CN107158353A - A kind of Chinese herbal disinfectant and preparation method thereof - Google Patents
A kind of Chinese herbal disinfectant and preparation method thereof Download PDFInfo
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- CN107158353A CN107158353A CN201710563327.3A CN201710563327A CN107158353A CN 107158353 A CN107158353 A CN 107158353A CN 201710563327 A CN201710563327 A CN 201710563327A CN 107158353 A CN107158353 A CN 107158353A
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/284—Atractylodes
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- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/30—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
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- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/12—Quaternary ammonium compounds
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Abstract
The invention discloses a kind of Chinese herbal disinfectant, include the raw material of following parts by weight：3~8 parts of rhizoma atractylodis, 8~12 parts of radix scutellariae, 8~20 parts of honeysuckle, 7~13 parts of kuh-seng, 12~18 parts of cloves, 5~15 parts of barberry, 15~25 parts of peppermint, 2~10 parts of felwort, 5~10 parts of manyleaf meadowure rhizome and root, 3~7 parts of Herba Andrographitis, 8~17 parts of Radix Isatidis, 10~20 parts of ginkgo leaf, 8~15 parts of tangerine peel, 2~5 parts of the fruit of glossy privet, 6~13 parts of garlic, 7~16 parts of ginger, 13~25 parts of chitosan, 7~15 parts of organic boronic, 10~30 parts of modified montmorillonoid, 3~8 parts of quaternary ammonium salt.The Chinese herbal disinfectant low toxicity, low irritant, smell are small, corrosivity is small and high with disinfection efficiency, the advantage of wide sterilization spectrum, are adapted to promote.
Description
Technical field
The invention belongs to disinfectant technical field, and in particular to a kind of Chinese herbal disinfectant and preparation method thereof.
Background technology
With developing rapidly for intensive culture industry, livestock and poultry and its surrounding environment are carried out disinfection using disinfectant to kill
Pathogen, cuts off the routes of infection, it has also become prevention and a kind of important measures of control livestock and poultry disease transmission.But often make at present
Disinfectant such as bleaching powder, sodium hypochlorite, peroxide, phenols, formaldehyde etc. have the shortcomings that some are common, such as stability
Difference, corrosivity are strong, have very strong and stimulating etc., and what is had is also harmful, or even has carcinogenesis.
The content of the invention
The invention provides a kind of Chinese herbal disinfectant and preparation method thereof, the problem of solving in above-mentioned background technology,
The Chinese herbal disinfectant safety non-toxic, noresidue, work fast, property are stable and high with disinfection efficiency, fungicidal spectrum
Wide advantage, is adapted to promote.
In order to solve the problem of prior art is present, adopt the following technical scheme that：
A kind of Chinese herbal disinfectant, includes the raw material of following parts by weight：3~8 parts of rhizoma atractylodis, 8~12 parts of radix scutellariae, honeysuckle 8~20
Part, 7~13 parts of kuh-seng, 12~18 parts of cloves, 5~15 parts of barberry, 15~25 parts of peppermint, 2~10 parts of felwort, manyleaf meadowure rhizome and root 5
~10 parts, it is 3~7 parts of Herba Andrographitis, 8~17 parts of Radix Isatidis, 10~20 parts of ginkgo leaf, 8~15 parts of tangerine peel, 2~5 parts of the fruit of glossy privet, big
6~13 parts of garlic, 7~16 parts of ginger, 13~25 parts of chitosan, 7~15 parts of organic boronic, 10~30 parts of modified montmorillonoid, quaternary ammonium
3~8 parts of salt.
It is preferred that, the Chinese herbal disinfectant includes the raw material of following parts by weight：4~7 parts of rhizoma atractylodis, 9~11 parts of radix scutellariae,
13~17 parts of honeysuckle, 9~12 parts of kuh-seng, 14~16 parts of cloves, 8~12 parts of barberry, 19~24 parts of peppermint, felwort 4~6
Part, 7~9 parts of manyleaf meadowure rhizome and root, 4~6 parts of Herba Andrographitis, 10~15 parts of Radix Isatidis, 11~17 parts of ginkgo leaf, 11~14 parts of tangerine peel, glossy privet
3~4 parts of son, 8~12 parts of garlic, 9~14 parts of ginger, 16~23 parts of chitosan, 9~12 parts of organic boronic, modified montmorillonoid 15
~28 parts, 4~7 parts of quaternary ammonium salt.
