 6 groups of 10, group 1 using the composition of example 1, group 2 using the composition of example 2, group 3 using the composition of example 3, group 4 using the composition of example 4, group 5 using the composition of example 5, and group 6 using the composition of comparative example 1.
The test method comprises the following steps: after the skin of the face of the subject is cleaned, 1ml of the corresponding slave product is firstly taken and then is smeared on the skin of the back, and the hands are rubbed gently and backwards for 2min, and the feelings of the subject after being smeared for 1min, 5min and 10min are recorded respectively.
Evaluation criteria: a score of 1-3 represents no heat or slightly heat, but not significant; a score of 4-7 represents a clear perceived sensation of heat, but no stimulus, acceptable; a score of 8-10 indicates that the heat sensation is too strong to be acceptable. Average scores of each subject were taken.
The test results are shown in Table 1 below.
TABLE 1
| Project | Feeling after 1min | Feeling after 5min | Feel after 10min |
| Comparative example 1 | 4.5 | 2.5 | 1.5 |
| Example 1 | 6.2 | 5.6 | 4.5 |
| Example 2 | 6.5 | 5.8 | 4.8 |
| Example 3 | 6.5 | 6.0 | 4.8 |
| Example 4 | 6.6 | 5.9 | 5.0 |
| Example 5 | 6.8 | 6.5 | 5.6 |
(2) Application testing
The compositions of comparative example 1 and example 1 were subjected to an anti-aging test, the test index being skin elasticity.
The experimental method comprises the following steps: the group of healthy, normal skin, non-cosmetic allergy history subjects was selected, aged 20-45 years, 10 men and 10 women in each group, for a total of 2 groups. One week is a treatment course, four treatment courses are taken, the face is cleaned before each use, the time for cleaning the face is the same each time, the corresponding products are used after the skin is dried, each group uses the corresponding products 1 time a day, 1ml of the products are uniformly smeared on the face, and the massage is carried out for 5 minutes.
Measurement: the cheek portion was selected as the test area and the test was performed after 10 minutes of product use. Skin elasticity curves were measured using a skin elasticity tester, and the anti-aging function was evaluated based on the stretching amount and rebound resilience data of the skin.
Experimental results: the skin elasticity test is based on the suction and stretching principle, negative pressure is generated on the surface of the skin to be tested, the skin is sucked into a special test probe, the sucked depth of the skin is measured by a non-contact optical detection system, the measurement result is usually expressed by an index, the unit is 1, and the larger the value is, the stronger the skin elasticity is indicated.
The test results are shown in table 2 below.
TABLE 2
| Project | 0 week | For 1 week | For 2 weeks |
| Comparative example 1 | 0.365 | 0.452 | 0.536 |
| Example 1 | 0.352 | 0.593 | 0.782 |
The above embodiments are only preferred embodiments of the present invention, and the scope of the present invention is not limited thereto, but any insubstantial changes and substitutions made by those skilled in the art on the basis of the present invention are intended to be within the scope of the present invention as claimed.
Claims (10)
1. The tangerine peel compound massage essential oil composition is characterized by comprising the following components in parts by weight:
30-50 parts of plant essential oil; 50-80 parts of ester lubricant; 0.01-0.5 part of heat-rubbing agent, wherein the plant essential oil consists of the following components in percentage by mass: (0.8-1.5): (0.2-0.6): (0.2-0.6) orange peel oil, jojoba seed oil, olive fruit oil, and sweet almond oil.
2. The citrus peel compound essential oil composition of claim 1, wherein the citrus peel oil is composed of 30-55wt% of hesperidin, 20-40wt% of limonoid, 5-15wt% of gamma-terpinene, and the balance being 2-methylamino-methyl benzoate.
3. The tangerine peel compound massage essential oil composition according to claim 1, wherein the plant essential oil comprises the following components in mass ratio 1: (1-1.2): (0.4-0.6): (0.2-0.4) orange peel oil, jojoba seed oil, olive fruit oil, and sweet almond oil.
4. The tangerine peel compound massage essential oil composition according to claim 1, wherein the ester lubricant comprises the following components in mass ratio 1: (0.5-0.8) ethylhexyl palmitate, caprylic/capric triglyceride.
5. The tangerine peel compound massage essential oil composition according to claim 4, wherein the ester lubricant comprises the following components in mass ratio 1: (0.7-0.8) ethylhexyl palmitate, caprylic/capric triglyceride.
6. The tangerine peel compound massage essential oil composition according to claim 1, wherein the heat-dissipating agent comprises the following components in mass ratio 1: (1.5-3) vanillyl butyl ether, PEG-40 hydrogenated castor oil.
7. The tangerine peel compound massage essential oil composition according to claim 6, wherein the heat-dissipating agent comprises the following components in mass ratio 1: (2-3) vanillyl butyl ether, PEG-40 hydrogenated castor oil.
8. The tangerine peel compound massage essential oil composition according to claim 1, wherein the tangerine peel compound massage essential oil composition further comprises the following components in parts by weight: 0.01-0.1 part of heat-rubbing auxiliary agent which is nano SiO 2 And (3) particles.
9. The preparation method of the tangerine peel compound massage essential oil composition is characterized by comprising the following preparation steps:
s1: uniformly mixing the tangerine peel oil, jojoba seed oil, olive fruit oil and sweet almond oil to obtain plant essential oil;
s2: mixing the components of the ester lubricant uniformly, adding plant essential oil, homogenizing for 10-30min, and dripping a heat-rubbing agent in the process of continuously stirring, and adding within 1-3 min.
10. An application is characterized in that the tangerine peel compound massage essential oil composition in claims 1-8 is applied to the preparation of massage products.
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