CN115885993A - Plant growth regulating compositions, formulations, uses and methods of application - Google Patents
Plant growth regulating compositions, formulations, uses and methods of application Download PDFInfo
- Publication number
- CN115885993A CN115885993A CN202111165347.8A CN202111165347A CN115885993A CN 115885993 A CN115885993 A CN 115885993A CN 202111165347 A CN202111165347 A CN 202111165347A CN 115885993 A CN115885993 A CN 115885993A
- Authority
- CN
- China
- Prior art keywords
- plant growth
- active ingredient
- growth regulating
- cotton
- plant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 87
- 230000008635 plant growth Effects 0.000 title claims abstract description 75
- 230000001105 regulatory effect Effects 0.000 title claims abstract description 72
- 238000000034 method Methods 0.000 title claims abstract description 24
- 238000009472 formulation Methods 0.000 title claims description 12
- 239000004480 active ingredient Substances 0.000 claims abstract description 80
- DARPYRSDRJYGIF-PTNGSMBKSA-N (Z)-3-ethoxy-2-naphthalen-2-ylsulfonylprop-2-enenitrile Chemical compound C1=CC=CC2=CC(S(=O)(=O)C(\C#N)=C/OCC)=CC=C21 DARPYRSDRJYGIF-PTNGSMBKSA-N 0.000 claims abstract description 50
- 238000002360 preparation method Methods 0.000 claims abstract description 37
- 239000005648 plant growth regulator Substances 0.000 claims abstract description 33
- 150000003839 salts Chemical class 0.000 claims abstract description 22
- 150000002148 esters Chemical class 0.000 claims abstract description 21
- RSVPPPHXAASNOL-UHFFFAOYSA-N Prodiamine Chemical compound CCCN(CCC)C1=C([N+]([O-])=O)C=C(C(F)(F)F)C(N)=C1[N+]([O-])=O RSVPPPHXAASNOL-UHFFFAOYSA-N 0.000 claims abstract description 19
- 229920000742 Cotton Polymers 0.000 claims description 89
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 47
- 241000196324 Embryophyta Species 0.000 claims description 45
- 235000013399 edible fruits Nutrition 0.000 claims description 35
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 30
- UDPGUMQDCGORJQ-UHFFFAOYSA-N (2-chloroethyl)phosphonic acid Chemical compound OP(O)(=O)CCCl UDPGUMQDCGORJQ-UHFFFAOYSA-N 0.000 claims description 27
- 239000005976 Ethephon Substances 0.000 claims description 26
- 238000005507 spraying Methods 0.000 claims description 23
- 239000007788 liquid Substances 0.000 claims description 19
- 239000003995 emulsifying agent Substances 0.000 claims description 18
- 239000002270 dispersing agent Substances 0.000 claims description 13
- 230000017260 vegetative to reproductive phase transition of meristem Effects 0.000 claims description 13
- 239000004563 wettable powder Substances 0.000 claims description 13
- 239000005987 S-Abscisic acid Substances 0.000 claims description 12
- 239000000080 wetting agent Substances 0.000 claims description 10
- RMOGWMIKYWRTKW-UONOGXRCSA-N (S,S)-paclobutrazol Chemical compound C([C@@H]([C@@H](O)C(C)(C)C)N1N=CN=C1)C1=CC=C(Cl)C=C1 RMOGWMIKYWRTKW-UONOGXRCSA-N 0.000 claims description 9
- 239000005985 Paclobutrazol Substances 0.000 claims description 9
- 239000000969 carrier Substances 0.000 claims description 9
- 239000004530 micro-emulsion Substances 0.000 claims description 9
- 239000007787 solid Substances 0.000 claims description 8
- 239000012752 auxiliary agent Substances 0.000 claims description 7
- 239000004094 surface-active agent Substances 0.000 claims description 7
- 239000002562 thickening agent Substances 0.000 claims description 6
- YNWVFADWVLCOPU-MDWZMJQESA-N (1E)-1-(4-chlorophenyl)-4,4-dimethyl-2-(1H-1,2,4-triazol-1-yl)pent-1-en-3-ol Chemical compound C1=NC=NN1/C(C(O)C(C)(C)C)=C/C1=CC=C(Cl)C=C1 YNWVFADWVLCOPU-MDWZMJQESA-N 0.000 claims description 5
- PWVXXGRKLHYWKM-UHFFFAOYSA-N 5-[2-(benzenesulfonyl)ethyl]-3-[(1-methylpyrrolidin-2-yl)methyl]-1h-indole Chemical compound CN1CCCC1CC(C1=C2)=CNC1=CC=C2CCS(=O)(=O)C1=CC=CC=C1 PWVXXGRKLHYWKM-UHFFFAOYSA-N 0.000 claims description 5
- 230000001276 controlling effect Effects 0.000 claims description 5
- 239000008187 granular material Substances 0.000 claims description 5
- 239000000375 suspending agent Substances 0.000 claims description 5
- 239000004562 water dispersible granule Substances 0.000 claims description 5
- 239000002671 adjuvant Substances 0.000 claims description 4
- 239000000839 emulsion Substances 0.000 claims description 4
- 239000003755 preservative agent Substances 0.000 claims description 4
- 230000002335 preservative effect Effects 0.000 claims description 4
- 150000001298 alcohols Chemical class 0.000 claims description 3
- 150000001408 amides Chemical class 0.000 claims description 3
- 230000002528 anti-freeze Effects 0.000 claims description 3
- 150000001491 aromatic compounds Chemical class 0.000 claims description 3
- 125000000623 heterocyclic group Chemical group 0.000 claims description 3
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 3
- 150000002576 ketones Chemical class 0.000 claims description 3
- 239000011707 mineral Substances 0.000 claims description 3
- 239000013530 defoamer Substances 0.000 claims description 2
- 241000208125 Nicotiana Species 0.000 claims 3
- HKPHPIREJKHECO-UHFFFAOYSA-N butachlor Chemical compound CCCCOCN(C(=O)CCl)C1=C(CC)C=CC=C1CC HKPHPIREJKHECO-UHFFFAOYSA-N 0.000 claims 1
- 239000000575 pesticide Substances 0.000 abstract description 21
- 230000002195 synergetic effect Effects 0.000 abstract description 18
- 230000002829 reductive effect Effects 0.000 abstract description 12
- 230000002045 lasting effect Effects 0.000 abstract description 9
- 230000000361 pesticidal effect Effects 0.000 abstract description 4
- 230000002035 prolonged effect Effects 0.000 abstract description 3
- 241000219146 Gossypium Species 0.000 description 87
- 238000012360 testing method Methods 0.000 description 70
- 230000000052 comparative effect Effects 0.000 description 52
- 239000000126 substance Substances 0.000 description 48
- 230000000694 effects Effects 0.000 description 45
- 244000061176 Nicotiana tabacum Species 0.000 description 44
- 230000012010 growth Effects 0.000 description 37
- 238000011282 treatment Methods 0.000 description 26
- 239000003795 chemical substances by application Substances 0.000 description 24
- 230000001965 increasing effect Effects 0.000 description 24
- 240000002024 Gossypium herbaceum Species 0.000 description 22
- 235000004341 Gossypium herbaceum Nutrition 0.000 description 22
- 239000002689 soil Substances 0.000 description 17
- 238000011156 evaluation Methods 0.000 description 14
- 239000003814 drug Substances 0.000 description 12
- 230000005764 inhibitory process Effects 0.000 description 12
- -1 carbitol Substances 0.000 description 11
- 239000003337 fertilizer Substances 0.000 description 11
- 239000002904 solvent Substances 0.000 description 11
- 230000001737 promoting effect Effects 0.000 description 10
- 239000000945 filler Substances 0.000 description 9
- 238000002156 mixing Methods 0.000 description 8
- 230000000295 complement effect Effects 0.000 description 7
- 230000002401 inhibitory effect Effects 0.000 description 7
- 238000003973 irrigation Methods 0.000 description 7
- 230000002262 irrigation Effects 0.000 description 7
- 229940051841 polyoxyethylene ether Drugs 0.000 description 7
- 229920000056 polyoxyethylene ether Polymers 0.000 description 7
- 238000010998 test method Methods 0.000 description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 6
- 235000020971 citrus fruits Nutrition 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 239000004575 stone Substances 0.000 description 6
- 235000013311 vegetables Nutrition 0.000 description 6
- 238000005303 weighing Methods 0.000 description 6
- 241000207199 Citrus Species 0.000 description 5
- 239000005978 Flumetralin Substances 0.000 description 5
- PWNAWOCHVWERAR-UHFFFAOYSA-N Flumetralin Chemical compound [O-][N+](=O)C=1C=C(C(F)(F)F)C=C([N+]([O-])=O)C=1N(CC)CC1=C(F)C=CC=C1Cl PWNAWOCHVWERAR-UHFFFAOYSA-N 0.000 description 5
- 230000000857 drug effect Effects 0.000 description 5
- 241000238631 Hexapoda Species 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- NNCAWEWCFVZOGF-UHFFFAOYSA-N mepiquat Chemical group C[N+]1(C)CCCCC1 NNCAWEWCFVZOGF-UHFFFAOYSA-N 0.000 description 4
- 239000002420 orchard Substances 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 239000004546 suspension concentrate Substances 0.000 description 4
- 238000011179 visual inspection Methods 0.000 description 4
- QFMDFTQOJHFVNR-UHFFFAOYSA-N 1-[2,2-dichloro-1-(4-ethylphenyl)ethyl]-4-ethylbenzene Chemical compound C1=CC(CC)=CC=C1C(C(Cl)Cl)C1=CC=C(CC)C=C1 QFMDFTQOJHFVNR-UHFFFAOYSA-N 0.000 description 3
- 239000005995 Aluminium silicate Substances 0.000 description 3
- 229920005682 EO-PO block copolymer Polymers 0.000 description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- 239000005984 Mepiquat Substances 0.000 description 3
- FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 230000009471 action Effects 0.000 description 3
- 230000009418 agronomic effect Effects 0.000 description 3
- 235000012211 aluminium silicate Nutrition 0.000 description 3
- SRSXLGNVWSONIS-UHFFFAOYSA-N benzenesulfonic acid Chemical compound OS(=O)(=O)C1=CC=CC=C1 SRSXLGNVWSONIS-UHFFFAOYSA-N 0.000 description 3
- 238000004166 bioassay Methods 0.000 description 3
- 229920005551 calcium lignosulfonate Polymers 0.000 description 3
- RYAGRZNBULDMBW-UHFFFAOYSA-L calcium;3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfonatopropyl)phenoxy]propane-1-sulfonate Chemical compound [Ca+2].COC1=CC=CC(CC(CS([O-])(=O)=O)OC=2C(=CC(CCCS([O-])(=O)=O)=CC=2)OC)=C1O RYAGRZNBULDMBW-UHFFFAOYSA-L 0.000 description 3
- 239000006229 carbon black Substances 0.000 description 3
- 239000004927 clay Substances 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 230000018109 developmental process Effects 0.000 description 3
- 230000006872 improvement Effects 0.000 description 3
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 3
- 235000015097 nutrients Nutrition 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 230000001850 reproductive effect Effects 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- 235000015424 sodium Nutrition 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- 238000009331 sowing Methods 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 230000035882 stress Effects 0.000 description 3
- ZSDSQXJSNMTJDA-UHFFFAOYSA-N trifluralin Chemical compound CCCN(CCC)C1=C([N+]([O-])=O)C=C(C(F)(F)F)C=C1[N+]([O-])=O ZSDSQXJSNMTJDA-UHFFFAOYSA-N 0.000 description 3
- 230000000007 visual effect Effects 0.000 description 3
- 238000009333 weeding Methods 0.000 description 3
- 244000105624 Arachis hypogaea Species 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- HDWLTPUVRXPMFW-UHFFFAOYSA-N C(CCCCCCCCCCC)OS(=O)(=O)C1=CC=CC=C1.[Ca].[Ca] Chemical compound C(CCCCCCCCCCC)OS(=O)(=O)C1=CC=CC=C1.[Ca].[Ca] HDWLTPUVRXPMFW-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
