CN115919692A - Hair moisturizing composition containing prinsepia utilis royle oil and preparation method and application thereof - Google Patents

Hair moisturizing composition containing prinsepia utilis royle oil and preparation method and application thereof Download PDF

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CN115919692A
CN115919692A CN202211566390.XA CN202211566390A CN115919692A CN 115919692 A CN115919692 A CN 115919692A CN 202211566390 A CN202211566390 A CN 202211566390A CN 115919692 A CN115919692 A CN 115919692A
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hair
oil
prinsepia utilis
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moisturizing
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CN115919692B (en
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蔡彬弟
张少暖
冯秋红
马占林
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Guangzhou Sifen Cosmetics Co ltd
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Guangzhou Sifen Cosmetics Co ltd
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Abstract

The invention discloses a hair moisturizing composition containing prinsepia utilis royle oil, and a preparation method and application thereof. The invention creatively discovers that the composition consisting of the prinsepia utilis royle oil, the olive oil and the papermulberry fruit oil has double moisturizing effects on hair and scalp, and the prinsepia utilis royle oil, the olive oil and the papermulberry fruit oil have certain synergistic effect on the effects, so that the composition is very suitable for hair care products.

Description

Hair moisturizing composition containing prinsepia utilis royle oil and preparation method and application thereof
Technical Field
The invention belongs to the field of cosmetics, and relates to a hair moisturizing composition containing prinsepia utilis royle oil as well as a preparation method and application thereof.
Background
Hair damage can be caused to different degrees by daily combing friction, chemical treatment, high-temperature styling, ultraviolet ray damage, air pollution and the like. Hair damage is classified into mild damage, moderate damage, and severe damage according to the degree of damage. For different damaged hair qualities, the phenomena of reduced water content of hair, reduced elasticity and toughness of hair, dryness, frightening hair, easy breakage and the like can occur. Since hair has no self-repairing ability, it is difficult to repair itself once it is damaged from the outside. The scalp serves as the "soil" for hair growth, and the quality and nutritional status of the scalp directly determine the hair quality. Therefore, in the daily moisturizing care of hair, not only basic moisturizing of hair dryness but also maintenance and moisturizing of scalp should be performed.
First, the hair shaft consists of hair follicles (scales), cortex and medulla from outside to inside. The integrity of the fur coat structure determines the apparent character of the hair. The outermost layer of the fur coat is attached with a layer of nonpolar lipid, whose main component is C16-22 alkane, which becomes lipid layer A and determines the glossiness of hair. The inner layer of the fur coat also contains about 25% of structural lipids, a Cell Membrane Complex (CMC), whose main components are ceramides, cholesterol sulfate, cholesterol, fatty alcohols and free fatty acids. The CMC lipid is combined with protein to form lipoprotein, and a continuous network structure is formed around hair fiber, so that the CMC lipid has an intercellular adhesion effect, and the integrity and the tensile strength of the hair stem fiber are maintained. Thus, achieving a basic moisturization of the hair dryness can be achieved by supplementing the hair with fatty acids in the CMC. Secondly, the scalp also has a barrier as a specific area of skin composition. The scalp barrier is formed by the combination of the stratum corneum cells and the "brick wall structure" composed of "lipids" (mainly composed of ceramide, cholesterol and free fatty acid) and "natural moisturizing factor" (NMF) between the cells, and the "sebum membrane" attached to the surface of the scalp barrier. Wherein the "sebaceous membrane" is a layer of aqueous membrane covering the skin surface, is the outermost layer of the skin barrier, is formed by emulsifying "sebum" secreted by sebaceous glands, "lipid" produced by the disintegration of cells of the stratum corneum, and "sweat" secreted by sweat glands, and has weak acidity. The main components of the health-care product are ceramide, squalene, linoleic acid, linolenic acid and lipid, and the health-care product has the functions of locking water and resisting inflammation. When the scalp barrier changes, the scalp permeability is increased, the moisture loss is serious, and the scalp structure is damaged. The basic moisture retention of the scalp can be realized by supplementing essential fatty acids such as linoleic acid and linolenic acid to the scalp.
