CN115413679B - Pollution-free Yang Meishu flower agent, preparation method and application thereof - Google Patents

Pollution-free Yang Meishu flower agent, preparation method and application thereof Download PDF

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CN115413679B
CN115413679B CN202211068395.XA CN202211068395A CN115413679B CN 115413679 B CN115413679 B CN 115413679B CN 202211068395 A CN202211068395 A CN 202211068395A CN 115413679 B CN115413679 B CN 115413679B
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flower
yang
meishu
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CN115413679A (en
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焦云
房聪玲
柴春燕
高中山
汪国云
屠挺
周超超
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Ningbo Academy of Agricultural Sciences
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/02Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01PBIOCIDAL, PEST REPELLANT, PEST ATTRACTANT OR PLANT GROWTH REGULATORY ACTIVITY OF CHEMICAL COMPOUNDS OR PREPARATIONS
    • A01P21/00Plant growth regulators
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05CNITROGENOUS FERTILISERS
    • C05C11/00Other nitrogenous fertilisers
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Zoology (AREA)
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  • Plant Pathology (AREA)
  • Wood Science & Technology (AREA)
  • Chemical & Material Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
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  • Organic Chemistry (AREA)
  • Botany (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention belongs to the technical field of fruit tree cultivation, and discloses a pollution-free Yang Meishu flower agent which comprises the following components: ammonium acetate, alternanthera philoxeroides extract, an auxiliary agent and water. Also discloses a preparation method and application thereof. The method can effectively balance the annual fruiting quantity of the waxberries and is convenient for relieving the annual phenomenon of the waxberries. The plant flower thinning agent has reasonable formula, main components of Chinese medicinal plants and non-toxic and harmless inorganic salt, no artificial synthetic hormone component, no pollution, simple and convenient operation and strong practicability, can effectively reduce the fruit setting rate of the waxberry in the year, and is safe and efficient.

