CN116114715A - Low-temperature quaternary ammonium salt disinfectant for livestock and preparation method thereof - Google Patents
Low-temperature quaternary ammonium salt disinfectant for livestock and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
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- A01N31/02—Acyclic compounds
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- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
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- A01P—BIOCIDAL, PEST REPELLANT, PEST ATTRACTANT OR PLANT GROWTH REGULATORY ACTIVITY OF CHEMICAL COMPOUNDS OR PREPARATIONS
- A01P1/00—Disinfectants; Antimicrobial compounds or mixtures thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/014—Deodorant compositions containing sorbent material, e.g. activated carbon
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- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
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- B01D53/34—Chemical or biological purification of waste gases
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- A61L2101/00—Chemical composition of materials used in disinfecting, sterilising or deodorising
- A61L2101/02—Inorganic materials
- A61L2101/24—Inorganic materials containing aluminium
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Abstract
The invention relates to the technical field of disinfectants, and discloses a low-temperature quaternary ammonium salt disinfectant for livestock and a preparation method thereof, wherein the low-temperature quaternary ammonium salt disinfectant comprises quaternary ammonium salt disinfectants, mugwort leaves, wild chrysanthemum, garlic, radix bupleuri, deodorant, antifreeze, 70% ethanol and water, and the low-temperature quaternary ammonium salt disinfectant comprises the following components in parts by weight: the quaternary ammonium salt disinfectant is 30-50 parts, the mugwort leaf is 5-10 parts, the wild chrysanthemum is 3-5 parts, the garlic is 6-15 parts, the bupleurum is 4-9 parts, the deodorant is 5-12 parts, the antifreeze is 2-5 parts, the 70% ethanol is 10-20 parts, and the balance is water.
Description
Technical Field
The invention relates to the technical field of disinfectants, in particular to a low-temperature quaternary ammonium salt disinfectant for livestock and a preparation method thereof.
Background
The low-temperature quaternary ammonium salt disinfectant is used for effectively disinfecting products in a low-temperature environment as the name implies. The quaternary ammonium salt disinfectant belongs to cationic surfactant and has the functions of sterilizing and decontaminating. Such disinfectants can alter the permeability of bacterial cell membranes because quaternary ammonium disinfectants are positively charged, while bacterial surfaces are negatively charged, thereby altering the permeability of cell walls, cell membranes. The existing disinfectant is easy to freeze and lose efficacy under the condition of low temperature, cannot efficiently play a role in disinfection, has low disinfection rate, has insufficient disinfection safety coefficient and heavier smell, and is harmful to physical and mental health of human bodies or animals. For this purpose, a corresponding technical solution needs to be designed to solve.
Disclosure of Invention
(one) solving the technical problems
Aiming at the defects of the prior art, the invention provides a veterinary low-temperature quaternary ammonium salt disinfectant and a preparation method thereof, which solve the technical problems that the disinfectant is easy to freeze and solidify and is invalid under the low temperature condition, cannot efficiently play a role in disinfection, has low disinfection rate, has insufficient disinfection safety coefficient, has heavy smell and is harmful to the physical and mental health of human bodies or animals.
(II) technical scheme
In order to achieve the above purpose, the invention is realized by the following technical scheme: a veterinary low-temperature quaternary ammonium salt disinfectant and a preparation method thereof, wherein the veterinary low-temperature quaternary ammonium salt disinfectant comprises quaternary ammonium salt disinfectant, mugwort leaf, wild chrysanthemum, garlic, radix bupleuri, deodorant, antifreeze, 70% ethanol and water, and the veterinary low-temperature quaternary ammonium salt disinfectant comprises the following components in percentage by weight: the quaternary ammonium salt disinfectant is prepared from 30-50 parts by weight, 5-10 parts by weight of mugwort leaf, 3-5 parts by weight of wild chrysanthemum flower, 6-15 parts by weight of garlic, 4-9 parts by weight of bupleurum root, 5-12 parts by weight of deodorant, 2-5 parts by weight of antifreeze solution, 10-20 parts by weight of 70% ethanol and the balance of water.