It is preferred that, the Chinese herbal disinfectant includes the raw material of following parts by weight：5 parts of rhizoma atractylodis, 10 parts of radix scutellariae, honeysuckle
14 parts, 11 parts of kuh-seng, 15 parts of cloves, 9 parts of barberry, 23 parts of peppermint, 5 parts of felwort, 8 parts of manyleaf meadowure rhizome and root, 5 parts of Herba Andrographitis, plate it is blue
14 parts of root, 13 parts of ginkgo leaf, 12 parts of tangerine peel, 3.5 parts of the fruit of glossy privet, 11 parts of garlic, 13 parts of ginger, 19 parts of chitosan, organic boronic
11 parts, 22 parts of modified montmorillonoid, 6 parts of quaternary ammonium salt.
It is preferred that, the modified montmorillonoid is made by following methods：By montmorillonite be crushed to granular size to particle diameter≤
1mm, is then immersed into clear water, and 15~25min is stirred with electric blender, and speed setting is 350~450r/min, then mistake
Solute is immersed into dilute mineral acid solution water-bath and is heat-treated 1~2h by filter, and temperature is set between 75~85 DEG C, then to after acidifying
Suspension in add dispersant sodium pyrophosphate and be sufficiently stirred for, collaboration supersonic, water-heating method is handled after 2~3h, finally it is carried out from
Heart processing, after centrifugation, takes upper strata suspension to be transported to 1~2h of roasting in swinging drying oven after filtering, drying,
Sintering temperature is 280~400 DEG C.
It is preferred that, the quaternary ammonium salt is benzalkonium bromide or benzalkonium chloride.
A kind of method for preparing the Chinese herbal disinfectant, comprises the following steps：
（1）Rhizoma atractylodis, radix scutellariae are weighed by above-mentioned formula, honeysuckle, kuh-seng, cloves, barberry, peppermint, felwort, manyleaf meadowure rhizome and root, worn
Heart lotus, Radix Isatidis, ginkgo leaf, tangerine peel, the fruit of glossy privet, garlic, ginger, chitosan, organic boronic, modified montmorillonoid, quaternary ammonium salt, it is standby
With；
（2）By rhizoma atractylodis, radix scutellariae, honeysuckle, kuh-seng, cloves, barberry, peppermint, felwort, manyleaf meadowure rhizome and root, Herba Andrographitis, Radix Isatidis,
Ginkgo leaf, tangerine peel, the fruit of glossy privet, garlic, ginger are crushed respectively, are well mixed, are obtained Traditional Chinese drug mixture；
（3）By step（2）The Traditional Chinese drug mixture obtained is added water to cook 1~3 time, and 1~2h is boiled every time, volatile oil and decoction is collected
Liquid, merges decoction liquor, and filtering stands 24h, and Aspirate supernatant, filtering adds chitosan, is uniformly mixed, obtains mixed liquor A；
（4）Quaternary ammonium salt is put into after emulsion tank emulsification, with step（3）The mixed liquor A of gained is well mixed, and adds modified cover
De- soil and step（3）Obtained volatile oil, is put into high speed dispersor and disperses 20~30min, adds organic boronic, and stirring mixing is equal
It is even, obtain mixed liquid B；
（5）After mixed liquid B filtering or centrifugal dehydration, filter residue is dried at less than 80 DEG C, uses airslide disintegrating mill dry pulverization process, or
Mixed liquid B is spray-dried to water content ＜ 10%, produce the Chinese herbal disinfectant.
It is preferred that, the step（3）In to add water to cook amount of water be 4~8 times of Traditional Chinese drug mixture weight.
It is preferred that, the step（4）The scattered speed of high speed is 1700~2200r/min.
Compared with prior art, it has the advantages that the present invention：
Acted synergistically between each raw material of Chinese herbal disinfectant of the present invention, the disinfectant of preparation has wide sterilization spectrum, effect effect
Insist on long, the anti-resistance to the action of a drug, production cost it is low, using it is safe the advantages of, and have the function of environment deodorization concurrently, can effectively improve foster
The economic benefit of industry is grown, it is specific as follows：
（1）Chinese herbal disinfectant of the present invention using the present invention be combined with rhizoma atractylodis, radix scutellariae, honeysuckle, kuh-seng, cloves, three
Pin, peppermint, felwort, manyleaf meadowure rhizome and root, Herba Andrographitis, Radix Isatidis, ginkgo leaf, tangerine peel, the fruit of glossy privet, garlic, ginger plurality of Chinese conduct
Raw material, collocation is reasonable, resists with good（Suppression）Bacterium function, has to staphylococcus aureus, Escherichia coli, Salmonella
Good bactericidal effect, prevents many advantages, such as microorganism produces resistance, and drug residue free, non-stimulated, environmental protection, is applicable
In plant；
（2）Chinese herbal disinfectant of the present invention also added quarternary ammonium salt compound as raw material, and quarternary ammonium salt compound is both to disappear
Toxic agent has and is cationic surfactant, and it can make protein denaturation, changes membrane passage, moisture is entered bacterium
In vivo, so that swelling ruptures.Quarternary ammonium salt compound be with good surface-active action, can high aggregation in phage surface,
Dehydrogenase, the oxidizing ferment in the metabolism of bacterium, inactivation somatic cells are influenceed, and can decomposition glucose, succinate, third
The enzyme system of ketonic acid salt etc., so as to reach sterilization, sterilization functions.