Based on the above analysis, dual moisturization of the hair and scalp can be achieved by supplementing the hair and scalp with the fatty acids required for them. Wherein, linoleic acid and linolenic acid required by the scalp belong to polyunsaturated fatty acid, and mainly act on the sebum layer to improve the scalp quality and maintain the scalp barrier function. While the hair-specific fatty acids are predominantly monounsaturated fatty acids. The monounsaturated fatty acid has a medium linear molecular structure and strong polarity, has strong adsorption capacity with polar keratin in hair fibers, can effectively permeate into a CMC layer of the fur cuticle, and can realize deep repair of hair shafts.
CN104510668A discloses a moisturizing composition, a preparation method and an application thereof, wherein the moisturizing composition comprises moisturizing active ingredients, the moisturizing active ingredients at least comprise prinsepia utilis royle oil and prinsepia utilis royle polysaccharide, and the weight ratio of the prinsepia utilis royle oil to the prinsepia utilis royle polysaccharide is 0.5-10. The moisturizing composition has good moisturizing effect, and is suitable for application in cosmetics, health products and medicines, especially in cosmetics.
CN108998301A discloses a milk soap for seborrheic alopecia and a preparation method thereof, wherein the milk soap for seborrheic alopecia comprises the following raw materials in parts by weight: 80-100 parts of olive oil, 10-20 parts of coconut oil, 15-25 parts of sodium hydroxide, 40-60 parts of deionized water, 10-30 parts of aloe gel, 5-10 parts of defatted goat milk, 3-5 parts of liquorice, 1-3 parts of radix stemonae, 1-2 parts of ginger, 3-5 parts of polygonum multiflorum, 3-5 parts of euphorbia tenuifolia inflorescence, 1-2 parts of salvia miltiorrhiza, 1-2 parts of pseudo-ginseng and 1-3 parts of compound essential oil. The milk soap prepared by the method has the effects of balancing scalp grease, cleaning hair and scalp, relieving cranial nerves, promoting cell regeneration, preventing alopecia and promoting hair growth under the combined action of various raw materials.
In order to solve the problems of low water content of hair, easy breakage of dry hair, damaged scalp and the like of people, realize double moisture preservation of the hair and the scalp, better maintain the barrier function of the scalp and deeply repair the dry hair, the development of the moisture-preserving hair care product for the hair is necessary.
Disclosure of Invention
Aiming at the defects and the actual needs of the prior art, the invention provides a hair moisturizing composition containing prinsepia utilis royle oil and a preparation method and application thereof, solves the problems that the hair of people is low in water content, dry and frigid hair is easy to break, the scalp is damaged and the like at present, realizes double moisturizing of the hair and the scalp, and better maintains the barrier function of the scalp and deeply repairs the hair.
In order to achieve the purpose, the invention adopts the following technical scheme:
in a first aspect, the present invention provides a prinsepia utilis royle oil-containing hair moisturizing composition comprising prinsepia utilis royle oil, olive oil and paper mulberry fruit oil.
The Prinsepia utilis Royle oil is also called as Prinsepia utilis oil, the content of 3 fatty acids of the Prinsepia utilis Royle oil is extremely close to the structure of the fatty acid 1; olive oil, also known as mediterranean nectar, liquid gold, vegetable oil queen, is rich in monounsaturated fatty acids, wherein the oleic acid content is as high as 77%. The oleic acid has a medium-linear molecular structure and strong polarity, has strong adsorption capacity with polar keratin in hair fibers, can effectively permeate into a CMC layer of the hair cuticle, and can realize deep repair of hair shafts; the fructus Broussonetiae is dried mature fruit of Broussonetia Papyrifera (Broussonetia Papyrifera) of Moraceae, and has oil content of above 40%. The content of polyunsaturated fatty acid in the papermulberry fruit oil is as high as more than 80%, and linoleic acid (omega-6) and alpha-linoleic acid (omega-3) which are active ingredients of the polyunsaturated fatty acid can permeate into the surface layer of the scalp as essential fatty acid of the skin, so that the scalp quality is improved by acting on the sebum layer, and the barrier function of the scalp is maintained.