Description

Pollution-free Yang Meishu flower agent, preparation method and application thereof
Technical Field
The invention belongs to the technical field of fruit tree cultivation, and discloses a pollution-free Yang Meishu flower agent, a preparation method and application thereof.
Background
The serious year-old fruiting phenomenon is common in the production of the waxberries, so that not only is the market supply relation unbalanced, but also the economic income of fruit farmers is seriously influenced due to the reduction of the fruit quality caused by the year of the year. Currently, chemical flower thinning agents and flowering agents are mainly used for regulating and controlling the annual output, and increasing the annual output so as to keep the output basically stable. The chemical flower and fruit thinning almost replaces the artificial flower and fruit thinning, and has the characteristics of labor saving, time saving, low cost, high speed and suitability for large-area intensive production compared with the artificial flower and fruit thinning. However, the chemical flower thinning agent mainly comprises some artificially synthesized plant hormones such as naphthylacetic acid, paclobutrazol, ethephon, 6-benzyl adenine, some pesticide preparations and the like, has long residual time, has certain food safety risks, is gradually challenged by consumers, and does not meet the increasing food safety requirements of people. Furthermore, the sensitivity of different fruit tree varieties is different, and various fruit trees and crop phytotoxicity events are endless. In view of the above, the chemical flower thinning agent has the advantages of low development cost, time and labor saving, no toxicity and harm to people and animals, safety to flower-visiting insects and no pollution to the environment, and is one of the important research subjects at present.
The alligator alternanthera Alternanthera philoxeroides (Mart.) Grisea is a plant of the genus Alternaria of the family Amaranthaceae, is native to south America, is now a global malignant weed, and is widely distributed in the provinces of Hebei, jiangsu, zhejiang, fujian, jiangxi, guangxi and the like in China. The existing researches show that the whole herb of the Chinese herbal medicine has the effects of clearing heat, promoting diuresis, cooling blood, removing toxicity, and has a certain chemosensory effect, and can inhibit seed germination and growth under the condition of specific concentration; it is notable that it is also a high potassium plant that can be used as a source of high-efficiency potash fertilizer. In view of the above, it is urgent to develop natural, environment-friendly agents with flower thinning effect suitable for bayberry. The invention surrounds the aim, is based on nontoxic and harmless traditional Chinese medicine components to be compounded into the pollution-free flower thinning agent, and has obvious effect on adjusting the size of the waxberry result.
Disclosure of Invention
The invention aims to provide a pollution-free Yang Meishu flower agent.
In order to achieve the above purpose, the invention adopts the following technical scheme:
a nuisanceless Yang Meishu flower, comprising: alternanthera philoxeroides powder and ammonium acetate.
Preferably, the solvent of the flower thinning agent is water, and the concentration of ammonium acetate is 0.05-0.1mol -1 150-300g.L of alternanthera philoxeroides powder -1
Preferably, the flower thinning agent is applied by taking the supernatant after centrifugation or filtration. The flower thinning agent can be directly applied without filtration, but the spraying holes are easy to be blocked when the flower thinning agent is applied by tools such as a sprayer, so that the application after filtration is more convenient.
Preferably, the agricultural organic silicon synergist also comprises a surfactant. For plants with revolutionary surfaces of leaves such as waxberries, the sprayed flower thinning agent is not easy to wall, the flower thinning effect is affected, and after the surfactant is added, the flower thinning agent is beneficial to stay on the surfaces of the plants, so that a better flower thinning effect is achieved.
Preferably, the agricultural organosilicon synergist is diluted by 1000-1500 times and sprayed.
The invention also discloses a preparation method of the pollution-free Yang Meishu flower agent, which comprises the following steps:
pulverizing Alternanthera philoxeroides, adding into water, adding ammonium acetate, and soaking for more than 20 hr to obtain nuisanceless Yang Meishu flower preparation.
Preferably, the soaking is carried out for every 2-6 hours.
Preferably, an agricultural organosilicon synergist is also added.
Preferably, the addition amount of the alternanthera philoxeroides is 150-300g.L -1 The addition amount of ammonium acetate is 0.05-0.1mol.L -1
Preferably, the addition amount of the agricultural organic silicon synergistic agent is 0.67-1.0ml -1
Preferably, after soaking, centrifuging or filtering with gauze, and collecting supernatant to obtain nuisanceless Yang Meishu flower.
The invention also discloses application of the pollution-free Yang Meishu flower agent in reducing the fruit setting rate of waxberries.
Preferably, the excessive flowering plants of the waxberries which enter the later stage of flower filling and have no plant diseases and insect pests and normal growth and development of leaves are selected, the flower thinning agent is uniformly sprayed on the crowns of the whole plants at least twice, and the time interval between the spraying of the flower thinning agent and the spraying of the water thinning agent is 72 hours after the spraying of the flower thinning agent onto the crowns each time.