Embodiment
With reference to specific embodiment, the present invention is expanded on further.These embodiments be merely to illustrate the present invention and without
In limitation the scope of the present invention.
Embodiment 1
The present embodiment is related to a kind of Chinese herbal disinfectant, includes the raw material of following parts by weight：3 parts of rhizoma atractylodis, 8 parts of radix scutellariae, honeysuckle 8
Part, 7 parts of kuh-seng, 12 parts of cloves, 5 parts of barberry, 15 parts of peppermint, 2 parts of felwort, 5 parts of manyleaf meadowure rhizome and root, 3 parts of Herba Andrographitis, Radix Isatidis 8
Part, 10 parts of ginkgo leaf, 8 parts of tangerine peel, 2 parts of the fruit of glossy privet, 6 parts of garlic, 7 parts of ginger, 13 parts of chitosan, 7 parts of organic boronic, modified illiteracy
De- soil 10 parts, 3 parts of quaternary ammonium salt.
Wherein, the modified montmorillonoid is made by following methods：Montmorillonite is crushed to granular size to particle diameter≤1mm,
Then it is immersed into clear water, stirs 15min with electric blender, speed setting is 350r/min, then filters and submerges solute
Into dilute mineral acid solution, water-bath is heat-treated 1h, and temperature is set between 75~85 DEG C, then is added into the suspension after acidifying
Dispersant sodium pyrophosphate is sufficiently stirred for, and after collaboration supersonic, water-heating method processing 2h, finally carries out centrifugal treating to it, after centrifugation,
Upper strata suspension is taken to be transported to roasting 1h in swinging drying oven after filtering, drying, sintering temperature is 280 DEG C.
Wherein, the quaternary ammonium salt is benzalkonium bromide.
A kind of method for preparing the Chinese herbal disinfectant, comprises the following steps：
（1）Rhizoma atractylodis, radix scutellariae are weighed by above-mentioned formula, honeysuckle, kuh-seng, cloves, barberry, peppermint, felwort, manyleaf meadowure rhizome and root, worn
Heart lotus, Radix Isatidis, ginkgo leaf, tangerine peel, the fruit of glossy privet, garlic, ginger, chitosan, organic boronic, modified montmorillonoid, quaternary ammonium salt, it is standby
With；
（2）By rhizoma atractylodis, radix scutellariae, honeysuckle, kuh-seng, cloves, barberry, peppermint, felwort, manyleaf meadowure rhizome and root, Herba Andrographitis, Radix Isatidis,
Ginkgo leaf, tangerine peel, the fruit of glossy privet, garlic, ginger are crushed respectively, are well mixed, are obtained Traditional Chinese drug mixture；
（3）By step（2）The Traditional Chinese drug mixture obtained is added water to cook 1 time, and 1h is boiled every time, volatile oil and decoction liquor is collected, and is merged
Decoction liquor, filtering stands 24h, and Aspirate supernatant, filtering adds chitosan, is uniformly mixed, obtains mixed liquor A；
（4）Quaternary ammonium salt is put into after emulsion tank emulsification, with step（3）The mixed liquor A of gained is well mixed, and adds modified cover
De- soil and step（3）Obtained volatile oil, is put into high speed dispersor and disperses 20min, add organic boronic, be uniformly mixed,
Obtain mixed liquid B；
（5）After mixed liquid B filtering or centrifugal dehydration, filter residue is dried at less than 80 DEG C, uses airslide disintegrating mill dry pulverization process, or
Mixed liquid B is spray-dried to water content ＜ 10%, produce the Chinese herbal disinfectant.
Wherein, the step（3）In to add water to cook amount of water be 4 times of Traditional Chinese drug mixture weight.
Wherein, the step（4）The scattered speed of high speed is 1700r/min.
Embodiment 2
The present embodiment is related to a kind of Chinese herbal disinfectant, includes the raw material of following parts by weight：8 parts of rhizoma atractylodis, 12 parts of radix scutellariae, honeysuckle
20 parts, 13 parts of kuh-seng, 18 parts of cloves, 15 parts of barberry, 25 parts of peppermint, 10 parts of felwort, 10 parts of manyleaf meadowure rhizome and root, 7 parts of Herba Andrographitis, plate
Blue 17 parts of root, 20 parts of ginkgo leaf, 15 parts of tangerine peel, 5 parts of the fruit of glossy privet, 13 parts of garlic, 16 parts of ginger, 25 parts of chitosan, organic boronic
15 parts, 30 parts of modified montmorillonoid, 8 parts of quaternary ammonium salt.
