CN115779126A - Long-acting scented chip and preparation method thereof - Google Patents
Long-acting scented chip and preparation method thereof Download PDFInfo
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- CN115779126A CN115779126A CN202310029837.8A CN202310029837A CN115779126A CN 115779126 A CN115779126 A CN 115779126A CN 202310029837 A CN202310029837 A CN 202310029837A CN 115779126 A CN115779126 A CN 115779126A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention provides a long-acting scented chip and a preparation method thereof, relating to the field of cosmetics, wherein the long-acting scented chip comprises a substrate and a perfume liquid; wherein, the spice liquid comprises the following raw materials: absolute ethyl alcohol, glycerol, an osmanthus fragrans extract, a curcuma longa extract, a murraya jasminorage extract, sodium alginate, a surfactant, jojoba oil, essential oil and water. The preparation method is simple and convenient, and the prepared fragrant piece is strong in durability, low in cost, safe and durable and can play a certain role in calming nerves.
Description
Technical Field
The invention relates to the field of cosmetics, and particularly relates to a long-acting scented chip and a preparation method thereof.
Background
Perfume generally contains ethanol, pigment, glycerin, surfactant and other components, has a fragrant smell, and is one of the more important cosmetics. However, the perfume generally has the problems of short fragrance retention time, high irritation and the like, and compared with the perfume, the perfume has the advantages that the fragrance is fixed in taste, is not easy to volatilize, is long in storage time, avoids the risk of explosion of the perfume at high temperature, and is high in safety.
At present, two types of incense chips are mainly used in the prior art, one type of incense chip is directly pressed by using incense powder and other base materials, for example, the incense chip disclosed in patent CN104043141A and the preparation method thereof, in particular, pure agilawood powder or sandalwood powder is pressed into a shape, the incense chip can uniformly release fragrance for a long time, and the introduction avoids heat waste caused by heating of common incense. For another example, CN103251967B discloses a vehicle-mounted incense tablet and a manufacturing method thereof, the incense tablet is composed of 25-35% of pregelatinized starch, 1-2% of superfine silicon powder, 5-8% of dextrin and 50-65% of aromatic materials, wherein the aromatic materials are agilawood, sandalwood or rosemary and the like, and the incense tablet has a refreshing effect, can improve air, and is safe and reliable, and relatively high in strength. Another type is a perfume which is processed to make the substrate contain perfume, such as a long-lasting perfume, a perfume sheet and a preparation method thereof disclosed in patent CN104922001B, comprising the following raw materials: benzoin cream, musk ketene, benzyl benzoate, isopropyl myristate, sandalwood 208, methyl cedryl ketone, patchouli oil, bergamot oil and the like, wherein the scented tablet is mainly prepared by pressing plant fiber pulp and a filler to prepare a card, and a specific perfume is contained in a substrate. For another example, patent CN110354024B discloses fragrance tablets suitable for underwear and underwear suitable for fragrance tablets, wherein the fragrance tablets are prepared from fragrance liquid and base sheets, and the specific raw materials comprise the following components: 1-3 parts of rose essential oil, 3-9 parts of sandalwood essential oil, 0.5-2 parts of rosewood essential oil, 1-3 parts of magnolia alba essential oil, 5-10 parts of edible essence, 20-40 parts of ethanol, 0.05-0.3 part of gelatin, 8-15 parts of propylene glycol and 20-40 parts of distilled water.
Compared with the first type of fragrance sheet, the second type of fragrance sheet has more excellent overall strength, is not dispersed due to external force application, has relatively low cost and is widely used.
However, at present, the related research on the scented strip is still less than that of products such as perfume, and the efficacy and durability of the scented strip still need to be developed.
Disclosure of Invention
Aiming at the problems in the prior art, the invention provides a long-acting scented chip and a preparation method thereof, the preparation method is simple and convenient, and the prepared scented chip is strong in durability, low in cost, safe and durable.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
the invention provides a fragrant piece, which comprises a substrate and a fragrant liquid;
the spice liquid comprises the following raw materials: absolute ethyl alcohol, glycerol, an osmanthus fragrans extract, a curcuma longa extract, a murraya jasminorage extract, sodium alginate, a surfactant, jojoba oil, essential oil and water.
Further, the spice liquid comprises the following raw materials in parts by weight: 10-20 parts of absolute ethyl alcohol, 2-4 parts of glycerol, 1-4 parts of sweet osmanthus extract, 2-5 parts of turmeric extract, 2-5 parts of murraya jasminorage extract, 0.5-1 part of sodium alginate, 3-7 parts of surfactant, 2-5 parts of jojoba oil, 2-3 parts of essential oil and 90-100 parts of water.