Preferably, the plant flower thinning agent is sprayed twice, and the interval time between the spraying of the plant flower thinning agent and the spraying of the plant flower thinning agent is 72 hours.
Notice that:
1) The waxberry flower thinning agent can be used only under the condition of excessive flowering, and can be used under the condition that the leaves of the waxberry plants grow healthily.
2) The spraying time of the waxberry flower thinning agent is important, and the waxberry flower thinning agent is suitable for the young fruits with the size of a matchhead at the end of Yang Meicheng flowers, and is used in continuous sunny windless weather during spraying.
Compared with the prior art, the invention has the beneficial effects that:
1) The flower thinning agent of the invention mainly comprises Chinese herbal plants, namely alternanthera philoxeroides and ammonium acetate which can be used as food additives, does not contain any artificial synthetic hormone, and is green, environment-friendly and pollution-free. In view of the fact that alternanthera philoxeroides is an invasive malignant weed, the alternanthera philoxeroides is gathered in pieces worldwide, and huge losses are caused to agricultural irrigation, aquaculture, grain transportation and travel. It can kill the higher plants in water, eliminate aquatic animals and destroy ecological balance in water area. The invention provides a new idea for reducing the pressure of the alternanthera philoxeroides on the ecological environment based on the purpose of comprehensive development and effective utilization of the alternanthera philoxeroides by local materials.
2) The flower thinning agent disclosed by the invention has the advantages that the components of the flower thinning agent are all water, the materials are convenient to obtain, the ammonium acetate is used as a strong electrolyte inorganic salt, the aqueous solution is neutral in acid-base, and the pollination fertilization of the gynoecia of the waxberry can be effectively inhibited. Wherein, acetate can promote the synthesis of plant hormone jasmonic acid, thereby improving the stress resistance of plants; ammonium ions belong to foliar fertilizers, and can effectively improve photosynthesis capacity of plant leaves under the condition of specific concentration; in addition, the ammonium acetate solution can help to dissolve and release bioactive substances and potassium elements of the alternanthera philoxeroides for plant absorption and utilization, and the two components complement each other, so that the alternanthera philoxeroides is safe and efficient and has no side effect.
Drawings
FIG. 1 shows the effect of the pollution-free flower-thinning agent on the older plant of the early plum variety of the red bayberry (A, the result after spraying the flower-thinning agent; B, the result without using the flower-thinning agent).
FIG. 2 shows the effect of the pollution-free flower-thinning agent on the older plant of the Myrica rubra 'chufa' variety (A, the result after spraying with the flower-thinning agent (combination of ammonium acetate and alligator alternanthera extract; B, the result after spraying with only alligator extract as the flower-thinning agent; C, the result after spraying with only ammonium acetate as the flower-thinning agent).
Detailed Description
The present invention will be specifically described with reference to examples. It is to be understood that the practice of the invention is not limited to the following examples and that any form of modification and/or variation in the concentration of the flower thinning agent component, etc. of the present invention will fall within the scope of the invention.
Example 1
The Yang Meishu flower formulation and the application method thereof comprise the following steps:
(1) Suitable agent spraying time:
selecting 3 plants of 8-year dwarf grafted seedlings of waxberry 'early plum' which have no plant diseases and insect pests, are healthy to grow and excessively bloom (year old) and have consistent physical and weather periods, selecting 5 groups of fruiting main branches with consistent sizes from each plant at the end stage of full bloom, namely 4 months and 4 days in 2022, and respectively carrying out uniform spraying treatment on different flower thinning agent formulas until a small amount of liquid drops are suitable for crowns. Wherein each treatment is divided into three replicates, one for each plant; spraying treatment is carried out according to the same method after the interval of 72 hours;
(2) Yang Meishu flower preparation method and treatment mode:
treatment a: 100g of fresh chives, crushing to granularity smaller than 3mm, soaking in 1L of water for 24 hours, and finally adding 0.5ml of agricultural organic silicon surfactant for preparation; spraying treatment is carried out according to the same method at intervals of 72 hours after the first spraying;
treatment B: 300g of whole plant fresh sample of alternanthera philoxeroides, crushing the whole plant fresh sample to be less than 3mm in granularity, and adding 0.1mol.L of ammonium acetate -1 Soaking in 1L of water for 24 hours, and finally adding 1.0ml of agricultural organosilicon surfactant for preparation; spraying treatment is carried out according to the same method at intervals of 72 hours after the first spraying;