Wherein, the modified montmorillonoid is made by following methods：Montmorillonite is crushed to granular size to particle diameter≤1mm,
Then it is immersed into clear water, stirs 25min with electric blender, speed setting is 450r/min, then filters and submerges solute
Into dilute mineral acid solution, water-bath is heat-treated 2h, and temperature is set between 75~85 DEG C, then is added into the suspension after acidifying
Dispersant sodium pyrophosphate is sufficiently stirred for, and after collaboration supersonic, water-heating method processing 3h, finally carries out centrifugal treating to it, after centrifugation,
Upper strata suspension is taken to be transported to roasting 2h in swinging drying oven after filtering, drying, sintering temperature is 400 DEG C.
Wherein, the quaternary ammonium salt is benzalkonium chloride.
A kind of method for preparing the Chinese herbal disinfectant, comprises the following steps：
（1）Rhizoma atractylodis, radix scutellariae are weighed by above-mentioned formula, honeysuckle, kuh-seng, cloves, barberry, peppermint, felwort, manyleaf meadowure rhizome and root, worn
Heart lotus, Radix Isatidis, ginkgo leaf, tangerine peel, the fruit of glossy privet, garlic, ginger, chitosan, organic boronic, modified montmorillonoid, quaternary ammonium salt, it is standby
With；
（2）By rhizoma atractylodis, radix scutellariae, honeysuckle, kuh-seng, cloves, barberry, peppermint, felwort, manyleaf meadowure rhizome and root, Herba Andrographitis, Radix Isatidis,
Ginkgo leaf, tangerine peel, the fruit of glossy privet, garlic, ginger are crushed respectively, are well mixed, are obtained Traditional Chinese drug mixture；
（3）By step（2）The Traditional Chinese drug mixture obtained is added water to cook 2 times, and 2h is boiled every time, volatile oil and decoction liquor is collected, and is merged
Decoction liquor, filtering stands 24h, and Aspirate supernatant, filtering adds chitosan, is uniformly mixed, obtains mixed liquor A；
（4）Quaternary ammonium salt is put into after emulsion tank emulsification, with step（3）The mixed liquor A of gained is well mixed, and adds modified cover
De- soil and step（3）Obtained volatile oil, is put into high speed dispersor and disperses 30min, add organic boronic, be uniformly mixed,
Obtain mixed liquid B；
（5）After mixed liquid B filtering or centrifugal dehydration, filter residue is dried at less than 80 DEG C, uses airslide disintegrating mill dry pulverization process, or
Mixed liquid B is spray-dried to water content ＜ 10%, produce the Chinese herbal disinfectant.
Wherein, the step（3）In to add water to cook amount of water be 8 times of Traditional Chinese drug mixture weight.
Wherein, the step（4）The scattered speed of high speed is 2200r/min.
Embodiment 3
The present embodiment is related to a kind of Chinese herbal disinfectant, includes the raw material of following parts by weight：4 parts of rhizoma atractylodis, 9 parts of radix scutellariae, honeysuckle
13 parts, 9 parts of kuh-seng, 14 parts of cloves, 8 parts of barberry, 19 parts of peppermint, 4 parts of felwort, 7 parts of manyleaf meadowure rhizome and root, 4 parts of Herba Andrographitis, Radix Isatidis
10 parts, 11 parts of ginkgo leaf, 11 parts of tangerine peel, 3 parts of the fruit of glossy privet, 8 parts of garlic, 9 parts of ginger, 16 parts of chitosan, 9 parts of organic boronic, change
15 parts of montmorillonite of property, 4 parts of quaternary ammonium salt.
Wherein, the modified montmorillonoid is made by following methods：Montmorillonite is crushed to granular size to particle diameter≤1mm,
Then it is immersed into clear water, stirs 18min with electric blender, speed setting is 375r/min, then filters and submerges solute
Into dilute mineral acid solution, water-bath is heat-treated 1.2h, and temperature is set between 75~85 DEG C, then adds into the suspension after acidifying
Enter dispersant sodium pyrophosphate to be sufficiently stirred for, after collaboration supersonic, water-heating method processing 2.3h, centrifugal treating finally is carried out to it, it is centrifuged
Afterwards, upper strata suspension is taken to be transported to roasting 1.2h in swinging drying oven after filtering, drying, sintering temperature is 320
℃。
Wherein, the quaternary ammonium salt is benzalkonium bromide.