- 239000005983 Maleic hydrazide Substances 0.000 description 2
- BGRDGMRNKXEXQD-UHFFFAOYSA-N Maleic hydrazide Chemical compound OC1=CC=C(O)N=N1 BGRDGMRNKXEXQD-UHFFFAOYSA-N 0.000 description 2
- 240000007594 Oryza sativa Species 0.000 description 2
- 235000007164 Oryza sativa Nutrition 0.000 description 2
- 231100000674 Phytotoxicity Toxicity 0.000 description 2
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 description 2
- 235000021307 Triticum Nutrition 0.000 description 2
- 244000098338 Triticum aestivum Species 0.000 description 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 2
- 241000219094 Vitaceae Species 0.000 description 2
- 235000009754 Vitis X bourquina Nutrition 0.000 description 2
- 235000012333 Vitis X labruscana Nutrition 0.000 description 2
- 240000006365 Vitis vinifera Species 0.000 description 2
- 235000014787 Vitis vinifera Nutrition 0.000 description 2
- 240000008042 Zea mays Species 0.000 description 2
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 2
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 238000012271 agricultural production Methods 0.000 description 2
- 239000002518 antifoaming agent Substances 0.000 description 2
- 239000000440 bentonite Substances 0.000 description 2
- 229910000278 bentonite Inorganic materials 0.000 description 2
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 2
- 229940077388 benzenesulfonate Drugs 0.000 description 2
- 230000004071 biological effect Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 235000013339 cereals Nutrition 0.000 description 2
- 230000002301 combined effect Effects 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 235000005822 corn Nutrition 0.000 description 2
- 235000012343 cottonseed oil Nutrition 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 235000014113 dietary fatty acids Nutrition 0.000 description 2
- 239000003085 diluting agent Substances 0.000 description 2
- 239000002552 dosage form Substances 0.000 description 2
- 239000000194 fatty acid Substances 0.000 description 2
- 229930195729 fatty acid Natural products 0.000 description 2
- 150000002191 fatty alcohols Chemical class 0.000 description 2
- 235000021021 grapes Nutrition 0.000 description 2
- 239000001963 growth medium Substances 0.000 description 2
- 239000003630 growth substance Substances 0.000 description 2
- 230000002363 herbicidal effect Effects 0.000 description 2
- 239000004009 herbicide Substances 0.000 description 2
- PVOAHINGSUIXLS-UHFFFAOYSA-O hydron;1-methylpiperazine Chemical compound CN1CC[NH2+]CC1 PVOAHINGSUIXLS-UHFFFAOYSA-O 0.000 description 2
- 238000011835 investigation Methods 0.000 description 2
- HJOVHMDZYOCNQW-UHFFFAOYSA-N isophorone Chemical compound CC1=CC(=O)CC(C)(C)C1 HJOVHMDZYOCNQW-UHFFFAOYSA-N 0.000 description 2
- 230000002147 killing effect Effects 0.000 description 2
- 238000004898 kneading Methods 0.000 description 2
- 238000009533 lab test Methods 0.000 description 2
- 230000000670 limiting effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000035800 maturation Effects 0.000 description 2
- 239000002609 medium Substances 0.000 description 2
- 230000004060 metabolic process Effects 0.000 description 2
- 235000010755 mineral Nutrition 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 229960000988 nystatin Drugs 0.000 description 2
- VQOXZBDYSJBXMA-NQTDYLQESA-N nystatin A1 Chemical compound O[C@H]1[C@@H](N)[C@H](O)[C@@H](C)O[C@H]1O[C@H]1/C=C/C=C/C=C/C=C/CC/C=C/C=C/[C@H](C)[C@@H](O)[C@@H](C)[C@H](C)OC(=O)C[C@H](O)C[C@H](O)C[C@H](O)CC[C@@H](O)[C@H](O)C[C@](O)(C[C@H](O)[C@H]2C(O)=O)O[C@H]2C1 VQOXZBDYSJBXMA-NQTDYLQESA-N 0.000 description 2
- 239000005416 organic matter Substances 0.000 description 2
- 230000036961 partial effect Effects 0.000 description 2
- 235000020232 peanut Nutrition 0.000 description 2
- 230000001766 physiological effect Effects 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 238000004382 potting Methods 0.000 description 2
- 235000009566 rice Nutrition 0.000 description 2
- 230000005070 ripening Effects 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 235000017060 Arachis glabrata Nutrition 0.000 description 1
- 235000010777 Arachis hypogaea Nutrition 0.000 description 1
- 235000018262 Arachis monticola Nutrition 0.000 description 1
- 229930192334 Auxin Natural products 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 208000003643 Callosities Diseases 0.000 description 1
- 239000005974 Chlormequat Substances 0.000 description 1
- 235000007516 Chrysanthemum Nutrition 0.000 description 1
- 244000189548 Chrysanthemum x morifolium Species 0.000 description 1
- 229920002261 Corn starch Polymers 0.000 description 1
- 239000005780 Fluazinam Substances 0.000 description 1
- 235000016623 Fragaria vesca Nutrition 0.000 description 1
- 240000009088 Fragaria x ananassa Species 0.000 description 1
- 235000011363 Fragaria x ananassa Nutrition 0.000 description 1
- 235000009438 Gossypium Nutrition 0.000 description 1
- 206010020649 Hyperkeratosis Diseases 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000005909 Kieselgur Substances 0.000 description 1
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 1
- 239000006057 Non-nutritive feed additive Substances 0.000 description 1
- 208000012868 Overgrowth Diseases 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 239000004372 Polyvinyl alcohol Substances 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 244000061456 Solanum tuberosum Species 0.000 description 1
- 235000002595 Solanum tuberosum Nutrition 0.000 description 1
- 241001464837 Viridiplantae Species 0.000 description 1
- 239000001089 [(2R)-oxolan-2-yl]methanol Substances 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 230000006578 abscission Effects 0.000 description 1
- 235000010489 acacia gum Nutrition 0.000 description 1
- 239000001785 acacia senegal l. willd gum Substances 0.000 description 1
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- SNAAJJQQZSMGQD-UHFFFAOYSA-N aluminum magnesium Chemical compound [Mg].[Al] SNAAJJQQZSMGQD-UHFFFAOYSA-N 0.000 description 1
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 1
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 1
- 235000011130 ammonium sulphate Nutrition 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 239000002363 auxin Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- SMLHHBQGIJMAIM-UHFFFAOYSA-N calcium;2-dodecylbenzenesulfonic acid Chemical compound [Ca].CCCCCCCCCCCCC1=CC=CC=C1S(O)(=O)=O SMLHHBQGIJMAIM-UHFFFAOYSA-N 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 239000001768 carboxy methyl cellulose Substances 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 230000032823 cell division Effects 0.000 description 1
- JUZXDNPBRPUIOR-UHFFFAOYSA-N chlormequat Chemical compound C[N+](C)(C)CCCl JUZXDNPBRPUIOR-UHFFFAOYSA-N 0.000 description 1
- 239000000306 component Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000008120 corn starch Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 230000006806 disease prevention Effects 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 230000005059 dormancy Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000004495 emulsifiable concentrate Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 230000035558 fertility Effects 0.000 description 1
- UZCGKGPEKUCDTF-UHFFFAOYSA-N fluazinam Chemical compound [O-][N+](=O)C1=CC(C(F)(F)F)=C(Cl)C([N+]([O-])=O)=C1NC1=NC=C(C(F)(F)F)C=C1Cl UZCGKGPEKUCDTF-UHFFFAOYSA-N 0.000 description 1
- 230000005078 fruit development Effects 0.000 description 1
- 230000005094 fruit set Effects 0.000 description 1
- 230000035784 germination Effects 0.000 description 1
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 239000005556 hormone Substances 0.000 description 1
- 229940088597 hormone Drugs 0.000 description 1
- 210000000987 immune system Anatomy 0.000 description 1
- SEOVTRFCIGRIMH-UHFFFAOYSA-N indole-3-acetic acid Chemical compound C1=CC=C2C(CC(=O)O)=CNC2=C1 SEOVTRFCIGRIMH-UHFFFAOYSA-N 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 238000010902 jet-milling Methods 0.000 description 1
- 230000003137 locomotive effect Effects 0.000 description 1
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 1
- 235000019341 magnesium sulphate Nutrition 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000003375 plant hormone Substances 0.000 description 1
- 229920005646 polycarboxylate Polymers 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
- 229920000053 polysorbate 80 Polymers 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 235000019422 polyvinyl alcohol Nutrition 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 235000012015 potatoes Nutrition 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000013138 pruning Methods 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000026267 regulation of growth Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000002786 root growth Effects 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000009758 senescence Effects 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 description 1
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 description 1
- 229920005552 sodium lignosulfonate Polymers 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
- 235000015096 spirit Nutrition 0.000 description 1
- 235000020354 squash Nutrition 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- BSYVTEYKTMYBMK-UHFFFAOYSA-N tetrahydrofurfuryl alcohol Chemical compound OCC1CCCO1 BSYVTEYKTMYBMK-UHFFFAOYSA-N 0.000 description 1
- 238000004078 waterproofing Methods 0.000 description 1
- 239000000230 xanthan gum Substances 0.000 description 1
- 235000010493 xanthan gum Nutrition 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
- 229940082509 xanthan gum Drugs 0.000 description 1
- 238000004383 yellowing Methods 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
Abstract
The invention provides a plant growth regulating composition, a preparation, an application and an application method, and relates to the technical field of plant growth regulators, wherein the plant growth regulating composition comprises an active ingredient A and an active ingredient B, and the active ingredient A is selected from at least one of prodiamine and derivatives thereof or agriculturally acceptable salts or esters thereof; the active ingredient B is selected from at least one of mepiquat chloride and derivatives thereof or agriculturally acceptable salts or esters thereof. The composition may also comprise an active ingredient C. The plant growth regulating composition provided by the invention has a remarkable synergistic effect by mutually matching the active ingredient A and the active ingredient B or further matching the active ingredient C, so that the safety is higher, the pesticide effect is more stable, the lasting period can be effectively prolonged, the pesticide application frequency is reduced, and the yield is improved.