The invention creatively discovers that the composition consisting of the prinsepia utilis royle oil, the olive oil and the papermulberry fruit oil has an obvious moisturizing effect on hair and scalp, has a certain synergistic effect on the effects, and is very suitable for hair care products.
Preferably, the mass ratio of the prinsepia utilis royle oil, the olive oil and the papermulberry fruit oil is (35-60): (10-45): (10-45).
When the three components are combined according to a specific mass ratio, the hair conditioner has a more remarkable effect on double moisture retention of hair and scalp.
The specific point value in the above (35-60) can be selected from 35, 36, 37, 38, 40, 50, 56, 58, 59, 60 and the like.
The specific point value in the above (10-45) can be selected from 10, 20, 30, 40, 41, 42, 43, 44, 45 and the like.
Other specific point values within the above numerical ranges can be selected, and are not described in detail herein.
In a second aspect, the present invention provides a use of the prinsepia utilis royle oil-containing moisturizing composition for hair of the first aspect in the preparation of cosmetics.
Preferably, the cosmetic comprises a hair oil, a conditioner, a shampoo or a hair mask.
Preferably, the weight percentage of the prinsepia utilis royle oil-containing hair moisturizing composition in the cosmetic is 1-10%, and more preferably 2-5%.
Specific values of the above-mentioned 1-10% may be selected from 1%, 2%, 3%, 4%, 5%, 6%, 7%, 8%, 9%, 10%, etc.
The specific value of the above 2-5% may be selected from 2%, 3%, 4%, 5%, etc.
Other specific values within the above ranges can be selected, and are not described in detail herein.
In a third aspect, the present invention provides a method for preparing the prinsepia utilis royle oil-containing moisturizing composition for hair of the first aspect, the method comprising: weighing Prinsepia utilis oil, olive oil and Broussonetia papyrifera seed oil respectively, and mixing the raw materials uniformly to obtain the composition.
In a fourth aspect, the present invention provides a prinsepia utilis royle oil-containing hair moisturizing and hair care oil, comprising the prinsepia utilis royle oil-containing hair moisturizing composition of the first aspect, a solvent, a hair conditioner, a brightener, and an antioxidant.
Preferably, the Prinsepia utilis oil-containing moisturizing hair care oil for hair further comprises a softening agent.
Preferably, the emollient comprises any one or a combination of at least two of caprylic/capric triglyceride, ethylhexyl palmitate, ethylhexyl cetyl alcohol, isononyl isononanoate or squalane.
Preferably, the emollient is a combination of caprylic/capric triglyceride, ethylhexyl palmitate and isononyl isononanoate.
According to the invention, when the emollient is prepared by combining three components of caprylic/capric triglyceride, ethylhexyl palmitate and isononyl isononanoate, the three components of caprylic/capric triglyceride, ethylhexyl palmitate and isononyl isononanoate have a synergistic effect, so that the moisture retention of hair can be better improved.
Preferably, the Prinsepia utilis oil-containing moisturizing and hair care oil for hair comprises the following components in parts by weight: the hair moisturizing composition containing prinsepia utilis royle oil comprises, by weight, 1-10 parts of the prinsepia utilis royle oil-containing hair moisturizing composition, 50-100 parts of a solvent, 0.5-5 parts of a softening agent, 1-6 parts of a hair conditioner, 1-8 parts of a brightening agent and 0.15-0.5 part of an antioxidant.
The weight parts of the composition can be selected from 1 part, 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts and the like.
The solvent can be selected from 50 parts, 60 parts, 70 parts, 80 parts, 90 parts, 100 parts and the like in parts by weight.
The weight parts of the softening agent can be selected from 0.5 part, 1 part, 2 parts, 3 parts, 4 parts, 5 parts and the like.
The hair conditioner can be selected from 1 part, 2 parts, 3 parts, 4 parts, 5 parts, 6 parts and the like in parts by weight.
The weight parts of the brightening agent can be selected from 1 part, 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts and the like.
The antioxidant can be selected from 0.15 part, 0.2 part, 0.3 part, 1 part, 2 parts, 3 parts, 4 parts, 5 parts and the like in parts by weight.