treatment C: 150g of whole plant fresh sample of alternanthera philoxeroides, crushing the whole plant fresh sample to a granularity smaller than 3mm, and adding 0.05mol.L of ammonium acetate -1 Soaking in 1L water for 24 hr, and adding 1.0ml agricultural organosilicon surfactantSex auxiliary agent, ready-to-use; spraying treatment is carried out according to the same method at intervals of 72 hours after the first spraying;
treatment D: 300g of whole plant fresh sample of alternanthera philoxeroides, crushing to granularity smaller than 3mm, soaking in 1L of water for 24 hours, and finally adding 1.0ml of agricultural organosilicon surfactant, so as to prepare the alternanthera philoxeroides as the active ingredient; spraying treatment is carried out according to the same method at intervals of 72 hours after the first spraying;
treatment E: 150g of whole plant fresh sample of alternanthera philoxeroides, crushing to granularity smaller than 3mm, soaking in 1L of water for 24 hours, and finally adding 1.0ml of agricultural organosilicon surfactant for preparation; spraying treatment is carried out according to the same method at intervals of 72 hours after the first spraying;
control treatment: 1.0ml of agricultural organic silicon surface active agent is added into 1L of clear water and is prepared for use at present; and spraying treatment is carried out in the same method at intervals of 72h after the first spraying.
(3) Flower thinning effect investigation and analysis:
counting the number of each processed flower before 4 months and 4 days of flower thinning, and carrying out statistical analysis on investigation results and fruit quality under 6 months and 10 days of investigation results. The results of the comparative analysis of the flower thinning effect after conditioning with different flower thinning agents are shown in table 1. The results show that the flower thinning agent of treatment C gives the best fruit quality (fig. 1), whereas treatments a, D, and E all have no significant differences from the control.
TABLE 1 Effect of treatment with different flower thinning Agents on the quality of Myrica rubra fruits
Note that: multiple difference comparisons were performed using the Duncan new complex polar difference test. Capital letters are expressed as 0.01 level difference significance. Very significant differences are achieved between treatments with different letter designations in the same column.
Example 2
The Yang Meishu flower formulation and the application method thereof comprise the following steps:
(1) Suitable agent spraying time:
selecting 7-year-old grafted seedlings 9 plants of waxberry 'water chestnut variety' which have no plant diseases and insect pests, are healthy to grow, are excessively flowering and have consistent physical and climatic periods, and respectively carrying out uniform spraying treatment on different flower thinning agent formulas at the end stage of full flowering, namely, at 4 th and 6 th of 2022, until a small amount of water drops are suitable for crowns. Wherein each treatment is divided into three replicates, one for each plant; spraying treatment is carried out according to the same method after the interval of 72 hours;
(2) Yang Meishu flower preparation method and treatment mode:
treatment a: 150g of whole plant fresh sample of alternanthera philoxeroides, crushing the whole plant fresh sample to a granularity smaller than 3mm, and adding 0.05mol.L of ammonium acetate -1 Soaking in 1L of water for 24 hours, and finally adding 1.0ml of agricultural organosilicon surfactant for preparation; spraying treatment is carried out according to the same method at intervals of 72 hours after the first spraying;
treatment B: 150g of whole plant fresh sample of alternanthera philoxeroides, crushing to granularity smaller than 3mm, soaking in 1L of water for 24 hours, and finally adding 1.0ml of agricultural organosilicon surfactant for preparation; spraying treatment is carried out according to the same method at intervals of 72 hours after the first spraying;
treatment C: ammonium acetate 0.05mol.L -1 Soaking in 1L of water for 24 hours, and finally adding 1.0ml of agricultural organosilicon surfactant for preparation; spraying treatment is carried out according to the same method at intervals of 72 hours after the first spraying;
control treatment: 1.0ml of agricultural organic silicon surface active agent is added into 1L of clear water and is prepared for use at present; and spraying treatment is carried out in the same method at intervals of 72h after the first spraying.
(3) Flower thinning effect investigation and analysis:
counting the number of each processed flower before 4 months and 1 day of flower thinning, and carrying out statistical analysis on investigation results and fruit quality under 6 months and 12 days of investigation results. The results of the comparative analysis of the flower thinning effect after conditioning with different flower thinning agents are shown in Table 2. The results show that the overall fruit quality after treatment with the flower thinning agent of treatment a is optimal, whereas treatment B is not significantly different from the control (fig. 2). Furthermore, only fruit set rate in treatment C was not very significantly different from optimal treatment a, however, both the single fruit weight and soluble solids content were very significantly lower than treatment a.
TABLE 2 Effect of treatment with flower thinning agents of different formulations on the quality of Myrica rubra fruits
Note that: multiple difference comparisons were performed using the Duncan new complex polar difference test. Capital letters are expressed as 0.01 level difference significance. Very significant differences are achieved between treatments with different letter designations in the same column.