A kind of method for preparing the Chinese herbal disinfectant, comprises the following steps：
（1）Rhizoma atractylodis, radix scutellariae are weighed by above-mentioned formula, honeysuckle, kuh-seng, cloves, barberry, peppermint, felwort, manyleaf meadowure rhizome and root, worn
Heart lotus, Radix Isatidis, ginkgo leaf, tangerine peel, the fruit of glossy privet, garlic, ginger, chitosan, organic boronic, modified montmorillonoid, quaternary ammonium salt, it is standby
With；
（2）By rhizoma atractylodis, radix scutellariae, honeysuckle, kuh-seng, cloves, barberry, peppermint, felwort, manyleaf meadowure rhizome and root, Herba Andrographitis, Radix Isatidis,
Ginkgo leaf, tangerine peel, the fruit of glossy privet, garlic, ginger are crushed respectively, are well mixed, are obtained Traditional Chinese drug mixture；
（3）By step（2）The Traditional Chinese drug mixture obtained is added water to cook 3 times, and 1.2h is boiled every time, volatile oil and decoction liquor is collected, and is closed
And decoction liquor, filtering, 24h is stood, Aspirate supernatant, filtering adds chitosan, is uniformly mixed, obtains mixed liquor A；
（4）Quaternary ammonium salt is put into after emulsion tank emulsification, with step（3）The mixed liquor A of gained is well mixed, and adds modified cover
De- soil and step（3）Obtained volatile oil, is put into high speed dispersor and disperses 23min, add organic boronic, be uniformly mixed,
Obtain mixed liquid B；
（5）After mixed liquid B filtering or centrifugal dehydration, filter residue is dried at less than 80 DEG C, uses airslide disintegrating mill dry pulverization process, or
Mixed liquid B is spray-dried to water content ＜ 10%, produce the Chinese herbal disinfectant.
Wherein, the step（3）In to add water to cook amount of water be 5 times of Traditional Chinese drug mixture weight.
Wherein, the step（4）The scattered speed of high speed is 1800r/min.
Embodiment 4
The present embodiment is related to a kind of Chinese herbal disinfectant, includes the raw material of following parts by weight：7 parts of rhizoma atractylodis, 11 parts of radix scutellariae, honeysuckle
17 parts, 12 parts of kuh-seng, 16 parts of cloves, 12 parts of barberry, 24 parts of peppermint, 6 parts of felwort, 9 parts of manyleaf meadowure rhizome and root, 6 parts of Herba Andrographitis, plate it is blue
15 parts of root, 17 parts of ginkgo leaf, 14 parts of tangerine peel, 4 parts of the fruit of glossy privet, 12 parts of garlic, 14 parts of ginger, 23 parts of chitosan, organic boronic 12
Part, 28 parts of modified montmorillonoid, 7 parts of quaternary ammonium salt.
Wherein, the modified montmorillonoid is made by following methods：Montmorillonite is crushed to granular size to particle diameter≤1mm,
Then it is immersed into clear water, stirs 22min with electric blender, speed setting is 430r/min, then filters and submerges solute
Into dilute mineral acid solution, water-bath is heat-treated 1.8h, and temperature is set between 75~85 DEG C, then adds into the suspension after acidifying
Enter dispersant sodium pyrophosphate to be sufficiently stirred for, after collaboration supersonic, water-heating method processing 2.7h, centrifugal treating finally is carried out to it, it is centrifuged
Afterwards, upper strata suspension is taken to be transported to roasting 1.8h in swinging drying oven after filtering, drying, sintering temperature is 330
℃。
Wherein, the quaternary ammonium salt is benzalkonium chloride.
A kind of method for preparing the Chinese herbal disinfectant, comprises the following steps：
（1）Rhizoma atractylodis, radix scutellariae are weighed by above-mentioned formula, honeysuckle, kuh-seng, cloves, barberry, peppermint, felwort, manyleaf meadowure rhizome and root, worn
Heart lotus, Radix Isatidis, ginkgo leaf, tangerine peel, the fruit of glossy privet, garlic, ginger, chitosan, organic boronic, modified montmorillonoid, quaternary ammonium salt, it is standby
With；
（2）By rhizoma atractylodis, radix scutellariae, honeysuckle, kuh-seng, cloves, barberry, peppermint, felwort, manyleaf meadowure rhizome and root, Herba Andrographitis, Radix Isatidis,
Ginkgo leaf, tangerine peel, the fruit of glossy privet, garlic, ginger are crushed respectively, are well mixed, are obtained Traditional Chinese drug mixture；
（3）By step（2）The Traditional Chinese drug mixture obtained is added water to cook 1 time, and 2h is boiled every time, volatile oil and decoction liquor is collected, and is merged
Decoction liquor, filtering stands 24h, and Aspirate supernatant, filtering adds chitosan, is uniformly mixed, obtains mixed liquor A；
（4）Quaternary ammonium salt is put into after emulsion tank emulsification, with step（3）The mixed liquor A of gained is well mixed, and adds modified cover
De- soil and step（3）Obtained volatile oil, is put into high speed dispersor and disperses 28min, add organic boronic, be uniformly mixed,
Obtain mixed liquid B；
（5）After mixed liquid B filtering or centrifugal dehydration, filter residue is dried at less than 80 DEG C, uses airslide disintegrating mill dry pulverization process, or
Mixed liquid B is spray-dried to water content ＜ 10%, produce the Chinese herbal disinfectant.