Other specific point values within the above numerical ranges can be selected, and are not described in detail herein.
Preferably, the solvent comprises any one of cyclopentadimethicone, isododecane, or dimethicone, or a combination of at least two thereof.
Preferably, the hair conditioning agent comprises any one of or a combination of at least two of dimethiconol, amodimethicone or phenyl trimethicone.
Preferably, the gloss agent comprises polydimethylsiloxane (and) aminopropylpolydimethylsiloxane and/or PPG-3 octyl ether.
Preferably, the antioxidant comprises any one of or a combination of at least two of tocopherol acetate, rosemary extract or pentaerythritol ester.
In a fifth aspect, the present invention provides a method for preparing a moisturizing hair care oil for hair containing prinsepia utilis royle oil, the method comprising:
mixing the solvent and the hair conditioner, homogenizing, adding the brightening agent, the hair moisturizing composition and the antioxidant, and stirring and mixing uniformly to obtain the hair conditioner;
preferably, the mixing homogenization also comprises an emollient.
Compared with the prior art, the invention has the following beneficial effects:
(1) The invention creatively discovers that the composition consisting of the prinsepia utilis royle oil, the olive oil and the papermulberry fruit oil has an obvious moisturizing effect on hair and scalp, has a certain synergistic effect on the effects, and is very suitable for hair care products.
(2) The invention creatively discovers that when the emollient in the hair care product is combined by three components of caprylic/capric triglyceride, ethylhexyl palmitate and isononyl isononanoate, the three components of caprylic/capric triglyceride, ethylhexyl palmitate and isononyl isononanoate have a synergistic effect, and can better improve the moisture retention of hair and scalp.
Detailed Description
To further illustrate the technical means and effects of the present invention, the present invention is further described with reference to the following examples. It is to be understood that the specific embodiments described herein are merely illustrative of the invention and are not limiting of the invention.
The examples do not show the specific techniques or conditions, according to the technical or conditions described in the literature in the field, or according to the product specifications. The reagents or apparatus used are conventional products commercially available from normal sources, not indicated by the manufacturer.
The Prinsepia utilis oil referred to in the following examples, comparative examples, application examples and comparative application examples is a product of type IG0108 available from yunnan english biotechnology limited; olive oil is a product available from yunnan english biotechnology limited with model number IG 1319; the papermulberry fruit oil is a product with the model number of IG1308 purchased from Yunnan England biotechnology limited company; cyclopentadimethylsiloxane is a product available from dow corning under model number DC 345; the polydimethylsiloxane is a product available from Dow under the model number PMX-200; dimethiconol is a product available from wacker under the model number bessil GB 50; (ii) a Dimethicone (and) aminopropyl dimethicone was a product available from san kesy under the model number KF-8020; the rosemary extract is a product of rosemary extract type available from Shanghai Boxuo industries, inc.
The prinsepia utilis royle oil is derived from Yunnan England biotechnology limited, and fatty acid composition measurement is performed by referring to the third method normalization method in GB 5009.168-2016 determination of fatty acid in food safety national standard food, and the results are shown in Table 1.
TABLE 1
Figure BDA0003986237540000071
Figure BDA0003986237540000081
Based on the above experimental determination results, the fatty acid composition ratio of the prinsepia utilis royle oil is as follows: saturated fatty acids monounsaturated fatty acids saturated fatty acids =0.65
The olive oil was obtained from yunnan english biotechnology limited, and the fatty acid composition was measured by the third normalization method in GB 5009.168-2016 national standard for food safety food determination of fatty acids, and the results are shown in table 2.
TABLE 2
Figure BDA0003986237540000082
Based on the above experimental determination results, the fatty acid composition ratio of the used olive oil is as follows: saturated fatty acids monounsaturated fatty acids saturated fatty acids =0.2
The papermulberry fruit seed oil is from the Yunnan England biotechnology limited, and fatty acid composition measurement is performed by referring to the third method normalization method in GB 5009.168-2016 fatty acid measurement in national standard food for food safety, and the results are shown in Table 3.