Preferably, the spice liquid comprises the following raw materials in parts by weight: 15-20 parts of absolute ethyl alcohol, 2-3 parts of glycerol, 2-3 parts of sweet osmanthus flower extract, 2-4 parts of turmeric extract, 2-4 parts of murraya jasminorage extract, 1 part of sodium alginate, 4-6 parts of surfactant, 2-3 parts of jojoba oil, 2 parts of essential oil and 95-100 parts of water.
Further preferably, the spice liquid comprises the following raw materials in parts by weight: 18 parts of absolute ethyl alcohol, 2 parts of glycerol, 2 parts of sweet osmanthus flower extract, 3 parts of turmeric extract, 3 parts of murraya jasminorage extract, 1 part of sodium alginate, 5 parts of surfactant, 3 parts of jojoba oil, 2 parts of essential oil and 100 parts of water.
Further, the weight ratio of the sweet osmanthus extract to the curcuma extract to the murraya jasminorage extract is (1-4) to (2-5); preferably 2.
Further, the weight ratio of the total weight of the sweet osmanthus extract, the turmeric extract and the murraya jasminorage extract to the jojoba oil is (5-14) to (2-3); preferably 8:3.
Further, the essential oil comprises one or more of rose essential oil, jasmine essential oil, chamomile essential oil, lavender essential oil and grapefruit essential oil.
Further, the surfactant comprises sodium dodecyl sulfate and/or polysorbate.
Further, the substrate comprises tissue paper or cork.
Further, the invention also provides a preparation method of the fragrant piece, which comprises the following steps:
(1) Adding sodium alginate into water, heating to dissolve, adding flos Osmanthi Fragrantis extract, curcuma rhizome extract, and folium Et cacumen Murrayae extract, and stirring to obtain solution A;
(2) Mixing the solution A, essential oil, surfactant, jojoba oil, glycerol and anhydrous ethanol, adding the rest water, stirring to obtain essence solution, and standing;
(3) Soaking the substrate in the essence liquid, taking out, naturally drying in the shade, and continuously drying for three times.
Further, the standing time in the step (2) is 2-3 days, and the soaking time in the step (3) is 3-4h.
Further, the adding amount of the water in the step (1) is 30-40% of the total weight of the water.
The technical effects obtained by the invention are as follows:
the fragrant sheet has wide application, can be placed in an automobile or a wardrobe, and can also be used next to the skin;
the fragrance sheet can slowly release fragrance, the fragrance is more durable, and meanwhile, the fragrance sheet is non-irritant and safer;
the fragrant sheet disclosed by the invention is simple in material and convenient and fast in preparation method, and the fragrance retaining effect of the fragrant sheet is lasting and the effect of calming nerves and calming qi is achieved by adding the plant extracts such as the osmanthus fragrans extract, the curcuma extract and the murraya jasminorage extract and matching the components of the jojoba oil and the essential oil.
Detailed Description
The embodiments of the present invention are described below with reference to specific embodiments, and other advantages and effects of the present invention will be easily understood by those skilled in the art from the disclosure of the present specification. The invention is capable of other and different embodiments and of being practiced or of being carried out in various ways, and its several details are capable of modification in various respects, all without departing from the spirit and scope of the present invention.
Before the present embodiments are further described, it is to be understood that the scope of the invention is not limited to the particular embodiments described below; it is also to be understood that the terminology used in the examples herein is for the purpose of describing particular embodiments only, and is not intended to limit the scope of the present invention.
When numerical ranges are given in the examples, it is understood that both endpoints of each of the numerical ranges and any value therebetween can be selected unless the invention otherwise indicated. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs.
It should be noted that the osmanthus fragrans extract, the curcuma longa extract, the lavender extract and the chrysanthemum extract used in the present invention are obtained from hibiscus knoot biotechnology limited, the murraya jasminorage extract is obtained from walt rice biotechnology limited, and the other raw materials are all common commercially available products, and thus the sources thereof are not particularly limited.
The ingredients and contents of the fragrance liquids of the products corresponding to examples 1 to 3 and comparative examples 1 to 3 are specifically shown in table 1.
TABLE 1 ingredients and contents of spice liquid in the product
The preparation method of the scented chips in examples 1-3 and comparative examples 1-3 specifically comprises the following steps:
(1) Adding sodium alginate into water (the adding amount of water accounts for 30% of the total weight of water), heating to dissolve, adding flos Osmanthi Fragrantis extract, curcuma rhizome extract, and folium Et cacumen Murrayae extract, and stirring to obtain solution A;
(2) Mixing the solution A, essential oil, surfactant, jojoba oil, glycerol and anhydrous ethanol, adding the rest water, stirring to obtain essence solution, and standing for 2 days;
(3) Soaking the substrate (made of water cotton paper) in the essence solution for 4 hr, taking out, naturally drying in the shade, and continuously drying for three times.