Preferably, the quaternary ammonium salt disinfectant is one or a mixture of a single quaternary ammonium salt component disinfectant, a plurality of quaternary ammonium salt compound disinfectants and isopropanol compound disinfectants.
Preferably, the deodorant is porous ore powder, and specifically is one or a mixture of a plurality of fine zeolite powder, attapulgite powder and coal ash.
Preferably, the antifreeze fluid consists of ethylene glycol, alcohol, disodium hydrogen phosphate, glycerol and water.
Preferably, the disinfectant comprises quaternary ammonium salt disinfectant, mugwort leaf, wild chrysanthemum flower, garlic, bupleurum, deodorant, antifreeze, 70% ethanol and water, wherein the components are prepared according to the weight ratio: the quaternary ammonium salt disinfectant is 50 parts, the mugwort leaf is 10 parts, the wild chrysanthemum is 5 parts, the garlic is 15 parts, the bupleurum is 9 parts, the deodorant is 5 parts, the antifreeze is 2 parts, the 70% ethanol is 10 parts, and the balance is water.
Preferably, the disinfectant comprises quaternary ammonium salt disinfectant, mugwort leaf, wild chrysanthemum flower, garlic, bupleurum, deodorant, antifreeze, 70% ethanol and water, wherein the components are prepared according to the weight ratio: the quaternary ammonium salt disinfectant is 30 parts, the mugwort leaf is 5 parts, the wild chrysanthemum is 3 parts, the garlic is 6 parts, the bupleurum is 4 parts, the deodorant is 12 parts, the antifreeze is 5 parts, the 70% ethanol is 20 parts, and the balance is water.
Preferably, the preparation steps include the following:
s1, firstly, cleaning different parts of Chinese patent medicines of mugwort leaf, wild chrysanthemum, garlic and bupleurum, and then placing the Chinese patent medicines into a pulverizer to pulverize the Chinese patent medicines into powder;
s2, placing the Chinese patent medicine powder in a stirring tank, sequentially adding quaternary ammonium salt disinfectant, deodorant, antifreeze, 70% ethanol and water, starting a driving motor above the stirring tank, and automatically mixing and stirring the disinfectant mixed solution;
and S3, continuously stirring until all the components are dissolved, and thus obtaining the low-temperature quaternary ammonium salt disinfectant.
Preferably, in the step S2, the stirring rotation speed is controlled to be 60-100 r/min, the time is controlled to be 20-50 min, the temperature is controlled to be 10-25 ℃, and the stirring and mixing of the disinfectant can be carried out by adjusting different rotation speeds, time and temperatures according to the needs, so that the design is reasonable.
(III) beneficial effects
Compared with the common disinfectant, the low-temperature quaternary ammonium salt disinfectant can not freeze, solidify and lose efficacy in the subzero environment, always keep liquid state, can spray and disinfect, effectively kill escherichia coli, staphylococcus aureus and the like, has the sterilization rate of 99.99 percent, adopts various Chinese patent medicine formulas, improves the safety of the disinfectant, has no peculiar smell, avoids endangering the physical and mental health of animals, and has good sterilization effect.
Drawings
FIG. 1 is a schematic diagram of a step frame of the present invention.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Referring to fig. 1, the embodiment of the invention provides a technical scheme: a veterinary low-temperature quaternary ammonium salt disinfectant and a preparation method thereof, wherein the veterinary low-temperature quaternary ammonium salt disinfectant comprises quaternary ammonium salt disinfectant, mugwort leaf, wild chrysanthemum, garlic, radix bupleuri, deodorant, antifreeze, 70% ethanol and water, and the veterinary low-temperature quaternary ammonium salt disinfectant comprises the following components in percentage by weight: the quaternary ammonium salt disinfectant is prepared from 30-50 parts by weight, 5-10 parts by weight of mugwort leaf, 3-5 parts by weight of wild chrysanthemum flower, 6-15 parts by weight of garlic, 4-9 parts by weight of bupleurum root, 5-12 parts by weight of deodorant, 2-5 parts by weight of antifreeze solution, 10-20 parts by weight of 70% ethanol and the balance of water.