TABLE 3
Figure BDA0003986237540000091
Based on the above experimental determination results, the used papermulberry fruit oil has the following fatty acid components in proportion: saturated fatty acids monounsaturated fatty acids saturated fatty acids =2
Example 1
The embodiment provides a prinsepia utilis royle oil-containing moisturizing composition for hair, which comprises the following components in parts by weight: 42 parts of prinsepia utilis royle oil, 16 parts of olive oil and 42 parts of papermulberry fruit oil.
The preparation method comprises the following steps: mixing Prinsepia utilis oil, olive oil and Broussonetia papyrifera seed oil under stirring.
Example 2
The embodiment provides a prinsepia utilis royle oil-containing moisturizing composition for hair, which comprises the following components in parts by weight: 42 parts of prinsepia utilis royle oil, 42 parts of olive oil and 16 parts of papermulberry fruit oil.
The preparation method is as in example 1.
Example 3
The embodiment provides a prinsepia utilis royle oil-containing moisturizing composition for hair, which comprises the following components in parts by weight: 60 parts of prinsepia utilis royle oil, 20 parts of olive oil and 20 parts of papermulberry fruit oil.
The preparation method is as in example 1.
Comparative example 1
This comparative example provides a moisturizing composition for hair containing prinsepia utilis royle oil, which differs from example 1 only in that: the olive oil and the papermulberry fruit oil are not contained, and the weight parts of the olive oil and the papermulberry fruit oil are proportionally distributed into the weight parts of the olive oil and the papermulberry fruit oil (37 parts of the olive oil and 63 parts of the papermulberry fruit oil). The preparation method is as in example 1.
Comparative example 2
This comparative example provides a moisturizing composition for hair containing prinsepia utilis royle oil, which differs from example 1 only in that: the olive oil is not contained, and the parts by weight of the olive oil are distributed into the weight of the prinsepia utilis royle oil and the papermulberry fruit oil (50 parts of the prinsepia utilis royle oil and 50 parts of the papermulberry fruit oil) in proportion. The preparation method is as in example 1.
Comparative example 3
This comparative example provides a moisturizing composition for hair containing prinsepia utilis royle oil, which differs from example 1 only in that: the olive oil contains no papermulberry fruit oil, and the weight parts of the papermulberry fruit oil are distributed into the weight parts of the prinsepia utilis royle oil and the olive oil (63 parts of the prinsepia utilis royle oil and 37 parts of the olive oil) in proportion. The preparation method is as in example 1.
Comparative example 4
This comparative example provides only one single component: prinsepia utilis Royle oil.
Comparative example 5
This comparative example provides only one single component: olive oil.
Comparative example 6
This comparative example provides only one single component: papermulberry fruit seed oil.
Comparative example 7
This comparative example provides a moisturizing composition for hair containing prinsepia utilis royle oil, which differs from example 1 only in that: the ingredients are 42 parts of sunflower seed oil, 16 parts of olive oil and 42 parts of papermulberry fruit oil. The preparation method is as in example 1.
Comparative example 8
This comparative example provides a moisturizing composition for hair containing prinsepia utilis royle oil, which differs from example 1 only in that: the ingredients are changed into 42 parts of prinsepia utilis royle oil, 16 parts of sunflower seed oil and 42 parts of paper mulberry fruit oil. The preparation method is as in example 1.
Comparative example 9
This comparative example provides a moisturizing composition for hair containing prinsepia utilis royle oil, which differs from example 1 only in that: the ingredients are changed into 42 parts of prinsepia utilis royle oil, 16 parts of olive oil and 42 parts of sunflower seed oil. The preparation method is as in example 1.
Application example 1
The application example provides a hair moisturizing and hair care oil containing prinsepia utilis royle oil, and the formula is as follows:
Figure BDA0003986237540000111
Figure BDA0003986237540000121
the preparation method comprises the following steps: mixing the solvent and the hair conditioner, homogenizing, adding the brightening agent, the hair moisturizing composition and the antioxidant, and stirring and mixing uniformly to obtain the hair conditioner.
Application example 2
The application example provides a hair moisturizing and hair care oil containing prinsepia utilis royle oil, and the formula is as follows:
Figure BDA0003986237540000122
preparation method reference application example 1.