Wherein, the step（3）In to add water to cook amount of water be 7 times of Traditional Chinese drug mixture weight.
Wherein, the step（4）The scattered speed of high speed is 2100r/min.
Embodiment 5
The present embodiment is related to a kind of Chinese herbal disinfectant, includes the raw material of following parts by weight：5 parts of rhizoma atractylodis, 10 parts of radix scutellariae, honeysuckle
14 parts, 11 parts of kuh-seng, 15 parts of cloves, 9 parts of barberry, 23 parts of peppermint, 5 parts of felwort, 8 parts of manyleaf meadowure rhizome and root, 5 parts of Herba Andrographitis, plate it is blue
14 parts of root, 13 parts of ginkgo leaf, 12 parts of tangerine peel, 3.5 parts of the fruit of glossy privet, 11 parts of garlic, 13 parts of ginger, 19 parts of chitosan, organic boronic
11 parts, 22 parts of modified montmorillonoid, 6 parts of quaternary ammonium salt.
Wherein, the modified montmorillonoid is made by following methods：Montmorillonite is crushed to granular size to particle diameter≤1mm,
Then it is immersed into clear water, stirs 20min with electric blender, speed setting is 400r/min, then filters and submerges solute
Into dilute mineral acid solution, water-bath is heat-treated 1.5h, and temperature is set between 75~85 DEG C, then adds into the suspension after acidifying
Enter dispersant sodium pyrophosphate to be sufficiently stirred for, after collaboration supersonic, water-heating method processing 2.5h, centrifugal treating finally is carried out to it, it is centrifuged
Afterwards, upper strata suspension is taken to be transported to roasting 1.5h in swinging drying oven after filtering, drying, sintering temperature is 340
℃。
Wherein, the quaternary ammonium salt is benzalkonium bromide.
A kind of method for preparing the Chinese herbal disinfectant, comprises the following steps：
（1）Rhizoma atractylodis, radix scutellariae are weighed by above-mentioned formula, honeysuckle, kuh-seng, cloves, barberry, peppermint, felwort, manyleaf meadowure rhizome and root, worn
Heart lotus, Radix Isatidis, ginkgo leaf, tangerine peel, the fruit of glossy privet, garlic, ginger, chitosan, organic boronic, modified montmorillonoid, quaternary ammonium salt, it is standby
With；
（2）By rhizoma atractylodis, radix scutellariae, honeysuckle, kuh-seng, cloves, barberry, peppermint, felwort, manyleaf meadowure rhizome and root, Herba Andrographitis, Radix Isatidis,
Ginkgo leaf, tangerine peel, the fruit of glossy privet, garlic, ginger are crushed respectively, are well mixed, are obtained Traditional Chinese drug mixture；
（3）By step（2）The Traditional Chinese drug mixture obtained is added water to cook 2 times, and 1.5h is boiled every time, volatile oil and decoction liquor is collected, and is closed
And decoction liquor, filtering, 24h is stood, Aspirate supernatant, filtering adds chitosan, is uniformly mixed, obtains mixed liquor A；
（4）Quaternary ammonium salt is put into after emulsion tank emulsification, with step（3）The mixed liquor A of gained is well mixed, and adds modified cover
De- soil and step（3）Obtained volatile oil, is put into high speed dispersor and disperses 25min, add organic boronic, be uniformly mixed,
Obtain mixed liquid B；
（5）After mixed liquid B filtering or centrifugal dehydration, filter residue is dried at less than 80 DEG C, uses airslide disintegrating mill dry pulverization process, or
Mixed liquid B is spray-dried to water content ＜ 10%, produce the Chinese herbal disinfectant.
Wherein, the step（3）In to add water to cook amount of water be 6 times of Traditional Chinese drug mixture weight.
Wherein, the step（4）The scattered speed of high speed is 2000r/min.