Further improved, the quaternary ammonium salt disinfectant is one or a mixture of a single quaternary ammonium salt disinfectant, a plurality of quaternary ammonium salt composite disinfectants and isopropanol composite disinfectants.
The deodorant is porous ore powder, specifically one or a mixture of a plurality of fine zeolite powder, attapulgite powder and coal ash, can be used in a production area where peculiar smell possibly appears in an animal living environment, does not need flushing after disinfection, has strong adsorptivity, has the functions of fine zeolite powder, attapulgite powder and coal ash, and has good decomposition and removal effects on malodor such as ammonia, hydrogen sulfide and the like in order to prevent the malodor of livestock and poultry feces from polluting the environment.
Further improved, the antifreeze fluid consists of glycol, alcohol, disodium hydrogen phosphate, glycerin and water, wherein the glycol is easy to generate acidic substances in use, corrodes metals, and an appropriate amount of disodium hydrogen phosphate and the like are needed to be added for corrosion prevention, so that the antifreeze fluid has a high boiling point and can not generate steam to be inhaled into a human body to cause poisoning.
Further improved, the disinfectant comprises quaternary ammonium salt disinfectant, mugwort leaf, wild chrysanthemum flower, garlic, bupleurum, deodorant, antifreeze, 70% ethanol and water, wherein the components are prepared according to the weight ratio: the quaternary ammonium salt disinfectant is 50 parts, the mugwort leaf is 10 parts, the wild chrysanthemum is 5 parts, the garlic is 15 parts, the bupleurum is 9 parts, the deodorant is 5 parts, the antifreeze is 2 parts, the 70% ethanol is 10 parts, and the balance is water.
Further improved, the disinfectant comprises quaternary ammonium salt disinfectant, mugwort leaf, wild chrysanthemum flower, garlic, bupleurum, deodorant, antifreeze, 70% ethanol and water, wherein the components are prepared according to the weight ratio: the quaternary ammonium salt disinfectant is 30 parts, the mugwort leaf is 5 parts, the wild chrysanthemum is 3 parts, the garlic is 6 parts, the bupleurum is 4 parts, the deodorant is 12 parts, the antifreeze is 5 parts, the 70% ethanol is 20 parts, and the balance is water.
Further improved, the preparation steps comprise the following steps:
s1, firstly, cleaning different parts of Chinese patent medicines of mugwort leaf, wild chrysanthemum, garlic and bupleurum, and then placing the Chinese patent medicines into a pulverizer to pulverize the Chinese patent medicines into powder;
s2, placing the Chinese patent medicine powder in a stirring tank, sequentially adding quaternary ammonium salt disinfectant, deodorant, antifreeze, 70% ethanol and water, starting a driving motor above the stirring tank, and automatically mixing and stirring the disinfectant mixed solution;
and S3, continuously stirring until all the components are dissolved, and thus obtaining the low-temperature quaternary ammonium salt disinfectant.
In the step S2, the stirring rotation speed is controlled to be 60-100 r/min, the stirring time is controlled to be 20-50 min, the stirring temperature is controlled to be 10-25 ℃, and the stirring and mixing of the disinfectant can be carried out by adjusting different rotation speeds, time and temperatures according to the needs, so that the design is reasonable.
Example 1
The embodiment of the invention provides a technical scheme that: a veterinary low-temperature quaternary ammonium salt disinfectant and a preparation method thereof, wherein the veterinary low-temperature quaternary ammonium salt disinfectant comprises quaternary ammonium salt disinfectant, mugwort leaf, wild chrysanthemum, garlic, radix bupleuri, deodorant, antifreeze, 70% ethanol and water, and the veterinary low-temperature quaternary ammonium salt disinfectant comprises the following components in percentage by weight: the quaternary ammonium salt disinfectant is 50 parts, the mugwort leaf is 10 parts, the wild chrysanthemum is 5 parts, the garlic is 15 parts, the bupleurum is 9 parts, the deodorant is 5 parts, the antifreeze is 2 parts, the 70% ethanol is 10 parts, and the balance is water.