Description
Technical Field
The invention relates to the technical field of plant growth regulators, in particular to a plant growth regulating composition, a preparation, an application and an application method.
Background
Higher plants almost have top advantages in their growth. The growth of the stem, the root, the lateral bud and the lateral root of the plant is inhibited by the growth of the main stem and the main root; when the main stem and the main root are removed, the lateral bud and the lateral root can grow without limitation, and the phenomenon is called as apical dominance. For example, cotton has the characteristic of unlimited growth, has obvious apical dominance, and can continuously grow upwards and simultaneously continuously differentiate new branches, stems and leaves under the condition of environment suitable. The growth of the main stem, ineffective buds, bolls and branches with unlimited growth consumes nutrients, so that the nutrition of plants is declined, and the growth and development of effective fruits are further influenced.
Pruning and topping are a technology for removing apical dominance, promoting reproductive growth and improving yield. The topping can control the longitudinal growth of the main stem, reduce the plant height, reduce the growth of ineffective nutrition, play a great role in the growth and development of reproductive organs, and can adjust the nutrient transmission direction of the plant body by timely and vigorously topping, so that more nutrients are transported to flowers and fruits and roots, the generation of ineffective flowers and fruits is reduced, and the effect of increasing the yield is obvious. The traditional topping is to manually nip and remove main stem growing points or trim branches, and the method has the defects of low production efficiency, high labor cost, large consumption of manpower and material resources and missing topping. Although the mechanical topping efficiency is high, the mechanical damage to plants is large, and the normal growth of the plants is not facilitated.
The chemical topping-free technology utilizes plant growth regulating substances to inhibit the growth of plant tops, group tops and vegetative branches, thereby achieving the purpose similar to artificial topping. The plant growth regulator can be sprayed in the field by machinery, so that the labor intensity can be reduced, the topping efficiency can be improved, and the labor cost can be saved. In recent years, chemical topping, shoot control and vigor control technologies using plant growth regulators such as mepiquat chloride, chlormequat chloride and paclobutrazol have been widely used in production.
The plant growth regulator is artificially synthesized chemical matter with plant growth regulating effect and natural plant hormone extracted from organism. At present, many plant growth regulators are used alone, often cannot achieve ideal effects, and have certain defects or bring certain side effects: if the biological activity is single, the growth regulation effect is relatively low, and generally the plant can only play a limited role in a certain growth period of crops. For example, the mepiquat chloride is a commonly used plant growth regulator in agricultural production, and can inhibit the overgrowth of stems and leaves, control lateral branches and shape an ideal plant type, so that the number and the activity of plant roots are improved, the reproductive growth of plants is promoted, the weight of fruits is increased, and the quality of the fruits is improved; the fertilizer is widely applied to crops such as cotton, wheat, rice, peanuts, corns, potatoes, grapes, vegetables, beans, flowers and the like. However, the current mepiquat chloride is generally used for a plurality of times in a single dose, and the problems of unstable drug effect, poor effect of inhibiting the growth of axillary buds, need to be used for a plurality of times, easy induction of the greedy and late maturity of crops and the like exist in the use of the mepiquat chloride.
With the continuous improvement of the automation and mechanization degree of modern agriculture, the market demand for novel chemical topping and tip control products with stable action effect and good crop safety is increasing, and the invention is especially provided in view of the above.
Disclosure of Invention
It is an object of the present invention to provide a plant growth regulating composition that ameliorates the technical problems associated with the current use of a single agent of mepiquat chloride.
The plant growth regulating composition provided by the invention comprises an active ingredient A and an active ingredient B, wherein the active ingredient A is selected from at least one of prodiamine and derivatives or agriculturally acceptable salts or esters thereof; the active ingredient B is at least one selected from the group consisting of mepiquat chloride and derivatives thereof or agriculturally acceptable salts or esters thereof.
Further, the mass ratio of the active ingredient A to the active ingredient B is 0.01-100, preferably 0.01-20.
Further, the composition can also comprise an active ingredient C, when the active ingredient C is ethephon, the mass ratio of the active ingredient A to the active ingredient B to the active ingredient C is 0.01-100; when the active component C is the S-abscisic acid, the mass ratio of the active component A to the active component B to the active component C is 0.01-100.
Further, the active ingredient C is selected from at least one of ethephon, maleic hydrazide, uniconazole, paclobutrazol, chlormequat chloride, S-abscisic acid and derivatives or agriculturally acceptable salts or esters thereof.
Further, the total content of the active ingredients A, B and optionally C is 0.1-99%, preferably 5-80%, more preferably 20-80% by mass of the plant growth regulating composition.
Further, the plant growth regulating composition also comprises an auxiliary agent and/or a carrier;
preferably, the carrier is a solid or a liquid;
further, preferably, the liquid includes at least one of water, aromatic compounds, paraffins, alcohols, ketones, amides, esters, and heterocycles;
preferably, the solid comprises at least one of natural minerals, carriers of vegetable origin, carriers of synthetic type and inorganic salts.
Preferably, the auxiliary agent comprises at least one of a surfactant, a thickener, an antifreeze, a defoamer and a preservative;
preferably, the surfactant includes at least one of a wetting agent, a dispersing agent, and an emulsifying agent.
The other purpose of the invention is to provide a plant growth regulating preparation, which comprises the plant growth regulating composition provided by the first purpose of the invention;
preferably, the formulation of the plant growth regulating preparation comprises one of a suspending agent, an emulsifiable solution, a wettable powder, a water dispersible granule, an aqueous emulsion, a microemulsion or a granule.
The invention also aims to provide the application of the plant growth composition or the plant growth regulating preparation in cotton topping, fruit tree tip control or tobacco bud inhibition.
The fourth purpose of the invention is to provide a using method of the plant growth regulating preparation, which comprises the following steps:
when the plant growth regulating preparation provided by the invention is applied to cotton fields, the plant growth regulating preparation provided by the invention is sprayed on cotton by stem and leaf spraying from the initial flowering period to the full flowering period of the cotton.
When the plant growth regulator preparation provided by the invention is applied to fruit trees, the plant growth regulator preparation provided by the invention is sprayed on the branch tips of the fruit trees by adopting spraying when the tender tips of the fruit trees germinate to the germination stage.
When the plant growth regulator provided by the invention is applied to a tobacco planting area, the plant growth regulator provided by the invention is applied to tobacco by adopting a stem and leaf spraying, smearing or cup spraying method in the initial flowering period of the tobacco.
The invention has at least the following beneficial effects:
the plant growth regulating composition provided by the invention has a remarkable synergistic effect by mutually matching the active ingredient A, the active ingredient B and the optional active ingredient C, has higher safety and more stable drug effect, can effectively increase the lasting period, reduce the application times and improve the yield.
The plant growth regulator provided by the invention is simple in application method and easy to operate, and can be used for obviously reducing the dosage of single mepiquat chloride, increasing the lasting period, reducing the application times, promoting the fruit development and maturity and effectively improving the yield of cotton, fruits and tobacco.
Detailed Description
The technical solutions of the present invention will be described clearly and completely with reference to the following embodiments, and it should be understood that the described embodiments are some, but not all, embodiments of the present invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
According to a first aspect of the present invention there is provided a plant growth regulating composition comprising an active ingredient A selected from one or more of prodiamine and derivatives thereof or agriculturally acceptable salts or esters thereof and an active ingredient B selected from one or more of mepiquat chloride and derivatives thereof or agriculturally acceptable salts or esters thereof.
The chemical name of the prodiamine is 2, 4-binitro-N3, N3-dipropyl-6- (trifluoromethyl) -1, 3-phenylenediamine, and the CAS registration number is as follows: 29091-21-2. Prodiamine is a selective preemergence soil-blocking herbicide and mainly acts in a mode of inhibiting the formation of spindles so as to inhibit cell division and the growth of roots and buds. The prodiamine is mainly used as a herbicide for lawn weeding and has no report on the application of the prodiamine as a plant growth regulator.