Application example 3
The application example provides a hair moisturizing and hair care oil containing prinsepia utilis royle oil, and the formula is as follows:
Figure BDA0003986237540000131
preparation method reference application example 1.
Application example 4
The application example provides a hair moisturizing and hair care oil containing prinsepia utilis royle oil, and the formula is as follows:
Figure BDA0003986237540000132
Figure BDA0003986237540000141
preparation method reference application example 1.
Application example 5
The application example provides a hair moisturizing and hair care oil containing prinsepia utilis royle oil, and the formula is as follows:
Figure BDA0003986237540000142
Figure BDA0003986237540000151
preparation method reference application example 1.
Application example 6
The application example provides a hair moisturizing and hair care oil containing prinsepia utilis royle oil, and the formula is as follows:
Figure BDA0003986237540000152
preparation method reference application example 1.
Application example 7
The application example provides a hair moisturizing and hair care oil containing prinsepia utilis royle oil, and the formula is as follows:
Figure BDA0003986237540000161
preparation method reference application example 1.
Application example 8
The application example provides a hair moisturizing and hair care oil containing prinsepia utilis royle oil, and the formula is as follows:
Figure BDA0003986237540000162
Figure BDA0003986237540000171
preparation method reference application example 1.
Application example 9
The application example provides a hair moisturizing and hair care oil containing prinsepia utilis royle oil, and the formula is as follows:
Figure BDA0003986237540000172
Figure BDA0003986237540000182
preparation method reference application example 1.
Application example 10
The application example provides a hair moisturizing and hair care oil containing prinsepia utilis royle oil, and the formula is as follows:
Figure BDA0003986237540000181
preparation method reference application example 1.
Comparative application examples 1 to 9
Nine hair tonics were provided, which differed from application example 1 only in that the compositions of example 1 were respectively replaced with the compositions of comparative examples 1 to 9 in equal amounts, and the other components and contents were kept unchanged. The preparation method is the same as application example 1.
Test example
1. Moisture Performance test of the composition on Hair
(a) 39 bundles (13 groups) of identical flat hair strands (1g, 6inch, slightly damaged hair strand) were pretreated: wetting hair bundles at the water temperature of 37.0 +/-2 ℃, uniformly coating 1mL of 10% sodium lauryl polyoxyethylene ether sulfate (SLES) on each of 3 hair bundles of examples 1-3, comparative examples 1-9 and a control group, gently kneading until the foam is enriched for 1min, removing oil stains on the hair surface, washing at a constant flow rate, hanging the hair bundles in a constant temperature and humidity chamber for balancing two sides of a flat narrow-tooth comb 10 times after the hair bundles are washed clean, and naturally drying.
(b) The weight of the hair tresses was measured using an electronic balance (accuracy 0.0001 g) (initial value), the hair tresses were evenly applied with an amount of 0.1g/g of hair, rubbed for 1min, combed with a comb to evenly attach the composition to the hair tresses until the hair tresses were absorbed, the hair tresses of the control group were treated with clean water instead of the composition, finally the hair tresses were suspended in a constant temperature and humidity chamber at 21 + -1 deg.C and 50 + -10 deg.H RH, the weight of the hair tresses after natural drying was measured using an electronic balance, and the change rates after treatment using samples of different groups were calculated (%) = (test value after using samples-before use)/100% before use), and the measurement results are shown in Table 4.
TABLE 4
Figure BDA0003986237540000191
Figure BDA0003986237540000201
As can be seen from the results in table 4, the hair care moisturizing composition consisting of the prinsepia utilis royle oil, the olive oil and the papermulberry fruit oil has a significant moisturizing effect on hair, and the three components have a certain synergistic effect on the above effects.
2. Hair conditioner moisture Performance test on Hair
(a) 60 tresses (20 groups) of identical flat hair tresses (1g, 6inch, slightly damaged hair tresses) were pretreated: wetting hair bundles at the water temperature of 37.0 +/-2 ℃, uniformly smearing 1mL of 10% SLES on each of 3 hair bundles of application examples 1-10, comparative application examples 1-9 and a control group, gently kneading until rich foam is formed for 1min, removing oil stains on the hair surface, washing at a constant flow rate, hanging the hair bundles in a constant-temperature constant-humidity chamber for balancing, and naturally drying.