Claims (9)

1. A pollution-free Yang Meishu floral formulation comprising: the flower thinning agent comprises alternanthera philoxeroides powder and ammonium acetate, wherein the solvent of the flower thinning agent is water, and the concentration of the ammonium acetate is 0.05-0.1mol.L -1 150-300g.L of alternanthera philoxeroides powder -1 The method comprises the steps of carrying out a first treatment on the surface of the Pulverizing Alternanthera philoxeroides, adding into water, adding ammonium acetate, and soaking for more than 20 hr to obtain nuisanceless Yang Meishu flower preparation.
2. The pollution-free Yang Meishu floral formulation of claim 1, wherein: the flower thinning agent is applied by taking supernatant after centrifugation or filtration.
3. The pollution-free Yang Meishu floral formulation of claim 1, wherein: the agricultural organic silicon synergistic agent is diluted by 1000-1500 times and sprayed.
4. The method for preparing the pollution-free Yang Meishu flower agent according to any one of claims 1 to 3, which is characterized in that the method comprises the steps of crushing alternanthera philoxeroides, adding the crushed alternanthera philoxeroides into water, adding ammonium acetate, and soaking for more than 20 hours.
5. The method for preparing the pollution-free type Yang Meishu flower agent according to claim 4, wherein the flower agent is stirred every 2 to 6 hours during soaking.
6. The method for preparing the pollution-free Yang Meishu flower agent according to claim 4, which is characterized in that: also addAdding agricultural organosilicon synergist with the addition amount of 0.67-1ml.L -1
7. The method for preparing the pollution-free Yang Meishu flower agent according to claim 4, which is characterized in that: the addition amount of the alternanthera philoxeroides is 150-300g.L -1 The addition amount of ammonium acetate is 0.05-0.1mol.L -1
8. The method for preparing the pollution-free Yang Meishu flower agent according to claim 4, which is characterized in that: after soaking, centrifuging or filtering with gauze, and collecting supernatant to obtain nuisanceless Yang Meishu flower.
9. Use of a nuisanceless Yang Meishu flower formulation as claimed in any one of claims 1-3 for reducing the fruit set rate of bayberry.
CN202211068395.XA 2022-09-02 2022-09-02 Pollution-free Yang Meishu flower agent, preparation method and application thereof Active CN115413679B (en)

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Citations (2)

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Publication number Priority date Publication date Assignee Title
CN108990592A (en) * 2018-08-29 2018-12-14 江苏农林职业技术学院 A kind of fourth Ao red bayberry Flower thinning agent and the preparation method and application thereof
CN111903705A (en) * 2020-08-27 2020-11-10 浙江瑞丰生物科技有限公司 Compound herbicide and application thereof

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Publication number Priority date Publication date Assignee Title
EP3876734A1 (en) * 2018-11-07 2021-09-15 Corteva Agriscience LLC Compositions comprising pyridine carboxylate herbicides and plant growth regulators

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Publication number Priority date Publication date Assignee Title
CN108990592A (en) * 2018-08-29 2018-12-14 江苏农林职业技术学院 A kind of fourth Ao red bayberry Flower thinning agent and the preparation method and application thereof
CN111903705A (en) * 2020-08-27 2020-11-10 浙江瑞丰生物科技有限公司 Compound herbicide and application thereof

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杨梅疏花剂、减花剂、促花剂和保花剂的调控作用及其使用技术;梁森苗, 等;浙江农业科学(第01期);36-38 *

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