The chemical name of mepiquat chloride is 1, 1-dimethylpiperidinium, and the CAS registry number is: 24307-26-4. At present, mepiquat chloride is generally continuously used in a single dose in agricultural production, and the problems of unstable pesticide effect, poor effect of inhibiting the growth of axillary buds, improvement of resistance, increase of dosage and the like exist in the use of the mepiquat chloride.
In the present invention, the prodiamine-based substance is a generic name of prodiamine and its derivatives or agriculturally acceptable salts or esters thereof, and the mepiquat chloride-based substance is a generic name of mepiquat chloride and its derivatives or agriculturally acceptable salts or esters thereof.
The inventor finds that the trifluralin substance and the mepiquat chloride substance have synergistic effect on plant growth when being mutually matched and acted on plants in research. The trifluralin substance and the mepiquat chloride substance are applied to plants together or sequentially, the growth of cotton buds and vegetative branches, fruit tree ineffective branch tips and tobacco ineffective axillary buds can be obviously inhibited, and the efficiency of controlling the growth of the cotton buds and vegetative branches, the fruit tree ineffective branch tips and the tobacco ineffective axillary buds is higher than that of singly applying the mepiquat chloride substance.
In the present invention, "regulating growth" includes limiting or promoting shoot growth, limiting or promoting root growth, hindering or promoting development, and the like.
In the present invention, "to apply together" means that two or more kinds of pesticides, fertilizers and auxiliaries are applied to a plant simultaneously or sequentially within a certain period of time, for example, within one day or one week.
The above "plant" refers to all tangible parts of a plant, including seeds, seedlings, plantlets, roots, tubers, stems, stalks, leaves, and fruits, and combinations thereof.
The plant growth regulating composition provided by the invention has a remarkable synergistic effect by mutually matching the active ingredient A (aminotrifluralin substances) and the active ingredient B (mepiquat chloride substances), so that the safety is higher, the drug effect is more stable, the lasting period can be effectively prolonged, the application frequency is reduced, and the yield is improved.
In a preferred embodiment of the present invention, when the mass ratio of the active ingredient a to the active ingredient B in the plant growth regulating composition provided by the present invention is 0.01 to 100, the two have an obvious synergistic effect when used in combination.
Typically but not by way of limitation, the mass ratio of active ingredient a and active ingredient B is 0.01.
Preferably, when the mass ratio of the active ingredient a to the active ingredient B in the plant growth regulator composition is 0.01 to 20.
In a preferred embodiment of the present invention, the composition further comprises an active ingredient C selected from at least one of ethephon, maleic hydrazide, uniconazole, paclobutrazol, chlormequat chloride and S-abscisic acid. After the active ingredient C is added into the composition, the cotton maturation can be obviously promoted, and the cotton yield is obviously improved.
The ethephon substances are collectively called ethephon and derivatives thereof or agriculturally acceptable salts or esters thereof, the nystatin substances are collectively called nystatin and derivatives thereof or agriculturally acceptable salts or esters thereof, the uniconazole substances are collectively called uniconazole and derivatives thereof or agriculturally acceptable salts or esters thereof, the paclobutrazol substances are collectively called paclobutrazol and derivatives thereof or agriculturally acceptable salts or esters thereof, the chlormequat substances are collectively called chlormequat chloride and derivatives thereof or agriculturally acceptable salts or esters thereof, and the S-abscisic substances are collectively called S-abscisic acid and derivatives thereof or agriculturally acceptable salts or esters thereof.
Wherein ethephon is a high-quality and high-efficiency plant growth regulator, and the CAS registration number is as follows: 16672-87-0. Has physiological effects of promoting ripening, abscission, aging, and flowering, and breaking dormancy, and can be used for promoting ripening, falling and flower differentiation of plant fruit; meanwhile, the plant growth regulator has the effects of inhibiting the synthesis of endogenous auxin and delaying the growth of plants, and has the physiological effects of promoting the flowering of plants and accelerating the maturation. The S-abscisic acid (S-ABA) is a pure natural product contained in green plants and is a key factor for balancing plant endogenous hormones and related metabolism of growth active substances. Has the functions of promoting plant to absorb water and fertilizer and coordinating metabolism. The S-abscisic acid is the 'first messenger' for starting the expression of the stress-resistant gene in the plant body, can effectively activate the stress-resistant immune system in the plant body, and improves the resistance of crops to the stress such as drought resistance, high temperature resistance, cold resistance, disease and insect resistance, salt and alkali resistance and the like.
Preferably, in the plant growth regulating composition provided by the invention, when the active component C is ethephon, the mass ratio of the active component a, the active component B and the active component C is 0.01-100; when the active component C is the S-abscisic acid, the mass ratio of the active component A to the active component B to the active component C is 0.01-100.
The active ingredient C is typically, but not limited to, 0.01.
When active ingredient C is S-rabeprinogen, the mass of active ingredient a, active ingredient B, and active ingredient C is, for example, 0.01. In a preferred embodiment of the present invention, when the total content of the active ingredient a, the active ingredient B and the optional active ingredient C in the plant growth regulator composition is 0.1 to 99% by mass based on the total amount of the plant growth regulator composition, the plant growth regulator composition has a remarkable synergistic effect when applied to plants such as cotton, fruit trees or tobacco.
Typically, but not limitatively, in the plant growth regulator compositions provided by the present invention, the total content (by mass) of active ingredients a, B and optionally C is, for example, 0.1%, 0.2%, 0.5%, 0.8%, 1%, 2%, 5%, 8%, 10%, 15%, 20%, 50%, 80%, 90%, 95% or 99%.
The plant growth regulator composition is more excellent in the growth regulating effect on plants when the total content (mass) of the active ingredients a, B and optionally C is 5 to 80%, and particularly more excellent in the growth regulating effect on plants when the total content (mass) of the active ingredients a, B and optionally C is 20 to 80%.
In a preferred embodiment of the present invention, the plant growth regulating composition further comprises an adjuvant and/or a carrier.
The above "and/or" means that any one of the adjuvants or carriers can be included in the plant growth regulating composition, and the adjuvants and the carriers can also be included at the same time.
[ Carrier ]
Preferably, the carrier may be either a solid or a liquid.
Preferably, when the carrier is a liquid, the liquid includes any one or a mixture of water, aromatic compounds, paraffins, alcohols, ketones, amides, esters and heterocycles.
Typically, but not by way of limitation, the liquid carrier is one or more of water, mineral spirits, paraffin wax, carbitol, tetrahydrofurfuryl alcohol, isophorone, fluquinamide, fatty acid esters, and NBP.
Preferably, when the carrier is a solid, the solid comprises any one or a mixture of several of natural minerals, plant-derived carriers, synthetic carriers and inorganic salts.
Typically, but not by way of limitation, the solid carrier is one or more of kaolin, talc, bentonite, diatomaceous earth, corn starch, white carbon, ammonium sulfate, magnesium sulfate, and sodium sulfate.
[ auxiliary Agents ]
Preferably, the auxiliary agent comprises one or more of a surfactant, a thickening agent, an organic solvent, an antifreezing agent, an antifoaming agent, a water-proofing agent and a preservative.
Preferably, the surfactant comprises one or more of a wetting agent, a dispersing agent and an emulsifying agent.
Typically, but not by way of limitation, the surfactant is one or more of fatty alcohol polyoxyethylene ether, castor oil polyoxyethylene ether, alkylphenol polyoxyethylene ether, aralkyl phenol polyoxyethylene ether, sodium alkyl sulfate, calcium alkyl benzene sulfonate, sodium alkyl benzene sulfonate, alkyl naphthalene sulfonate, sodium/calcium lignosulfonate, and polycarboxylate; the thickening agent is one or more of xanthan gum, arabic gum, sodium carboxymethylcellulose, polyvinyl alcohol, magnesium aluminum silicate and white carbon black; the defoaming agent is one or more of organic silicone oil, fatty alcohol and fatty acid; the antifreeze is one or more of ethylene glycol, propylene glycol, glycerol, urea and calcium chloride; the preservative is one or more of BIT, CIT and MIT.
In a preferred embodiment of the present invention, the plant growth regulating composition is prepared by a method comprising the steps of:
and uniformly mixing the active components A and B, optional C, optional auxiliary agents and carriers to obtain the plant growth regulating composition.
According to a second aspect of the present invention there is provided a plant growth regulating formulation comprising a plant growth regulating composition as provided in the first aspect of the present invention.
The plant growth regulating preparation provided by the invention is mainly prepared from the plant growth regulating composition provided by the first aspect of the invention, and the active ingredient A (aminotrifluralin substances), the active ingredient B (mepiquat chloride substances) and the optional active ingredient C are matched with each other, so that the plant growth regulating preparation has a remarkable synergistic effect, is higher in safety and more stable in drug effect, can effectively increase the lasting period, reduce the application times and improve the yield.
Furthermore, the plant growth regulator provided by the invention is prepared from the plant growth regulating composition provided by the first aspect of the invention, and the active ingredient A (prodiamine substances), the active ingredient B (mepiquat chloride substances) and the active ingredient C are matched with each other, so that the safety is higher, the pesticide effect is more stable, the lasting period can be effectively prolonged, the pesticide application frequency is reduced, and the yield is improved.
[ dosage forms ]
Typically, but not limitatively, the plant growth regulating preparation is in the form of any one of suspending agent, emulsifiable solution, wettable powder, water dispersible granule, aqueous emulsion, microemulsion or granule.
The plant growth regulator provided by the invention can be processed and formed into various dosage forms by using the auxiliary agents commonly used in preparation processing technology. Such as emulsifiable concentrates, sprayable or dilutable solutions, wettable emulsions, wettable powders, dusts, suspensions, granules or capsules, etc.
The formulations are prepared in a known manner, for example by mixing, comminuting and/or stirring the plant growth regulator and the processing aid to dissolve and/or grind.
According to a third aspect of the invention, there is provided the use of a plant growth regulating formulation for capping cotton, for shoot control in fruit trees or for shoot suppression in tobacco.
According to a fourth aspect of the invention, there is provided a method of applying a plant growth regulating formulation.
When the plant growth regulating preparation provided by the invention is applied to cotton fields for chemical capping of cotton, the plant growth regulating preparation is applied according to the following steps: the plant growth regulating preparation provided by the invention is uniformly sprayed on the top and leaves of cotton by stem and leaf spraying in the period from the initial flowering stage to the full flowering stage of cotton.