The specific embodiment of the present invention is described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring the substantive content of the present invention.
Claims (8)
1. a kind of Chinese herbal disinfectant, it is characterised in that include the raw material of following parts by weight：3~8 parts of rhizoma atractylodis, radix scutellariae 8~12
Part, 8~20 parts of honeysuckle, 7~13 parts of kuh-seng, 12~18 parts of cloves, 5~15 parts of barberry, 15~25 parts of peppermint, felwort 2
~10 parts, 5~10 parts of manyleaf meadowure rhizome and root, 3~7 parts of Herba Andrographitis, 8~17 parts of Radix Isatidis, 10~20 parts of ginkgo leaf, 8~15 parts of tangerine peel, female
Loyal 2~5 parts of son, 6~13 parts of garlic, 7~16 parts of ginger, 13~25 parts of chitosan, 7~15 parts of organic boronic, modified montmorillonoid
10~30 parts, 3~8 parts of quaternary ammonium salt.
2. Chinese herbal disinfectant according to claim 1, it is characterised in that include the raw material of following parts by weight：Rhizoma atractylodis 4~
7 parts, 9~11 parts of radix scutellariae, 13~17 parts of honeysuckle, 9~12 parts of kuh-seng, 14~16 parts of cloves, 8~12 parts of barberry, peppermint 19
~24 parts, 4~6 parts of felwort, 7~9 parts of manyleaf meadowure rhizome and root, 4~6 parts of Herba Andrographitis, 10~15 parts of Radix Isatidis, 11~17 parts of ginkgo leaf,
11~14 parts of tangerine peel, 3~4 parts of the fruit of glossy privet, 8~12 parts of garlic, 9~14 parts of ginger, 16~23 parts of chitosan, organic boronic 9~
12 parts, 15~28 parts of modified montmorillonoid, 4~7 parts of quaternary ammonium salt.
3. Chinese herbal disinfectant according to claim 1, it is characterised in that include the raw material of following parts by weight：Rhizoma atractylodis 5
Part, 10 parts of radix scutellariae, 14 parts of honeysuckle, 11 parts of kuh-seng, 15 parts of cloves, 9 parts of barberry, 23 parts of peppermint, 5 parts of felwort, manyleaf meadowure rhizome and root 8
Part, 5 parts of Herba Andrographitis, 14 parts of Radix Isatidis, 13 parts of ginkgo leaf, 12 parts of tangerine peel, 3.5 parts of the fruit of glossy privet, 11 parts of garlic, 13 parts of ginger, shell
19 parts of glycan, 11 parts of organic boronic, 22 parts of modified montmorillonoid, 6 parts of quaternary ammonium salt.
4. Chinese herbal disinfectant according to claim 1, it is characterised in that the modified montmorillonoid is by following methods system
：Montmorillonite is crushed to granular size to particle diameter≤1mm, is then immersed into clear water, with electric blender stirring 15~
25min, speed setting is 350~450r/min, then filter by solute be immersed into dilute mineral acid solution water-bath heat treatment 1~
2h, temperature is set between 75~85 DEG C, then into the suspension after acidifying, addition dispersant sodium pyrophosphate is sufficiently stirred for, and is cooperateed with
Supersonic, water-heating method is handled after 2~3h, finally carries out centrifugal treating to it, after centrifugation, is taken upper strata suspension by filtering, is dried
After be transported to 1~2h of roasting in swinging drying oven, sintering temperature is 280~400 DEG C.
5. Chinese herbal disinfectant according to claim 1, it is characterised in that the quaternary ammonium salt is that benzalkonium bromide or benzene prick chlorine
Ammonium.
6. a kind of method for preparing any one of Claims 1 to 5 Chinese herbal disinfectant, it is characterised in that including following step
Suddenly：
（1）Rhizoma atractylodis, radix scutellariae are weighed by above-mentioned formula, honeysuckle, kuh-seng, cloves, barberry, peppermint, felwort, manyleaf meadowure rhizome and root, worn
Heart lotus, Radix Isatidis, ginkgo leaf, tangerine peel, the fruit of glossy privet, garlic, ginger, chitosan, organic boronic, modified montmorillonoid, quaternary ammonium salt, it is standby
With；
（2）By rhizoma atractylodis, radix scutellariae, honeysuckle, kuh-seng, cloves, barberry, peppermint, felwort, manyleaf meadowure rhizome and root, Herba Andrographitis, Radix Isatidis,
Ginkgo leaf, tangerine peel, the fruit of glossy privet, garlic, ginger are crushed respectively, are well mixed, are obtained Traditional Chinese drug mixture；
（3）By step（2）The Traditional Chinese drug mixture obtained is added water to cook 1~3 time, and 1~2h is boiled every time, volatile oil and decoction is collected
Liquid, merges decoction liquor, and filtering stands 24h, and Aspirate supernatant, filtering adds chitosan, is uniformly mixed, obtains mixed liquor A；
（4）Quaternary ammonium salt is put into after emulsion tank emulsification, with step（3）The mixed liquor A of gained is well mixed, and adds modified cover
De- soil and step（3）Obtained volatile oil, is put into high speed dispersor and disperses 20~30min, adds organic boronic, and stirring mixing is equal
It is even, obtain mixed liquid B；
（5）After mixed liquid B filtering or centrifugal dehydration, filter residue is dried at less than 80 DEG C, uses airslide disintegrating mill dry pulverization process, or
Mixed liquid B is spray-dried to water content ＜ 10%, produce the Chinese herbal disinfectant.