Example 2
The embodiment of the invention provides a technical scheme that: a veterinary low-temperature quaternary ammonium salt disinfectant and a preparation method thereof, wherein the veterinary low-temperature quaternary ammonium salt disinfectant comprises quaternary ammonium salt disinfectant, mugwort leaf, wild chrysanthemum, garlic, radix bupleuri, deodorant, antifreeze, 70% ethanol and water, and the veterinary low-temperature quaternary ammonium salt disinfectant comprises the following components in percentage by weight: the quaternary ammonium salt disinfectant is 30 parts, the mugwort leaf is 5 parts, the wild chrysanthemum is 3 parts, the garlic is 6 parts, the bupleurum is 4 parts, the deodorant is 12 parts, the antifreeze is 5 parts, the 70% ethanol is 20 parts, and the balance is water
Virus and disinfectant mixing experiments
Example 1
Uniformly mixing virus and disinfectant according to equal volume, reacting at-20deg.C for 10min, adding neutralizing agent, reacting at room temperature for 10min, adding cell maintenance solution, setting neutralizing agent control group, culturing in 37 deg.C and 5% CO2 incubator, observing cell state and fluorescence generated by virus replication every 24 hr, and observing 96 hr later to obtain statistical test result.
Example 2
Uniformly mixing virus and disinfectant according to equal volume, reacting at-40deg.C for 20min, adding neutralizing agent, reacting at room temperature for 10min, adding cell maintenance solution, setting neutralizing agent control group, culturing in 37 deg.C and 5% CO2 incubator, observing cell state and fluorescence generated by virus replication every 24h, and observing 96h later to obtain statistical test result.
Example 3
Uniformly mixing virus and disinfectant according to equal volume, reacting for 15min at-50deg.C, adding neutralizing agent, reacting at room temperature for 10min, adding cell maintenance solution, setting neutralizing agent control group, culturing in 37 deg.C and 5% CO2 incubator, observing cell state and fluorescence generated by virus replication every 24h, and counting test result after 96 h.
Overview: the low-temperature quaternary ammonium salt disinfectant for animals is very stable in low-temperature conditions, can still have excellent sterilization effect at the low temperature of 50 ℃ below zero, and has strong adaptability to low temperature and good sterilization effect.
The components of the invention are all universal standard components or components known by the technicians in the field, the structure and principle of the components are known by the technicians through technical manuals or known by conventional experimental methods, the problems that the components are easy to freeze and solidify and lose effectiveness under the low temperature condition, the disinfection effect cannot be effectively achieved, the disinfection rate is low, the disinfection safety coefficient is insufficient, the smell is heavy, the physical and psychological health of human bodies or animals is endangered, and compared with the common disinfection solution, the low-temperature quaternary ammonium salt disinfection solution can not freeze, solidify and lose effectiveness in the subzero environment, always keep the liquid state, can spray for disinfection, effectively kills escherichia coli, staphylococcus aureus and the like, the disinfection rate also can reach 99.99%, and the adoption of various Chinese patent medicine methods improves the safety of the disinfectant, has no peculiar smell, avoids the physical and psychological health of animals, and has good disinfection effect.
While the fundamental and principal features of the invention and advantages of the invention have been shown and described, it will be apparent to those skilled in the art that the invention is not limited to the details of the foregoing exemplary embodiments, but may be embodied in other specific forms without departing from the spirit or essential characteristics thereof. The present embodiments are, therefore, to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Furthermore, it should be understood that although the present disclosure describes embodiments, not every embodiment is provided with a separate embodiment, and that this description is provided for clarity only, and that the disclosure is not limited to the embodiments described in detail below, and that the embodiments described in the examples may be combined as appropriate to form other embodiments that will be apparent to those skilled in the art.
Claims (8)
1. A low-temperature quaternary ammonium salt disinfectant for animals is characterized in that: comprises quaternary ammonium salt disinfectant, mugwort leaf, wild chrysanthemum, garlic, bupleurum, deodorant, antifreeze, 70% ethanol and water, wherein the components are mixed according to the weight proportion: the quaternary ammonium salt disinfectant is prepared from 30-50 parts by weight, 5-10 parts by weight of mugwort leaf, 3-5 parts by weight of wild chrysanthemum flower, 6-15 parts by weight of garlic, 4-9 parts by weight of bupleurum root, 5-12 parts by weight of deodorant, 2-5 parts by weight of antifreeze solution, 10-20 parts by weight of 70% ethanol and the balance of water.