Preferably, when 3-4 fruit branches bloom in the full-bloom stage of the cotton, the cotton is uniformly sprayed on the top of the cotton in a flat spraying mode.
When the plant growth regulating preparation provided by the invention is used for controlling the tip of a fruit tree, the plant growth regulating preparation is applied according to the following steps: when the young shoots of the fruit trees sprout to the sprouting period, the plant growth regulating preparation provided by the invention is uniformly sprayed on all the shoots by adopting stem and leaf spraying.
When the plant growth regulator preparation provided by the invention is used for inhibiting the buds of tobacco, the plant growth regulator preparation provided by the invention is applied to each axillary bud by adopting a stem and leaf spraying, smearing or cup spraying method in the initial flowering period of the tobacco.
The application method of the plant growth regulating preparation provided by the invention is simple and easy to operate, and meanwhile, the dosage of single mepiquat chloride can be obviously reduced, the lasting period is increased, the application times are reduced, the cost is saved, and the potential phytotoxicity is reduced.
When the plant growth regulating preparation provided by the invention is applied to cotton fields as a chemical topping agent for cotton, the chemical topping agent does not need to be closely combined with water and fertilizer, is safe to cotton, has stable effect, has better topping effect on cotton, has higher safety than the existing chemical topping agents, such as flumetralin and mepiquat chloride, is simpler to use, has more obvious yield increasing effect, and is easy to popularize.
When the plant growth regulating preparation provided by the invention is applied to the fruit tree tip control, the fruit tree tip control preparation is safe to fruit trees after being applied to the fruit trees, the dosage of each single agent can be reduced, the growth of ineffective branch tips is inhibited, the lasting period is increased, the pesticide application frequency is reduced, and the fruit yield and quality are improved. Compared with the existing tip control product paclobutrazol, the tip control agent has better effect and more obvious yield increasing effect.
When the plant growth regulating preparation provided by the invention is applied to tobacco bud inhibition, the plant growth regulating preparation is safe to tobacco after being applied to the tobacco, the dosage of each single agent can be reduced, the growth of ineffective axillary buds is inhibited, the lasting period is increased, the tobacco yield is increased, and the first-class tobacco ratio is increased. Compared with the current tip control product flumetralin, the effect is better.
1. Composition combination evaluation test
In order to verify the synergistic effect of the active ingredient A and the active ingredient B in the plant growth regulating composition provided by the invention, an indoor bioassay test is carried out, wherein the active ingredient A is the aminotrifluralin, and the active ingredient B is the mepiquat chloride, and the details are as follows:
test method and test standard
1. Bioassay test methods:
refer to the stem leaf spraying method of the plant growth promoting/inhibiting test of the agricultural Ministry 'indoor bioassay test for pesticides test guideline NY/T2061.2-2011' part 2.
Preparing a liquid medicine:
raw materials: accurately weighing a certain mass of raw medicine, dissolving with DMF (dimethyl formamide), adding clear water containing 0.1% Tween 80 emulsifier, stirring well, and preparing into a solution with a certain concentration for later use.
Preparation: the preparation is directly weighed and is treated after being diluted by water.
2. Evaluation of the Combined Effect of Individual Agents and compositions of Amofloxacin and Methylpiperazinium
The evaluation method of the combined action type of the single preparation and the composition of the aminotrifluralin and the mepiquat chloride refers to the royal literature 'judgment method of synergistic action of pesticide composition invention patent' (pesticide market information, 2013,000 (029): P.4-7.). The method comprises the following specific steps: the two plant growth regulators A and B are respectively used, the dosage of A is P, the dosage of B is Q, the dosage of the composition is P + Q, and if the test effect of the compositions A and B is better than that of each single agent, the synergistic effect of the two plant growth regulators at the P + Q content can be obtained.
(II) assay for measuring biological Activity
Test 1: cotton test
Test targets: cotton (Gossypium spp), xinlazao 45, cotton seeds, purchased in the market, and stored in seed banks in laboratories.
Adopting a greenhouse potting method, wherein test soil is sieved and air-dried loam and a vegetable seedling culture medium according to the ratio of 1:2 volume ratio of the mixed soil. A plastic flowerpot (12 cm multiplied by 10 cm) is filled with composite soil (vegetable garden soil: seedling substrate =1, 2 v/v) to 3/4 of the place. 6 cotton seeds are sown, and the soil is covered by 0.5-2 cm. Then the soil is transferred to a greenhouse for conventional culture after being completely moistened by water absorption in a mode of infiltrating irrigation at the bottom of the basin. After the true leaves are unfolded, 2-3 plants are set for seedling in each flowerpot, the cotton grows to 3-4 leaf stages, 1 plant is reserved in each flowerpot, and the cultivation is carried out until the flowering stage. The spraying liquid is uniformly sprayed by adopting an intelligent walking type spraying tower (HCL-2000 type), and the spraying liquid amount (mixed with water) is 600L/ha. Each treatment was repeated 3 times, and plant height was investigated 15 days after application, and inhibition rate was calculated.
TABLE 1-1 results of laboratory tests on the application of individual doses and compositions of prodiamine and mepiquat chloride to cotton
TABLE 1-2 evaluation of the results of the combined effect of the individual doses of aminotrifluralin, mepiquat chloride, ethephon and the composition on cotton in the laboratory
Tables 1-3 evaluation of the results of the laboratory tests on the combined action of the individual agents and compositions of aminotrifluralin, mepiquat chloride and S-abscisic acid on cotton
Test 2: tobacco test
Test targets: tobacco (Nicotiana tabacum L.), mizhong tobacco 100, tobacco seeds are purchased from the market, and the seed bank of a laboratory is used for storage.
Adopting a greenhouse potting treatment method, wherein test soil is sieved and air-dried loam and a vegetable seedling culture medium according to the ratio of 1:2 volume ratio of the mixed soil. A plastic flowerpot (12 cm multiplied by 10 cm) is filled with compound soil (vegetable garden soil: seedling substrate =1:2,v/v) to 3/4 of the place. 4-5 tobacco seeds are sowed in each pot, and fine sand-mixed soil with the thickness of 1-3 cm is covered. Then the soil is transferred to a greenhouse for conventional culture after being completely wetted by water absorption in a mode of infiltrating irrigation at the bottom of the basin. Thinning after the tobacco grows to 2-3 leaves, fixing 1 plant in each flowerpot, topping the tobacco in time at the beginning of flowering period, and cutting off axillary buds more than 2.5cm for later use. After topping tobacco, selecting tobacco plants with consistent leaf number and growth vigor, taking cotton swabs, dipping the cotton swabs in diluent, and carefully smearing the diluent on axillary buds to ensure that each axillary bud is contacted with the liquid medicine. Each treatment was repeated 3 times with a blank control. After the liquid medicine is completely absorbed by the plants, the plants are returned to the greenhouse for culture and growth, and the test results are observed at regular time.
TABLE 2 indoor test results of the application of individual doses and compositions of prodiamine and mepiquat chloride to tobacco
As can be seen from the test results in tables 1-1 and 2, when the mass ratio of the trifluralin to the mepiquat chloride in the plant growth regulating composition is (1-100): 1-100, the inhibition effect of the obtained composition on plants is synergistic compared with that of a single-component medicament; especially, when the proportion of the prodiamine to the mepiquat chloride is 0.01-20, the inhibition effect on cotton or tobacco shows obvious synergistic action; when the proportion of the prodiamine to the mepiquat chloride is 0.5-20, the inhibition effect on cotton and tobacco shows obvious synergistic effect.
As can be seen from the test results of tables 1-2, when aminotrifluralin, mepiquat and ethephon were applied to cotton, a synergistic effect was exhibited on the cotton control effect.
As can be seen from the test results of tables 1 to 3, when aminotrifluralin, mepiquat chloride and S-abscisic acid are applied to cotton, a synergistic effect is exhibited on the cotton control effect.
In addition, the invention also adopts a method for evaluating the synergistic effect of the plant growth regulating composition, which is the same as the test, to test the pesticide effect of the plants such as wheat, corn, rice, peanut, strawberry, chrysanthemum and the like, and the result shows that the test result of the plant growth regulating composition provided by the invention on the crops is closer to that of cotton, and the plant growth regulating composition shows obvious synergistic effect.
2. Formulation examples
In the following examples, the percentages are by mass, unless otherwise indicated.
Example 1% Amofloxacin-Methylpiperidinium microemulsion
| Components | Composition of% | Remarks to note |
| Amoflalin | 5 | Active ingredient |
| Mepiquat chloride | 10 | Active ingredient |
| Phenylsulfonat CAL dodecyl benzene sulfonic acid calcium | 4 | Emulsifiers, commercially available from Clariant |
| Emulsogen TS 160 tristyryl polyoxyethylene ether | 6 | Emulsifiers, commercially available from Clariant |
| Ethylan NS-500LQ ethylene oxide propylene oxide block copolymer | 2 | Emulsifiers, commercially available from Nolon |
| N, N-dimethyl acetamide | 30 | Solvent(s) |
| Water (I) | Complement 100 | Solvent(s) |
The microemulsion provided by the invention is prepared by the following steps: the effective components, the emulsifier, the solvent and the like are weighed according to the formula and stirred and dissolved to form uniform transparent liquid, and the 15 percent of the amiloride-mepiquat chloride microemulsion is obtained.
EXAMPLE 2 56% Amifluoralin mepiquat chloride wettable powder
| Components | Composition of% | Remarks for note |
| Amoflalin | 20 | Active ingredient |
| Mepigonium chloride | 36 | Active ingredient |
| Morwet IP alkyl naphthalene sulfonate | 4 | Wetting agents, commercially available from Nolon |
| Morwet D-425 alkyl naphthalene sulfonate formaldehyde condensate | 6 | Dispersant from Nolon |
| Kaolin clay | Complement 100 | Filler material |
The wettable powder provided by the invention is prepared according to the following steps: weighing the effective components, the wetting agent, the dispersant, the filler and the like, uniformly mixing, and then crushing by an airflow crushing system until the average particle size is less than 5 microns to obtain 56% of the prodiamine-mepiquat chloride wettable powder.