7. preparation method according to claim 6, it is characterised in that the step（3）In add water to cook during amount of water is
4~8 times of medicine mixture weight.
8. preparation method according to claim 6, it is characterised in that the step（4）The scattered speed of high speed is
1700~2200r/min.
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107912467A (en) * | 2017-12-16 | 2018-04-17 | 柳州市晟铂贸易有限公司 | A kind of high effect nontoxic bacteriostatic agent |
| CN108294069A (en) * | 2018-02-07 | 2018-07-20 | 合肥华盖生物科技有限公司 | A kind of disinfectant for animals and preparation method thereof |
| CN108576081A (en) * | 2018-01-24 | 2018-09-28 | 合肥华盖生物科技有限公司 | A kind of medical equipment environment-friendly type Chinese medicine antiseptic and preparation method thereof |
| CN108739892A (en) * | 2018-05-18 | 2018-11-06 | 丁永胜 | A kind of preparation method of sheep hurdle cleaning and sterilizing agent |
| CN109793015A (en) * | 2019-01-18 | 2019-05-24 | 北京弘纳绿源科技发展有限公司 | A kind of plant source extracts disinfection sanitizer and its preparation process |
| CN111296499A (en) * | 2020-03-18 | 2020-06-19 | 王智洋 | Environment-friendly disinfectant containing antiviral traditional Chinese medicine and preparation method thereof |
| CN114176099A (en) * | 2021-12-15 | 2022-03-15 | 何连旺 | Preparation process of environment-friendly disinfectant |
| CN116114715A (en) * | 2022-12-29 | 2023-05-16 | 江苏康巴特生物工程有限公司 | Low-temperature quaternary ammonium salt disinfectant for livestock and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105412879A (en) * | 2015-12-21 | 2016-03-23 | 青岛拓联信息技术有限公司 | Traditional Chinese herbal medicine disinfectant fluid |
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2017
- 2017-07-12 CN CN201710563327.3A patent/CN107158353A/en not_active Withdrawn
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105412879A (en) * | 2015-12-21 | 2016-03-23 | 青岛拓联信息技术有限公司 | Traditional Chinese herbal medicine disinfectant fluid |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107912467A (en) * | 2017-12-16 | 2018-04-17 | 柳州市晟铂贸易有限公司 | A kind of high effect nontoxic bacteriostatic agent |
| CN108576081A (en) * | 2018-01-24 | 2018-09-28 | 合肥华盖生物科技有限公司 | A kind of medical equipment environment-friendly type Chinese medicine antiseptic and preparation method thereof |
| CN108294069A (en) * | 2018-02-07 | 2018-07-20 | 合肥华盖生物科技有限公司 | A kind of disinfectant for animals and preparation method thereof |
| CN108739892A (en) * | 2018-05-18 | 2018-11-06 | 丁永胜 | A kind of preparation method of sheep hurdle cleaning and sterilizing agent |
| CN109793015A (en) * | 2019-01-18 | 2019-05-24 | 北京弘纳绿源科技发展有限公司 | A kind of plant source extracts disinfection sanitizer and its preparation process |
| CN111296499A (en) * | 2020-03-18 | 2020-06-19 | 王智洋 | Environment-friendly disinfectant containing antiviral traditional Chinese medicine and preparation method thereof |
| CN114176099A (en) * | 2021-12-15 | 2022-03-15 | 何连旺 | Preparation process of environment-friendly disinfectant |
| CN114176099B (en) * | 2021-12-15 | 2023-08-11 | 安徽绿阳生物科技有限公司 | Environment-friendly disinfectant preparation process |
| CN116114715A (en) * | 2022-12-29 | 2023-05-16 | 江苏康巴特生物工程有限公司 | Low-temperature quaternary ammonium salt disinfectant for livestock and preparation method thereof |
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Application publication date: 20170915 |