(b) The weight of the hair tresses was measured using an electronic balance (accuracy 0.0001 g) (initial value), the hair tresses were evenly applied with an amount of 0.1g/g of hair, rubbed for 1min, combed with a comb to evenly attach the composition to the hair tresses until the hair tresses were absorbed, the hair tresses of the control group were treated with clean water instead of the composition, finally the hair tresses were suspended in a constant temperature and humidity chamber at 21 + -1 deg.C and 50 + -10 deg.H RH, the weight of the hair tresses after natural drying was measured using an electronic balance, and the change rates after treatment using samples of different groups were calculated (%) = (test value after using samples-before use)/100% before use), and the measurement results are shown in Table 5.
TABLE 5
Figure BDA0003986237540000202
Figure BDA0003986237540000211
As can be seen from the results in table 5, the hair care oil containing the prinsepia utilis royle oil, the olive oil and the papermulberry fruit oil has a significant moisturizing effect on hair, and the three have a certain synergistic effect on the above effects, and in addition, when the emollient in the hair care oil is selected from the preferable combination of caprylic/capric triglyceride, ethylhexyl palmitate and isononyl isononanoate, a certain synergistic effect is also achieved, so that the moisturizing effect on hair can be enhanced.
3. Moisture Performance test of hair conditioner to scalp
According to 3D-based epidermal skin model
Figure BDA0003986237540000221
The method for detecting the water content of the skin.
Test consumables and instrumentation: epiGrowth culture solution (Boxi organism), PBS (Solibao), glycerol (national medicine), CO 2 Incubator (Thermo, 150I), ultra-clean bench (SW-CJ-1F, antai Suzhou),
Figure BDA0003986237540000222
CM 825 skin moisture tester (Courage + Khazaka electronic)
The test mode is as follows:
(1) Positive control group (glycerol) working solution preparation: aspirate 400. Mu.L of glycerol in 1.6mL PBS to make 20% glycerol.
Experimental groups: application examples 1-10, comparative application examples 1-9.
Blank control group: how to do is not done.
(2) Testing and grouping according to the table, transferring the model to a 6-well plate (0.9 mL of EpiGrowth culture solution is added in advance), marking the serial number of a test group on the 6-well plate, adding working solution with corresponding concentration into a positive control group (20% glycerol) and an experimental group, uniformly distributing the sample on the surface of the model, placing the model on CO 2 Incubator (37 ℃,5% CO) 2 ) And (4) performing medium incubation for 24h.
(3) The samples on the surface of the model were washed clean and wiped dry, and 24-well plates were prepared and labeled. 0.3mL of EpiGrowth broth was added to each well. And (3) placing the 24-hole plate with the model in a superclean bench, opening the cover of the 24-hole plate, standing for 30min, and then measuring.
(4) Debugging an instrument: will be provided with
Figure BDA0003986237540000223
The CM 825 skin moisture content test probe was connected to the MPA6 adapter, the instrument measurement software was turned on, the measurement parameter was selected as moisture content, the measurement mode was selected as single point measurement, and the probe was cleaned with 75% alcohol.
(5) Wiping water at the bottom of the model, cutting the model from the bottom of the cell chamber by an operation blade, placing the model on a probe of a tester by tweezers to ensure that one surface of the horny layer of the model is completely contacted with the probe, then pressing the probe to measure, measuring each model for 3 times to obtain 9 data, and taking an average value. After the measurement was completed, the probe was cleaned with 75% alcohol, and the next model was measured after the surface of the probe was dried, and the results are shown in table 6.
TABLE 6
Figure BDA0003986237540000231
Figure BDA0003986237540000241
As can be seen from the results in table 6, the hair care oil containing the prinsepia utilis royle oil, the olive oil and the papermulberry fruit oil has a remarkable moisturizing effect on the scalp, and the three have a certain synergistic effect on the above effects.