Example 3 60% Amofloxacin-Methylpiperazinium Water dispersible granules
The effective components, the wetting agent, the dispersing agent and the filler are weighed according to the formula, are uniformly mixed, are crushed to have the average particle size of less than 5 microns by an airflow crushing system, are added with 12 percent of water in a kneading machine for kneading for 30 minutes, and are granulated by a granulator, and are dried and sieved to obtain the 60 percent of the prodiamine-mepiquat chloride water dispersible granule.
EXAMPLE 4 68% Amifluoralin mepiquat ethephon wettable powder
| Components | Composition of% | Remarks for note |
| Amoflalin | 20 | Active ingredient |
| Mepigonium chloride | 36 | Active ingredient |
| Ethephon | 12 | Active ingredient |
| Sodium dodecyl sulfate | 4 | Wetting agent |
| Borresperse CA calcium lignosulfonate | 6 | Dispersant from Nolon |
| White carbon black | 5 | Filler material |
| Kaolin clay | Complement 100 | Filler material |
The wettable powder provided by the invention is prepared according to the following steps: weighing the effective components, the wetting agent, the dispersant, the filler and the like, uniformly mixing, and then crushing by an airflow crushing system to obtain 68 percent aminotrifluralin, mepiquat chloride and ethephon wettable powder with the average grain diameter of less than 5 microns.
Example 5% Amifluoralin Mepighianium ethephon suspension
| Components | Composition of% | Remarks to note |
| Amoflalin | 10 | Active ingredient |
| Mepiquat chloride | 18 | Active ingredient |
| Ethephon | 6 | Active ingredient |
| Atlas G-1086 | 10 | Emulsifiers, ex Croda |
| Atlax 4914 | 3 | Dispersant from Croda |
| Morwet D-425 alkyl naphthalene sulfonate formaldehyde condensate | 3 | Dispersants from Noron |
| Organic bentonite | 1.5 | Thickening agent |
| Soybean oil | Complement 100 | Solvent(s) |
The wettable powder provided by the invention is prepared by the following steps: weighing effective components, emulsifier, dispersant, thickener, solvent, etc., mixing well, and grinding with sand mill to average particle size below 5 μm.
3. Test of field drug effect
In order to facilitate the technical solution for the skilled in the art, the efficacy of the plant growth regulator provided by the present invention is measured by combining the above examples and comparative examples. In the following examples and comparative examples, the percentages are by mass.
Example (A)
Example 1% Amofloxacin-Methylpiperidinium microemulsion
EXAMPLE 2 56% Amifluoralin mepiquat chloride wettable powder
Example 3 aqueous Dispersion granules of 60% Amofloxacin-Mepighium
EXAMPLE 4 68% Amifluoralin mepiquat ethephon wettable powder
The specific compositions of examples 1 to 4 are as described above and will not be described herein.
(II) comparative example setting
Comparative example 1
The comparative example provides a chemical topping agent, which is prepared by barrel mixing 25% of flumetralin suspending agent and 98% of mepiquat chloride soluble powder, wherein the product name of the 25% of flumetralin suspending agent is Hefuke, and the product is produced by Zhejiang Hetian chemical company; 98% of mepiquat chloride soluble powder, manufactured by Nantong Jinling agricultural chemical Co.
The application method of the chemical topping agent provided by the comparative example refers to the actual barrel mixing and matching use of the fluazinam and the mepiquat chloride in the field for chemical topping.
Comparative example 2
The comparative example provides a chemical topping agent, 250g/L mepiquat chloride aqua, trade name of which is trans-ringing, produced by Henan Like chemical Co.
Comparative example 3
This comparative example provides a suspension concentrate which is 25% paclobutrazol suspension concentrate produced by zhouhing pesticide limited.
Comparative example 4
The comparative example provides a suspension concentrate, which is a 25% flumetralin suspension concentrate produced by Zhejiang cereal field chemical Co.
Comparative example 5% Methylpiperazinium microemulsion
| Components | Composition of% | Remarks for note |
| Mepiquat chloride | 10 | Active ingredient |
| Phenylsulfonat CAL calcium dodecylbenzene sulfonate calcium | 4 | Emulsifiers, commercially available from Clariant |
| Emulsogen TS 160 tristyryl polyoxyethylene ether | 6 | Emulsifiers, commercially available from Clariant |
| Ethylan NS-500LQ ethylene oxide propylene oxide block copolymer | 2 | Emulsifiers, commercially available from Nolon |
| N, N-dimethyl acetamide | 30 | Solvent(s) |
| Water (W) | Complement 100 | Solvent(s) |
Weighing the effective components of mepiquat chloride, emulsifier, solvent and the like according to the formula, and stirring and dissolving the effective components to obtain uniform transparent liquid.
Comparative example 6% Amoflalin microemulsion
| Components | Composition of% | Remarks to note |
| Amoflalin | 5 | Active ingredient |
| Phenylsulfonat CAL calcium dodecylbenzene sulfonate calcium | 4 | Emulsifiers from Clariant |
| Emulsogen TS 160 tristyryl polyoxyethylene ether | 6 | Emulsifiers, commercially available from Clariant |
| Ethylan NS-500LQ ethylene oxide propylene oxide block copolymer | 2 | Emulsifiers, commercially available from Nolon |
| N, N-Dimethylacetamide | 30 | Solvent(s) |
| Water (W) | Complement 100 | Solvent(s) |
The effective components of the prodiamine, the emulsifier, the solvent and the like are weighed according to the formula and stirred and dissolved to form uniform transparent liquid, thus obtaining the product.
Comparative example 7% ethephon wettable powder
| Components | Composition of% | Remarks to note |
| Ethephon | 12 | Active ingredient |
| Sodium dodecyl sulfate | 4 | Wetting agent |
| Borreperse CA calcium lignosulfonate | 6 | Dispersants from Noron |
| White carbon black | 5 | Filler material |
| Kaolin clay | Complement 100 | Filler material |
Weighing the effective components ethephon, wetting agent, dispersant, filler, etc., mixing well, and pulverizing to average particle size below 5 μm by jet milling system.
(III) evaluation of drug efficacy
The plant growth regulating preparations prepared in examples 1 to 4 and comparative examples 1 to 2 were used to carry out field plot tests in cotton fields, and locomotive field demonstration tests were carried out in some examples and comparative examples to confirm the safety, capping effect and yield of cotton.
2.1 field plot test
2.1.1 evaluation criteria for chemical capping of Cotton
Refer to the field efficacy test method of the No. 134 part of the pesticide field efficacy test guideline (II) and the cotton growth regulator test GB/T17980.134-2004. Evaluation standard of chemical capping visual inspection method: the chemical capping effect of the medicament is visually observed according to the growth condition of the cotton plant top cores, 0 represents that all the cotton plant top cores continue to grow, the chemical capping effect is equivalent to that of a blank control, the capping effect is not generated, 100 percent represents that all the cotton plant top cores are locked and do not grow any more, and the evaluation standard of a visual method is shown in a table 3.
TABLE 3 evaluation criteria for chemical capping of cotton by visual inspection
| Grading | Capping effect (%) | Evaluation index of capping effect by visual inspection |
| Level 1 | 100％ | All cotton plants applied with the pesticide are locked; ideal effect |
| Stage 2 | 85-99％ | The top core dead lock cotton plant accounts for 85-99% of the cotton plant applied with the medicine; has better effect |
| Grade 3 | 75-84％ | The top core dead lock cotton plant accounts for 75-84% of the cotton plant applied with the medicine; general effects |
| Grade 4 | 65-74％ | The top core dead lock cotton plants account for 65 to 74 percent of the pesticide application cotton plants; partial influence |
| Grade 5 | 55-64％ | The top core dead lock cotton plant accounts for 55-64% of the cotton plant applied with the medicine; partial influence |
| Grade 6 | 45-54％ | The top core dead lock cotton plant accounts for 45-54% of the cotton plant applied with the medicine; with a slight effect |
| Stage 7 | 35-44％ | The top core dead lock cotton plant accounts for 35-44% of the cotton plant applied with the medicine; have slight influence on |
| Stage 8 | 25-34％ | The top core dead lock cotton plants account for 25-34% of the cotton plants applied with the pesticide; basic ineffectiveness |
| Grade 9 | 0-24％ | The top core dead lock cotton plants account for 0 to 24 percent of the pesticide application cotton plants; invalidation |
2.1.2 test procedures and results
Test time: year 2020, month 4 to year 2020, month 12.
Test site: and the quartet fields of the stone and river stone total field are 4 connected.
And (3) test crops: cotton.
Test subjects: chemical topping and yield increase in the cotton field growing in the flourishing area.
The test field is close to the well house, the cotton grows vigorously, and the water and fertilizer of the whole cotton field are normally managed. The test cells are arranged in unidirectional random blocks, and each cell has an area of 30m 2 4 repeats.
The plant growth regulator preparations and compositions prepared in examples 1 to 4 were sprayed on the stems and leaves of cotton in the full-bloom stage (when 3 to 4 fruit branches bloom) of 7 months and 8 days, respectively, as single agents and control agents 1 and 2 (comparative examples 1 and 2), and the amount of the sprayed liquid (added with water) was 450L/ha. The water and fertilizer chemical control is carried out according to normal management without additional control. Recording the soil type, meteorological data, insect control, disease prevention and other field management conditions of the test field. After the application of the pesticide, whether the cotton of the target crop has abnormal (symptoms such as yellowing, twisting and shrinking) or not and whether the apical bud continues to grow or not are regularly observed. The plant height and fruit set of each treatment were investigated at 7 days 9 months, and the capping rate was visually observed, and the yield was measured at the time of cotton harvesting, and the results are shown in Table 4.