Comparative example 4
A fragrance sheet comprises a base sheet and a fragrance liquid, wherein the fragrance liquid comprises the following raw materials: 10 parts of absolute ethyl alcohol, 2 parts of glycerol, 1 part of lavender extract, 2 parts of turmeric extract, 2 parts of chrysanthemum extract, 0.5 part of sodium alginate, 3 parts of sodium dodecyl sulfate, 2 parts of jojoba oil, 2 parts of rose essential oil and 90 parts of water.
The preparation method of the fragrant slice comprises the following steps:
(1) Adding sodium alginate into water (the amount of water is 30% of the total weight of water), heating to dissolve, adding Lavender extract, curcuma rhizome extract, and flos Chrysanthemi extract, and stirring to obtain solution A;
(2) Mixing the solution A, essential oil, surfactant, jojoba oil, glycerol and anhydrous ethanol, adding the rest water, stirring to obtain essence solution, and standing for 2 days;
(3) Soaking the substrate (made of water cotton paper) in the essence solution for 4 hr, taking out, naturally drying in the shade, and continuously drying for three times.
1. Fragrance retention durability test
The test number was 5PCS (single piece 2cm × 2 cm), the fragrance sheets in each example were placed in an electronic fragrance machine, the fragrance machine was started, the fragrance-remaining time at room temperature of 25 ℃ was measured, and the number of days when fragrance was faded was recorded.
The volunteers selected women of 18-40 years old, had no discomfort such as cold, had healthy and unobstructed nasal cavity, had no smoking, and had no use of flavored products during the test, 5 persons of each group underwent the fragrance smelling test, and were recorded every 3 days, each time compared with the newly prepared scented tablets, and evaluated (yes/no) whether the scented tablets were light, with the results of evaluation of 3 or more persons as the results of the day (for example, when 3 or more persons considered light, the results were recorded as light), and the results were counted in table 2.
TABLE 2 fragrance retention durability test results
| Examples of the invention | Time (sky) |
| Example 1 | 15 |
| Example 2 | 15 |
| Example 3 | 18 |
| Comparative example 1 | 9 |
| Comparative example 2 | 12 |
| Comparative example 3 | 12 |
| Comparative example 4 | 9 |
The result records show that the fragrance retaining effect of the fragrance sheet is long, the lasting fragrance and flavor-change-free time can reach more than 15 days, and the longest fragrance retaining and flavor-change-free time of the fragrance sheet corresponding to the embodiment 3 can reach 18 days.
2. Aneuropaea conditions testing
The test quantity of the scented chips is 1PC (single chip 2cm multiplied by 2 cm), kunming mice with the weight of 20 plus or minus 2g are selected for the mice, the mice are randomly divided into 8 groups after being adaptively raised, wherein 1 group is a control group, 7 groups are test groups, and each group comprises 5 mice;
the aromatherapy machine with the scented tablets is not placed in the control group, the scented tablets in the examples are respectively placed in the electronic aromatherapy machine in the test group, then the test group is placed in a test box (40 cm multiplied by 40 cm) with a 10-hole plate for 5min, then the mouse is placed in the central area of the test field, the timing is continued, the average hole probing times of the mouse within 5min are counted, wherein the hole depth is 2.2cm, when the hole probing depth of the mouse exceeds 1cm, the number is recorded as 1, and the results are counted in a table 3.
TABLE 3 results of the probing situation of the mice
| Examples of the invention | Number of exploratory holes (times) |
| Control group | 16.8 |
| Example 1 | 12.4 |
| Example 2 | 11.4 |
| Example 3 | 10.6 |
| Comparative example 1 | 13.0 |
| Comparative example 2 | 13.8 |
| Comparative example 3 | 13.4 |
| Comparative example 4 | 14.6 |
The result records show that the scented tea has a certain nerve soothing effect, can inhibit the activity behavior of mice, and reduces the hole probing times.
Finally, it should be noted that the above-mentioned contents are only used for illustrating the technical solutions of the present invention, and not for limiting the protection scope of the present invention, and that the simple modifications or equivalent substitutions of the technical solutions of the present invention by those of ordinary skill in the art can be made without departing from the spirit and scope of the technical solutions of the present invention.
Claims (9)
1. A scented tablet, which is characterized in that: comprises a substrate and a perfume liquid;
the spice liquid comprises the following raw materials in parts by weight: 10-20 parts of absolute ethyl alcohol, 2-4 parts of glycerol, 1-4 parts of sweet osmanthus extract, 2-5 parts of turmeric extract, 2-5 parts of murraya jasminorage extract, 0.5-1 part of sodium alginate, 3-7 parts of surfactant, 2-5 parts of jojoba oil, 2-3 parts of essential oil and 90-100 parts of water.
2. The fragrance sheet of claim 1 wherein: the spice liquid comprises the following raw materials in parts by weight: 15-20 parts of absolute ethyl alcohol, 2-3 parts of glycerol, 2-3 parts of sweet osmanthus flower extract, 2-4 parts of turmeric extract, 2-4 parts of murraya jasminorage extract, 1 part of sodium alginate, 4-6 parts of surfactant, 2-3 parts of jojoba oil, 2 parts of essential oil and 95-100 parts of water.
3. The fragrance sheet of claim 1 wherein: the weight ratio of the sweet osmanthus extract to the turmeric extract to the murraya jasminorage extract is 2.
4. The fragrance sheet of claim 1 wherein: the weight ratio of the total weight of the sweet osmanthus extract, the turmeric extract and the murraya jasminorage extract to the jojoba oil is 8:3.
5. The fragrance sheet of claim 1 wherein: the essential oil comprises one or more of rose essential oil, jasmine essential oil, chamomile essential oil, lavender essential oil and grapefruit essential oil.
6. The fragrance sheet of claim 1 wherein: the surfactant comprises sodium dodecyl sulfate and/or polysorbate.
7. The fragrance sheet of claim 1 wherein: the substrate comprises tissue paper or cork.
8. A process for the preparation of a fragranced sheet as claimed in any one of claims 1 to 7, characterized in that: the method comprises the following steps:
(1) Adding sodium alginate into water, heating to dissolve, adding flos Osmanthi Fragrantis extract, curcuma rhizome extract, and folium Et cacumen Murrayae extract, and stirring to obtain solution A;
(2) Mixing the solution A, essential oil, surfactant, jojoba oil, glycerol and anhydrous ethanol, adding the rest water, stirring to obtain essence solution, and standing;
(3) Soaking the substrate in the spice liquid, taking out, naturally drying in the shade, and continuously drying for three times to obtain the final product.
9. The method of claim 8, wherein: the standing time in the step (2) is 2-3 days, and the soaking time in the step (3) is 3-4 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310029837.8A CN115779126A (en) | 2023-01-09 | 2023-01-09 | Long-acting scented chip and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310029837.8A CN115779126A (en) | 2023-01-09 | 2023-01-09 | Long-acting scented chip and preparation method thereof |
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| Publication Number | Publication Date |
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| CN115779126A true CN115779126A (en) | 2023-03-14 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202310029837.8A Pending CN115779126A (en) | 2023-01-09 | 2023-01-09 | Long-acting scented chip and preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004244756A (en) * | 2003-02-14 | 2004-09-02 | Toray Ind Inc | Fiber material for inner pad and bedding using the same |
| CN101632761A (en) * | 2008-11-22 | 2010-01-27 | 中山市中南烛业有限公司 | Nerves-soothing compound oil, essential oil of traditional Chinese medicine and aromatherapy products having nerves-soothing function |
| CN103432029A (en) * | 2013-08-15 | 2013-12-11 | 金红叶纸业集团有限公司 | Composition and tissue employing same |
| CN110354024A (en) * | 2019-07-19 | 2019-10-22 | 深圳市越昌科技有限公司 | Suitable for underclothes fragrant atmosphere scented tea and be applicable in the personal clothing of scented tea |
-
2023
- 2023-01-09 CN CN202310029837.8A patent/CN115779126A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004244756A (en) * | 2003-02-14 | 2004-09-02 | Toray Ind Inc | Fiber material for inner pad and bedding using the same |
| CN101632761A (en) * | 2008-11-22 | 2010-01-27 | 中山市中南烛业有限公司 | Nerves-soothing compound oil, essential oil of traditional Chinese medicine and aromatherapy products having nerves-soothing function |
| CN103432029A (en) * | 2013-08-15 | 2013-12-11 | 金红叶纸业集团有限公司 | Composition and tissue employing same |
| CN110354024A (en) * | 2019-07-19 | 2019-10-22 | 深圳市越昌科技有限公司 | Suitable for underclothes fragrant atmosphere scented tea and be applicable in the personal clothing of scented tea |
Non-Patent Citations (1)
| Title |
|---|
| 张连峰等, 中国协和医科大学出版社 * |
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