In conclusion, the invention creatively discovers that the composition consisting of the prinsepia utilis royle oil, the olive oil and the papermulberry fruit oil has a remarkable moisturizing effect on hair and scalp, has a certain synergistic effect on the effects, is very suitable for hair care products, and has a certain synergistic effect when the emollient in the hair care oil is selected from the preferable combination mode of caprylic/capric triglyceride, ethylhexyl palmitate and isononyl isononanoate, so that the moisturizing effect on hair and scalp can be enhanced.
The applicant states that the present invention is illustrated in detail by the above examples, but the present invention is not limited to the above detailed methods, i.e. it is not meant that the present invention must rely on the above detailed methods for its implementation. It should be understood by those skilled in the art that any modifications of the present invention, equivalent substitutions of the raw materials of the product of the present invention, and the addition of auxiliary components, selection of specific modes, etc., are within the scope and disclosure of the present invention.

Claims (10)

1. The Prinsepia utilis royle oil-containing hair moisturizing composition is characterized by comprising Prinsepia utilis royle oil, olive oil and paper mulberry fruit oil.
2. The prinsepia utilis royle oil-containing hair moisturizing composition according to claim 1, wherein the mass ratio of the prinsepia utilis royle oil, the olive oil and the papermulberry fruit oil is (35-60): (10-45).
3. Use of the prinsepia utilis royle oil-containing hair moisturizing composition of claim 1 or 2 in the preparation of a hair product.
4. Use according to claim 3, wherein the hair product comprises a hair oil, conditioner, shampoo or hair mask;
preferably, the weight percentage of the prinsepia utilis royle oil-containing hair moisturizing composition in the hair product is 1-10%, and more preferably 2-5%.
5. The method for preparing the prinsepia utilis royle oil-containing moisturizing composition for hair according to claim 1 or 2, wherein the preparation method comprises: weighing Prinsepia utilis oil, olive oil and Broussonetia papyrifera seed oil respectively, and mixing the raw materials uniformly to obtain the composition.
6. A Prinsepia utilis oil-containing moisturizing and hair care oil for hair, characterized by comprising: a hair moisturizing composition, solvent, hair conditioner, shine agent, and antioxidant according to claim 1 or 2.
7. The Prinsepia utilis oil-containing hair moisturizing and hair care oil according to claim 6, further comprising a softening agent;
preferably, the emollient comprises any one or a combination of at least two of caprylic/capric triglyceride, ethylhexyl palmitate, ethylhexyl cetyl palmitate, isononyl isononanoate or squalane;
preferably, the emollient is a combination of caprylic/capric triglyceride, ethylhexyl palmitate and isononyl isononanoate.
8. The Prinsepia utilis oil-containing hair moisturizing and hair care oil according to claim 6 or 7, comprising in parts by weight: the hair moisturizing composition containing prinsepia utilis royle oil of claim 1 or 2, 1-10 parts of solvent, 50-100 parts of softening agent, 0.5-5 parts of conditioning agent for hair, 1-6 parts of brightening agent and 0.15-0.5 part of antioxidant.
9. The Prinsepia utilis oil-containing hair moisturizing and hair care oil according to any one of claims 6 to 8, wherein the solvent comprises any one or a combination of at least two of cyclopentadidimethyl siloxane, isododecane, or polydimethylsiloxane;
preferably, the hair conditioning agent comprises any one of or a combination of at least two of dimethiconol, amodimethicone or phenyl trimethicone;
preferably, the gloss agent comprises polydimethylsiloxane (and) aminopropylpolydimethylsiloxane and/or PPG-3 octyl ether;
preferably, the antioxidant comprises any one of or a combination of at least two of tocopherol acetate, rosemary extract or pentaerythritol ester.
10. The method for preparing the prinsepia utilis royle oil-containing moisturizing and hair-care oil for hair according to any one of claims 6 to 9, wherein the preparation method comprises the following steps:
mixing solvent and hair conditioner, homogenizing, adding brightener, hair moisturizing composition containing Prinsepia utilis Royle oil and antioxidant, stirring, and mixing;
preferably, the mixing homogenization also comprises an emollient.
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