TABLE 4 comparison of agronomic traits and yields in field plot experiments
As can be seen from Table 4, the plant heights and fruit tops of the treatments of examples 1-4 are substantially the same as those of comparative examples 1-2 and single agents 5-7, and are lower than those of the clear water control but higher than those of the manual topping treatment; the safety of each treatment of examples 1 to 4 and each single agent 5 to 7 on other tissues such as cotton leaves, young buds and the like is obviously higher than that of comparative examples 1 to 2; examples 1-4 were visually rated for higher capping than comparative example 2 and single dose comparative examples 5-7, which are essentially equivalent to comparative example 1; the yield of the ginned cotton measured by the examples 1-4 is basically higher than that of the cotton fields treated by the single-dose comparative examples 5-7 and the comparative examples 1-2 and artificially topped, the chemical capping effect is good, and the yield is obviously increased; compared with the example 2, the application amount of mepiquat chloride and the application amount of aminotrifluralin are consistent, the application amount of ethephon is increased by 60 g/hectare in the example 4, and the test result shows that the plant height, the fruit table and the capping rate are basically consistent, but the yield of the plant is obviously higher than that of the plant, and the yield increasing effect is obvious after ethephon is added.
The field observation shows that comparative example 1 has serious phytotoxicity of top tender leaf shrinkage, the later part can recover, comparative example 2 has the phenomena of top sealing fastness (the visual capping rate is only 83.2 percent), cotton regrowth in the later part and early senescence of middle and lower leaves, and examples 1-4 do not have the phenomena. It can be seen that after the plant growth regulator provided in examples 1-4 is sprayed, the bifloran, mepiquat chloride and ethephon binary or ternary composition are applied under the condition of no deliberate water and fertilizer control, the cotton is better in safety due to synergistic cooperation, the chemical capping rate and the yield are higher than those of the common control topping agents for cotton fields, the effect is more stable, and the yield increasing effect of the ternary composition added with ethephon is more obvious.
2.2 conventional growth Cotton field demonstration test
2.2.1 test procedures and results
Test time: year 2020, month 4 to year 2020, month 12.
Test site: and the quartet fields of the total stone field of the stone river are 4 connected.
And (3) test crops: cotton; the water and fertilizer conditions are controlled according to the growth of cotton, belonging to the conventional growth cotton field.
Test subjects: stable growth of cotton field, chemical topping and increasing yield.
The cotton variety is ZY6 (hybrid cotton), the cotton has stable full growth vigor, the soil type is loam, the cotton field adopts the water-saving drip irrigation technology, the cotton field is 2.05 meters of ultra-wide film, precision dibbling is carried out on the film, one film is provided with six lines and three tubes, the line spacing is configured to be 10+66 centimeters, drip irrigation is carried out under the film, and the sowing density is 14000 plants/mu. The test field is sown in 4 months and 7 days, seedlings emerge in 8 days in 4 months, seedlings emerge in 18 days in 4 months, and all the uniformly suspended mepiquat chloride is sprayed by 10 g/mu in 16 days in 7 months to control flourishing. The test is carried out for 4 treatments, each treatment is 20 mu, the top spraying treatment is carried out by using a John Dier 1404 tractor on 7, 8 and 525L/ha of liquid spraying amount (water adding), water and fertilizer are fed 5 days after the application, the data of 9, 10 and 9 days are investigated, and the mechanical collection is carried out on 28 and 9 days. The conventional management of weeding, killing insects, fertilizing and chemical control among all the cells is consistent, and the measurement results are shown in table 5.
TABLE 5 comparison of agronomic traits and yields for field demonstration experiments (conventional Cotton field)
As can be seen from Table 5, in example 1, compared with each single agent and comparative example, the plant height and fruit table control effect are equivalent to those of comparative example 2, and are equivalent to or slightly superior to those of comparative examples 5-6 of each treatment single agent; the visual inspection of the capping rate and the yield of the real harvested ginned cotton are equivalent to those of the comparative example 2 and are superior to those of the treatments of the comparative examples 5 to 6 of each single agent; the safety of example 1 on cotton is better than that of comparative example 2, the example 1 and the single-dose comparative examples 5-6 are both safe on cotton, and the phenomenon that the leaves are brittle and senilis exists in the later period of the comparative example 2. It can be seen that example 1 has good control effect on the plant height and the fruit table of cotton, has obvious capping effect, has better safety on cotton than comparative example 2, and has certain yield increasing effect.
2.3 Wangcheng Cotton field demonstration test
2.3.1 test procedures and results
Test time: year 2020, month 4 to year 2020, month 12.
Test site: and the quartic field of the total stone field of the stone river is 7-stage.
And (3) test crops: cotton; the water and fertilizer are not controlled according to the growth condition of the cotton, and the cotton is a vigorous growing cotton field.
Test subjects: chemical topping and yield increase in the cotton field growing in the flourishing area.
The cotton variety is Shicheng No. 1, the cotton has vigorous growth, the soil type is loam, the cotton field adopts the water-saving drip irrigation technology, the film is 2.05 meters of ultra-wide, precision dibble seeding is carried out on the film, one film is six lines and three tubes, the line spacing is configured to be 10+66 centimeters, drip irrigation is carried out under the film, and the sowing density is 13000 plants/mu. Sowing the seeds in the test field for 4 months and 13 days, sprouting water in 17 days in 4 months, sprouting in 24 days in 4 months, and controlling the growth of all the seedlings by uniformly spraying 15 g/mu of mepiquat chloride in 17 days in 7 months. The test is carried out for 6 treatments, each treatment is 20 mu, the top spraying treatment is carried out by using a John Diel 1404 tractor on 7 months and 8 days, the liquid spraying amount (water is added) is 555L/ha, water and fertilizer are fed 3 days after the application, data investigation is carried out on 9 months and 11 days, and mechanical collection is carried out on 10 months and 4 days. The conventional management of weeding, killing insects, fertilizing and chemical control among all the cells is consistent, and the results are shown in table 6.
TABLE 6 comparison of agronomic traits and yields in field demonstration experiments (Wangcheng cotton field)
As can be seen from Table 6, in examples 2 and 4, compared with comparative examples 5 to 7 and comparative examples 1 to 2, the plant height and fruit table control effect are equivalent to those of comparative examples 1 to 2, and equivalent to or slightly superior to those of comparative examples 5 to 7 of each treatment single agent; visual capping rate example 4 was highest, example 2 was second, comparative example 1 was second, these treatments were significantly higher than the others, and some of the cotton plants of comparative example 2 had a top center regrowth at a later stage; the safety of examples 2 and 4 to cotton is obviously superior to that of comparative examples 1-2, the top leaves are wrinkled and yellow after the pesticide is applied to the comparative example 1, and the leaves are brittle and senescent in the comparative example 2; example 4 has the highest yield of lint, example 2 is the second, comparative example 2 is the second, the treatments are obviously better than other treatments, and the yield increasing effect of the example is obvious. Therefore, the embodiments 2 and 4 have good control effect on the height of the vigorous cotton plant, good fruit table control effect, obvious capping effect, good safety on the cotton and remarkable yield increasing effect. After ethephon is added in the example 4, the capping effect is better and the yield increasing effect is more obvious compared with the example 2. As can be seen, the binary or ternary compound composition of the prodiamine, the mepiquat chloride and the ethephon has good topping effect on the Wangcheng cotton fields and obvious yield increasing effect.
2.4 Citrus shoot control field efficacy test
2.4.1 evaluation Standard for shoot control of Citrus
Since the related regulation and growth field efficacy criterion of the fruit trees can only inquire the related evaluation criterion of the grapes, the test refers to the grape criterion part 143 of the pesticide field efficacy test criterion (II): grape growth regulator test GB/T17980.143-2004.
2.4.2 test procedures and results
Test time: year 2020, month 4 to year 2020, month 12.
Test site: guangxi Guilin Lipu city, qingshan Zhen Li Shu village.
And (3) test crops: orange, sugar orange, age 5 years old.
Test subjects: controlling tip and increasing yield.
The citrus orchard is a gentle slope land, contains red loam, has a pH value of 6.2 and has a common organic matter content. The single sheet is planted in the orchard, the biology is relatively simple, the orchard management level is general, and the orchard is managed conventionally during the test period. The test is carried out for 5 treatments, 2 trees are treated each, the pesticide is uniformly applied in 25 days in 4 months, spring shoots are aged when the pesticide is applied, summer shoots are not taken out, the peripheral tree crowns are uniformly sprayed with the pesticide, the pesticide is sprayed to the front and back surfaces of the leaves to be wet, water does not drip, the water consumption for all treatments is 4500L/ha, data investigation is carried out in 5 days in 5 months and 15 days, 5 spring shoots in the last year are selected from each tree in different directions, the number of all the newly taken summer shoots on each tree is observed in fixed strips, and the trees are picked in 2 days in 12 months. The results are shown in Table 7.
TABLE 7 Citrus shoot control field efficacy test results for compositions
As can be seen from Table 7, the number of new shoots is reduced compared with that of single dose in example 1, the shoot control duration is longer, and the method is safe for other tissues such as young citrus fruits and can improve the yield of citrus. Compared with the paclobutrazol provided by the comparative example 3, the effective period is longer, the dosage is lower, and the yield is greatly increased.
2.5 tobacco bud inhibition field test for efficacy
2.5.1 evaluation criteria for tobacco bud inhibition
Referring to section 136 of the pesticide field efficacy test criteria (second): tobacco bud inhibitor test GB/T17980.136-2004.
2.5.2 test procedures and results
Test time: year 2020, 4 months to year 2020, 10 months.
Test site: baichi river town of various cities in Shandong province.
And (3) test crops: tobacco.
Test subjects: inhibiting tobacco bud and increasing yield.
The test variety is medium tobacco 100, the soil type of the test field is loam, the fertility is medium, the terrain is flat, the irrigation and drainage are convenient, and the previous crop is flue-cured tobacco. The organic matter content of the soil is 1.2 percent, the hydrolyzed nitrogen is 80.3mg/kg, the available phosphorus is 64.5mg/kg, and the quick-acting potassium is 33.3mg/kg. The experiment was repeated 4 times for 5 treatments, and the number of treatments was 20 cells, and 80 tobacco plants (40 m) were planted in each cell 2 ). And random block arrangement is carried out in the fields of all the cells. The items are punched once when 50% of central flowers of tobacco plants in the tobacco field are opened. And applying after wiping off all axillary buds within 24 h. The application method is cup drenching, the dosage of each plant is 20mL, the water consumption for treatment is 450L/ha, and the control effect is investigated 2 weeks, 4 weeks and 6 weeks after the application. The results are shown in Table 8.