2. A veterinary low temperature quaternary ammonium salt disinfectant as set forth in claim 1, wherein: the quaternary ammonium salt disinfectant is one or a mixture of a single quaternary ammonium salt disinfectant, a plurality of quaternary ammonium salt composite disinfectants and isopropanol composite disinfectants.
3. A veterinary low temperature quaternary ammonium salt disinfectant as set forth in claim 1, wherein: the deodorant is porous ore powder, and is one or more of fine zeolite powder, attapulgite powder and coal ash.
4. The low-temperature quaternary ammonium salt disinfectant for animals and a preparation method thereof as set forth in claim 1, wherein: the antifreezing solution consists of ethylene glycol, alcohol, disodium hydrogen phosphate, glycerol and water.
5. The low-temperature quaternary ammonium salt disinfectant for animals and a preparation method thereof as set forth in claim 1, wherein: comprises quaternary ammonium salt disinfectant, mugwort leaf, wild chrysanthemum, garlic, bupleurum, deodorant, antifreeze, 70% ethanol and water, wherein the components are mixed according to the weight proportion: the quaternary ammonium salt disinfectant is 50 parts, the mugwort leaf is 10 parts, the wild chrysanthemum is 5 parts, the garlic is 15 parts, the bupleurum is 9 parts, the deodorant is 5 parts, the antifreeze is 2 parts, the 70% ethanol is 10 parts, and the balance is water.
6. The low-temperature quaternary ammonium salt disinfectant for animals and a preparation method thereof as set forth in claim 1, wherein: comprises quaternary ammonium salt disinfectant, mugwort leaf, wild chrysanthemum, garlic, bupleurum, deodorant, antifreeze, 70% ethanol and water, wherein the components are mixed according to the weight proportion: the quaternary ammonium salt disinfectant is 30 parts, the mugwort leaf is 5 parts, the wild chrysanthemum is 3 parts, the garlic is 6 parts, the bupleurum is 4 parts, the deodorant is 12 parts, the antifreeze is 5 parts, the 70% ethanol is 20 parts, and the balance is water.
7. The method for preparing the low-temperature quaternary ammonium salt disinfectant for animals according to claim 1, wherein the preparation steps comprise the following steps:
s1, firstly, cleaning different parts of Chinese patent medicines of mugwort leaf, wild chrysanthemum, garlic and bupleurum, and then placing the Chinese patent medicines into a pulverizer to pulverize the Chinese patent medicines into powder;
s2, placing the Chinese patent medicine powder in a stirring tank, sequentially adding quaternary ammonium salt disinfectant, deodorant, antifreeze, 70% ethanol and water, starting a driving motor above the stirring tank, and automatically mixing and stirring the disinfectant mixed solution;
and S3, continuously stirring until all the components are dissolved, and thus obtaining the low-temperature quaternary ammonium salt disinfectant.
8. The method for preparing the low-temperature quaternary ammonium salt disinfectant for animals according to claim 7, wherein the method comprises the following steps: in the step S2, the stirring rotation speed is controlled to be 60-100 r/min, the time is controlled to be 20-50 min, and the temperature is controlled to be 10-25 ℃.
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| CN113383775A (en) * | 2021-07-19 | 2021-09-14 | 广东环凯生物技术有限公司 | Compound quaternary ammonium salt low-temperature disinfectant and preparation method thereof |
| CN113396906A (en) * | 2021-06-28 | 2021-09-17 | 白燕波 | Composite quaternary ammonium salt low-temperature disinfectant and preparation method thereof |
| CN113519518A (en) * | 2021-06-16 | 2021-10-22 | 浙江施维康生物医学材料有限公司 | Low-temperature disinfectant |
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| CN106234458A (en) * | 2016-08-20 | 2016-12-21 | 裕龙农牧科技股份有限公司 | A kind of pig farm compound Chinese herb disinfectant |
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