TABLE 8 tobacco suckering inhibition field efficacy test results for compositions
As can be seen from Table 8, the tobacco bud inhibition effect of example 3 is better, the bud inhibition rate after 42 days is higher than that of the single-dose treatment of mepiquat chloride of comparative example 5 and the single-dose treatment of prodiamine of comparative example 6, and the effect is basically equivalent to that of comparative example 4; the safety, yield and tobacco quality of the tobacco were higher than those of comparative examples 5 to 6 and slightly higher than that of comparative example 4. Therefore, the embodiment 3 has better tobacco bud inhibition effect, good safety and obvious quality and income improvement effect.
Finally, it should be noted that: the above embodiments are only used to illustrate the technical solution of the present invention, and not to limit the same; while the invention has been described in detail and with reference to the foregoing embodiments, it will be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some or all of the technical features may be equivalently replaced; and these modifications or substitutions do not depart from the spirit of the corresponding technical solutions of the embodiments of the present invention.
Claims (10)
1. A plant growth regulating composition, which is characterized by comprising an active ingredient A and an active ingredient B, wherein the active ingredient A is at least one selected from the group consisting of prodiamine and derivatives thereof or agriculturally acceptable salts or esters thereof; the active ingredient B is selected from at least one of mepiquat chloride and derivatives thereof or agriculturally acceptable salts or esters thereof.
2. The plant growth regulating composition according to claim 1, wherein the mass ratio of active ingredient a to active ingredient B is from 0.01 to 100, preferably from 0.01 to 20.
3. The plant growth regulating composition according to claim 1, characterized in that the composition comprises an active ingredient C selected from at least one of ethephon, butachlor, uniconazole, paclobutrazol, chlormequat chloride, S-abscisic acid and derivatives thereof or agriculturally acceptable salts or esters thereof;
preferably, the active component C is ethephon, and the mass ratio of the active component A to the active component B to the active component C is 0.01-100;
preferably, the active component C is S-abscisic acid, and the mass ratio of the active component A to the active component B to the active component C is 0.01-100.
4. A plant growth regulating composition according to any one of claims 1 to 3, characterized in that the total content of active ingredient a, active ingredient B and optionally active ingredient C is 0.1-99%, preferably 5-80%, more preferably 20-80% by mass of the plant growth regulating composition.
5. A plant growth regulating composition according to any one of claims 1 to 3, further comprising an adjuvant and/or a carrier;
preferably, the carrier is a solid or a liquid;
preferably, the liquid comprises at least one of water, aromatic compounds, paraffins, alcohols, ketones, amides, esters, and heterocycles;
preferably, the solid comprises at least one of natural minerals, plant-derived carriers, synthetic carriers and inorganic salts;
preferably, the auxiliary agent comprises at least one of a surfactant, a thickener, an antifreeze, a defoamer and a preservative;
preferably, the surfactant includes at least one of a wetting agent, a dispersing agent, and an emulsifying agent.
6. A plant growth regulating formulation comprising the plant growth regulating composition of any one of claims 1 to 5;
preferably, the formulation of the plant growth regulating preparation comprises one of a suspending agent, an emulsifiable solution, a wettable powder, a water dispersible granule, an aqueous emulsion, a microemulsion or a granule.
7. Use of the plant growth regulating composition according to any one of claims 1 to 5 or the plant growth regulating formulation according to claim 6 for capping cotton, controlling shoots of fruit trees or suppressing shoots of tobacco.
8. The method of applying a plant growth regulating formulation according to claim 6, comprising the steps of: the plant growth regulating preparation of claim 6 is sprayed on the top of cotton by stem and leaf spraying from the initial flowering period to the full flowering period of cotton.
9. The method of applying a plant growth regulator according to claim 6, comprising the steps of: spraying the plant growth regulating preparation of claim 6 to the top of the fruit tree branch by spraying when the young fruit tree branch sprouts to the sprouting stage.
10. The method of applying a plant growth regulator according to claim 6, comprising the steps of: the plant growth regulating preparation of claim 6 is applied to tobacco axillary buds by stem and leaf spraying, smearing or cup spraying at the initial stage of tobacco flowering.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111165347.8A CN115885993A (en) | 2021-09-30 | 2021-09-30 | Plant growth regulating compositions, formulations, uses and methods of application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111165347.8A CN115885993A (en) | 2021-09-30 | 2021-09-30 | Plant growth regulating compositions, formulations, uses and methods of application |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN115885993A true CN115885993A (en) | 2023-04-04 |
Family
ID=86481264
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202111165347.8A Pending CN115885993A (en) | 2021-09-30 | 2021-09-30 | Plant growth regulating compositions, formulations, uses and methods of application |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN115885993A (en) |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2079760A1 (en) * | 1991-10-04 | 1993-04-05 | Thomas Denny O'neal | Plant growth regulator compositions |
| EP0535415A1 (en) * | 1991-10-04 | 1993-04-07 | Basf Corporation | Plant growth regulator compositions |
| WO1999009832A1 (en) * | 1997-08-25 | 1999-03-04 | Basf Corporation | Potentiated mepiquat plant growth regulator compositions |
| US20110028324A1 (en) * | 2008-01-25 | 2011-02-03 | Syngenta Crop Protection, Inc. | Herbicidal compositions |
| CN102835400A (en) * | 2012-09-14 | 2012-12-26 | 刘勤学 | Application of pesticide composite containing uniconazole and prodiamine as tobacco bud-restraining agent |
| CN103355292A (en) * | 2012-03-26 | 2013-10-23 | 刘勤学 | Prodiamine water dispersible granule serving as tobacco suckercide |
| CN103975952A (en) * | 2013-06-04 | 2014-08-13 | 桂林桂开生物科技股份有限公司 | Plant growth regulator and preparation method thereof |
| CN106818855A (en) * | 2017-02-16 | 2017-06-13 | 新疆农业大学 | One chemistry that grows cotton is pinched agent |
-
2021
- 2021-09-30 CN CN202111165347.8A patent/CN115885993A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2079760A1 (en) * | 1991-10-04 | 1993-04-05 | Thomas Denny O'neal | Plant growth regulator compositions |
| EP0535415A1 (en) * | 1991-10-04 | 1993-04-07 | Basf Corporation | Plant growth regulator compositions |
| WO1999009832A1 (en) * | 1997-08-25 | 1999-03-04 | Basf Corporation | Potentiated mepiquat plant growth regulator compositions |
| US20110028324A1 (en) * | 2008-01-25 | 2011-02-03 | Syngenta Crop Protection, Inc. | Herbicidal compositions |
| CN103355292A (en) * | 2012-03-26 | 2013-10-23 | 刘勤学 | Prodiamine water dispersible granule serving as tobacco suckercide |
| CN102835400A (en) * | 2012-09-14 | 2012-12-26 | 刘勤学 | Application of pesticide composite containing uniconazole and prodiamine as tobacco bud-restraining agent |
| CN103975952A (en) * | 2013-06-04 | 2014-08-13 | 桂林桂开生物科技股份有限公司 | Plant growth regulator and preparation method thereof |
| CN106818855A (en) * | 2017-02-16 | 2017-06-13 | 新疆农业大学 | One chemistry that grows cotton is pinched agent |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109392587B (en) | Planting method for rapidly forming pear garden | |
| CN105493812B (en) | A kind of middle temperate zone spring wheat, winter rape, buckwheat 2 years three ripe cultural methods | |
| CN113016549B (en) | Cultivation method for promoting tillering and stem forming of sugarcane and internode sugar accumulation under continuous cropping obstacle | |
| CN108633669B (en) | Method for cultivating medium-ripened trailing short cowpea variety in south China in open field in summer | |
| CN108782061A (en) | A kind of processing method prevented pineapple dehiscent fruit and split bar | |
| Whiley et al. | 12 Crop Management | |
| CN108782091A (en) | A method of improving South China's asparagus bean breeding yield | |
| Singh et al. | Aonla (Emblica officinalis) in India: A review of its improvement, production and diversified uses | |
| CN112293428A (en) | Synergistic composition containing organic silicon plant growth regulator | |
| CN111493095A (en) | Plant growth regulator composition containing hypersensitive protein and application thereof | |
| CN107155599A (en) | A kind of planting culture method of Momordica grosvenori | |
| Chartzoulakis | Effects of saline irrigation water on germination, growth and yield of greenhouse cucumber | |
| CN115053911B (en) | Herbicide composition containing fenpyrad and pinoxaden | |
| CN115885993A (en) | Plant growth regulating compositions, formulations, uses and methods of application | |
| CN104521703B (en) | The cottage method of yew | |
| Richards | The breeding, selection and propagation of tea | |
| CN114982761B (en) | Application of streptavidin-free glucan in preparation of plant immunity elicitor | |
| CN110367052A (en) | A kind of implantation methods of wild chrysanthemum | |
| CN111109263A (en) | Herbicide for preventing and controlling weeds in ophiopogon root lawn | |
| CN115413679B (en) | Pollution-free Yang Meishu flower agent, preparation method and application thereof | |
| WO2021172594A1 (en) | Plant heat resistance or drought resistance improving agent, salt tolerance improving agent, activity improving agent | |
| EL-GEDDAWY et al. | TRANSPLANTING USING PAPER POTS TECHNIQUE AND MICRO NUTRITION WITH RELATION TO YIELD AND IT'S ATTRIBUTES OF SUGAR BEET AT DIFFERENT PLANTING DATES | |
| CN115868490A (en) | Application of trifluralin-containing plant growth regulator or preparation thereof in cotton pruning and shaping, cotton topping or fruit tree shoot control | |
| CN112314621A (en) | Multi-effect sterilization composition containing organic silicon plant growth regulator | |
| Kohinoor et al. | Effect of ethrel on flower production and fruit yield of snakegourd (Trichosanthes anguina) |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |